residues and contaminants - Ministério da Agricultura

Transcription

ANALYSIS OF
Secretariat of
Animal and Plant
Health and Inspection
Ministry of
Agriculture, Livestock
and Food Supply
RESIDUES AND
CONTAMINANTS
B R A Z I L I A N
G O V E R N M E N T
IN FOOD
ANALYSIS OF
Secretariat of
Animal and Plant
Ministry of
and Food Supply
RESIDUES AND
CONTAMINANTS
B R A Z I L I A N
G O V E R N M E N T
IN FOOD
Secretariat of
Animal and Plant
Ministry of
and Food Supply
B R A Z I L I A N
G O V E R N M E N T
© 2011 by Ministry of Agriculture, Livestock and Food Supply.
All rights reserved. It is authorized the partial or total reproduction of this material, on
condition that the source be identified, without sale purpose or any commercial end.
The copyright responsibility of the texts and images of this work belongs to the author.
Circulation: 3000 copies
First edition: 2011
Preparetion, distribution, information:
MINISTRY OF AGRICULTURE, LIVESTOCK AND FOOD SUPPLY
Secretariat of Animal and Plant Health and Inspection
Laboratories Support General Coordination - CGAL
Residues and Contaminants in Food - RCA
Address: Esplanada dos Ministérios, Bloco D – Ed. Anexo - Ala “B” Sala 433
Zip code: 070043-900, Brasília – DF
Phone: (61) 3225 5098 / 3218 2535
Fax.: (61) 3218 3094
www.agricultura.gov.br
e-mail: [email protected] / [email protected]
Photography: Alain Barki / Guilherme Teixeira
Customer Service: 0800 704 1995
Editorial Coordination: Social Communication Department
Printed in Brazil
Catalogação na Fonte
Biblioteca Nacional de Agricultura – BINAGRI
Brasil. Ministério da Agricultura, Pecuária e Abastecimento.
Analysis of Residues and Contaminants in Food / Ministério da Agricultura, Pecuária e
Abastecimento. Secretaria de Defesa Agropecuária. – Brasília : MAPA/ACS, 2011.
32 p.
ISBN 978-85-7991-051-7
1. Agricultura. 2. Resíduo. 3. Poluente. I. Secretaria de Defesa Agropecuária. II. Título.
AGRIS Q03
CDU 631.879
1
Ministry of Agriculture, Livestock and Food Supply
Secretariat of Plant and Animal Health and Inspection
Analysis of Residues and
Contaminants in Food
Mission
To “promote the sustainable development
and the agribusiness competitiveness
in benefit of the Brazilian society”.
Brasilia - DF
2011
Analysis of
Residues and
Contaminants
in Food - Lanagros
Contaminants in Food – Lanagros
When dealing with food safety, the control of
residue and contaminants has a fundamental
role. It is through the National Residue and
Contaminants Control Plan – PNCRC that
MAPA ensures that the product which is
delivered to the internal as well as the external
consumer is free of hazardous substances
and contaminants at non-acceptable levels.
2
The quality and safety of the products
are attested by the analysis performed
in the National Agriculture and Livestock
Laboratories Network, which is composed
by the Lanagros and authorized laboratories.
The Lanagros – National Agriculture and
Livestock Laboratories – are the official
laboratories of MAPA.
The 6 Lanagros are located in the 5 Brazilian
regions, being 2 in the Southeast region
(Pedro Leopoldo/MG and Campinas/SP), 1
in the South region (Porto Alegre/RS), 1 in the
Mid-West (Goiânia/GO), 1 in the Northeast
(Recife/PE) and 1 in the North (Belém/PA).
3
Lanagro - PE
Lanagro - PA
Lanagro - MG
CGAL/SDA - DF
Lanagro - GO
Lanagro - SP
Lanagro - RS
Each Lanagro acts concentrating more in determined segments,
based on the location and regional production profile, developing
specific scopes, which, when summed, cover the list of monitored
substances and matrices in the PNCRC, together with the scopes of
the authorized laboratories.
