item referencia descripción cant. 1 edpac evaporador de

Transcription

INGENIERÍA QUÍMICA. MÓDULO AVANZADO
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REFERENCIA
DESCRIPCIÓN
CANT.
EDPAC
EVAPORADOR DE PELICULA ASCENDENTE DE DOBLE
EFECTO , CONTROLADO DESDE COMPUTADOR,
COMPUESTO POR:
1
EDPAC.Unit
EFECTO
1
EDPAC/CIB
CAJA-INTERFACE DE CONTROL ELECTRÓNICA PARA
EFECTO
1
DAB
TARJETA DE ADQUISICION DE DATOS
1
EDPAC/CCSOF
SOFTWARE DE CONTROL DESDE COMPUTADOR +
ADQUISICIÓN DE DATOS + MANEJO DE DATOS PARA
EFECTO
1
2
EDPAC/CAL
SOFWARE DE APRENDIZAJE ASISTIDO DESDE
COMPUTADOR PARA EVAPORADOR DE PELICULA
ASCENDENTE DE DOBLE EFECTO (CÁLCULO Y
ANÁLISIS DE RESULTADOS)
1
3
EDPDC
EVAPORADOR DE PELICULA DESCENDENTE DE DOBLE
EFECTO, CONTROLADO DESDE COMPUTADOR (PC).
(Accesorio de EDPAC), FORMADO POR:
1
4
QDTLC
EQUIPO PARA ESTUDIO DEL COEFICIENTE DE
DIFUSION Y TRANSFERENCIA DE MASA LIQUIDA,
CONTROLADO DESDE COMPUTADOR (PC), COMPUESTO
POR:
1
QDTLC.Unit
DIFUSION Y TRANSFERENCIA DE MASA LIQUIDA
1
QDTLC/CIB
DIFUSION Y TRANSFERENCIA DE MASA LIQUIDA
1
DAB
1
QDTLC/CCSOF
ADQUISICION DE DATOS + MANEJO DE DATOS PARA
EQUIPO PARA EQUIPO PARA ESTUDIO DEL
COEFICIENTE DE DIFUSION Y TRANSFERENCIA DE
MASA LIQUIDA
1
5
QDTLC/CAL
SOFTWARE DE APRENDIZAJE
COMPUTADOR PARA EQUIPO
COEFICIENTE DE DIFUSION
MASA LIQUIDA (CÁLCULO Y
RESULTADOS)
1
6
QDTGC
EQUIPO PARA ESTUDIO DE COEFICIENTE DE
DIFUSION Y TRANSFERENCIA DE MASA GASEOSA,
CONTROLADA DESDE COMPUTADOR (PC), COMPUESTO
POR:
1
QDTGC.Unit
EQUIPO PARA ESTUDIO DE COEFICIENTE DE
DIFUSION Y TRANSFERENCIA DE MASA GASEOSA
1
QDTGC/CIB
CAJA-INTERFACE DE CONTROL ELECTRONICA
PARA EQUIPO PARA EL ESTUDIO DEL COEFICIENTE
DE DIFUSION Y TRANSFERENCIA DE MASA GASEOSA
1
DAB
1
ASISTIDO DESDE
PARA ESTUDIO DEL
Y TRANSFERENCIA DE
ANÁLISIS DE
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REFERENCIA
DESCRIPCIÓN
CANT.
6
QDTGC/CCSOF
EQUIPO PARA EL ESTUDIO DEL COEFICIENTE DE
DIFUSION Y TRANSFERENCIA DE MASA GASEOSA
1
7
QDTGC/CAL
SOFTWARE DE APRENDIZAJE ASISTIDO DESDE
COMPUTADOR PARA EQUIPO PARA ESTUDIO DE
COEFICIENTE DE DIFUSION Y TRANSFERENCIA
DE MASA GASEOSA (CÁLCULO Y ANÁLISIS DE
RESULTADOS)
1
8
QCCC
COLUMNA DE CRAQUEO, CONTROLADA DESDE
COMPUTADOR (PC), COMPUESTA POR:
1
QCCC.Unit
COLUMNA DE CRAQUEO
1
QCCC/CIB
LA COLUMNA DE CRAQUEO
1
DAB
1
QCCC/CCSOF
ADQUISICIÓN DE DATOS + MANEJO DE DATOS
PARA LA COLUMNA DE CRAQUEO.
