THE `40th INTERNATIONAL SYMPOSIUM ON CAPILLARY

Transcription

THE ‘40th INTERNATIONAL SYMPOSIUM ON CAPILLARY
CHROMATOGRAPHY’
and
THE ‘13th GC×GC SYMPOSIUM’
May 29 – June 03, 2016
Riva del Garda Fierecongressi, Riva del Garda, Italy
The ‘M.J.E. Golay Award 2016’ will be presented
The ‘Leslie S. Ettre Award 2016’ will be presented
The ‘Giorgio Nota Award 2016’ will be presented
The ‘John Phillips Award 2016’ will be presented
The ‘GCxGC Lifetime Achievement Award 2016’ will be presented
The ‘Genzo Shimadzu Best Oral/Poster Award 2016’ will be presented
The ‘Richard Sacks Best Poster Award 2016’ will be presented
The ‘Springer Best Poster Award 2016’ will be presented
- Conference Address -
Riva del Garda Fierecongressi
Parco Lido
I-38066 Riva del Garda,
Italy
Tel.:
Fax:
E-mail:
Web:
+39-0464-520000 (Info Desk)
+39-0464-555255
[email protected]
http://www.rivadelgardafierecongressi.it
- Symposium Office The Symposium Office is located in the entrance hall of the Congress Center.
Opening Hours:
Sunday, May 29
Monday, May 30
08:30 until 10:00
GC×GC Course
16:00 until 18:00
13 GC×GC Symposium
08:00 until 11:30
13 GC×GC Symposium
16:00 until 20:00
40 ISCC
Tuesday, May 31
08:00 until 16:00
and thereafter
08:30 until 16:00
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- Posters With the exception of the plenary and key note lectures, all contributions are posters.
Posters will not be introduced by oral presentation
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For the 40 ISCC, the posters will be shown from Tuesday to Friday (till 11:00).
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For the 13 GC×GC, the posters will be shown from Monday to Friday (till 11:00).
For discussion, please meet the authors at their numbered poster board at the time indicated
in the scientific program.
Special stickers to hang up the posters are available at the Registration Desk. The use
of pins is not allowed.
- Submission of Manuscripts Participants are invited to contribute manuscripts connected to their presented work at the
RIVA 2016 Conference for possible publication in either the Journal of Chromatography A with
the intention of eventual publication in a Virtual Special Issue (VSI) that is dedicated to the
meeting. All manuscripts will be subject to the usual peer reviewing procedure.
A Virtual Special Issue implies that all papers will be handled and reviewed as regular
submissions to the journal. Once accepted, papers will be published individually in regular
issues. A footnote will indicate at which conference the paper was presented, and this will be
used for selection and linking to the Virtual Special Issue.
The Virtual Special Issue will be prepared and subsequently placed on an individual Journal
Special Issue site – with links to the papers on Science Direct.
The Preface and photos (with a possibility also for videos, e.g. from the poster sessions) can
be added to the Virtual Special Issue resulting in an expanded special issue, not available in
the printed version.
When preparing your manuscript please carefully follow the journal's Guide to Authors, which
you can find on the online submission site: http://ees.elsevier.com/chroma.
At the beginning of May you will be invited by Journal of Chromatography A to submit your
article via the journal's online submission and reviewing system which is accessible at
http://ees.elsevier.com/chroma.
To submit:
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•
•
•
Go to: http://ees.elsevier.com/chroma
Click on the “Submit Paper” option from the top menu
Enter your user name and password (first time users will have to register)
After entering the title of your manuscript, please select RIVA 2016 as the ‘Article
Type’
Follow the remaining step-by-step instructions to submit your paper
Points to note:
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The deadline to submit your manuscript for the RIVA 2016 symposium issue of
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Journal of Chromatography A is 24 September 2016
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In your cover letter please mention that your manuscript is intended for the RIVA
2016 special issue
If you experience any technical problems or have any technical questions during the
submission process, please contact Elsevier Author’s Support: [email protected].
If you have any questions on the submission and reviewing process, please contact the
Editorial Office: [email protected]
Book of Abstracts
The book of abstracts will be delivered on a USB upon registration
- Badges -
Delegates are requested to wear their badges at all times.
Failure to do so will result in refusal of admission to the scientific and social activities.
Only yellow badges have access to the Scientific Program of GC×GC and blue badges
to the Scientific Program of ISCC. Red badges have access only to the exhibition area
as booth personnel. Participants registered to the GC×GC short course will receive an
additional badge valid only for Sunday MAY 29, 2016. White badges for accompanying
persons have no access to the scientific activities.
- Coffee Breaks -
Coffee and soft drinks will be served in the exhibition hall during the coffee break times only.
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The coffee breaks for the 13 GC×GC Symposium (Monday, May 30) will take place on the
first floor of the Congress Hall.
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- Exhibition Exhibition opening hours:
Tuesday, May 31
Wednesday, June 01
Thursday, June 02
Friday, June 03
10:00 – 17:30
09:00 – 17:30
09:00 – 17:00
09:00 – 11:00
Exhibiting Companies
Agilent Technologies
Brechbühler AG
Chromaleont
DANI Instruments S.p.a.
Thermo Fisher Scientific
Trajan
Vici AG International
VUV Analytics
Elementar/Isoprime
Waters
Entech Instruments
YMC
Est Analytical
Zoex Europe
Gerstel GmbH & Co. KG
GL Sciences B.V.
Hamilton Bonaduz AG
HTA
Ion Bench
Labservice Analytica S.r.l.
LECO
Markes International
Merck/Sigma-Aldrich/Supelco
PAS Technology Deutschland GmbH
Peak Scientific
Restek
Shimadzu Europa GmbH
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Publishing Houses
Advanstar (LCGC Europe)
Chromatography Today
Elsevier
LAB world
Separation Science
Springer
Technology Networks
Tecnoedizioni
The Analytical Scientist
TKS Teknoscienze/Chemistry Today
- Social Program The following program is offered to the delegates:
All Days
Coffee Breaks offered by the
Diamond Sponsor Shimadzu Europa
GmbH
Sunday, May 29
18:00
GCxGC Course Cocktail offered by
Location: First floor Congress Centre
Monday, May 30
19:15
Welcome Reception
offered by DANI Instruments
Location: Exhibition Hall
Tuesday, June 01
21:00
Concert offered by PerkinElmer Inc.,
Location: Room 1000, Congress
Centre
22:15
Cocktail offered by Gerstel GmbH &
Co. KG
Location: the Congress Centre
18:45
Wine and Cheese offered by Agilent
Technologies
Location: Hotel Sole, Piazza 3
Novembre, Riva del Garda (TN)
Wednesday, June 02
- Company Dinners -
Sunday, May 29
19:00
Invited SILEP program Dinner
offered by Merck/SigmaAldrich/Supelco
Location: Hotel Du Lac et Du Park
Please bring your invitation card
Thursday, June 02
19.00
Invited Speaker Dinner offered by
Location: Hotel Du Lac et Du Park
Please bring your invitation card
- Guest Program Guided tours will be organized by Travel Agency Rivatour.
The registration and the purchase of the tickets will take place at the Congress Hall
Desk.
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- Travel -
Symposium coaches from Riva del Garda to the main Airports will be organized.
For reservation and tickets, please contact the Congress Hall desk.
- COMMITTEE MEMBERS th
- Scientific Committee 40 ISCC Daniel Armstrong
(U.S.A.)
Carlo Bicchi
(Italy)
Salvatore Fanali
(Italy)
Christian Huber
(Austria)
Hans-Gerd Janssen
(The Netherlands)
Kyokatsu Jinno
(Japan)
James Jorgenson
(U.S.A.)
Robert T. Kennedy
(U.S.A.)
Milton L. Lee
(U.S.A.)
Luigi Mondello
(Italy)
Milos V. Novotny
(U.S.A.)
Michael Ramsey
(U.S.A.)
Pat Sandra
(Belgium)
Frantisek Svec
(U.S.A.)
Guowang Xu
(China)
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- Organizing Committee 40 ISCC Flavio Bedini
(Italy)
Achille Cappiello
(Italy)
Frank David
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(Belgium)
John Dimandja
(USA)
Paola Dugo
(Italy)
Peter Myers
(United Kingdom)
Albino Sironi
(Italy)
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- Honorary Committee 40 ISCC Keith D. Bartle
(United Kingdom)
Carel A. Cramers
(The Netherlands)
Rudolf E. Kaiser
Harold M. McNair
Gerhard Schomburg
(Germany)
(U.S.A.)
(Germany)
Shigeru Terabe
(Japan)
Sorin Trestianu
(Italy)
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- Scientific Committee 13 GC×GC Philip Marriott
John Dimandja
Hans-Gerd Janssen
Luigi Mondello
(Australia)
(U.S.A.)
(The Netherlands)
(Italy)
John Seeley
(U.S.A.)
Robert Synovec
(U.S.A.)
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- Organizing Committee 13 GC×GC Chiara Cordero
Frank Dorman
Hans-Georg Schmarr
Peter Q. Tranchida
(Italy)
(U.S.A.)
(Germany)
(Italy)
- CHAIRMAN Luigi Mondello
Dipartimento di Scienze Chimiche, Biologiche,
Farmaceutiche ed Ambientali
Viale Annunziata, University of Messina
98168, Messina, Italy
Tel:
+39-090-6766536
Fax:
+39-090-358220
E-mail:
[email protected]
Web:
www.sepsci.unime.it
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- LOCAL ORGANIZATION Margherita Barilà
([email protected])
Elisa Giglio
([email protected])
Tel.:
+39-334-3612788
Fax:
+39-090-9080155
Chromaleont S.r.l.
Viale Boccetta, 70, 98122 – Messina, Italy
- SPONSORS RIVA 2016 We would like to thank the sponsors for their generous support.
DIAMOND SPONSOR
Agilent Technologies
PLATINUM SPONSORS
Advanstar (LCGC Europe)
DANI Instruments S.p.a.
Gerstel GmbH & Co. KG
PerkinElmer, Inc.
Merck/Sigma-Aldrich/Supelco
Waters
GOLD SPONSOR
LECO
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SILVER SPONSORS
Markes International
Peak Scientific
Zoex Europe
BRONZE SPONSORS
Aqualis
Brechbühler AG
CASSS
Elementar/Isoprime
Hamilton Bonaduz AG
JEOL Europe
Pfizer
Restek
Thermo Fisher Scientific
VUV Analytics
OTHER SPONSOR
Ion Bench
MSExpertise
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PUBLISHING HOUSES
Advanstar/UBM (LCGC Europe)
Chromatography Today
Elsevier
LABworld
Separation Science
Springer
Technology Networks
TecnoEdizioni
TKS (Tekno Scienze Publisher)
COOPERATING ORGANIZATIONS
Association Francophone des Sciences Séparatives
Central European Group for Separation Sciences
Chinese American Chromatography Association
Chromatography and Electrophoresis Group of the Czech Chemical Society
Italian Chemical Society
Environment Chemistry and Cultural Heritage Division of the Italian Chemical Society
Division of Mass Spectrometry of the Italian Chemical Society
Interdivisional Group of Food Chemistry of the Italian Chemical Society
Interdivisional Group of Separation Science of the Italian Chemical Society
Hungarian Society for Separation Sciences
Norwegian Chromatographic Group of the Norwegian Chemical Society
Separation Science Group Royal Society of Chemistry
Separation Science Section of the Societatea de Chimie din Romania
Slovenian Chemical Society
Sociedad Espagnola dem Cromatografia y Tecnicas Afines
The Japanese Society for Chromatographic Sciences
Ukranian Chromatographic Society
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Comprehensive Two-Dimensional Gas
Chromatography (GC×GC)Course:
Introduction, Advances, Mass Spectrometry and
Applications
Sunday, May 29, 2016
08:30 – 09:00
On-site registration/Welcome - Room 300
09:00 – 10:00
PRINCIPLES AND INSTRUMENTATIONS
John Dimandja
Spelman College, Atlanta, GA, United States
10:00 – 10:45
OPTIMIZATION
Hans-Gerd Janssen
Unilever, Vlaardingen, The Netherlands
10:45 – 11:15
Coffee Break
11:15 – 12:00
DATA ANALYSIS
Robert Synovec
University of Washington, Seattle, WA, United States
12:00 – 12:45
GC×GC-MS
Peter Q. Tranchida
University of Messina, Messina, Italy
12:45 – 14:15
Lunch (own arrangement)
14:15 – 15:40
APPLICATIONS
Philip Marriott
Monash University, Clayton, Australia
15:40 – 16:30
LATEST TRENDS IN GC×GC
John Dimandja, Hans-Gerd Janssen, Robert Synovec, Peter Q. Tranchida, Philip Marriott
Spelman College, Atlanta, GA, United States, University of Washington, Seattle, WA, United States,
University of Messina, Messina, Italy, and Monash University, Clayton, Australia.
