CIRA-CF-15

Transcription

CIRA-CF-15

DOCUMENT NUMBER:
REV.:
CIRA-CF-15-0387
DISTRIBUTION STATEMENT
NATURA DOCUMENTO
RISTRETTO
ARCHIVIO
PROJECT
PROGETTO
JOB
COMMESSA
TASK
SHS
PROGRESSIVO DI ARCHIVIO
/CIRA/PRST
1
0021
NO. OF PAGES
DELIVERABLE
3+22
TITLE
SHS-UHTC Coated SiC. Technical specification for the UHTC coating deposition on CMC and metallic
substrates.
PREPARED
PREPARATO
REVISED
VERIFICATO
APPROVED
APPROVATO
AUTHORIZED
AUTORIZZATO
Gardi Roberto
(INSS)
Gardi Roberto
(INSS)
Gardi Roberto
(INSS)
Marino Giuliano
(INTS)
DATE/DATA
DATE/DATA
10/06/2015
10/06/2015
DATE/DATA
10/06/2015
DATE/DATA
10/06/2015
BY THE TERMS OF THE LAW IN FORCE ON COPYRIGHT, THE REPRODUCTION, DISTRIBUTION OR USE OF
THIS DOCUMENT WITHOUT SPECIFIC WRITTEN AUTHORIZATION IS STRICTLY FORBIDDEN
A NORMA DELLE VIGENTI LEGGI SUI DIRITTI DI AUTORE QUESTO DOCUMENTO E' DI PROPRIETA' CIRA E NON POTRA'
ESSERE UTILIZZATO, RIPRODOTTO O COMUNICATO A TERZI SENZA AUTORIZZAZIONE
I
DOCUMENT NUMBER:
CIRA-CF-15-0387
REV.:
1
TITLE:
SHS-UHTC Coated SiC. Technical specification for the UHTC coating deposition on CMC and
metallic substrates.
ABSTRACT:
This document contains the specification for the procurement of the metallic samples and for the
posizion o the HUTC coating on different substrates.
AUTHORS:
Gardi Roberto
APPROVAL REVIEWERS:
Gardi Roberto
APPROVER
Gardi Roberto
AUTHORIZATION REVIEWERS:
Marino Giuliano;Del Vecchio Antonio
AUTHORIZER
Marino Giuliano
II
DOCUMENT NUMBER:
REV.:
CIRA-CF-15-0387
1
DISTRIBUTION RECORD:
DEPT
NAME
INSS
Richiello Camillo
SPAZ
Cantoni Stefania
*
DEPT
NAME
*
* PT = PARTIAL
A = ALL
III
DOCUMENT NUMBER: CIRA-CF-15-0387
REV.:1
Technical specification for UHTC coating on
metallic and CMC samples.
10/06/2015
Page 1 of 22
Project SHS
REVISION LIST
REV
DESCRIPTION
DATE
EDITOR
0
First release
16/04/15
R.Gardi
1
Updated schedule and authorization plan.
10/06/15
R.Gardi
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Project SHS
INDEX
REVISION LIST..................................................................................................................................1
1. Introduction..................................................................................................................................3
1.1 Scope .....................................................................................................................................3
1.2 Applicability..........................................................................................................................3
1.3 Documents.............................................................................................................................3
1.3.1
Applicable documents....................................................................................................3
1.4 Abbreviations and acronyms .................................................................................................4
2. Aim of the activity .......................................................................................................................5
2.1 Phases of the activity.............................................................................................................5
2.1.1
Phase 1 ...........................................................................................................................5
2.1.2
Phase 2 ...........................................................................................................................5
2.1.3
Phase 3 ...........................................................................................................................6
3. Detailed description of the procurement......................................................................................6
3.1 Sub-phase-1a Metallic substrate............................................................................................7
3.2 Sub-phase-1b CMC substrate................................................................................................8
3.3 Phase-2 details.....................................................................................................................10
3.4 Phase-3 details.....................................................................................................................11
4. Gantt Updated on 30/03/2015 ....................................................................................................12
5. Annex-2. Drawings of Flat, Blunt and Sharp geometries ..........................................................14
6. Annex-3 Drawing of the conical sample....................................................................................17
7. Annex-4. Drawings of the DISK for standard model holder .....................................................19
8. Annex-5. Drawings of the PWT TA ..........................................................................................20
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Project SHS
1. Introduction
1.1 Scope
This document contains the technical specification for the procurement of the UHTC coated
samples for the test aimed to the develop the coating technology.
1.2 Applicability
This document is applicable to the project “TPS a base di SiC Rivestito con UHTC” (TPS based on
UHTC coated SiC) part of the SHS project.