1
QCCC/CAL
COMPUTADOR PARA COLUMNA DE CRAQUEO (CÁLCULO
Y ANÁLISIS DE RESULTADOS)
1
CAPC
COLUMNA DE ABSORCIÓN DE GASES PELICULAR,
CONTROLADA DESDE COMPUTADOR (PC), COMPUESTA
POR:
1
CAPC.Unit
COLUMNA DE ABSORCIÓN DE GASES PELICULAR
1
CAPC/CIB
CAJA-INTERFACE DE CONTROL ELECTRONICA PARA
COLUMNA DE ABSORCIÓN DE GASES PELICULAR
1
DAB
1
CAPC/CCSOF
LACOLUMNA DE ABSORCIÓN DE GASES PELICULAR
1
11
CAPC/CAL
COMPUTADOR PARA LA COLUMNA DE ABSORCIÓN DE
GASES PELICULAR (CÁLCULO Y ANÁLISIS DE
RESULTADOS)
1
12
QUCC
UNIDAD DE CRISTALIZACIÓN, CONTROLADO DESDE
COMPUTADOR (PC), FORMADO POR:
1
QUCC.Unit
UNIDAD DE CRISTALIZACIÓN
1
QUCC/CIB
CAJA INTERFACE DE CONTROL ELECTRÓNICA PARA
1
DAB
1
QUCC/CCSOF
1
13
QUCC/CAL
SOFWARE DE APRENDIZAJE ASISTIDO DESDE
COMPUTADOR PARA UNIDAD DE CRISTALIZACIÓN
1
14
QRQC
SISTEMA DE ENTRENAMIENTO DE REACTORES
QUIMICOS, CONTROLADO DESDE COMPUTADOR (PC),
COMPUESTO POR:
QRUBI
UNIDAD BASE PARA SISTEMA DE ENTRENAMIENTO
DE REACTORES QUÍMICOS
1
QRQC/CIB
EL SISTEMA DE ENTRENAMIENTO DE REACTORES
QUÍMICOS
1
9
10
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REFERENCIA
DESCRIPCIÓN
CANT.
DAB
1
QRQC/CCSOF
SOFTWARE DE CONTROL + ADQUISICIÓN DE DATOS
+ MANEJO DE DATOS PARA EL SISTEMA DE
ENTRENAMIENTO DE REACTORES QUÍMICOS
1
QRIA
REACTOR ISOTERMO CON AGITADOR
1
QRFT
REACTOR DE FLUJO TUBULAR
1
QRAD
REACTOR ADIABATICO E ISOTERMO
1
QRSA
REACTORES CON AGITADOR EN SERIE
1
15
QRQC/CAL
COMPUTADOR PARA SISTEMA DE ENTRAMIENTO DE
REACTORES QUIMICOS (CÁLCULO Y ANÁLISIS DE
RESULTADOS) DE LOS REACTORES: ISOTERMO CON
AGITACIÓN,FLUJO TUBULAR, ADIABATICO E
ISOTERMO Y CON AGITADOR EN SERIE
1
16
QRCC
REACTORES CATALÍTICOS, CONTROLADOS POR
COMPUTADOR, FORMADO POR:
1
QRCC.Unit
REACTORES CATALÍTICOS.
1
QRCC/CIB
CAJA-INTERFACE DE CONTROL ELECTRONICA PARA
1
DAB
1
QRCC/CCSOF
ADQUISICIÓN DE DATOS + MANEJO DE DATOS PARA
1
17
QRCC/CAL
COMPUTADOR PARA REACTORES CATALÍTICOS.
(CÁLCULO Y ANÁLISIS DE RESULTADOS)
1
18
QRCC-IF
UNIDAD DE ANÁLISIS DE INYECCIÓN EN FLUJO
(FIA)
1
19
QALFC
EQUIPO DE ADSORCIÓN DE LECHO FIJO,
CONTROLADO DESDE COMPUTADOR (PC), COMPUESTO
POR:
1
QALFC.Unit
EQUIPO DE ADSORCIÓN DE LECHO FIJO
1
QALFC/CIB
CAJA-INTERFACE ELECTRONICA PARA EQUIPO DE
ADSORCIÓN DE LECHO FIJO
1
DAB
1
QALFC/CCSOF
EQUIPO DE ADSORCIÓN DE LECHO FIJO
1
20
QALFC/CAL
COMPUTADOR PARA EQUIPO DE ADSORCIÓN DE
LECHO FIJO
1
21
TGV/6KW
GENERADOR DE VAPOR (6KW)
1
22
1112PARTS
COMPONENTES Y REPUESTOS
1
23
1112PA
PARTIDA ALZADA
1
24
1112IYPM
INSTALACIÓN Y PUESTA EN MARCHA
1
25
1112CAPRO
CAPACITACIÓN Y ACTUALIZACIÓN DE PROFESORES
1
26
1112TD
TÉCNICAS DIDÁCTICAS "KNOW-HOW"
1
27
1112MANU
DOCUMENTACIÓN Y MANUALES
1
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REFERENCIA
DESCRIPCIÓN
Notas:
a)Opción de multipuesto:
* Este módulo tiene una unidad solamente en cada item, nosotros podemos recomendar el número
de unidades para que 10 o 30 estudiantes puedan trabajar simultáneamente.
b)Condiciones de suministro:
* Condiciones técnicas:
- Adaptación de los laboratorios.