16:30 – 17:00
Coffee Break
17:00 – 17:45
Q/A SESSION
17:45 – 18:00
CLOSING REMARKS
18:00
Cocktail offered by Shimadzu Europe GmbH for the GC×GC Course Participants
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SCIENTIFIC PROGRAM 13th GC×GC
Monday, May 30, 2016
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08:30 – 08:40
Opening Address 13 GC×GC and Lifetime Achievement Award Presentation - Room 1000
Chairperson:
Philip Marriott
John Dimandja
Luigi Mondello
08:40 – 09:05
Award Lecture
Chairperson:
John Dimandja
Le.01 COMPREHENSIVE 2D GAS CHROMATOGRAPHY. A 17-YEAR “BALANCE”
Luigi Mondello
09:10 – 10:50
GC×GC Session 1 - FUNDAMENTALS 1Room 1000
Chairperson:
John Dimandja
GC×GC Session 2 - APPLICATIONS –
Food 1 - Room 300 + Belvedere
Chairperson:
Lourdes Ramos
Dpt Instrum Anal & Environ Chem - IQOG-CSIC,
Madrid, Spain
09:10
Le.02
CHIRALITY, MOLECULAR
INTERCONVERSIONS AND OTHER
SEPARATIONS AND PROCESSES
REVEALED IN COMPREHENSIVE TWODIMENSIONAL GAS CHROMATOGRAPHY
SPACE
Philip Marriott, Yong Foo Wong, Yada Nolvachai,
Chadin Kulsing, Sung-Tong Chin
Monash University, Wellington Rd, 3800 Clayton,
Australia
Le.07
APPLICATION OF TWO DIMENSIONAL GAS
CHROMATOGRAPHY TO THE
MEASUREMENT OF FATTY ACIDS AND
ALKENYL ETHERS IN ANIMAL TISSUES
1
2
Pierluigi Delmonte , Xabier Belaunzaran , John
3
2
Kramer , Noelia Aldai
1
Office of Regulatory Science - Center for Food
Safety and Applied Nutrition, Food and Drug
Administration, 20740 College Park, MD, United
States
2
University of the Basque Country, Avda. Miguel
de Unamuno 3, 01006 Vitoria-Gasteiz, Spain
3
Retired from Agriculture and Agri-Food Canada,
93 Stone Road West, N1G 5C9 Guelph, Ontario,
Canada
09:30
Le.03
OPTIMISATION IN FLOW-MODULATED
COMPREHENSIVE GC×GC WITH FLAME
IONISATION AND VACUUM UV DETECTION
1,2
3
Hans-Gerd Janssen , Sjaak de Koning , Larissa
3
Ram
1
Central Analytical Science Unit – Unilever
Research Laboratory, P.O. Box 114 A3280, 3130
AC Vlaardigen, Netherlands
2
Analytical-Chemistry Group – University of
Amsterdam, Sciece Park 904, 1098 XH,
Netherlands
3
Da Vinci, Cairostraat 10, 3047 BC Rotterdam,
Netherlands
Le.08
CHALLENGES IN TRANSFERING METHODS
FROM THERMAL TO DIFFERENTIAL FLOW
MODULATED GC×GC-MS/FID: FOOD “OMICS”
INVESTIGATIONS
1
2
Chiara Cordero , Stephen E. Reichenbach ,
1
1
3
Federico Magagna , Erica Liberto , Luigi Cobelli ,
4
4
Armando Miliazza , Matthew Giardina , Carlo
1
Bicchi
1
Dipartimento di Scienza e Tecnologia del
Farmaco - University of Turin, Via Pietro Giuria, 9,
I-10125 Turin, Italy
2
University of Nebraska , 1400 R Street, 685880115 Lincoln, United States
3
SRA Instruments, Via alla Castellana 3, 20063
Cernusco sul Naviglio (Milan), Italy
4
Agilent Technologies, Cernusco sul Naviglio,
20063 Cernusco sul Naviglio (Milan), Italy
13
09:50
Le.04
CURRENT STATE OF THERMODYNAMICBASED PREDICTIONS OF GC AND GC×GC
SEPARATIONS
James J. Harynuk, Keisean A. Stevenson
Department of Chemistry - University of Alberta,
11227 Saskatchewan Drive, T6G2G2 Edmonton,
AB, Canada
Le.09
CULTIVAR-SPECIFIC CHANGES OF APPLE
METABOLITE PROFILE DURING COLD
STORAGE DETERMINED BY GC×GC-QMS
Christoph H. Weinert, Mona Ehlers, Carina I.
Mack, Björn Egert, Bernhard Trierweiler, Sabine
E. Kulling
Department of Safety and Quality of Fruit and
Vegetables - Max Rubner-Institut, Haid-und-NeuStr. 9, 76131 Karlsruhe, Germany
10:10
Le.05
FAST MULTIPLEXING OF ANALYTICAL
PARAMETERS FOR PERFORMANCE
IMPROVEMENTS IN GCxGC-TOF MS
Laura McGregor, Nick Bukowski, Matthew
Edwards, Massimo Santoro, Joe Blanch
Markes International, Gwaun Elai Medi-Science
Campus, CF72 8XL Llantrisant, United Kingdom
Le.10
VOLATILES OF COSTA RICAN PAPAYA
(CARICA PAPAYA L.) FRUIT PURÉES
ANALYZED BY MULTIDIMENSIONAL GC
METHODS
1
2
Hans-Georg Schmarr , Veronika Lieb , Reinhold
2,3
2
Carle , Christof B. Steingass
1
Viticulture and Enology - DLR Rheinpfalz,
Breitenweg 71, 67431 Neustadt an der
Weinstrasse, Germany
2
Institute of Food Science and Biotechnology University of Hohenheim, Garbenstr. 25, 70599
Hohenheim, Germany
3
Biological Science Department - King Abdulaziz
University, P.O. Box 80257, 21589 Jeddah, Saudi
Arabia
10:30
Le.06
A METHOD DEVELOPMENT SOFTWARE
TOOL FOR COMPREHENSIVE TWO
DIMENSIONAL GAS CHROMATOGRAPHY
EVALUATED FOR GC×GC-TOFMS
1
2
Mark Merrick , Leonid M. Blumberg , Viatcheslav
1
Artaev
1
Separation Science R&D - LECO Corporation,
3000 Lakeview Avenue R&D, 49085 St. Joseph,
MI, United States
2
Advachrom, P.O. Box 1243, 19801 Wilmington,
DE, United States
Le.11
GCxGC-TOFMS QUANTIFICATION OF THE
EXTENDED LIST OF SUSPECTED
ALLERGENS AND REGULATED COMPOUNDS
IN FRAGRANCE MATERIALS, FROM A
CRITICAL CHOICE OF GC×GC PARAMETERS
TO AN IMPLEMENTATION FOR A GLOBAL
PROGRAM
1
1
Thomas Dutriez , Laetitia Duffour , Diane
1
2
3
Pétermann , Neil Owen , Greg Adamson
1
RAPS Analytical Laboratory - Givaudan, Chemin
de la parfumerie 5, 1214 Vernier, Switzerland
2
RAPS Analytical - Givaudan UK Ltd, Kennington
Road Ashford Kent, TN24 0LT Ashford, United
Kingdom
3
Global Regulatory Affairs, Product Safety &
Sustainability - Givaudan Fragrances Corp. 717
Ridgedale Avenue, 07936 East Hanover
Ridgedale, United States
10:50-11:20
11:20 – 13:00
11:20
Coffee Break
GC×GC Session 3 - FUNDAMENTALS 2 Room 1000
Chairperson:
Philip Marriott
GC×GC Session 4 - APPLICATIONS - Food 2Room 300 + Belvedere
Chairperson:
Hans-Georg Schmarr
Viticulture and Enology - Neustadt an der
Weinstrasse, Germany
Le.12
HYPHENATIONS OF (LOW-)FLOW
MODULATION COMPREHENSIVE 2D GC
WITH SINGLE QUADRUPOLE, TRIPLE
QUADRUPOLE AND HIGH-RESOLUTION
TIME-OF-FLIGHT MASS SPECTROMETRY
1
2
Peter Q. Tranchida , Flavio A. Franchina ,
2
1
Giorgia Purcaro , Mariarosa Maimone , Simona
1
1,2
Salivo , Luigi Mondello
1
Dipartimento di Scienze Chimiche, Biologiche,
Farmaceutiche ed Ambientali - University of
Messina, viale Annunziata, 98168 Messina, Italy
2
Chromaleont s.r.l, c/o University of Messina,
viale Annunziata, 98168 Messina, Italy
Le.17
SCREENING FOR NIAS: THE POTENTIAL OF
GC×GC FOR COMPREHENSIVE ANALYSIS OF
MIGRANTS FROM FOOD CONTACT
MATERIALS
Maurus Biedermann
Official Food Control Authority - of the Canton of
Zurich, Fehrenstrasse 15, 8032 Zurich,
Switzerland
14
11:40
Le.13
EXPLODING A PEAK CAPACITY INCREASE
RECORD BY USING HYDROGEN CARRIER
GAS FOR COMPREHENSIVE TWODIMENSIONAL GAS CHROMATOGRAPHY TIME-OF-FLIGHT MASS SPECTROMETRY
1
1
Jack Cochran , Julie Kowalski , Christopher
1
1
1
Rattray , Amanda Rigdon , Jaap de Zeeuw ,
2
Mark Merrick
1
Innovations - Restek Corporation, 110 Benner
Circle, 16823, PA Bellefonte, United States
2
LECO, 3000 Lakeview Drive, 49085 St Joseph,
United States
Le.18
IDENTIFICATION OF COMPOUNDS
MIGRATING FROM CONSUMER PRODUCTS
USING GC×GC-TOFMS
1
1
Natalie Rosenfelder , Susanne Maier , Uwe
1
2
Lauber , Juergen Wendt
1
Department Consumer Goods - Chemical and
Veterinary Investigations Office Stuttgart
(CVUAS), Schaflandstr. 3/2, 70736 Fellbach,
Germany
2
European Application & Technology Centre LECO, Max-Dohrn-Straße 8-10, 10589 Berlin,
Germany
12:00
Le.14
CHARACTERIZATION OF METABOLOME IN
DEVELOPMENT OF METABOLIC COMORBIDIS OF PSYCHOSIS BY GC×GC-TOF
MS
1
1
Kajetan Trost , Tommi Suvitaival , Outi
2,3
2,4
1
Mantere , Tuula Kieseppä , Ismo Mattila ,
5
1
Päivi Pöhö , Tuulia Hyötyläinen , Jaana
2
1
Suvisaari , Matej Oresic
1
Steno Diabetes Center A/S, Niels Steensens
Vej 2-4, 2820 Gentofte, Denmark
2
Mental Health Unit - National Institute for
Health and Welfare, Mannerheimintie 166 A,
00271 Helsinki, Finland
3
Department of Psychiatry - McGill University,
1033 Pine Avenue West, H3A 1A1 Montréal, QC,
Canada
4
Department of Psychiatry - Helsinki University
and Helsinki University Hospital, P.O. Box 590,
5
Faculty of Pharmacy - University of Helsinki,
Viikinkaari 5 E, 00014 Helsinki, Finland
Le.19
ASSESSMENT OF THE
ORGANOHALOGENATED BURDEN IN
BIOLOGICAL SAMPLES BY NON-TARGET
GC×GC−TOF MS
1
2
Juan Escobar-Arnanz , Xavier Ortiz , Miren
2
2
1
Pena-Abaurrea , Eric Reiner , Lourdes Ramos
1
Dpt Instrum Anal & Environ Chem - IQOG-CSIC,
Juan de la Cierva 3, 28006 Madrid, Spain
2
Ontario Ministry of the Environmental and
Climate Change, 125 Resources Road, M9P 3V6
Toronto, Canada
12:20
Le.15
EVALUATION OF ORTHOGONALITY
ASSESSMENT TOOLS IN GC×GC