1.3 Documents
1.3.1
[AD 1]
[AD 2]
[AD 3]
[AD 4]
[AD 5]
[AD 6]
Applicable documents
CIRA-VER-14-0145 “Progetto SHS - UHTC Coating on CMC: Kick-Off meeting (via
teleconference)” 10/03/2014
CIRA-VER-14-0146 “Progetto SHS - UHTC Coating on CMC: Progress Meeting”
05/06/2014
CMC Specification
I. Moretti M.Tului “Test di campioni metallici rivestiti in UHTC Rapporto Finale”
Roma, Luglio 2012. Commessa N°. RD 010 066 Rapporto N° 16007R.
CIRA-CF-11-0207. Specifica per la realizzazione e test di campioni metallici rivestiti in
UHTC.
M. Tului, R. Gardi, A. Del Vecchio “PLASMA SPRAYED CERAMIC COATINGS,
ON REFRACTORY METALS FOR SPACE APPLICATIONS” 63rd International
Astronautical Congress, Naples, Italy.
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Project SHS
1.4 Abbreviations and acronyms
AD
AIL
AIV
AR
ATV
CFI
CIRA
COTS
CDR
CFD
CMC
C/SiC
DDP
DJF
DM
DOC
ECSS
FLPP
FMECA
GEO
GQR
GSE
GSP
HTV
HV
H/W
ICD
IRD
IPR
ITAR
KOM
LEO
LLI
Applicable Document
Action Item List
Assembly, Integration and
Verification
Acceptance Review
Automated Transfer Vehicle
Customer Furnished Item
Centro Italiano Ricerche
Aerospaziali
Commercial Off The Shelf
Critical Design Review
Computational Fluid Dynamics
Ceramic matrix Composite
Silicon carbide reinforced with
carbon fibers
Design Development Plan
Design Justification File
Development Model
Demise Observation Capsule
European Cooperation for Space
Standardization
Future Launchers Preparatory
Program
Failure Modes Effects and Criticality
Analysis
Geosynchronous Equatorial Orbit
Ground Qualification Review
Ground Support Equipment
General Studies Program
H-II Transfer Vehicle
Host Vehicle
Hardware
Interface Control Document
Interface Requirements Document
Intellectual property rights
International Traffic of Arms
Regulation
Kick Off Meeting
Low Earth Orbit
Long Lead Items
LUS
MAIT
Launcher Upper Stage
Manufacturing, Assembly,
Integration, Testing
MoM
Minutes of Meeting
MRD
Mission Requirements Document
MSDS
Material Safery Data Sheet
N/A
Not Applicable
NDA
Non-Disclosure Agreement
OBDH
On-Board Data Handling
PA
Product Assurance
PDR
Preliminary Design Review
PFM
Proto-Flight Model
PM
Progress Meeting
PR
Progress Report
PWT
Plasma Wind Tunnel
QF
Qualification Flight
QM
Qualification Model
RAMS
Reliability, Availability,
Maintainability, Safety
RBB
Re-Entry “Black Box”
RD
Reference Document
REBR
Re-Entry Breakup Recorder
RID
Review Item Discrepancy
SCIROCCO CIRA PWT
SHARK Sounding Hypersonic Atmospheric
Re-entering Kapsule
SoW
Statement of Work
SRD
System Requirement Document
SRR
System Requirement Review
TRB
Test Review Board
TRR
Test Readiness Review
S/S
Sub-System
S/W
Software
TN
Technical Note
UHTC
Ultra High Temperature Ceramic
VCD
Verification Control Document
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Project SHS
2.
Aim of the activity
The aim of this activity is to improve the performances of the UHTC plasma spray coating, for
protection of parts exposed to the high heat loads generated by hypersonic flight regime.
UHTC coatings have been used in many different research activities at CIRA. The present activity
will investigate different substrate/coating systems, in particular bot metallic and CMC substrates
shall be tested. A wide plasma wind tunnel test campaign, executed on different materials
combinations and different shapes, shall provide a good set of results, able to identify the real
performances of the systems.
The metallic substrate procurement shall be in charge of the supplier, the CMC substrates shall be
provided by the customer and shall be coated my the supplier.
2.1 Phases of the activity
The whole activity is divided in three main phases.
2.1.1
Phase 1
The first phase is divided in two sub-phases, the first one oriented to the study of UHTC coating on
metallic substrate, the second sub-phase is devoted to the CMC substrate.
The investigation on metallic substrates is aimed to improve the results achieved in past CIRA
activities and will be a benchmark for the performances of the UHTC coating on the CMC.