- Instalación de todos los equipos.
- Puesta en marcha de todos los equipos.
- Entrenamiento de cada uno de los ejercicios a ser realizados con cada uno de los equipos.
- Formación de profesores, relacionada con cada equipo didáctico y cada una de las técnicas de
enseñanza aplicada.
- Transferencia de tecnología.
* Condiciones comerciales:
- Embalaje.
- Gastos de financiación.
- Gastos C.I.F.
* Otras condiciones:
- 8 Manuales para cada uno de los equipos didácticos de EDIBON:
. Manual de servicios requeridos.
. Manual de montaje e instalación.
. Manual de la interface y del software/consola de control.
. Manual de puesta en marcha.
. Manual de normas de seguridad.
. Manual de prácticas.
. Manual de mantenimiento.
. Manual de calibración.
Ver catálogos en las páginas siguientes
CANT.
11.210 Chemical Engineering (General)
(continuation)
EDPAC. Computer Controlled Double Effect Rising Film Evaporator
Always included
in the supply:
Teaching
Technique
used
SCADA. EDIBON Computer Control System
3
5 Cables and Accessories
6 Manuals
4
Data
Software for:
Acquisition - Computer Control
Board
- Data Acquisition
- Data Management
OPEN CONTROL + MULTICONTROL + REAL TIME CONTROL
1 Unit: EDPAC. Double Effect Rising Film Evaporator
PRACTICAL POSSIBILITIES
SPECIFICATIONS SUMMARY
Items supplied as standard
EDPAC. Unit:
Anodized aluminium structure. Diagram in the front panel with similar distribution that the elements in the real unit.
2 evaporation columns with a heating area of 0.122 m2, 30 mm inner dia., 60 mm outer dia. and length of 1300 mm.2
diaphragm dosing pumps, with max. flow of 15 l/h. with flow control (0.43 ml impuls). Simple effect vacuum pump with max.
Flow of 3 m3/h and max. vacuum of 150 microns. Five 10 litre tanks (feed, concentrated and evaporated). Four 500 ml
graduated vessel for collecting concentrated and evaporated product. 2 Coil coolants with length of 400 mm. 2 High safety
pressure cut out for pressure control in the columns. Sensors: 15 of temperature, 1 of flow, 2 of pressure and 5 of level. 200 W
immersion heater, computer controlled. Solenoid valves.
The unit allows to work with several configurations:
a) Columns receive steam from the generator in an independent way. b) Steam from the first column´s jacket can be used to
heat the second column.
OPTIONAL ACCESSORY: (not included in the standard supply)
-EDPDC. Double Effect Falling Film Column for adding to EDPAC.
2 EDPAC/CIB. Control Interface Box :
With process diagram in the front panel. The unit control elements are permanently computer controlled. Simultaneous
visualization in the PC of all parameters involved in the process. Calibration of all sensors involved in the process. Real time
curves representation. All the actuators’ values can be changed at any time from the keyboard. Shield and filtered signals to
avoid external interferences. Real time PID control with flexibility of modifications from the PC keyboard of the PID
parameters, at any moment during the process. Open control allowing modifications, at any time and in a real time, of
parameters involved in the process. 3 safety levels: mechanical in the unit, electronic in control interface, and the third one in
the control software.
3 DAB. Data Acquisition Board:
PCI Data acquisition National Instruments board to be placed in a computer slot. 16 Analog inputs. Sampling rate up to:
250 KS/s. 2 Analog outputs. 24 Digital Inputs/Outputs.
4 EDPAC/CCSOF. Computer Control+Data Acquisition+Data Management Software:
Flexible, open and multicontrol software. Management, processing, comparison and storage of data. Sampling velocity up
to 250,000 data per second. It allows the registration of the alarms state and the graphic representation in real time.
5 Cables and Accessories, for normal operation.
6 Manuals: This unit is supplied with 8 manuals.
Dimensions (approx.)= Unit: 2300x1000x2300 mm. Weight :200 Kg. Control Interface: 490x330x310 mm. Weight: 10 Kg.
1
More information in: www.edibon.com/products/catalogues/en/units/chemicalengineering/
chemicalengineeringgeneral/EDPAC.pdf
1.2.3.4.-
Heating efficiency calculation.
Sugared solution concentration.
Evaporation speed determination.
Study of the evaporation speed in
function of the working conditions.
5.- Study of the relation between
condensed and evaporated product.