1,2
1,3
Jaroslava Jacova , Alzbeta Gardlo , David
1,2
3
1,2
Friedecky , Karel Hron , Tomas Adam , Jean
4,5
Marie D. Dimandja
1
Laboratory of Metabolomics - Palacky
University Olomouc, Hnevotinska 5, 779 00
Olomouc, Czech Republic
2
Laboratory for Inherited Metabolic Disorders University Hospital Olomouc, I. P. Pavlova 6, 775
20 Olomouc, Czech Republic
3
Department of Mathematical Analysis and
Applications of Mathematics - Palacky University,
Faculty of Science, 17. Listopadu 12, 77146
Olomouc, Czech Republic
4
Institute for Bioengineering and Bioscience Georgia Tech, 315 Ferst Dr. NW, 30332 Atlanta,
United States
5
Department of Chemistry and Biochemistry Spelman College, Spelman Lane SW, 30314
Atlanta, United States
Le.20
PROFILING VOLATILE COMPOUNDS WITH
ANALYSIS OF KEY ODORANTS FOR
MONITORING TECHNOLOGICAL AND
QUALITY CHANGES IN VIRGIN OILS
Henryk H. Jelen, Anna Gracka, Malgorzata
Majcher
Faculty of Food Science and Nutrition - Poznan
University of Life Sciences, Wojska Polskiego 31,
60-624 Poznan, Poland
15
12:40
Le.16
ION PEAK DETECTION FOR
COMPREHENSIVE MULTIDIMENSIONAL
CHROMATOGRAPHY
1
1
Qingping Tao , Chase Heble , Stephen
2,1
2
Reichenbach , Davis W. Rempe , Chiara
3
4
Cordero , Claudia Zini
1
GC Image, LLC, PO Box 57403, 68505-7403
Lincoln, United States
2
Computer Science & Engineering - University
of Nebraska, 260 Avery, 68588-0115 Lincoln,
United States
3
Universita degli Studi di Torino, Via Pietro
Giuria, 9, I-10125 Torino, Italy
4
Universidade Federal do Rio Grande do Sul,
Av. Bento Gonçalves, 9500, 91501-970 Porto
AlegreRS, Brazil
Le.21
ALL ION DIFFERENTIAL ANALYSIS IN
PRODUCT CONTROL APPLICATIONS USING
COMPREHENSIVE GC×GC/MS
Marco Ruijken
R&D - MsMetrix, Doornhoecklaan 81, 3601JT
maarssen, Netherlands
13:00-14:00
Lunch Break (on your own)
14:00-16:20
GC×GC Session 5: APPLICATIONS –
Environmental - Room 1000
Chairperson:
James J. Harynuk
University of Alberta, Edmonton, Canada
GC×GC Session 6: APPLICATIONS –
Food/Biological - Room 300 + 100
Chairperson:
Hans-Gerd Janssen
Unilever, Vlaardigen, Netherlands
14:00
Le.22
ENVIRONMENTAL FORENSIC
INVESTIGATION OF WATER QUALITY
UTILIZING GC×GC-TOF MS AND GC×GC-HRT
TOF MS
Frank Dorman
Forensic Science - Penn State University, 107
Whitmore Laboratory, 16802 University Park,
PA, United States
Le.29
GC×GC-(HR)TOFMS IN CANCER RESEARCH
1
1
Romain Pesesse , Pierre-Hughes Stefanuto ,
2
2
Virginie Bertrand , Marie-Claire Gillet , Marie3
3
3
Alice Meuwis , Edouard Louis , Renaud Louis ,
1
Jean-Francois F. Focant
1
CART, Organic and Biological Analytical
Chemistry, Department of Chemistry - University
of Liège, Allée du 6 aoùt B6C, B-4130 Liège,
Belgium
2
CART, Mammalian Cell Culture Laboratory University of Liège, Allée du 6 aoùt B6C, B-4130
Liège, Belgium
3
University Hospital Center (CHU) - University of
Liège, Allée du 6 aoùt B6C, B-4130 Liège, Belgium
14:20
Le.23
STRATEGIES AND TECHNIQUES FOR
IDENTIFYING TARGET AND NON-TARGET
COMPOUNDS IN ENVIRONMENTAL
SAMPLES
1
2
3
Eric J. Reiner , Karl J. Jobst , Liad Haimovici ,
3
3
Dave Megson , Alina Muscalu , Miren
3
3
3
PenaAbaurrea , Li Shen , Ralph Ruffolo , Paul
3
Helm
1
University of Toronto, 58 Beaver Bend Cres ,
ON M9B 5R3 Toronto, Canada
2
Department of Chemistry and Chemical Biology
- McMaster University, 1280 Main St W, L8S
4M1 Hamilton, Canada
3
LaSB MOCC, 125 Resources Rd, M9P 3V6
Toronto, Canada
Le.30
CHARACTERIZATION OF THE CLINICAL P.
AERUGINOSA VOLATILE METABOLOME
USING GC×GC-TOFMS
1,
2
Heather D. Bean Christiaan A. Rees , Mavra
2
2
Nasir , Jane E. Hill
1
School of Life Sciences - Arizona State
University, PO Box 874501, 85287-4501 Tempe,
United States
2
Thayer School of Engineering - Dartmouth
College, 14 Engineering Drive, 03755 Hanover,
United States
14:40
Le.24
COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHY FOR THE ANALYSIS
OF ENVIRONMENTAL CONTAMINANTS:
THERMAL- AND VALVE-BASED
APPROACHES
1
1
Tadeusz Gorecki , Haleigh Boswell , Matthew
2,1
Edwards
1
Department of Chemistry - University of
Waterloo, 200 University Avenue W., N2L 3G1
Waterloo, Ontario, Canada
2
Markes International Ltd, Gwaun Elai MediScience Campus, CF72 8XL Llantrisant, United
Kingdom
Le.31
URINARY STEROID PROFILING BY
COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHY/ MASS
SPECTROMETRY
1
2
Zhanpin Wu , Bernhard Dick
1
Zoex Corporation, 12221 Fuqua Rd, Suite A,
77034 Houston, United States
2
Department of Nephrology - University of
Hospital Bern, Freiburgstrasse 10, 3010 Bern,
Switzerland
16
15:00
Le.25
IDENTIFICATION OF PERSISTENT ORGANIC
POLLUTANTS IN HOUSEHOLD DUST BY
GC×GC/MS USING AN LC/MS INSTRUMENT
1
2
Karl J. Jobst , Eric J. Reiner
1
Department of Chemistry and Chemical Biology
- McMaster University, 1280 Main Street West,
L8S 4M1 Hamilton, Canada
2
Toronto, 80 St. George Street, M5S 3H6
Toronto, Canada
Le.32
USING EXHALED BREATH TO DIAGNOSE
RESPIRATORY INFECTIONS: APPLYING
MULTIDIMENSIONAL CHROMATOGRAPHY
COUPLED TO MASS SPECTROMETRY TO
THE CLINIC
1
2
3
Jane E. Hill , Heather D. Bean , Edith Zemanick ,
4
5
Alix Ashare , Theodore Mellors , Christiaan
5
5
6
Rees , Mavra Nasir , Andrew Black , Boitumelo
6
Maitshotlo
1
School of Engineering - Dartmouth College, 14
Engineering Drive, 03755 Hanover, United States
2
Arizona State University, 427 East Tyler Mall,
85287 Tempe, United States
3
School of Medicine - University of Colorado,
13123 E 16th Avenue, 80045 Aurora, United
States
4
School of Medicine - Dartmouth College, 1 Rope
Ferry Rd, 03755 Hanover, United States
5
United States
6
Wits Reproductive Health and HIV Institute, 22
Esselen St, 2001 Hillbrow, South Africa
15:20
Le.26
ANALYSIS OF RIVER, BOREHOLE AND
SWIMMING POOL WATER BY
COMPREHENSIVE GAS CHROMATOGRAPHY
– TIME OF FLIGHT MASS SPECTROMETRY
AND COMPREHENSIVE GAS
CHROMATOGRAPHY – HIGH RESOLUTION
TIME OF FLIGHT MASS SPECTROMETRY
1
2
Charles P. Gorst-Allman , Yvette Naude
1
Separation Science - LECO Africa (Pty) Ltd, 3
Vuurslag Avenue, 1620 Spartan Ext.7, Kempton,
South Africa
2
University of Pretoria, Pretoria, South Africa,
0028 Pretoria, South Africa
Le.33
DATA PROCESSING AND IDENTIFICATION
WORKFLOW IN BIOMARKER DISCOVERY
WITH GC×GC-TOF MS AND GC×GC-HRT TOF
MS
1
1
Tuulia Hyötyläinen , Ismo Mattila , Tomás
2
2
2
Kovalczuk , David E. Alonso , Joe Binkley , Matej
3
Oresic
1
Steno Diabetes Center, Niels Steensens Vej 2,
2820 Gentofte, Denmark
2
LECO Corporation, Plaská 66, 323 00 Plzen,
Czech Republic
3
Turku Centre for Biotechnology, University of
Turku and Åbo Akademi University, Tykistokatu 6,
20520 Turku, Finland
15:40
Le.27
USING GC×GC-MDGC TO FIND TRACE
ANALYTES IN ENVIRONMENTAL MATRICES
1
2
Marco Gomes da Silva , Eduardo Mateus Philip
3
Marriott
1
Faculdade de Ciencias e Tecnologia - LAQV,
REQUIMTE-DQ, Universidade Nova de Lisboa,
2829-516 Caparica, Portugal
2
CENSE-Center for Environmental and
Sustainability Research - DCEA - Universidade
Nova de Lisboa, Faculdade de Ciências e
Tecnologia, Campus da Caparica, 2829-516
Caparica, Portugal
3
Australian Centre for Research on Separation
Science - School of Chemistry, Monash
University, Wellington Road, Clayton , VIC 3800
Melboune, Australia
Le.34
GC-HRMS AND GC×GC-HRMS FOR THE
TARGETED AND UNTARGETED ANALYSIS OF
HIGHLY COMPLEX FOOD MATRICES
Daniela Peroni
Zoex Europe, Tramstraat 15, 5611 CM,
Eindhoven, the Netherland
JSB Nederland, Apolloweg 2B, 8239DA, Lelystad,
the Netherlands
16:00
Le.28
ENVIRONMENT APPLICATION OF GC×GC:
ANALYSIS OF PYROLYTIC PRODUCTS
DERIVED FROM RESIDUAL BIOMASS
1
1
Elina B. Caramao , Claudia A. Zini , Rosângela
1
2
A. Jacques , Laiza C. Krause , Maria Elisabete
2
1
Machado , Maria Silvana A. Moraes , Débora
1
Tomasini
1
Instituto de Quimica - UFRGS, av.Bento
Goncalves,9500, 91510-960 Porto Alegre, Rs,
Brazil
2
Unit, av. Murilo Dantas, 300, 49032-490
Aracaju, Brazil
Le.35
THE MOLECULAR ORIGINS OF LIFE
INVESTIGATED BY GC×GC
Uwe J. Meierhenrich
Department of Chemistry - Institute de Chimie de
Nice, 28, Avenue Valrose, 06108 Nice, France
17
16:20-17:00
Coffee Break – Poster K
17:00-19:03
GC×GC KEYNOTE LECTURES: Young
Scientist 1 - Room 1000
Chairperson:
Jean-Francois F. Focant
University of Liège, Liège, Belgium
GC×GC KEYNOTE LECTURES: Young
Scientist 2- Room 300 + Belvedere