Lanagro Network’s Vision is to be recognized as world reference in
agriculture and livestock laboratorial services, capable of providing
responses with readiness, quality and scientific excellence, striving
for innovation, rigor and efficiency in the conduction of its processes.
For this, great investments in capacity building, infrastructure and
quality management tools are necessary.
4
The Lanagros are equipped in the state of the art in analytical chemistry,
whose techniques are based mainly on liquid and gas chromatography
coupled with mass spectrometry (triple quadrupole and time-of-flight),
gas chromatography coupled to high resolution mass spectrometry,
atomic absorption spectrometry, inductively coupled plasma mass
spectrometry, besides microbiological screening methods. The
laboratories staffs are constantly seeking development and innovation
in terms of analytical methodology, aiming to optimize the time of
analysis, capacity, resources and quality.
5
The work developed by the Lanagros is being presented in large-sized
international congresses and symposia, besides reputable scientific
journals in the analytical chemistry, foodstuffs and agriculture areas.
All the Lanagros analysis methods follow rigorous orientations of validation
and internal quality control, in a way to substantiate the issued results.
The Analytical Validation and Quality Control Guide itself, prepared by
CGAL together with the Lanagros is used with this objective.
Besides the analytical routine and development of new methods,
the Lanagros staffs are constantly involved also in audits to the
authorized laboratories, in order to evaluate the compliance with
MAPA normatives from the technical and procedural point of view,
to ensure that these laboratories keep control of the phases of their
processes satisfactorily and increase the efforts for the continuous
improvement of their analytical competence. They also contribute
effectively in the formulation and review of normatives, technical
manuals and procedures of the areas.
The Lanagros have a Quality Management System running according
to standard ISO/IEC 17025. Lanagros MG, RS and SP are
accredited against this standard by INMETRO and this accreditation
is the demonstration of the competence and reliability of their work,
recognized internationally. The other Lanagros are in advanced
process for obtaining accreditation.
In the Residues and Contaminants in Food Area, the scope of the
Lanagros is divided into the fronts: Vet Drug Residues, Organic
Contaminants, Inorganic Contaminants, Mycotoxins and
Pesticide Residues.
CGAL
6
The
Laboratories
Support
General Coordination - CGAL,
more specifically the Area of
Residues and Contaminants
in Food, is responsible for the
management of the laboratories
which act in the National Residues
and
Contaminants
Control
Plan, the PNCRC. Besides the
authorized laboratories which
also perform analysis for the
National Plan, it is responsibility
of CGAL to manage, allocate
resources and define guidelines
and strategies for the operation
of the LANAGROs. Together with
the LANAGROs staffs, CGAL
established the Procedures
Manual of PNCRC for laboratories
and the Analytical Validation and
Quality Control Guide. CGAL
also has the role of promoting
the publication of articles in
specialized scientific journals
and participation in national and
international congresses and
symposia, to participate in forums
for the formulation of harmonized
methodological guides and
protocols and internationally
recognized, having the mission
of putting Brazil at the forefront
for the analysis of residues and
contaminants in food.
7
Interlaboratory Program
Lanagro - MG
8
MAPA’s Interlaboratory Program (IP) is coordinated by
LANAGRO-MG. It periodically conducts rounds of proficiency
assays of which participate the laboratories from the National
Network, official as well as authorized. According to the planning
performed between the IP staff and CGAL, the other Lanagros
will collaborate producing reference materials for the Program,
each on its expertise and on its scope. With this, the network
participates actively in the interlaboratory activities, not only
receiving and analyzing samples, but also producing them
so that the IP conducts the rounds and treat the results with
statistical reasoning.
9
The participation in proficiency assays programs provides to
the laboratories an objective way of assuring their competence
to perform analysis and guarantee the result that is issued and,
consequently, the conformity of the product or process assessed.
The use of reference materials, in turn, ensures traceability and
is fundamental for method validation, equipments’ performance
verification, efficacy assessment of trainings, among others. This
way the generated data can be used for self-assessment of the
laboratory, for evaluation by the clients, or by other parties, such as
accreditation or regulatory bodies. It supplements, consequently,
the internal procedures of quality control themselves, providing an
additional control for analytical quality assurance.