6.- Study of mass balance in solute.
7.- Study of mass balance in solvent.
8.- Energy balance in the evaporation
unit.
9.- Energy balance in the tubular
refrigerator.
10.-Heat transfer global coefficient
determination.
11.-Coefficient determination for a
tubular refrigerator.
12.-Study of mass balance in solute in
one column.
13.-Fruit juices and vegetable extracts
concentration.
14.-Concentrated milk obtaining.
15.-Efficiency determination of the steam
used in the process.
16.-S t e a m g e n e r a t o r e f f i c i e n c y
determination.
17.-Investigation of effect of varying
process parameters such as: vacuum,
flow rate, temperature, recycle rate.
18.-Heat transfer measurements and
calculation.
19.-Temperature Sensors Calibration.
20.-Level Sensors Calibration.
21.-Pressure Sensors Calibration.
22.-Feed Pumps Calibration.
23-41.- Practices with PLC.
CAPC. Computer Controlled Wetted Wall Gas Absorption Column
Always included
in the supply:
Teaching
Technique
used
2
3
4
Data
Software for:
Board - Data Acquisition
- Data Management
6 Manuals
Control
Interface Box
1 Unit: CAPC. Wetted Wall Gas Absorption Column
CAPC. Unit:
Unit used for demonstration and determination of liquid film mass transfer coefficients. Anodized aluminium structure.
Diagram in the front panel. Wetted wall column of glass, with water inlet and outlet sections,
height: 900 mm, internal dia.:32 mm. Feed pump of the absorption column. Air flow sensor. Water flow sensor.
Deoxygenating column of transparent acrylic material, height: 1570 mm, internal dia.: 25 mm. Deoxygenerator feed
pump. Oxygen meter. Air pump. Water tank, capacity 50 l. approx. Pumps control.
2 CAPC/CIB. Control Interface Box :
4 CAPC/CCSOF. Computer Control+Data Acquisition+Data Management Software:
Dimensions (approx.)= Unit: 1000x500x2500 mm. Weight :250 Kg. Control Interface: 490x330x310 mm. Weight: 10 Kg.
1
chemicalengineeringgeneral/CAPC.pdf
Non computer controlled version available.
Page 15
1.- Absorption process study.
2.- Calculation of liquid film mass
transfer coefficients.
3.- Variation of coefficient with mass
flow rate.
4.- Variation of oxygen flow rate to
determine power law relationship.
5.- The system chosen for the
experiment is the absorption of
oxygen into free water. In this system
the solubility and enthalpy of
solution are small and by saturating
the inlet air with water, humidification
effects are eliminated. Thus it is
possible to maintain reasonably the
isothermal conditions throughout the
column.
6.- These experiments allow a power
law relationship to be calculated.
7.- Effect of water flow rate.
8.- Effect of oxygen flow rate.
Other possible practices:
9.- Sensors calibration.
www.edibon.com
11.Chemical Engineering
2
Control
Interface Box
11.2- Chemical Engineering (General)
11
(continuation)
QDTLC. Computer Controlled Liquid Mass Transfer and Diffusion Coefficient Unit
Always included
in the supply:
Teaching
Technique
used
3
2
4
Data
Software for:
Board
- Data Acquisition
- Data Management
Control
Interface Box
6 Manuals
1
Unit: QDTLC. Liquid Mass Transfer and Diffusion
Coefficient Unit
QDTLC. Unit:
This unit allows to students to familiarise with the notions of mass transfer theory, specially about the
diffusion in liquid systems, obtaining experimental data and results which are very useful for a correct practice understanding
of the process and consequently, for the technical teaching of the students.
The experimental determination of the diffusion coefficient DAB for a binary mixture, can be done.
Anodized aluminium structure. Diagram in the front panel with similar distribution that the elements in the real unit.
Thermostatic bath. Liquid vessel. Magnetic stirrer and magnet. Heater resistance. Conductivity meter. Conductivity sensor.
Temperature sensor. Level switch. Diffusion cell, with special calculated capillaries for an accurate diffusion.
2 QDTLC/CIB. Control Interface Box :
visualization in the computer of all parameters involved in the process. Calibration of all sensors involved in the process. Real
time curves representation. All the actuators’ values can be changed at any time from the keyboard. Shield and filtered
signals to avoid external interferences. Real time PID control with flexibility of modifications from the computer keyboard of
the PID parameters, at any moment during the process. Open control allowing modifications, at any time and in a real time,
of parameters involved in the process. 3 safety levels: mechanical in the unit, electronic in control interface, and the third one
in the control software.
250 KS/s . 2 Analog outputs. 24 Digital Inputs/Outputs.
4 QDTLC/CCSOF.Computer Control+Data Acquisition+Data Management Software:
Dimensions (approx.) = Unit: 400 x 300 x 450 mm. Weight: 18 Kg.