Chairperson:
Heather Bean
Arizona State University, Tempe, United States
17:00
KNLe.01
MASS SPECTROMETRY AND TWODIMENSIONAL RETENTION INDICES WITH
COMPREHENSIVE TWO DIMENSIONAL GAS
CHROMATOGRAPHY: AN ADVANCED TOOL
FOR PROFILING OF VOLATILE CHEMICALS
1
2
1
Chadin Kulsing , Ming Jiang , Yada Nolvachai ,
1
Philip J. Marriott
1
Science, School of Chemistry - Monash
University, Wellington Rd. Clayton, 3800
Melbourne, Australia
2
School of Pharmacy, Tongji Medical College Huazhong University of Science & Technology,
#13 Hangkong Road, Wuhan, 430030 Hubei,
China
KNLe.11
COMPUTATIONAL STRATEGIES FOR
MATERIAL SELECTION IN COMPREHENSIVE
TWO-DIMENSIONAL GAS
CHROMATOGRAPHY
Yada Nolvachai, Chadin Kulsing, Philip J. Marriott
Science, School of Chemistry - Monash
University, Wellington Rd., Clayton, 3800
Melbourne, Australia
17:15
KNLe.02
IDENTIFICATION OF ENDOCRINE
DISRUPTING CHEMICALS IN WATER BY
NOVEL SORPTIVE EXTRACTION, GC×GCTOFMS AND UPLC-MS/MS
1
2
Madelien Wooding , Natalie Aneck-Hahn , Riana
2
1
1
Bornman , Egmont Rohwer , Yvette Naude
1
Pretoria, Private bag X20, 0028 Hatfield, South
Africa
2
Department of Urology - University of Pretoria,
Bophelo Road , 0001 Pretoria, South Africa
KNLe.12
DETERMINING THE CAPABILITIES OF
ANALYSING CHLORINATED PARAFFINS IN
ENVIRONMENTAL MATRICES BY
COMPARING CURRENT INSTRUMENTAL
TECHNIQUES
1,2
1
Louise van Mourik , Pim E.G. Leonards ,
2
1
Caroline Gaus , Jacob de Boer
1
Institute for Environmental Studies (IVM) \
Chemistry & Biology - VU University, De
Boelelaan 1087, 1081HV Amsterdam,
Netherlands
2
National Research Centre for Environmental
Toxicoligy (ENTOX) - University of Queensland,
39 kessels road, 4108 Coopers Plains, Australia
17:27
KNLe.03
DISCRIMINATION BETWEEN
INFLAMMATORY BOWEL DISEASE (IBD)
PHENOTYPES BY GC×GCHRTOFMS
1
2
Nicolas J. Di Giovanni , Marie-Alice Meuwis ,
2
1
Edouard Louis , Jean-Francois Focant
1
MS Laboratory Organic and Biological
Analytical Chemistry - ULG, Allée du Six Août
B6c, 4000 Liège, Belgium
2
Gastroenterology unit, GIGA-R - CHU, CHU B34 Quartier Hôpital Avenue de l’hopital, 11,
4000 Liège, Belgium
KNLe.13
CHARACTERIZATION OF ORGANIC
RESIDUES FROM ARCHAEOLOGICAL
ARTEFACTS USING GC×GCTOFMS
1
1
Katelynn A. Perrault , Lena Dubois , Pierre1
2
2
Hugues Stefanuto , Dries Cnuts , Veerle Rots ,
1
Jean-François Focant
1
Organic and Biological Analytical Chemistry
Group - University of Liège, Allée du 6 Août 11,
B6c, Quartier Agora, 4000 Liège, Belgium
2
Archéologie préhistorique / Traceolab University of Liège, Quai Roosevelt 1B (Bât. A4),
4000 Liège, Belgium
17:39
KNLe.04
IDENTIFYING VOLATILE BIOMARKERS OF
BACTERIAL LUNG INFECTIONS IN CYSTIC
FIBROSIS
1
2
Mavra Nasir , Heather D. Bean , Edith T.
3
1
Zemanick , Jane E. Hill
1
United States
2
School of Life Sciences - Arizona State
University, 427 East Tyler Mall, 85287 Tempe,
United States
3
School of Life Sciences - University of
Colorado, 13123 E 16th Avenue, 80045 Aurora,
United States
KNLe.14
RETENTION TIME PREDICTION IN FLOWMODULATION COMPREHENSIVE GAS
CHROMATOGRAPHY: THE CONTRIBUTION
OF PRESSURE ON SOLUTE RETENTION
Antoine Burel, Marie Vaccaro, Séverine Tisse,
Yohann Cartigny, Valérie Peulon-Agasse, Pascal
Cardinael, Gérard Coquerel
Laboratoire Sciences et Méthodes Séparatives Normandie Université, Université de Rouen, 1,
Rue Tesnière, 76821 MONT SAINT AIGNAN
CEDEX, France
18
17:51
KNLe.05
INVESTIGATING THE INTER-INDIVIDUAL
VARIATION OF BLOOD ODOUR DETECTED
BY BLOOD-DETECTION DOGS UTILISING
GC×GC-TOFMS
Latara Rust, Katie D. Nizio, Shari L. Forbes
Centre for Forensic Science - University of
Technology Sydney, PO Box 123, 2007 Sydney,
Australia
KNLe.15
ON-LINE LIQUID VALVE COUPLED TO GCxGC
TECHNIQUE
Adrien Maniquet
Process Experimentation - IFPEN, Rond point de
l'echangeur de Solaize, les levees, 69360
SOLAIZE, France
18:03
KNLe.06
COMBINATION OF GC×GC AND
CHEMOMETRICS FOR ODOR-PRINTING IN
FORENSIC ANALYSES
1,2
2
Vincent Cuzuel , Guillaume Cognon , Isabelle
3
2
1
Rivals , François Heulard , Didier Thiebaut ,
1
Jérôme Vial
1
Department of Analytical, Bioanalytical
Sciences and Miniaturization (LSABM) - ESPCI
Paris, 10 rue Vauquelin, 75005 PARIS, France
2
Institut de Recherche Criminelle de la
Gendarmerie Nationale (IRCGN), 5 boulevard de
l'Hautil, 95037 CERGY PONTOISE CEDEX,
France
3
Equipe de Statistique Appliquée - ESPCI Paris,
10 rue Vauquelin, 75005 PARIS, France
KNLe.16
ARE WE READY FOR A THREE-DIMENSIONAL
COMPREHENSIVE ONLINE APPROACH FOR
THE ANALYSIS OF COMPLEX
PETROCHEMICAL MATRICES? LIQUID
CHROMATOGRAPHY COUPLED TO GAS
CHROMATOGRAPY COMBINATIONS FOR
THE ANALYSIS OF PETROCHEMCIAL
MATRICES: AN IN-DEPTH COMPARISON
1
1
Aimee C. Sutherland , Thomas Groger , Jutta
1
1,2
Lintelmann , Ralf Zimmermann
1
Comprehensive Molecular Analytics - Helmholtz
Zentrum Muenchen, Ingolstädter Landstraße 1,
Building 24, 85764 Munich, Germany
2
Institute of Chemistry - University of Rostock,
Dr.-Lorenz-Weg 1, 18051 Rostock, Germany
KNLe.07
PRE-PROCESSING OF RAW GC×GC-TOFMS
DATA FOR CHEMOMETRIC ANALYSIS
Lawrence A. Adutwum, James J. Harynuk
Chemistry - University of Alberta, 11227
Saskatchewan Drive, T6G2G2 Edmonton, AB,
Canada
KNLe.17
SCREENING AND PRIORITIZATION OF
WASTE WATER CONTAMINANTS BASED ON
GC×GC-MS – AN EVALUATION OF ON-SITE
SEWAGE TREATMENT FACILITIES
1
1
Kristin M. Blum , Patrik L. Andersson , Gunno
2
1
Renman , Peter Haglund
1
Department of Chemistry - Umea University,
Linneus väg 1, 90187 Umea, Sweden
2
Department of Sustainable Development,
Environmental Science and Engineering - KTH
Royal Institute of Technology, Teknikringen 76,
10044 Stockholm, Sweden
KNLe.08
FEATURE SELECTION AND THE
EVALUATION OF EVIDENCE FOR FORENSIC
GC×GC-MS COMPARISON
1,2
3
Martin Lopatka , Gabriel Vivo-Truyols , Andjoe
3
4,5
Sampat , Arian van Asten , Peter
3
1,4
Schoenmakers , Marjan Sjerps
1
Korteweg de Vries Institute for Mathematics University of Amsterdam, P.O. Box 94248 , 1090
GE Amsterdam, Netherlands
2
Department of Forensic Chemical Research Netherlands Forensic Institute, P.O. Box 24044,
2490 AA The Hague, Netherlands
3
Van 't Hoff Institute for Molecular Sciences University of Amsterdam, PO Box 94157 , 1090
GD Amsterdam, Netherlands
4
Department of Science, Interdisciplinary
Research, Statistics and Knowledge
Management (WISK) - Netherlands Forensic
Institute, P.O. Box 24044, 2490 AA The Hague,
Netherlands
5
Co van Ledden Hulsebosch Center - University
of Amsterdam, Science Park – Building 904 ,
1098 XH Amsterdam, Netherlands
KNLe.18
COMBINED MATHEMATICAL METHODS IN
GC-MS DATA ANALYSIS
Andrei Barcaru, Gabriel Vivo-Truyols
Analytical-Chemistry Group - University of
Amsterdam, Science Park 904, 1098 XH
Amsterdam, Netherlands
18:15
18:27
19
18:39
KNLe.09
ACHIEVING A NEAR-THEORETICAL
MAXIMUM IN PEAK CAPACITY GAIN FOR
THE ANALYSIS OF IGNITABLE LIQUIDS
USING GC×GC-TOFMS
1
2
Katie D. Nizio , Jack W. Cochran , Shari L.
1
Forbes
1
Centre for Forensic Science - University of
Technology Sydney, PO Box 123, 2007 Sydney,
Australia
2
Restek Corporation, 110 Benner Circle, 16823
Bellefonte, United States
KNLe.19
SOLVING THE CHALLENGE OF SEPARATION
AND QUANTIFICATION OF SHORT AND
MEDIUM-CHAIN CHLORINATED PARAFFINS
IN ENVIRONMENTAL SAMPLES USING
GC×GC-ECNI-HRTOF-MS
Dan Xia, Lirong Gao, Minghui Zheng
State Key Laboratory of Environmental Chemistry
and Ecotoxicology - Research Center for
EcoEnvironmental Sciences, Chinese Academy
of Sciences, No.18, Shuangqing Road, Haidian
District, Beijing 100085, China, 100085 Beijing ,
China
18:51
KNLe.10
SUPERBUGS: HOW TO DIAGNOSE THEM
RAPIDLY USING ANALYTICAL CHEMISTRY
1
2
Christiaan A. Rees , Agnieszka Smolinska ,
1
3
Mavra Nasir , Paola C. Zucchi , Elizabeth B.
3
4,1
Hirsch , Jane E. Hill
1
Geisel School of Medicine - Dartmouth College,
1 Rope Ferry Road, 03755 Hanover, United
States
2
Department of Toxicology - Maastricht
University, PO Box 616, 6200 MD Maastricht,
Netherlands
3
Department of Pharmacy and Health Systems
Sciences - Northeastern University, 360
Huntington Avenue, 02115 Boston, United States
4
United States
KNLe.20
TOWARDS A RAPID DIAGNOSTIC FOR
URINARY TRACT INFECTIONS: BACTERIAL
VOLATILES ANALYSIS VIA GC×GC-TOFMS
1
2
Rocco P. Morra , Christiaan A. Rees , Jane E.