Assay
Technique
Matrix / Species
 Diethylstilbestrol (DES)
Dienestrol
Hexestrol
 α-zearalanol
10
Anabolics
 β-zearalenol
Zearalenone
Ethisterone
Norethandrolone
Drostanolone
Methil-boldenone
HPLC-MS/MS
Urine/ Bovine, Swine
and Equine
Nitroimidazoles
and metabolites
 β-boldenone
Methenolone
Avermectins
Animal Area - LANAGRO-MG
 β-zearalanol
Dimetridazole
Ipronidazole
Ronidazole
Metronidazole
HPLC-MS/MS
Abamectin
Ivermectin
Doramectin
Eprinomectin
Moxidectin
HPLC-FL and
HPLC-MS/MS
Muscle/ Bovine,
Poultry, Swine
Milk / Bovine;
Liver and Muscle/
Bovine, Equine,
Swine and Poultry
Antimicrobials
Macrolides and
Lincosamides
Antimicrobials
Aminoglycosides
Sulfonamides
Assay
Technique
Matrix / Species
Sulfathiazole
Sulfamethazine
Sulfadimethoxine
Sulfaquinoxaline
Sulfadiazine
Sulfamerazine
Sulfamethoxypyridazine
Sulfachloropyridazine
Sulfadoxine
Sulfisoxazole
Sulfamethoxazole
HPLC-MS/MS
Liver/ Bovine,
Equine, Swine and
Poultry
Lincomycin
Erythromycin
Tylosin
Clindamycin
Tilmicosin
HPLC-MS/MS
(confirmatory
quantitative)
Kidney/ Bovine,
Equine, Swine
and Poultry
Spectinomycin
Hygromycin
Streptomycin
Dihydrostreptomycin
Amikacin
Kanamycin
Apramycin
Tobramycin
Gentamicin
Neomycin
HPLC-MS/MS
(confirmatory
quantitative)
Kidney/ Bovine,
Equine, Swine
and Poultry
11
12
– Betalactams
Antimicrobials Antimicrobials
and tetracyclines
Matrix/Species
HPLC-MS/MS
(confirmatory
quantitative)
Kidney/ Bovine,
Equine, Swine
and Poultry
Chloramphenicol
HPLC-MS/MS
(confirmatory
quantitative)
Muscle/ Bovine,
Equine, Swine
and Poultry
Dyes
Technique
Ampicillin
Cefazolin
Oxacillin
 Penicillin G
 Penicillin V
Chlortetracycline
Oxytetracycline
Tetracycline
Doxicycline
 Malachite Green
HPLC-MS/MS
Muscle/ Fish and
Shrimp
F AAS
Kidney / Bovine, Swine
and Poultry
HG AAS
Kidney / Bovine and
Swine;
Muscle/ Poultry, Fish
Cd
Pb
Inorganic
Contaminants
Assay
As
Cd
Pb
As
ICP-MS
Kidney / Bovine and
Swine;
Muscle/ Poultry;
Fish; Honey
 Benzo [a] anthracene
Chrysene
 Benzo[b]-fluoranthene
 Benzo [k] fluoranthene
Benzo[a]-pyrene
 Indeno-[1,2,3 cd] pyrene
Dibenzo[ah]anthracene
Benzo-[g,h,i]perylene
Technique
GC-MS
Matrix/Species
Muscle / Fish
TLC/Densitometry
 Aflatoxin M1
Mycotoxins
PAHs
Assay
Milk (raw and powder)
HPLC-F
 Aflatoxin B1
HPLC-F
Liver/Poultry, Swine
 Ocratoxin A
HPLC-F
13
14
GC-MS
(High Resolution)
Liver/Bovine
Chloramphenicol
HPLC-MS/MS
Honey
Tapazole
CLAE-EM/EM
Urina/Suíno
HPLC-MS/MS
Urine/Swine
HPLC-MS/MS
Urine/Swine
HPLC-MS/MS
Urine/Bovine
HPLC-MS/MS
Muscle/Swine and
Poultry
Thyrostats
Anabolics
Matrix/Species
Anphenicols
Technique
 DES and Zeranol
Thiouracil
Tiouracil
Methylthiouracil
Beta-agonists
Propylthiouracil