Control Interface: 490x330x310 mm. Weight: 10 Kg.
1
1.- Fick´s law application to calculate
the diffusivity.
2.- Direct measurement of mass
transfer rates.
3.- Determination of molar density rate.
4.- Effect of concentration of diffusion
coefficients.
5.- Simple analysis of a first order
unsteady state process.
6.- Concentration and conductivity
relation.
7.- Study the effect of the temperature
on diffusion coefficients.
chemicalengineeringgeneral/QDTLC.pdf
QDTGC. Computer Controlled Gaseous Mass Transfer and Diffusion Coefficient Unit
Always included
in the supply:
Teaching
Technique
used
2
Control
Interface Box
3
4
Data
Software for:
Board
- Data Acquisition
- Data Management
6 Manuals
1
Unit: QDTGC. Gaseous Mass Transfer
and Diffusion Coefficient Unit
QDTGC. Unit:
This unit is a teaching unit that allows to students familiarise with the notions of mass transfer theory, specifically about
the diffusion of a volatile liquid into an inert gas, obtaining experimental data and results which are very useful for a correct
practice understanding of the process and, consequently, for the technical teaching of the students.
The experimental determination of the diffusion coefficient, DAB for a binary mixture, can be done.
Anodized aluminium structure. Diagram in the front panel with similar distribution that the elements in the real unit. A
precision glass capillary tube. Air pump with regulation. Traveling optic system accurate focus adjustment and mounted for
vertical axis movement against a Vernier scale (Vernier range: 0-300mm). Thermostatically controlled water transparentsided Bath. (capacity: 36 l). Heater resistance: 500W. Temperature sensor. Level switch.
2 QDTGC/CIB. Control Interface Box :
visualization in the computer of all parameters involved in the process. Calibration of all sensors involved in the process. Real
time curves representation. All the actuators’ values can be changed at any time from the keyboard. Shield and filtered
signals to avoid external interferences. Real time PID control with flexibility of modifications from the computer keyboard of
the PID parameters, at any moment during the process. Open control allowing modifications, at any time and in a real time,
of parameters involved in the process. 3 safety levels: mechanical in the unit, electronic in control interface, and the third one
in the control software.
PCI Data acquisition National Instruments board to be placed in a computer slot. 16 Analog inputs. Sampling rate up
to: 250 KS/s. 2 Analog outputs. 24 Digital Inputs/Outputs.
4 QDTGC/CCSOF. Computer Control+Data Acquisition+Data Management Software:
Dimensions (approx.)= Unit: 600 x 570 x 500 mm . Weight: 25 Kg.
Control Interface : 490x330x310 mm. Weight: 10 Kg.
1
chemicalengineeringgeneral/QDTGC.pdf
Page 16
1.- Fick´s law application to calculate
the diffusivity.
2.- Direct measurement of mass transfer
rates.
3.- Determination of molar density
transfer rate.
4.- Study of the effect of temperature on
diffusion coefficients.
5.- Use of gas laws to calculate
concentration differences in terms of
partial pressures.
6.- Plot of concentration profiles.
11.210 Chemical Engineering (General)
(continuation)
QCCC. Computer Controlled Cracking Column
Always included
in the supply:
Teaching
Technique
used
3
2
4
Data
Software for:
Board
- Data Acquisition
- Data Management
6 Manuals
1
Unit: QCCC. Cracking Column.
QCCC Unit:
This unit is a complete lab tool that allows to the students to carry out a cracking reaction, and the
study and the control of different variables that condition it. Also, the production cycle will be completed, by means of a
separation, purification and analysis of the obtained products in that cracking reaction. This unit works controlled from a
computer (PC), which allows a register of temperature and pressure data and the control of the cracking and distillation
processes. The software is of easy and intuitive control.
Anodized aluminium structure. Panels and main metallic elements in stainless steel.
Glass elements made of “Pyrex” of high thermal and mechanical resistance, as well as a perfect
chemical inertia. 250 ml. reactor flask. Reactor´s cap, with 4 inlets. Distillation column type Villeoux.
Stirring rod with stirring lock , that assures a perfect insulation of the system. Graduated filling funnel. Triplex fastening pliers.
Glass- glass joints.
4 Temperature sensors, type “J”. 2 Pressure sensors. Pressure and temperature in tables placed in the main points of the
system. Maximum working temperature: 260 ºC.Heating blanket. Plastic elements of high thermal resistance. Vacuum
pump.
2 QCCC/CIB. Control Interface Box :
4 QCCC/CCSOF. Computer Control+Data Acquisition+Data Management Software:
Dimensions (approx.) = Unit:1000 x470 x1070 mm. Weight: 75 Kg.