1,2
Hill
1
United States
2
Geisel School of Medicine - Dartmouth College,
1 Rope Ferry Road, 03755 Hanover, United
States
19:15
Welcome reception ISCC offered by DANI INSTRUMENTS
20
Tuesday, May 31, 2016
08:45 – 10.20
ISCC Opening Address Award and
Opening Lecture
See page 25 for details
10:20-10:50
Coffee Break - Exhibition
10:50-12.45
GC×GC Session 7 – FUNDAMENTALS 3 Room 300 + Belvedere
Chairperson:
Tadeusz Gorecki
University of Waterloo, Waterloo, Ontario,
Canada
ISCC Session 1 - MICROCOLUMN
SEPARATIONS - Room 1000
10:50-11.00
John Phillips Award Presentation
Sponsored by Restek/LECO
Giorgio Nota Award Presentation
Sponsored by Waters
11:00
Le.36 Phillips Award Lecture
METABOLOMICS BY
MULTIDIMENSIONAL GCMS
APPROACH: ROUTE TO SYSTEMATIC
IDENTIFICATION OF VOC BIOMARKERS
Sung-Tong Chin
Dept of Surgery & Cancer - Imperial College
London, St Mary Campus, W2 1NY London,
United Kingdom
11:25
Le.37
COMPLEX PROBLEM SOLVING WITH
THERMAL INDEPENDENT MODULATOR
AND COMPREHENSIVE TWO
DIMENSIONAL GAS CHROMATOGRAPHY
1,2
3
Jim Luong , Xiaosheng Guan , Roger
4
1,5
5,6
Firor , Ronda Gras , Robert A. Shellie
1
Analytical Technology Center - Dow
Chemical Canada, PO BAG 16, Highway 15,
T8L2P4 Fort Saskatchewan, AB, Canada
2
Australian Center for Research on
Separation Science (ACROSS) - University
of Tasmania, Private Bag 75, 7001 Hobart,
Australia
3
Agilent Technologies (Ret.), Shanghai,
China, 412 Ying Lun Road, 200131
Shanghai, China
4
Agilent Technologies (Ret.) Little Falls,
USA, 2850 Centerville Road, 19808
Wilmington, United States
5
ARC Training Centre for Portable Analytical
Separation Technologies (ASTech) University of Tasmania, Private Bag 75,
7001 Hobart, Australia
6
Trajan Scientific & Medical, 75 Argent
Place, 3134 Ringwood, Australia
11:45
Le.38
A NOVEL CONCEPT IN GC×GC(-MS)
SYSTEM OPTIMIZATION AND METHOD
TRANSLATION
1
1
2
Zhijun Zhao , Xiaosheng Guan , Jim Luong
1
J&X Technologies, Room 1034, Building
1st, 1599 Jungong Road,Yangpu District,
200438 Shanghai, China
2
Analytical Technology Center (ATC) - Dow
Chemical Canada, Highway 15, PO BAG 16,
T8L 2P4 Fort Saskatchewan, Canada
21
12:05
Le.39
QUANTIFICATION BASED ON VACUUM
ULTRAVIOLET ABSORPTION
SPECTROSCOPY (VUV): THE
APPLICATION OF COMPREHENSIVE
TWO-DIMENSIONAL GAS
CHROMATOGRAPHY - VUV TOWARDS
MIDDLE DISTILLATES
1
1
Thomas M. Gröger , Beate Gruber ,
2
1,3
Maximilian Jennerwein , Ralf Zimmermann
1
Comprehensive molecular analytics Helmholtzentrum München, Ingolstädter
Landstrasse 1, 85764 Oberschleiheim,
Germany
2
ASG Analytik-Service Gesellschaft mbH,
Trentiner Ring 30, 86356 Neusäß, Germany
3
Analytical Chemsitry - University of
Rostock, Dr.-Lorenz-Weg 1, 18051 Rostock,
Germany
12:25
Le.40
DEVELOPMENT AND VALIDATION OF A
PNEUMATIC CALCULATOR FOR THE
REVERSED-FLOW DIFFERENTIAL FLOW
MODULATOR FOR COMPREHENSIVE
TWO-DIMENSIONAL GAS
CHROMATOGRAPHY
Matthew Giardina, James D. McCurry
Gas Phase Separations Division - Agilent
Technologies, 2850 Centerville Road, 19808
Wilmington, United States
12:45-14:00
14:00 – 15:20
GC×GC Session 8 - APPLICATIONS Petrochemical/Industry - Room 300 +
Belvedere
Chairperson:
Robert Shellie
University of Tasmania, Hobart, Tasmania,
Australia
14:00
Le.41
ANALYSIS OF COMPLEX MIXTURES OF
ORGANIC COMPOUNDS FROM COAL OR
TYRE PYROLYSIS BY GC×GC-MS
Philipp Rathsack
Institute of Analytical Chemistry - TU
Bergakademie Freiberg, Leipziger Str. 29,
09599 Freiberg, Germany
14:20
Le.42
A PARADIGM SHIFT IN PETROLEOMICS:
GC×GC-HRMS, MASS DEFECT PLOTS,
DECONVOLUTION AND THEIR ROLE IN
SPECIATION
Jonathan D. Byer, Joe Binkley
LECO Corporation, 3000 Lakeview Avenue,
49085 Saint Joseph, United States
14:40
Le.43
QUALITATIVE AND QUANTITATIVE
GC×GC: USING OFF-LINE AND
AUTOMATED APPROACHES TO
IMPROVE HIGH THROUGHPUT
RESEARCH PROJECTS AND
MANUFACTURING PROCESSES
1
1
Melissa Dunkle , Pascal Pijcke , Mubasher
1
2
2
Bashir , Murat Palit , Georgios Bellos
1
Analytical Sciences - Dow Benelux, Herbert
H. Dowweg 5, 4542 NM Hoek, Netherlands
2
Dow Benelux, Herbert H. Dowweg 5, 4542
NM Hoek, Netherlands
ISCC Session 2 - BIO-ANALYTICAL Room 1000
22
15:00
Le.44
QUALITATIVE AND QUANTITATIVE
SCREENING OF SURFACE AND
DRINKING WATERS USING ON-LINE SPE
GC×GC-TOF MS
1,2
1
Pieter Joos , Els Van Meenen
1
Laboratory - water-link, Mechelsesteenweg
2
64, 2018 Antwerp, Belgium Department of
Bioengineering - University of Antwerp,
Groenenborgerlaan 171, 2020 Antwerpen,
Belgium
15:20 – 16:50
Coffee Break – Exhibition – Seminars – Posters A, B, L, K*
15:45 – 16:45
Room 1000
Seminar
SHIMADZU
15:45 – 16:45
Room 300
Seminar
LECO
Room 100
Seminar
ZOEX Europe
16:50 – 18:30
GC×GC Session 9 - APPLICATIONS Petrochemical - Room 300 + Belvedere
Chairperson:
Jane Hill
College, Hanover, United States
16:50
Le.45
OVER THE HUMP, OR OVER THE HILL?
GC×GC-MS OF UNRESOLVED COMPLEX
MIXTURES FROM PETROLEUM
Steven Rowland
Biogeochemistry Research Centre University of Plymouth, Drake Circus, PL4
8AA Plymouth, United Kingdom
17:10
Le.46
COMPREHENSIVE TWO-DIMENSIONAL
GAS CHROMATOGRAPHY OF COMPLEX
SYNGAS AND CONDENSATES SAMPLES
FROM BIOMASS GASIFICATION
1
2
Didier Thiebaut , Etienne Basset , Marianne
2
2
2
Gallardo , Yilmaz Kara , Olivier Guerrini ,
1
3
Fanny Hilaire , Patrick Sassiat , Jérôme
3
Vial
1
PECSA-LSABM - ESPCI, 10 Rue
Vauquelin, 75005 Paris, France
2
ENGIE Research and Technologies
Division, CRIGEN, 93200 Saint Denis la
Plaine, France
3
CBI-LSABM - ESPCI, 10 Rue Vauquelin,
75005 Paris, France
17:30
Le.47
AUTOMATED SPE FRACTIONATION
COUPLED WITH GC×GC-FID FOR THE
CHARACTERIZATION OF GASOILS: ON
THE WAY TO ROUTINE ANALYSIS
Vincent Souchon, Manuel Ménard, Marjorie
Boiron
Physics and Analysis Division - Products
Characterisation Department - IFP Energies
Nouvelles, Rond-point de l'échangeur de
Solaize - BP3, 69360 Solaize, France
ISCC Session 3 - MICROSCALE LC - Room
1000
23
17:50
Le.48
STRUCTURAL CLASSIFICATION AND
CHARACTERIZATION OF HEAVY
PETROLEUM BASE OIL
HYDROCARBONS BY GC×GC-HRTOF/MS
1
2
Anupam Giri , Marion Courtiade , Amandine
2
1
Racaud , Jean-François Focant
1
Liège, Allée du 6 août, 11, B6c, Quartier
Agora, B-4000 Liège, Belgium
2
Centre de Recherche de Solaize - Total
Marketing Services, Chemin du Canal - BP
22, 69360 Solaize, France
18:10
Le.49
COMPARATIVE STUDY OF TRUE
BOILING POINT FRACTIONS OF TWO
KUWAITI HEAVY CRUDE OILS USING
GAS CHROMATOGRAPHY
Hassan A. Al-Rabiah, Abdullwahab Al-Hendi,
Latifa Al-Ostad, Tahani Al-Shamary, Hisham
AlHenayyan, Roaya Khazemi
Petroleum Research Centre - Kuwait
Institute for Scientific Research, P.O. Box:
24885 Safat, 13109 Kuwait, Kuwait
18.30 – 18.45
Presentation of the Richard Sacks Best Poster Award
th
Closing Address 13 GC×GC Symposium
18:45 – 20:00
AGILENT TECHNOLOGIES Users Meeting
– Room 100 see page 43 for details
21:00
Concert offered by PERKINELMER, Inc.,
Room 1000, Congress Centre
22:15
Cocktail offered by GERSTEL GmbH & Co. KG,
Congress Centre
24
SCIENTIFIC PROGRAM 40th ISCC
Tuesday, May 31, 2016
th
08:45 – 09:15
Opening Address 40 ISCC - Room 1000
Luigi Mondello
Aldo Laganà
President of the Analytical Chemistry Division of the Italian Chemical Society, Italy
Adalberto Mosaner
Mayor of Riva del Garda, Italy
09:15 – 09:25
M.J.E. Golay Award Presentation
Sponsored by PerkinElmer, Inc.
Chairperson:
Milos Novotny
Department of Chemistry - Indiana University, Bloomington, IN, United States
09:25 – 09:55
LE.01 Award Lecture
MULTIDIMENSIONAL GC WITH CHEMOMETRICS: DISTILLING INFORMATION FROM
COMPLEX SAMPLES
Robert Synovec
Chemistry - University of Washington, Box 351700, 98195 Seattle, WA, United States
09:55 – 10:20
LE.02 Opening Lecture
ADVANCES IN THE ANALYSIS OF PROTEIN BIOPHARMACEUTICALS THROUGH
APPLICATION OF CONTEMPORARY 2D-LC
Pat Sandra, Gerd Vanhoenacker, Koen Sandra
R.I.C., President Kennedypark 26, 8500 Kortrijk, Belgium
10:20-10:50
10:50 – 12:45
ISCC Session 1 - MICROCOLUMN
SEPARATIONS - Room 1000
Chairperson:
Pat Sandra
R.I.C., Kortrijk, Belgium
GC×GC Session 7 – Fundamentals 3 Room 300 + Belvedere
10:50
Giorgio Nota Award Presentation
Sponsored by Waters
John Phillips Award Presentation
Sponsored by Restek/LECO
11:00
LE.03 Giorgio Nota Award Presentation
DUAL TWO-DIMENSIONAL LC×LC ON A
ZWITTERIONIC POLYMETHACRYLATE
CAPILLARY COLUMN IN ALTERNATING
HILIC / RP MODES IN COMBINATION
WITH SHORT C18 COLUMNS
Pavel Jandera, Tomas Hajek, Magda
Stankova
Analytical Chemistry - University of
Pardubice, Studentská 573, 532 10
Pardubice, Czech Republic
11:25
LE.04
CAPILLARY UHPLC WITH POROUS
GRAPHITIC CARBON
James W. Jorgenson, Daniel Lunn
Department of Chemistry, CB#3290 University of North Carolina at Chapel Hill,
South Rd, 27599 Chapel Hill, United States.