Antimicrobials:
Nitrofuran Metabolites
Animal Area - LANAGRO-SP
Assay
Ractopamine
Clembuterol
Salbutamol
 Furazolidone (AOZ)
 Furaltadone (AMOZ)
 Nitrofurantoin (AHD)
 Semicarbazide / Nitrofurazone (SEM)
Assay
Inorganic
Contaminants
Cd
Pb
Technique
GF AAS
As
HG AAS
Hg
TDA AAS
Cd
Pb
GF AAS
Matrix/Species
Liver, Muscle and
Kidney/Bovine,
Swine, Equine
and Poultry
Muscle / Fish
and Shrimp
 α-hexachlorocyclohexane (α-HCH)
 Aldrin (ALD)
 Dieldrin (DLD)
Organochlorine Pesticides and PCBs
Animal Area - LANAGRO-SP
 Hexachlorocyclobenzene (HCB)
 cis-chlordane (c-CLD)
 trans-chlordane (t-CLD)
 Heptachlor (HEP)
 Heptachlor epoxide (HPX)
 pp’-DDT (ppT)
 pp’-DDE (ppE)
 op’-DDT (opT)
 pp’-DDD (ppD)
 PCB 101
 PCB 118
 PCB 138
 PCB 153
 PCB 180
 Mirex
GC-ECD for
determination and
quantification;
GC-MS for
confirmation
Fat/Bovine,
Equine, Swine
and Poultry
15
Assay
Technique
Matrix/Species
Sulfadiazine
Sulfonamides
Sulfathiazole
Sulfamethazine
Sulfamethoxazole
Sulfaquinoxaline
HPLC-MS/MS
Sulfadimethoxine
Eggs;
Milk;
Liver/ Bovine,
Swine, Equine
and Poultry
Sulfadoxine
16
Sulfamerazine
(Fluoro) Quinolones
 Ciprofloxacin
 Enrofloxacin
 Sarafloxacin
 Difloxacin
HPLC-MS/MS
 Nalidixic acid
Milk;
Muscle/ Bovine,
Poultry and Fish
 Oxolinic acid
 Flumequine
Anticoccidials Tetracyclines
Animal Area - LANAGRO-RS
Sulfachlorpyridazine
 Oxytetracycline
 Tetracycline
 Chlortetracycline
HPLC-MS/MS
Milk;
Muscle / Bovine,
Swine, Equine
and Poultry
 Doxicycline
 Nicarbazin
HPLC-MS/MS
Muscle/ Poultry
Assay
Technique
Matrix/Species
Avermectins
 Abamectin
 Doramectin
HPLC-MS/MS
Milk;
Muscle / Bovine; Liver
/ Bovine, Swine and
Equine
Chloramphenicol
HPLC-MS/MS
Honey;
Muscle /Bovine, Swine,
Fish and Shrimp
Florphenicol
HPLC-MS/MS
Fish and Shrimp
Tianphenicol
HPLC-MS/MS
Fish and Shrimp
HPLC-MS/MS
Milk
 Ivermectin
 Eprinomectin
Anphenicols
 Ceftiofur
 Penicillin G
Antimicrobials
Betalactams
 Moxidectin
 Penicillin V
 Oxacillin
 Cloxacillin
 Dicloxacillin
 Ampicilin
 Amoxicilin
17
 Cyfluthrin
 Cypermethrin
GC-ECD
Milk
 Deltamethrin
 Fenvalerate
 Permethrin
Hg
Inorganic Contaminants
Matrix/Species
 Lambda-Cyhalothrin
Assay
18
Technique
 Gama-Cyhalothrin
Pyrethroids
Assay
As
Cd
Pb
Technique
Matrix/Species
CV AAS
Muscle / Fish and
Shrimp
HG AAS
Muscle/ Fish and
Shrimp; Kidney/ Bovine
and Swine; Muscle/
Equine and Poultry
GF AAS
Muscle / Fish and
Shrimp; Kidney/
Bovine, Swine and
Poultry; Muscle/ Equine
GF AAS
Muscle / Fish and
Shrimp; Kidney/
Bovine, Swine, Equine
and Poultry;
As
Animal Area - LANAGRO-PE
Assay
Antimicrobials – Macrolides and Dapsone
Muscle, Liver and
Kidney / Bovine,
Swine and Poultry
F AAS
Muscle, Liver and