1
chemicalengineeringgeneral/QCCC.pdf
1.- Carry out cracking reactions.
2.- Influence of temperature in the
Ricinoleic Acid cracking reaction
(gradual increment of temperature).
3.- Influence of temperature in the
Ricinoleic Acid cracking reaction
(sudden increment of temperature).
4.- Influence of pressure in the
Ricinoleic Acid pyrolysis reaction
(working pressure too low).
5.- Influence of pressure in the
Ricinoleic Acid pyrolysis reaction
(low working pressure).
6.- Work with different heating
gradients, regulated through the
computer.
7.- Pitch as a catalyst.
8.- Simple distillation. Separation in
its components of the product
mixture of cracking.
9.- Simple distillation. Heptanal
purification.
10.- Simple distillation. Undecylenic
acid purification.
11.- Choosing the mobile phase in thin
layer Chromatography.
12.- Application of samples on TLC
plates.
13.- Thin layer chromatography plates
analysis.
14.- Work with different pressures,
regulated through the computer.
16.- Cleaning the system.
17.-Monogram of pressure.
QUCC. Computer Controlled Crystallisation Unit
Always included
in the supply:
Teaching
Technique
used
2
3
4
Data
EDIBON Software for:
Board
- Data Acquisition
- Data Management
6 Manuals
Control
Interface Box
1
Unit: QUCC. Crystallisation Unit
QUCC. Unit:
This unit demonstrates an industrially important type of crystallisation, namely solution cooling crystallisation. It introduces
students to the fundamentals of crystallisation and understanding of this industrial technique.
Anodized aluminium structure. Diagram in the front panel. Main metallic elements in stainless steel.
Jacketed crystallisation vessel with temperature control and agitation. The crystallisation reactor is thermally controlled by
means of heated water circulating in the reactor jacket. Water heater. Temperature sensor and water heater with PID control
for accurate process temperature control. Variable speed agitator. Cooling action controlled indirectly by the valved
flowmeter. Different cooling rates can be investigated by the application of different water flowrates. Water flowmeter. Heat
exchanger. Temperature sensors. Conductivity sensor for measuring solution conductivity. Set of sieves for crystal size
distribution determination. Protection devices for all electrical circuits. Batch operation. Available an accessory for continuous
operation.
2 QUCC/CIB. Control Interface Box :
4 QUCC/CCSOF. Computer Control+Data Acquisition+Data Management Software:
Dimensions (approx.) = Unit: 1000x550x700 mm. Weight: 50 Kg.
1
chemicalengineeringgeneral/QUCC.pdf
Page 17
1.- Understanding the principles of
crystallisation.
2.- Evaluation of crystallisation
efficiency and crystallisation kinetics.
3.- Mass balancing.
4.- Energy balancing.
5.- Crystall size distribution.
6.- Study of the effect of agitation rate.
7.- Study of the effect of cooling rate.
8.- Bath operation.
9.- Continuous operation (optional, if
Continuous Feed Accessory is
acquired).
10.-Sensor calibration.
www.edibon.com
Control
Interface Box
11.3- Chemical Reactors
11
QRQC. Computer Controlled Chemical Reactors Training System:
Always included
in the supply:
Teaching
Technique
used
2
1 QRUBI. Base Service Unit
Control
Interface Box
3
( )
Data
Acquisition
Board
Computer Control
Sotfware for each
Chemical Reactor
6 Manuals
4 Chemical Reactors available to be used with the Base Service Unit:
4.1
QRIA. Isothermal Reactor
with Stirrer ( )
4.2
QRIA/D. Isothermal
Reactor with Distillation (
)
4.3
QRFT. Tubular
Flow Reactor (
)
4.4
QRAD. Adiabatic
and Isothermal Reactor (
1
2
3
4
Common items for Chemical Reactors type “QR”:
QRQC Unit:
This unit is common for Chemical Reactors type “QR” and can work with one or
several reactors. It supplies all the services for the operation of each reactor.
2 dosing pumps. 3 tanks of 10 l.: two for the reagents and the other for
the products. 2 flow meters for liquids, flow range : 0.7-7 and 0.54-5.4 l/h.
Flow meter for gas, max. flow of 1440N l/h and max. pressure of 0.5 Kg cm-2O.
Thermostatic
bath of 9 l. that regulates the temperature between Tenvironment+ 5
and 200OC. Level switch. A magnetic-creep pump to impeller the water that
comes from the thermostatic bath and goes to the reactor module.Temperature
sensor to get the temperature of the reactor in a continuos way. Control system
of the reaction. Conductivity cell and conductimeter, connected to the control
interface. Dimensions (approx.) =Unit: 1100x1000x980 mm. Weight: 75 Kg.