25
11:45
LE.05
POLYMER INCLUSION MEMBRANE
BASED MICROFLUIDIC LATERAL FLOW
DEVICES FOR DETERMINATION OF
AQUEOUS HEAVY METAL IONS
Gayan C. Bandara, Sumate Pengpumkiat,
Kelly Ramzy, Vince Remcho
Department of Chemistry - Oregon State
University, 153 Gilbert Hall, 97331 Corvallis,
United States
12.05
LE.06
ANALYSIS OF EXTROGENS: A
CHALLENGING ISSUE FOR CAPILLARY
SEPARATION TECHNIQUES
1
1,2
Salvatore Fanali , Giovanni D'Orazio ,
3
Maria Asensio-Ramos , Javier Hernandez2
2
Borges , Miguel Angel Rodrigues-Delgado
1
Institute of Chemical Methodologies Italian National Research Council-C.N.R.,
Area della Ricerca di Roma I, Via Salaria
Km 29,300, 00015 Monterotondo Scalo
(Roma), Italy
2
Departamento de Quimica - Universidad
de la Laguna (ULL), Avenida Astrofisico
Francisco Sanchez, 38206 La Laguna,
Tenerife, Spain
3
Instituto Volcanologico de Canarias INVOLCAN, Parque Taoro 22, 38400
Puerto de la Cruz (Tenerife), Spain
12:25
LE.07
RECENT DEVELOPMENTS IN
ENANTIOSEPARATION WITH
CAPILLARY ELECTROMIGRATION
TECHINIQUES
Bezhan Chankvetadze
Institute of Physical and Analytical
Chemistry, School of Exact and Natural
Sciences, - Tbilisi State University,
Chavchavadze Ave 3,Tbilisi 0179, Georgia
12:45 - 14:00
14:00 - 15:20
ISCC Session 2 - BIO-ANALYTICAL Room 1000
Chairperson:
Alejandro Cifuentes
Foodomics Lab, CIAL, CSIC, Madrid, Spain
14:00
GC×GC Session 8 - APPLICATIONS Petrochemical/ Industry - Room 300 +
Belvedere
LE.08
SEARCHING THE GLYCOME OF HUMAN
URINARY EXOSOMES FOR
BIOMARKERS
Milos Novotny, Guozhang Zou, Solomon G.
Gizaw
Department of Chemistry - Indiana
University, 800 E Kirkwood Avenue, 474054001 Bloomington, IN, United States
26
14:20
LE.09
TOXICITY ASSESSMENT OF CHEMICALS
AND NANOMATERIALS EMPLOYING
CELL CULTURE MODELS,
PROTEOMICS, AND METABOLOMICS
1
1
Christina Ranninger , Matthew S. Boyles ,
1
2
Reischl Roland , Rurik Marc , Oliver
2
1
Kohlbacher , Albert Duschl , Christian
1,3
Huber
1
Department of Molecular Biology University of Salzburg, Hellbrunner Strasse
34, 5020 Salzburg, Austria
2
University of Tübungen, Sand 14, 72076
Tübingen, Germany
3
Christian Doppler Laboratory for Biosimilar
Characterization, University of Salzburg,
Hellbrunner Strasse 34, 5020 Salzburg,
Austria
14:40
LE.10
LIPIDOMICS BY DATA-INDEPENDENT
WORKFLOWS
Michael Laemmerhofer, Agnes Petker,
Joerg Schlotterbeck
University of Tuebingen - Institute of
Pharmaceutical Sciences, Auf der
Morgenstelle 8, D-72076 Tuebingen,
Germany
15:00
LE.11
LIPIDOMICS STUDY OF STROKE
INDUCED BY SMALL VESSEL DISEASE
BY 2D(NP/RP)LC-MS/MS
Huwei Liu, Li Yang, Yu Bai
Beijing National Laboratory for Molecular
Sciences Key Laboratory of Bioorganic
Chemistry and Molecular Engineering,
Institute of Analytical Chemistry, College of
Chemsitry and Molecular Engineering Peking University, Zhong Guan Cun,
100871 Beijing, China
15:20 – 16:50
Coffee Break – Exhibition – Seminars – Posters A, B, L, K*
15:45 – 16:45
Room 1000
Seminar
SHIMADZU
15:45 – 16:45
Room 300
Seminar
LECO
Room 100
Seminar
ZOEX Europe
16:50 – 18:30
ISCC Session 3 - MICROSCALE LC Room 1000
Chairperson:
J.Michael Ramsey
University of North Carolina, Chapel Hill,
United States
GC×GC Session 9 - APPLICATIONS Petrochemical - Room 300 + Belvedere
27
16:50
LE.12
PROSPECTS FOR NEW PARTICLE
SHAPES IN ANALYTICAL AND MICROSCALE SEPARATIONS
Gert Desmet
Vrije Universiteit Brussel, Dienst CHIS
Pleinlaan 2, Brussels, Belgium
17:10
LE.13
A TRULY PORTABLE HPLC USING
MICRO COLUMN CARTRIDGES
1
2
Peter Myers , Claire Armstrong , Adham
1
3
3
Ahmed , Peter Dawes , Andrew Minett ,
4
David Goodall
1
Liverpool, Oxford Street, L69 7ZD Liverpool,
United Kingdom
2
University of Liverpool, Oxford Street, L69
7ZD Liverpool, United Kingdom
3
Eprep, 14/35 Dunlop Rd, Victoria 3170
Mulgrave, Australia
4
Paraytec Limited, York House, YO19 5UP
York, United Kingdom
17:30
LE.14
ADVANCEMENTS IN LC DIRECT-EIMS:
STATE OF THE ART AND
APPLICATIONS
Achille Cappiello
University of Urbino, P. Rinascimento 6,
61029 Urbino, Italy
17:50
LE.15
3D PRINTING IN RAPID DESIGN OF LED
ON-CAPILLARY DETECTION DEVICES
1
1,2
Farhan Cecil , Michael C. Breadmore ,
1
1,2
Rosanne M. Guijt , Brett Paull , Pavel N.
1,2
3
Nesterenko , Alan Henderson , Andrew A.
4
1
Cole , Mirek Macka
1
School of Physical Sciences and
Australian Centre for Research on
Australia
2
ARC Centre of Excellence for
Electromaterials Science and School of
Physical Sciences - University of Tasmania,
Private Bag 75, 7001 Hobart, Australia
3
School of Engineering Sciences University of Tasmania (UTAS), Private Bag
65, 7001 Hobart, Australia
4
School of Physical Sciences - University of
Tasmania (UTAS), Private Bag 37, 7001
Hobart, Australia
18:10
LE.16
NANO-LCMS OF HISTONES USING
CAPILLARIES PACKED WITH 0.5 um
PARTICLES
Mary Wirth
Department of Chemistry - Purdue
University, 560 Oval Drive, 47907 West
Lafayette, IN, United States
18:45 – 20:00
AGILENT TECHNOLOGIES Users Meeting – Room 100 see page 43 for details
21:00
Concert offered by PERKINELMER, Inc., Room 1000, Congress Centre
22:15
Cocktail offered by GERSTEL GmbH & Co. KG, Congress Centre
28
Wednesday, June 01, 2016
08:30 – 10:30
ISCC Session 4 - CAPILLARY GC 1 Room 1000
Chairperson:
Carlo Bicchi
University of Turin, Turin, Italy
ISCC Session 5 - MICRO LC 1 - Room 300
08:30
LE.17
MICROCHIP THERMAL GRADIENT GAS
CHROMATOGRAPHY
1
1
Milton L. Lee , Abhijit Ghosh , Luke T.
1
2
Tolley , Aaron R. Hawkins , Brian D.
3
4
Iverson , H. Dennis Tolley
1
Chemistry and Biochemistry - Brigham
Young University, C-267 BNSN, 84602
Provo, UT, United States
2
Computer and Electrical Engineering Brigham Young University, 435B CB, 84602
Provo, UT, United States
3
Mechanical Engineering - Brigham Young
University, 435 CTB, 84602 Provo, UT,
United States
4
Statistics - Brigham Young University, 223
J TMCB, 84602 Provo, UT, United States
LE.23
TOWARDS THE DEVELOPMENT OF A
MICROFLUIDIC CHIP PLATFORM FOR
ION-EXCHANGE SEPARATIONS
1
2
Sam Wouters , Sebastiaan Eeltink
1
Department of Chemical Engineering - Vrije
Universiteit Brussel, Pleinlaan 2, B-1050
Brussels, Belgium
2
Vrije Universiteit Brussel, Pleinlaan 2, B1050 Brussels, Belgium
08:50
LE.18
IS CAPILLARY GC A VIABLE
TECHNIQUE FOR RESEARCH IN LIFE
SCIENCES?
Frank David, Pat Sandra, Koen Sandra
R.I.C., President Kennedypark 26, 8500
Kortrijk, Belgium
LE.24
CHIP-BASED SEPARATION DEVICES
COUPLED TO MASS SPEC
Detlev Belder, Josef Heiland, Carsten Lotter
Leipzig, Johannisallee 29, 04103 Leipzig,
Germany
09:10
LE.19
APPLICATIONS AND PERSPECTIVES OF
FLOW FIELD THERMAL GRADIENT GAS
CHROMATOGRAPHY
Peter Boeker
Workgroup on Trace Gas Measurements University of Bonn, Nussallee 5, D-53115
Bonn, Germany
LE.25
ONLINE CAPILLARY LC WITH ONE
MINUTE TIME RESOLUTION FOR
NEUROTRANSMITTER DETERMINATIONS
BY MICRODIALYSIS: OPTIMIZATION AND
APPLICATION OF ACTIVE TEMPERATURE
CONTROL
Khanh Ngo, Stephen R. Groskreutz, Stephen
G. Weber
Pittsburgh, 219 Parkman Drive, 15260
Pittsburgh, PA, United States
09:30
LE.20
TIME INTERVAL DECONVOLUTION OF
POLYCHLORINATED BIPHENYLS IN
ARACLOR MIXTURES USING GAS
CHROMATOGRAPHY - VACUUM
ULTRAVIOLET SPECTROSCOPY
1
1
Kevin A. Schug , Changling Qiu , Jonathan
2
2
3
Smuts , Phillip Walsh , Jack Cochran
1
Chemistry and Biochemistry - University of
Texas at Arlington, 700 Planetarium PI., Box
19065, TX 76019-0065 Arlington, United
States
2
VUV Analytics, 715 Discovery Blvd Suite
502, 78613 Cedar Park, United States
3
Restek Corporation, 110 Benner Circle,
16823 Bellefonte, United States
LE.26
HIGH PERFORMANCE MICROSCALE
SEPARATIONS USING SPECIFIC
INTERACTIONS
Takuya Kubo, Madoka Tsuzuki, Eisuke
Kanao, Toyohiro Naito, Koji Otsuka
Department of Material Chemistry, Graduate
School of Engineering - Kyoto University,
Katsura, Nishikyo-ku, 6158510 Kyoto, Japan
Chairperson:
Frantisek Svec
Lawrence Berkeley Nat. Lab., Berkeley,
United States
29
09:50
LE.21
EVALUATING THE UNIQUE SELECTIVITY
OF IONIC LIQUID CAPILLARY COLUMNS
Len Sidisky, Gustavo Serrano, James L.
Desorcie, Greg A. Baney, Katherine K.
Stenerson, Michael Halpenny, Michael D.