In [AD4] [AD5] [AD6] CIRA, in cooperation with CSM, has identified an effective coating process
suitable for tungsten components. These coated metallic sample sustained temperature exceeding
1700°C for more than 5 minutes, experiencing no damages.
The identified technique has been successfully used in the realization of the CIRA payload for the
SCRAMSPACE flight, but some machinability difficulties have been found.
The part of the present activity, oriented toward the metallic substrates, is aimed to identify a
refractory alloy able to replace the tungsten, providing an improved machinability, and able to
maintain the same performances when coated with UHTC.
The supplier shall identify a set of refractory alloys able to sustain temperature exceeding 1700°C
without significant mechanical properties degradations and shall perform coating tests on these
samples aimed to improve the mechanical adhesion. Downstream this activity one or two alloys
shall be identified for the successive part of the activity. A number of metallic samples shall be then
procured and coated for the plasma wind tunnel tests.
The second sub-phase shall be carried out in parallel. The customer shall provide the supplier with a
number of CMC samples. The supplier shall optimize the coating process on these samples and
shall deliver the samples for the plasma wind tunnel tests.
2.1.2
Phase 2
The second phase of the activity consists in the coating of a second sent of CMC samples,
introducing, if needed, further improvement in the process, applying the lessons learned during the
PWT test held in the first phase.
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Project SHS
2.1.3
Phase 3
The third and final phase is divided in two sub-phases as the phase 1. The first sub-phase shall
complete the research activity on the metallic alloys coated with UHTC. In this phase the supplier
shall produce a number of larger metallic test articles, machined from the same refractory alloy
selected in phase 1. These samples shall be coated and shall be delivered to the customer for plasma
wind tunnel testing.
The second sub-phase consist in the coating of larger CMC samples. These samples shall be
provided by the customer and shall tested in a larger facility.
3. Detailed description of the procurement.
The three phases of the activity are here described:
 Phase 1
a. Sub-phase 1a Metallic substrate
o Identification of candidate refractory alloys.
o Optimization of coating process on selected refractory alloys.
o Selection one or two alloys for PWT tests.
o Procurement of the metallic samples for PWT test.
o Deposition of UHTC coating on metallic samples. (Within Mar. 2016)
o Reporting
b. Sub-phase 1b CMC substrate
o Optimization of the UHTC coating deposition.
o Deposition of UHTC coating on the first set of CMC samples. (Within Mar. 2016)
o Reporting
 Phase 2
o Deposition of UHTC coating on the second set of CMC samples. (Within Oct. 2016)
o Reporting
 Phase 3
a. Sub-phase 1a Metallic substrate
o Procurement of the metallic samples for PWT test.
o Deposition of UHTC coating on metallic samples.
o Reporting
b. Sub-phase 1b CMC substrate
o Procurement of refractory alloy disks for standard model testing
o Deposition of the UHTC coating on disks for standard model testing.
o Deposition of the UHTC coating on the third set of CMC samples. (Within Jul. 2017)
o Reporting
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Project SHS
3.1 Sub-phase-1a Metallic substrate
As stated in previous chapter Phase-1 consists of:
o
o
o
o
o
o
Identification of candidate refractory alloys.
Optimization of coating process on selected refractory alloys.
Selection one or two alloys for PWT tests.
Procurement of the metallic samples for PWT test.
Deposition of UHTC coating on metallic samples
Reporting
The optimization and selection of the best alloy(s) can be executed on simple flat samples.
The flat samples that show better performances shall be heated with the same plasma facility used
for the coting deposition. This test is aimed to preliminary evaluate the ability of the
substrate/coating system to sustain heating and cooling without spallation.
The heating should exceed 1500°C for at least two minutes.
The supplier shall provide the following metallic samples coated with UHTC within Sept. 2015:
Geometry
Quantity
CONICAL SAMPLE
1
CONICAL SAMPLE
1
BLUNT SEMICYLINDER
3
BLUNT SEMICYLINDER
1
SHARP EDGE
3
SHARP EDGE
1
DISK FOR EMISSIVITY TEST
2
2
DISK FOR CATALICITY TEST
2
4
Material
UHTC coated
Tungsten
UHTC coated
Refractory alloy
UHTC coated
Refractory alloy
Uncoated
Refractory alloy
UHTC coated
Refractory alloy
Uncoated
Refractory alloy
UHTC coated
Refractory alloy
Uncoated
Refractory alloy
UHTC coated
Refractory alloy
Uncoated
Refractory alloy
Notes
Drawings in Annex-3
Drawings in Annex-3
Drawings Annex-2 Detail C
Drawings Annex-2 Detail C
Drawings Annex-2 Detail D
Drawings Annex-2 Detail D
Diameter: 40 mm
Thickness: 2 mm
Diameter: 40 mm
Thickness: 2 mm
Diameter: 25 mm
Thickness: 2 mm
Diameter: 25 mm
Thickness: 2 mm
The supplier shall deliver a report including activities description and test results.