Kidney / Bovine,
Swine and Poultry
HG AAS
Muscle / Fish and
Shrimp
Pb
Hg
Matrix/Species
HG AAS
Cd
Assay
Animal Area - LANAGRO-GO
Technique
Technique
Matrix/Species
 Tylosin
 Lincomycin
 Dapsone
 Erythromycin
 Rifampycin
 Clindamycin
 Tilmicosin
HPLC-MS/MS
Kidney/ Bovine,
Equine, Swine and
Poultry
19
Assay
Technique
Matrix/Species
 Spectinomycin
Antimicrobials – Aminoglycosides
 Streptomycin
 Dihydrostreptomycin
 Amikacin
 Kanamycin
HPLC-MS/MS
Kidney/ Bovine,
Equine, Swine and
Poultry
HPLC-MS/MS
Milk;
Muscle / Bovine
 Apramycin
 Tobramycin
 Gentamicin
 Neomycin
Antimicrobials - Anphenicols
20
 Hygromycin
 Cloranphenicol
 Florphenicol
Assay
Technique
Matrix/Species
Antimicrobials – Betalactams and tetracyclines
 Ampicillin
 Penicillin G
 Penicillin V
 Oxacillin
 Cloxacillin
 Dicloxacillin
 Naficillin
HPLC-MS/MS
Milk;
Kidney/ Bovine,
Equine, Swine and
Poultry
CV AAS
Muscle/ Fish, Shrimp
HG AAS
Kidney / Bovine,
Swine;
Muscle / Fish, Shrimp,
Equine and Poultry
GF AAS
Muscle / Fish and
Shrimp;
Kidney/ Bovine, Swine
and Poultry;
Muscle/ Equine
GF AAS
Muscle / Fish and
Shrimp;
Kidney/ Bovine, Swine,
Poultry and Equine
 Cefazollin
 Ceftiofur
 Chlortetracycline
 Oxytetracycline
 Tetracycline
 Doxicycline
Hg
 Amoxicillin
As
Cd
Pb
21
Assay
Technique
Matrix/Species
22
Animal Area - LANAGRO-PA
Cd
GF AAS
Muscle/ Fish, Shrimp;
Kidney / Bovine
Hg
CV AAS
Muscle/ Fish, Shrimp;
Honey
As
FIAS AAS
Muscle/ Fish, Shrimp
Pb
Assay
Technique
Matrix/Species
Lettuce
Banana
Mango
Coffee
 Multi Residue - Pesticides
Plant Area - LANAGRO-MG
HPLC-MS/MS
GC-MS/MS
Apples
Papaya
Strawberries
Tomatoes
Grapes
Rice
Corn
 Benzo [a] anthracene
 Benzo[b]-fluoranthene
 Benzo [k] fluoranthene
PAHs
Multi Residue - Pesticides
Citrus
 Benzo[a]-pyrene
 Indeno-[1,2,3 cd] pyrene
 Dibenzo[ah]anthracene
 Benzo-[g,h,i]perylene
GC-MS
Edible plant oils
23
Assay
Technique
Product
Mango
Plant Area - LANAGRO-GO
Lettuce
24
Grape juice
 Multi Residue - Pesticides
HPLC-MS/MS
Citrus
Cereals
Potato
Garlic
Mycotoxins
Assay
Technique
Product
Almonds (Brazil Nut,
Pistachio and others)
Peanuts, Peanuts
Butter
Rice
Barley and Rye
TLC
Beans
Dried Fruits
Corn
Sorghum
Wheat
Aflatoxins
Plant Area - LACQSA/LANAGRO-MG
Coconut

Feed and Feed
ingredients
B1, B2, G1 and G2
Pepper
Cotton Seed
Almonds (Brazil nut,
Pistachio and others)
Peanuts, peanuts butter
Rice
Beans
HPLC-F
Coconut
Dried Fruits
Corn
Feed
Pepper
Wheat
25
Assay
Technique
Product
Coffee
(Processed, Roasted,
Ground and Soluble)
Corn
Beans
Rice

Ochratoxin A
HPLC-F
Wheat
26
Barley
Oats
Rye
Dried Fruits
Feed
Corn
Sorghum
Rice
Barley
Beer

Zearalenone
HPLC-F
Wheat
Hay
Cotton seed
Feed
Beans
Assay