QRQC/CIB. Control Interface Box :
This is common for Chemical Reactors type “QR” and can work with one or
several reactors. It has a process diagram in the front panel. The unit control
elements are permanently computer controlled. Simultaneous visualization in
the PC of all parameters involved in the process. Calibration of all sensors
involved in the process. Real time curves representation. All the actuators’
values can be changed at any time from the keyboard. Shield and filtered
signals to avoid external interferences. Real time PID control with flexibility of
modifications from the PC keyboard of the PID parameters, at any moment
during the process. Open control allowing modifications, at any time and in a
real time, of parameters involved in the process. 3 safety levels:one mechanical
in the unit, electronic in control interface, and the third one in the control
software. Dimensions (approx.): 490x330x310 mm. Weight: 10 Kg.
DAB. Data Acquisition Board:
PCI Data acquisition National Instruments board . 16 Analog inputs. Sampling
rate up to: 250 KS/s . 2 Analog outputs. 24 Digital Inputs / Outputs.
Chemical Reactors available to be used with the Base Service Unit:
QRIA. Isothermal Reactor with Stirrer:
Reactor insulated made of Pyrex-glass, with a max. volume of 2 l.
Agitation system with speed control and indication from 0 to 2000 rpm.
Temperature sensor. This unit is supplied with 8 manuals.
Computer Control Software for Isothermal Reactor with Stirrer (QRIA):
(#) Flexible, open and multicontrol software. Management, processing,
comparison and storage of data. Sampling velocity up to 250,000
data per second. It allows the registration of the alarms state and the
graphic representation in real time.
Dimensions (approx.) = Unit: 750x500x700mm. Weight: 50 Kg.
4.2
QRIA/D. Isothermal Reactor with Distillation:
Reactor insulated made of Pyrex-glass, with a max. volume of 2l.
Agitation system with speed control and indication from 0 to 2000 rpm.
Distillation column. Balls coolant. Coil coolant. Vacuum pump and tramp.
Funnel. Temperature sensors. This unit is supplied with 8 manuals manuals.
Computer Control Software for Isothermal Reactor with Distillation
(QRIA/D).(#)
4.3 QRFT. Tubular Flow Reactor:
Temperature controlled by a jacket of water, through a temperature
sensor. Electrical preheater of 265 W for both feeding lines. Reactor with
inner coil made of teflon of 6mm of interior dia., length 14.5 m, volume:
0.393 l. Temperature sensor, that controls the preheating temperature. This
unit is supplied with 8 manuals.
Computer Control Software for Tubular Flow Reactor (QRFT).(#)
Dimensions (approx.) =700x500x500 mm. Weight: 75 Kg.
4.4
QRAD. Adiabatic and Isothermal Reactor:
Reactor insulated made of Pyrex-glass, with a max. volume of 2l.
Nickel-plated cooper coil of 2500mm long, outer dia. of 6.7mm and inner
one of 4.1 mm. Stirrer. Water flow control of 0-6 l/min. Outer jacket made of
anodised aluminium and inner jacket made of expanded polyurethane foam
rubber. 3 Temperature sensors. This unit is supplied with 8 manuals.
Computer Control Software for Adiabatic and Isothermal Reactor
(QRAD).(#).
4.5
QRSA. Reactors with Stirrer in Series:
3 Reactors insulated made of Pyrex-glass, with a max. volume of 1 l. Each
one. Agitation system with speed control and indication from 0 to 2000 rpm.
3 Temperature sensors.This unit is supplied with 8 manuals.
Computer Control Software for Reactors with Stirrer in Series (QRSA). (#)
4.1
More information in: www.edibon.com/products/catalogues/en/units/
chemicalengineering/reactors/QRQC.pdf
)
4.5
QRSA. Reactors with
Stirrer in Series ( )
Isothermal Reactor with Stirrer (QRIA):
1.- Calibration of the temperature
sensors.
2.- Calibration of the conductivity cell.
3.- D e t e r m i n a t i o n o f t h e i o n i c
conductivities.
4.- Discontinuous operation. Obtaining
of the reaction order respect to ethylacetate.Initial velocity method.
5.- Discontinuous operation. Obtaining
of the reaction order respect to sodium
hydroxide. Initial velocity method.
6.- Discontinuous operation. Velocity
Constant Computation. Constant
sodium hydroxide initial
concentration.
7.- Discontinuous Operation. Velocity
ethyl-acetate initial concentration.
8.- Velocity equation formulation.
9.- Discontinuous Operation. Variation of
the kinetic constant with temperature.
Arrhenius Equation.
10.- Discontinuous Operation. Theoretical
and experimental conversion
comparative. Deviation from ideality.
11.- Discontinuous Operation. Mixture
effects.