 The alumina sample holder shown in the drawings is not part of this procurement.
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Project SHS
3.2 Sub-phase-1b CMC substrate
o Optimization of the UHTC coating deposition.
o Deposition of UHTC coating on the first set of CMC samples.
o Reporting
The customer shall provide the supplier with the following CMC items:
Geometry
Quantity
Material
Notes
FLAT DISK
9
CMC
Drawings in Annex-2 Detail B
BLUNT SEMICYLINDER
9
CMC
Drawings in Annex-2 Detail C
SHARP EDGE
5
CMC
Drawings in Annex-2 Detail D
OPTIMIZATION SAMPLES
8
CMC
Disk 25mm in diameter
5mm thick
PULL TEST SAMPLES
10
CMC
Square sample 25-50mm edge
3
CMC
4
CMC
Diameter: 40 mm
Thickness: 2 mm
Diameter: 25 mm
Thickness: 2 mm
Half of the CMC samples shall be realized in C/SiC and half in SiC/SiC.
The OPTIMIZATION SAMPLEs and the PULL TEST SAMPLES shall be used for tuning the
deposition process, in order to achieve a good adhesion between the metallic and CMC substrate
and the UHTC.
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Project SHS
Once the adhesion tests give satisfactory results, the samples shall be coated in conformity with the
drawings in Annex-2.
The supplier shall provide the following UHTC coated items:
Geometry
Quantity
FLAT DISK
9
BLUNT SEMICYLINDER
9
SHARP EDGE
5
OPTIMIZATION SAMPLES
8
PULL TEST SAMPLES
10
3
4
Material
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
CMC
Notes
Disk 25mm in diameter
5mm thick
Square sample 25-50mm edge
Diameter: 40 mm
Thickness: 2 mm
Diameter: 25 mm
Thickness: 2 mm
The report shall include a comparison between CMC and metallic substrate behavior.
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Project SHS
3.3 Phase-2 details
o Deposition of UHTC coating on the second set of CMC samples.
o Reporting
The customer shall provide the supplier with the following CMC items:
Geometry
FLAT DISK
BLUNT SEMICYLINDER
SHARP EDGE
Quantity
10
10
5
Material
CMC
CMC
CMC
Notes
The samples shall be coated using the same procedure assessed in Phase-1.
Geometry
Quantity
FLAT DISK
10
BLUNT SEMICYLINDER
10
SHARP EDGE
5
Material
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
CMC
Notes
The supplier shall deliver a report including activities description and results.
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Project SHS
3.4 Phase-3 details
o
o
o
o
Procurement of refractory alloy disks for standard model testing
Deposition of the UHTC coating on disks for standard model testing.
Deposition of the UHTC coating on the third set of CMC samples.
Reporting
The customer shall provide the supplier with the following CMC items within Feb. 2017:
Geometry
Quantity
Material
Notes
DISK for Standard model holder
2
CMC
Drawings in Annex-4
PWT TA Blunt Cone
2
CMC
Drawings in Annex-5
PWT TA Blunt Wedge
2
CMC
Drawings in Annex-5
Geometry
Quantity
2
2
PWT TA Blunt Cone
2
PWT TA Blunt Wedge
2
PWT TA Blunt Cone
1
PWT TA Blunt Wedge
1
Material
UHTC coated
refractory alloy
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
CMC
UHTC coated
refractory alloy
UHTC coated
refractory alloy
Notes
Drawings in Annex-4
Drawings in Annex-4
Drawings in Annex-5
Drawings in Annex-5
Drawings in Annex-5
Drawings in Annex-5
The report shall include a comparison between CMC and metallic substrate behavior.
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Technical specification for UHTC coating on metallic and CMC samples.
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4. Gantt Updated on 10/06/2015
(next page)
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5. Annex-2. Drawings of Flat, Blunt and Sharp geometries
The first page contains the drawings of the CMC components. The second page contains the drawings of the CMC components with the UHTC coating applied.
(next two pages)
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6. Annex-3 Drawing of the conical sample.
(next page)
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7. Annex-4. Drawings of the DISK for standard model holder
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8. Annex-5. Drawings of the PWT TA
The first page contains the drawings of the CMC components. The second page contains the drawings of the CMC components with the UHTC coating applied.
(next two pages)
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CIRA-CF-15

Transcription

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