Technique
Deoxynivalenol (DON)
HPLC-UV
Fumonisin
TLC

Cereals and their
by-products
Corn
Rice
Grits

Citreoviridin
HPLC-UV
Rice Husk Bran (semi
quantitative analysis)
Rice Husk (semi
quantitative analysis)
Assay
Plant Area - LANAGRO-PA
Product

Aflatoxins
Technique
B1, B2, G1 and G2
IAC-HPLC
Product
Brazil Nut
27
CONTACT INFO
Address: Esplanada dos Ministérios, Bloco D Anexo B Sala 433
Zip Code: 70043-900 / City: Brasília-DF
Laboratories Support General Coordinator: Jorge Caetano Júnior
E-mail: [email protected]
Phone: +55 (61) 3225 5098 / Fax: +55 (61) 3218 2697
•
28
Residues and Contaminants in Food - RCA / CGAL
Head of the unit: Angelo de Queiroz Mauricio
Phone: +55 (61) 3218 2535 / Fax: +55 (61) 3218 3094
LANAGRO-GO
NATIONAL AGRICULTURAL LABORATORY IN GOIÁS
•
Laboratory of Residue and Contaminants in Food/LANAGRO-GO
Address: Rua da Divisa, s/nº
Setor Jaó
ZIP Code: 74674-025 / City: Goiânia-GO
Director: Cleia Ferreira Duarte
Phone: +55 (62) 3232 7205 / Fax: +55 (62) 3232 7211
29
LANAGRO-MG
NATIONAL AGRICULTURAL LABORATORY IN MINAS GERAIS
BELO HORIZONTE BASE
• Laboratory of Quality Control and Food Safety – LACQSA/
LANAGRO-MG
Address: Av. Raja Gabaglia, nº 245
Cidade Jardim
Zip Code: 30.380-090 / City: Belo Horizonte
Phone: +55 (31) 3250-0398 / Fax: +55 (31) 3250-0399
Director: Ricardo Aurélio Pinto Nascimento
LANAGRO-MG
NATIONAL AGRICULTURAL LABORATORY IN MINAS GERAIS
PEDRO LEOPOLDO BASE
• Laboratory of Veterinary Medicine Residues – LRM/LANAGRO-MG
• Laboratory of Inorganic Elements – LEI/LANAGRO-MG
• Laboratory of Dioxins and PCBs – LDP/LANAGRO-MG
• Laboratory of Pesticides – LP/LANAGRO-MG
Address: Avenida Rômulo Joviano, s/nº Centro
Zip Code: 33600-000 / City: Pedro Leopoldo-MG
Director: Ricardo Aurélio Pinto Nascimento
Phone: +55 (31) 3660 9642 / Fax: +55 (31) 3661 2383
LANAGRO-PA
NATIONAL AGRICULTURAL LABORATORY IN PARÁ
• Laboratory of Residue and Contaminants – RES/LANAGRO-PA
Address: Av. Almirante Barroso, nº 1234
Marco
Zip Code: 66093-020 / City: Belém-PA
Phone: +55 (91) 3226 4233 / Fax: +55 (91) 3226 2683
Director: Francisco Airton Nogueira
30
LANAGRO-PA
NATIONAL AGRICULTURAL LABORATORY IN PARÁ
SFA-PA BASE
• Laboratory of Residue and Contaminants - Mycotoxins/SFA-PA/
LANAGRO-PA
Address: Avenida Almirante Barroso, nº 5384
Castanheira
Zip Code: 66.645-250 / City: Belém-PA
Phone: +55 (91) 3226 8814 / Fax: +55 (91) 3226 2683
Director: Francisco Airton Nogueira
31
LANAGRO-PE
NATIONAL AGRICULTURAL LABORATORY IN PERNAMBUCO
• Laboratory of Residue and Inorganic Contaminants/LANAGRO-PE
Address: Rua Dom Manuel de Medeiros, s/nº
Dois Irmãos
Zip Code: 52.171-030 / City: Recife-PE