Buchanan
Sigma Aldrich/ Supelco, 595 North Harrison
Road, 16823 Bellefonte, United States
LE.27
CHEMISTRY-SENSITIZED LC-MS/MS OF
TRACE BIO-FUNCTIONAL ORGANIC
ACIDS IN SUB-MICROGRAM FRESH
PLANT SAMPLES
Yi Chen
Institute of Chemistry - Chinese Academy of
Sciences, North 1str. No.2, Zhonguancun,
Haidian, 100190 Beijing, China
10:10
LE.22
3D PRINTED CAPILLARY COLUMNS
Roy Lautamo, William Bromps
Restek West - Restek Corporation, 4211-C
Business Drive, 95682 Cameron Park, CA,
United States
LE.28
OPEN TUBULAR LIQUID
CHROMATOGRAPHY-MASS
SPECTROMETRY: A TOOL FOR CANCER
BIOMARKER DISCOVERY IN ULTRASMALL SAMPLES
Steven Wilson, Tore Vehus, Hanne Roberg
Larsen, Ole Kristian Brandtzaeg, Elsa
Lundanes
University of Oslo, Sem Saelands vei 23,
Blindern, 561 Oslo, Norway
10:30 – 12:00
Coffee Break – Seminars – Exhibition – Posters C, D, I
10:45 – 11:45
Room 1000
Seminar
Room 300
Seminar
AGILENT TECHNOLOGIES
See page 44 for detail
DANI INSTRUMENTS
Room 100
Seminar
PEAK SCIENTIFIC
12:00 – 14:00
11:45 – 12:45
Room 1000
Lunch Seminar
WATERS
Room 300
Seminar
MARKES INTERNATIONAL
Room 100
ELEMENTAR/ISOPRIME
14:00 – 15:40
14:00
ISCC Session 6 - CAPILLARY GC-MS Room 1000
Chairperson:
Kevin A. Schug
Texas at Arlington, Arlington, United States
ISCC Session 7 - SAMPLE PREPARATION
1 - Room 300
Chairperson:
Fernando M. Lancas
Institute of Chemistry at Sao Carlos University of Sao Paulo, Sao Carlos, Brazil
LE.29
GC-MS WITH COLD EI AND ITS
UNEXPECTED BENEFITS
Aviv Amirav, Alexander B. Fialkov, Tal Alon,
Uri Keshet
Department of Chemistry - Tel Aviv
University, Ramat Aviv, 69978 Tel Aviv,
Israel
LE.34
DEVELOPMENT AND APPLICATION OF
MATRIX COMPATIBLE SPME
TECHNOLOGY
Janusz Pawliszyn
Chemistry Department - University of
Waterloo, 200 University Avenue West, N2L
3G1 Waterloo, ON, Canada
30
14:20
LE.30
GC-MS IN THE FIELD WITHOUT A
SHERPA
Edgar Lee, Nathan L. Porter, Tai V. Truong
Portable MS/GCMS - PerkinElmer, 796 East
Utah Valley Drive, 84003 American Fork,
United States
LE.35
GREEN FOODOMICS: NEW APPROACHES
FOR THE ISOLATION AND PURIFICATION
OF BIOACTIVE COMPOUNDS WITH
ANTIPROLIFERATIVE ACTIVITY USING
GREEN TECHNOLOGIES
Andrea del Pilar Sánchez-Camargo, Miguel
Herrero, Lidia Montero, Jose A. Mendiola,
Virginia García-Cañas, Alejandro Cifuentes,
Elena Ibanez
Instituto de Investigación en Ciencias de la
Alimentación-CIAL (CSIC), c/Nicolas Cabrera
9, 28049 Madrid, Spain
14:40
LE.31
EXTENDING THE APPLICABILITY OF
VACUUM-OUTLET GC/MS
Erwin Rosenberg, Chrysoula Kanakaki
Institute of Chemical Technologies and
Analytics - Vienna University of Technology,
Getreidemarkt 9/164 AC, A-1060 Vienna,
Austria
LE.36
CONSIDERATIONS ON
MICROEXTRACTION TECHNIQUES ADVANTAGES, LIMITATIONS AND
FUTURE TRENDS
José M.F. Nogueira
Centro de Química e Bioquímica - Faculdade
de Ciências, Universidade de Lisboa, Campo
Grande Ed. C8, 1749-016 Lisboa, Portugal
15:00
LE.32
HYPHENATION OF GC AND APCI-FTICR-MS FOR ANALYSIS OF PYROLYSIS
OILS FROM A GERMAN BROWN COAL
Jan Zuber, Marius Kroll, Philipp Rathsack,
Matthias Otto
Faculty of Chemistry and Physics - Institute
of Analytical Chemistry, Leipziger Strasse
29, 09599 Freiberg, Germany
LE.37
ON-LINE SAMPLE PREPARATION IN
MINIATURIZED SEPARATION
TECHNIQUES
Michal Szumski, Damian Grzywinski, Kinga
Meller, Boguslaw Buszewski
Department of Environmental Chemistry and
Bioanalytics - Faculty of Chemistry, Nicolaus
Copernicus University in Torun, Gagrin 7 St.,
87-100 Torun, Poland
15:20
LE.33
ORBITRAP GC-MS: ONE YEAR ON
Dominic Roberts, Paul Silcock, Cristian
Cojocariu, Jason Cole, Fausto Pigozzo
GC-MS - Thermo Fisher Scientific, Tudor
Road, WA7 1TA Runcorn, United Kingdom
LE.38
SOLVENT-ASSISTED STIR BAR SORPTIVE
EXTRACTION (SA-SBSE) FOR ENHANCED
RECOVERIES OF POLAR SOLUTES IN
AQUEOUS SAMPLES
1
1
Nobuo Ochiai , Kikuo Sasamoto , Frank
2
2
David , Pat Sandra
1
Gerstel K.K., 1-3-1 Nakane, Meguro-ku,
152-0031 Tokyo, Japan
2
Research Institute for Chromatography,
Kennedypark 26, 8500 Kortrijk, Belgium
15.40 – 17:00
Coffee Break – Seminars – Exhibition – Posters E, F, G, H, N, Q
15:45 – 16:45
Room 1000
Seminar
PerkinElmer
Room 300
Seminar
GERSTEL
Room 100
Seminar
VUV Analytics
17:00 – 18.30
ISCC KEYNOTE LECTURES: Young
Scientists 1 – Room 1000
Chairperson:
Peter J. Schoenmakers
Analytical Chemistry (HIMS) - University of
Amsterdam, Amsterdam, Netherlands
ISCC KEYNOTE LECTURES: Young
Scientists 2 – Room 300
Chairperson:
Gert Desmet
Universiteit Brussel, Brussels, Belgium
31
17:00
KNL.01
CHARACTERIZATION OF AN
IMMOBILIZED ENZYME REACTOR
(IMER) FOR ON-LINE PROTEIN
DIGESTION
Stephanie Moore, Stephanie M. Hess,
James W. Jorgenson
Department of Chemistry - UNC-Chapel HIll,
125 South Road, 27599 Chapel Hill, United
States
KNL.08
DEVELOPMENT AND APPLICATIONS OF A
MICROCHIP CE-nESI-HPMS PLATFORM
1
2
William M. Gilliland , John S. Mellors , John
1
M. Ramsey
1
University of North Carolina, 251 Chapman
Hall, CB#3216, NC 27599 Chapel Hill, United
States
2
908 Devices, Inc., 27 Drydock Ave, 02210
Boston, United States
17:15
KNL.02
INVESTIGATION OF LIVER AND
PLASMA VOLATOLOME BY SOLIDPHASE MICROEXTRACTION COUPLED
WITH GAS CHROMATOGRAPHY-MASS
SPECTROMETRY TO REVEAL DIETARY
EXPOSURE TO POLLUTANTS
1
2
Jihene Bouhlel , Jeremy Ratel , Said
2
3
Abouelkaram , Elisabeth Baeza , Catherine
4
1
Jondreville , Douglas Rutledge , Erwan
2
Engel
1
Analytical Engineering and Food Quality Agroparistech, 16 Rue Claude Bernard,
75005 PARIS, France
2
UR 370 QuaPA - INRA, Mass Group,
63122 Saint-Genes-Champanelle, France
3
URA83 - INRA, MOCA Group, 37380
Nouzilly, France
4
USC 340 - University Lorraine, URAFPA,
54500 Vandoeuvre-Lès-Nancy, France
KNL.09
EXPLORING THE POTENTIAL OF A NEW
ANALYTICAL APPROACH, NTME/GC-MS,
TO ESTABLISH THE VOLATOMIC
PATTERN OF URINE SAMPLES
1
1
Priscilla Porto-Figueira , Jorge A. Pereira ,
1,2
José S. Câmara
1
Analytical Chemistry and Enology Lab Centro de Química da Madeira, Universidade
da Madeira, Campus da Penteada, 9000-390
Funchal, Portugal
2
Faculdade de Ciências Exactas e da
Engenharia - Universidade da Madeira,
Campus da Penteada, 9000-390 Funchal,
Portugal
17:27
KNL.03
EVALUATION OF DYNAMIC
MULTIDIMENSIONAL GAS
CHROMATOGRAPHY WITH ACCURATE
MASS TIME-OF-FLIGHT MASS
SPECTROMETRY FOR THE STUDY OF
MOLECULAR TRANSFORMATION
Yong Foo Wong, Chadin Kulsing, SungTong Chin, Philip Marriott
School of Chemistry, Monash University,
Wellington Rd, Clayton 3800, Victoria, 3800
Clayton, Victoria, Australia
KNL.10
STUDY OF LARGE MOLECULES USING
ON-LINE LIQUID CHROMATOGRAPHY
× GAS CHROMATOGRAPHY-MASS
SPECTROMETRY
1
2
Marta P. Mourao , Joen Hermans , Pieter
2
1
1,3
Iedema , Arend Kolk , Hans-Gerd Janssen
1
Analytical Chemistry Group - University of
Amsterdam, P.O. Box 94157, 1090 GD
2
Computational Polymer Chemistry Group University of Amsterdam, P.O. Box 94157,
1090 GD Amsterdam, Netherlands
3
Advanced Measurement and Data Modelling
- Unilever R&D, P.O. Box 114, 3130 AC
Vlaardingen, Netherlands
17:39
KNL.04
UNDERSTANDING THE EFFECT OF THE
PDMS-LAYER ON THE KINETICS AND
THERMODYNAMICS OF ANALYTES
SORPTION ONTO THE MATRIXCOMPATIBLE COATING
1
Erica A. Souza-Silva , Emanuela
2
2
Gionfriddo , Janusz Pawliszyn
1
Instituto de Quimica - Universidade
Federal do Rio Grande do Sul, Avenida
Venancio Aires, 306 - ap 204, 90040-190
Porto Alegre, Brazil
2
University of Waterloo, 200 University Ave
W, N2L 3G1 Waterloo, Canada
KNL.11
VAN DE GRAAFF GENERATOR FOR
CAPILLARY ELECTROPHORESIS
1
1
Seung Jae Lee , Eric R. Castro , Rosanne M.
2
3
1
Guijt , Mark D. Tarn , Andreas Manz
1
Microfluidics group - KIST-Europe, Campus
E7 1, 66123 Saarbrucken, Germany
2
School of Medicine and ACROSS, Private
Bag 26, HobartTAS 7001 Tasmania, Australia
3
Department of Chemistry, Cottingham Road,
HU67RX Hull, United Kingdom
32
17:51
KNL.05
HYDROCHARS AS NEW COATING
MATERIAL FOR BAR ADSORPTIVE
MICROEXTRACTION FOR THE
DETERMINATION OF
PHARMACEUTICALS AND PERSONAL
CARE PRODUCTS IN AQUEOUS
MATRICES
Samir M. Ahmad, Ana S. Mestre, Nuno R.
Neng, Ana P. Carvalho, José M. F.