12.- Continuous Operation.
13.- Continuous Operation. Mixture
effects.
14.-Measurement conductivity system:
conductimeter.
Isothermal Reactor with Distillation
(QRIA/D):
34.-Calibration of the temperature
sensors.
35.- Calibration of the conductivity cell.
36.- Determination of the ionic conductivities.
37.-Discontinuous operation. Obtaining of
the reaction order respect to ethylacetate.Initial velocity method.
38.-Discontinuous operation. Obtaining of
the reaction order respect to sodium
39.-Discontinuous operation. Velocity
sodium hydroxide initial
concentration.
40.-Discontinuous Operation. Velocity
ethyl-acetate initial concentration.
41.- Velocity equation formulation.
42.- Discontinuous Operation. Variation of
the kinetic constant with temperature.
Arrhenius Equation.
43.- Discontinuous Operation. Theoretical
and experimental conversion
comparative. Deviation from ideality.
44.- Discontinuous Operation. Mixture
effects.
45.- Continuous Operation.
46.- Continuous Operation. Mixture
effects.
conductimeter.
48.-Study of the reactive distillation.
49.-Study of alcohols condensation.
50.-Study of the organic anhydrides.
51.-Synthesis of esters.
Page 18
Tubular Flow Reactor (QRFT):
71.- Calibration of the temperature
sensors.
72.- Analysis of reagents and products.
73.- Ionic conductivities determination.
74.- Theoretical conversion of the
tubular reactor.
75.- Experimental determination of the
conversion of the tubular reactor.
76.- Dependence in the residence time.
77.- Determination of the reaction order.
78.- Dependence of the speed constant
and the conversion with the
temperature.
79.- Measurement conductivity system:
conductimeter.
80.- Complete emptying of the unit.
Adiabatic and Isothermal Reactor
(QRAD):
Sensors.
101.-Calibration of the flow sensor.
102.-Calibration of the conductivity
sensor.
103.-Determination of the ionic
conductivities.
104.-Discontinuous work. Calculation
of the order of the reaction
referred to the ethyl-acetate. Initial
velocity method.
105.-Discontinuous operation.
Determination of the order of the
reaction referred to t h e s o d i u m
Determination of the speed
constant, the initial concentration of
the sodium hydroxide is constant.
Determination of the speed constant,
the initial concentration of the ethyl
acetate is constant.
108.-Formulation of the speed equation.
109.-Discontinuous operation. Variation
of the kinetic constant when the
temperature is not constant:
Arrhenius equation.
Comparison of the theoretical and
the experimental conversion:
Deviation from the ideality.
111.-Calculation of the heat transference
coefficient of the coil.
112.-Calculation of the hydrolysis
reaction enthalpy.
113.-Discontinuous operation. Mixture
effects.
114.-Continuous operation.
conductimeter.
Practices to be done with the Reactors
with Stirrer in Series (QRSA):
sensors.
136.-Calibration of the conductivity cell.
137.-Determination of the ionic
conductivities.
138.-Work with just one reactor in
continuous.
139.-Work with just one reactor in
continuous with mixture effects.
140.-Work with 3 reactors in continuous.
11.3- Chemical Reactors
www.edibon.com/products/index.php?area=chemicalengineering&subarea=reactors&lang=en
QRC. Computer Controlled Chemical Reactors Trainer:
3
Data
Acquisition
Board
2
Control
Interface Box
1
QUSC.
Service Unit
QRCAC. Continuous Stirred
Tank Reactor ( )
3.2
6 Manuals
PID CONTROL
(Open Control + Multicontrol + Real Time Control)
- From COMPUTER (standard)
- From PLC (optional)
Available Chemical Reactors to be used with
Service Unit (QUSC) and SCADA System
4
3.1
QRTC. Tubular Flow
Reactor (
3.3
)
QRDC. Batch Reactor
( )
Other available Chemical Reactors
3.4
NE
W
to be used with the Unit (QUSC) and SCADA system:
- QRLC. Laminar Flow Reactor
- QRPC. Plug Flow Reactor
NE
W
QRCC. Computer Controlled Catalytic Reactors
3
2
4
Data
Acquisition
Board
Control
Interface Box
Software for:
- Computer Control
- Data Acquisition
- Data Management
6 Manuals
PID CONTROL
(Open Control + Multicontrol + Real Time Control)
- From COMPUTER (standard)
- From PLC (optional)
1
( )
Computer Control
Software for each
Chemical Reactor
Unit: QRCC. Catalytic Reactors
Non computer controlled version available too.
www.edibon.com
Optional accessory:
QRCC-IF. Flow Injection
Analysis (FIA) unit
Page 72
QRSC. Stirred Tank Reactors in Series
( )

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