Phone: +55 (81) 3268 8834 / Fax: +55 (81) 3441 6477
Director: Diana Sione Barbosa Pinheiro
LANAGRO-RS
NATIONAL AGRICULTURAL LABORATORY IN RIO GRANDE DO SUL
• Laboratory of Pesticide and Veterinary Medicine Residues - RPM/
LANAGRO-RS
• Laboratory of Heavy-Metals Traces and Contaminants - MTC/
LANAGRO-RS
Address: Estrada da Ponta Grossa, nº 3036
Belém Novo
Zip Code: 91780-580 / City: Porto Alegre-RS
Phone: +55 (51) 3248 2133 / Fax: +55 (51) 3248 1926
Director: Aguinaldo Parussolo
LANAGRO-SP
NATIONAL AGRICULTURAL LABORATORY IN SÃO PAULO
• Laboratory of Veterinary Drug Residues - RDV/LANAGRO-SP
• Laboratory of Inorganic Contaminants - COI/LANAGRO-SP
• Laboratory of Organic Contaminants - ORG/LANAGRO-SP
Address: Rua Raul Ferrari, s/n
Jardim Santa Marcelina
Zip Code: 13100-105 / City: Campinas-SP
Phone: +55 (19) 3252 0155 / Fax: +55 (19) 3252 4835
Director: André de Oliveira Mendonça
32
© 2011 by Ministry of Agriculture, Livestock and Food Supply.
All rights reserved. It is authorized the partial or total reproduction of this material, on
condition that the source be identified, without sale purpose or any commercial end.
The copyright responsibility of the texts and images of this work belongs to the author.
Circulation: 3000 copies
First edition: 2011
Preparetion, distribution, information:
MINISTRY OF AGRICULTURE, LIVESTOCK AND FOOD SUPPLY
Secretariat of Animal and Plant Health and Inspection
Residues and Contaminants in Food - RCA
Address: Esplanada dos Ministérios, Bloco D – Ed. Anexo - Ala “B” Sala 433
Zip code: 070043-900, Brasília – DF
Phone: (61) 3225 5098 / 3218 2535
Fax.: (61) 3218 3094
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Printed in Brazil
Catalogação na Fonte
Biblioteca Nacional de Agricultura – BINAGRI
Brasil. Ministério da Agricultura, Pecuária e Abastecimento.
Analysis of Residues and Contaminants in Food / Ministério da Agricultura, Pecuária e
Abastecimento. Secretaria de Defesa Agropecuária. – Brasília : MAPA/ACS, 2011.
32 p.
ISBN 978-85-7991-051-7
1. Agricultura. 2. Resíduo. 3. Poluente. I. Secretaria de Defesa Agropecuária. II. Título.
AGRIS Q03
CDU 631.879
ANALYSIS OF
Secretariat of
Animal and Plant
Ministry of
and Food Supply
RESIDUES AND
CONTAMINANTS
B R A Z I L I A N
G O V E R N M E N T
IN FOOD
ANALYSIS OF
Secretariat of
Animal and Plant
Ministry of
and Food Supply
RESIDUES AND
CONTAMINANTS
B R A Z I L I A N
G O V E R N M E N T
IN FOOD
Secretariat of
Animal and Plant
Ministry of
and Food Supply
B R A Z I L I A N
G O V E R N M E N T

residues and contaminants - Ministério da Agricultura

Transcription

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