Nogueira
Center of Chemistry and Biochemistry Faculty of Sciences, University of Lisbon,
Faculdade de Ciências da Universidade de
Lisboa, Campo Grande, 1749-016 Lisbon,
Portugal
KNL.12
DO FLUORINATED SURFACTANTS STICK
AROUND? LONGITUDINAL TRENDS OF
PFAS SERUM LEVELS FROM THE
PROSPECTIVE INVESTIGATION OF THE
VASCULATURE IN UPPSALA SENIORS
(PIVUS)
1
1,2
Jordan A. Stubleski , Samira Salihovic , Lars
3
4
1
Lind , Monica Lind , Anna Kärrman , Bert Van
1,5
Bavel
1
Environmental Chemistry - Örebro
University, Fakultetsgatan 1, 702 81 Örebro,
Sweden
2
Medical Sciences, Molecular Epidemiology Uppsala University, BMC, Navet, 751 41
Uppsala, Sweden
3
Medical Sciences, Cardiovascular
Epidemiology; EpiHealth - Uppsala University,
Dag Hammarskölds väg 10B, 75237 Uppsala,
Sweden
4
Medical Sciences, Occupational and
Environmental Medicine - Uppsala University,
Ulleråkersv. 40, 751 85 Uppsala, Sweden
5
Environmental Chemistry - Norwegian
Institute for Water Research, Gaustadalléen
21, 0349 Oslo, Norway
18:03
KNL.06
DEVELOPING (CAPILLARY) LC×LC
METHODS RAPIDLY AND EFFECTIVELY
WITH OPTIMIZED SHIFTING GRADIENTS
IN THE SECOND DIMENSION
1,2
1
Bob W. Pirok , Gabriel Vivó-Truyols ,
1
Peter J. Schoenmakers
1
Analytical Chemistry (HIMS) - University
of Amsterdam, Science Park 904, 1098 XH
2
TI-COAST, Science Park 904, 1098 XH
KNL.13
A HIGHLY SENSITIVE GC-DETECTOR
BASED ON DIELECTRIC BARRIER
DISCHARGE IONIZATION
Ansgar T. Kirk, Torben Last, Stefan
Zimmermann
Institute of Electrical Engineering and
Measurement Technology, Department of
Sensors and Measurement Technology Leibniz University Hannover, Appelstr. 9A,
30167 Hannover, Germany
18:15
KNL.07
ANALYSIS OF COMPLEX
HYDROCARBON MIXTURES AS FOOD
+
CONTAMINANTS BY ON-LINE LC(AG )LC-GC
1
2
Martin Lommatzsch , Maurus Biedermann ,
1
2
Thomas J. Simat , Konrad Grob
1
Chair of Food Science and Food Contact
Materials - TU Dresden, Bergstr. 66, 01062
Dresden, Germany
2
KLZH, Fehrenstr. 15, 8032 Zurich,
Switzerland
KNL.14
CONDENSATION VERSUS CHAINGROWTH POLYMERIZED IONIC LIQUIDS
AS HIGH TEMPERATURE STABLE
STATIONARY PHASE IN GAS
CHROMATOGRAPHY
1
2
Kevin Roeleveld , Frank David , Frédéric
1
Lynen
1
Separation Science Group - Ghent
University, Krijgslaan 281, 9000 Gent,
Belgium
2
Research Institute for Chromatography,
President Kennedypark 26, 8500 Kortrijk,
Belgium
18:45
Wine and Cheese offered by AGILENT TECHNOLOGIES, Terrace Hotel Sole
33
Thursday June 2, 2016
08:30 – 10:30
ISCC Session 8 – OTHER
COMPREHENSIVE TECHNIQUES - Room
1000
Chairperson:
Mark Schure
Kroungold Analytical Inc., Blue Bell, United
States
ISCC Session 9 - ELECTRODRIVEN
TECHNIQUES - Room 300
Chairperson:
Salvatore Fanali
Italian National Research Council-C.N.R.,
Monterotondo Scalo (Roma), Italy
08:30
LE.39
IN PURSUIT OF THE MICROBOSPHERE
1
Francesco Cacciola , Domenica
2
3
Mangraviti , Francesca Rigano , Paola
1
2,3
2,3
Donato , Paola Dugo , Luigi Mondello ,
4
Yukari Nishizawa-Brennen , Karen M.
4
4
5
Draths , John W. Frost , Hernan J. Cortes
1
Dipartimento di Scienze Biomediche,
Odontoiatriche e delle Immagini
Morfologiche e Funzionali - University of
Messina, Viale Consolare Valeria, 98165
Messina, Italy
2
Dipartimento di Scienze Chimiche,
Biologiche, Farmaceutiche ed Ambientali University of Messina, Viale Annunziata,
Polo Annunziata, 98168 Messina, Italy
3
Chromaleont s.r.l, c/o University of
Messina, Viale Annunziata, Polo
Annunziata, 98168 Messina, Italy
4
Department of Chemistry - Michigan State
University, 578 S. Shaw Lane, 48824 East
Lansing, United States
5
Hernan Cortes Consulting LLC, 4613
Springbrook Court, 48642 Midland, United
States
LE.45
CAPILLARY ZONE ELECTROPHORESISTANDEM MASS SPECTROMETRY FOR
PHOSPHOPROTEOMIC ANALYSIS
Norman Dovichi
University of Notre Dame, 251 Nieuwland
Science Hall, 46556-5670 Notre Dame, IL,
United States
08:50
LE.40
RECENT APPLICATIONS OF LC×LC TO
NATURAL PRODUCTS ANALYSIS
1,2
3
Paola Dugo , Francesco Cacciola , Paola
3
1,2
Donato , Luigi Mondello
1
Biologiche, Farmaceutiche ed Ambientali University of Messina, Polo Annunziata,
Viale Annunziata s.n., 98168 Messina, Italy
2
3
Messina, Italy
LE.46
NANOSPRAY INTERFACING FOR
CAPILLARY ELECTROPHORESIS-MASS
SPECTROMETRY
Frantisek Foret, Jana Krenkova, Anna Tycova,
Karel Kleparnik
Institute of Analytical Chemistry, ASCR, v.v.i.,
60200 Brno, Czech Republic
09:10
LE.45
LE.41
DEVELOPING AND IMPROVING LC×LC
SEPARATIONS
Peter Schoenmakers, Anna Baglai, Henrik
Cornelisson van de Ven, Andrea Gargano,
Bob Pirok, Bert Wouters.
University of Armsterdam, Nieuwe
Achetergracht 166, 1018 WV Amsterdam,
The Netherlands
LE.47
MICROFABRICATED CE-NESI DEVICES
FOR THE ANALYSIS OF
BIOPHARMACEUTICAL MATERIALS
1
2
Erin A. Redman , J. Scott Mellors , J.Michael
1
Ramsey
1
University of North Carolina, 251 Chapman
Hall, CB#3216, NC 27599 Chapel Hill, United
States
2
908 Devices Inc., 27 Drydock Ave., 02210
Boston, United States
34
09:30
LE.42
QUANTITATION IN MULTIPLE-HEARTCUTTING TWO-DIMENSIONAL LIQUID
CHROMATOGRAPHY WITH UV AND ESIMS DETECTION
1
2
Monika Dittmann , Stephan Buckenmaier ,
3
Matthias Pursch
1
Agilent Technologies, Hewlett-Packard
Str. 8, 76337 Waldbronn, Germany
2
R&D - Agilent Technologies, HewlettPackard Str. 8, 76337 Waldbronn,
Germany
3
Analytical Technology Center - Dow
Deutschland Anlagengesellschaft mbH,
Industriestrasse 1, 77836 Rheinmuenster,
Germany
LE.48
SOLID-PHASE EXTRACTION,
FLUORESCENCE LABELING AND
ELECTROPHORETIC SEPARATION OF
PRE-TERM BIRTH BIOMARKERS USING
AN INTEGRATED MICROFLUIDIC DEVICE
Adam T. Woolley, Vishal Sahore, Suresh
Kumar, Anna V. Nielsen, Mukul Sonker, Ellen
K. Parker, Jacob B. Nielsen
Department of Chemistry/Biochemistry Brigham Young University, C100 BNSN,
84602 Provo, UT, United States
09:50
LE.43
LIQUID CHROMATOGRAPHY USING RPUHPLC AS THE SECOND SEPARATION
DIMENSION FOR CAROTENOID
ANALYSIS
1
2
Paola Donato ,Veronica Inferrrera ,
1
1
Daniele Giuffrida , Francesco Cacciola ,
3
2,4
Kevin Schug , Paola Dugo , Luigi
2,4
Mondello
1
Messina, Italy
2
Biologiche, Farmaceutiche ed Ambientali University of Messina, Polo Annunziata,
Viale Annunziata s.n., 98168 Messina, Italy
3
Texas at Arlington, 700 Planetarium PI.,
Box 19065, TX 76019-0065 Arlington,
United States
4
LE.49
TEMPERATURE MODULATION IN PACKED
AND OPEN TUBULAR CAPILLARY
ELECTROCHROMATOGRAPHY
Frederic Lynen
Separation Science Group - Department of
Organic and Macromolecular Chemistry Ghent University, Krijgslaan 281 S4-bis, 9000
Ghent, Belgium
10:10
LE.44
LIQUID CHROMATOGRAPHY COUPLED
TO MASS SPECTROMETRY (LC×LCMS/MS) FOR GEOGRAPHICAL ORIGIN
ASSIGNMENT OF LICORICE
1
1
Lidia Montero , Elena Ibanez , Mariateresa
2
2
3
Russo , Rosa di Sanzo , Luca Rastrelli ,
1
1
Alejandro Cifuentes , Miguel Herrero
1
Institute of Food Science Research-CIAL
(CSIC), Spain, Nicolas Cabrera 9, 28049
Madrid, Spain
2
Dipartimento di Agraria (QuaSic.A.Tec.),
Università Mediterranea di Reggio Calabria,
loc. Feo di Vito, 89122 Reggio Calabria,
Italy
3
Dipartimento di Farmacia, Università di
Salerno, Via Giovanni Paolo II 132, 84084
Fisciano, Italy
LE.50
CAPILLARY ELECTROPHORESIS FOR
DESCRIPTION OF NANOPARTICLES IONIC
CORONA
Jan Petr, Daniel Baron, Jana Horska, Andrea
Sebestova
Department of Analytical Chemistry - Palacky
University in Olomouc, Regional Centre of
Advanced Technologies and Materials, 17.
listopadu 12, 77146 Olomouc, Czech Republic
35
10:30 – 12:00
Coffee Break – Seminars – Exhibition – Posters J, P
10:45 – 11:45
Room 1000
Seminar
THERMO FISHER SCIENTIFIC
Room 300
Seminar
BRECHBUELER
Room 100
Seminar
JEOL EUROPE
12:00 – 14:00
14:00 – 15:40
ISCC Session 10 - STATE OF THE ART
GC APPLICATIONS - Room 1000
Chairperson:
Milton L. Lee
Brigham Young University, Provo, UT,
United States
ISCC Session 11 - MONOLITHS AND
COLUMN TECHNOLOGY - Room 300
Chairperson:
Marja-Liisa Riekkola
University of Helsinki, Helsinki, Finland
14:00
LE.51
DIRECT MEASUREMENT OF
ELEMENTAL MERCURY BY GAS
CHROMATOGRAPHY AND
ULTRAVIOLET PHOTOMETRIC
DETECTION
1,2
3,2
Robert A. Shellie , Ronda Gras , Jim
3,4
Luong
1
Trajan Scientific and Medical, 7 Argent
2
ASTech - University of Tasmania, Private
Bag 75, 7001 Hobart, Australia
3
Analytical Technology Centre - Dow
Chemical Canada, Highway 15, T8L2P4
Fort Saskatchewan, Canada
4
ACROSS - University of Tasmania,
Private Bag 75, 7001 Hobart, Australia
LE.56
PRACTICE AND RAMIFICIATIONS OF
ULTRAFAST LC AND SFC
Daniel W. Armstrong
Department of Chemistry and Biochemistry University of Texas at Arlington, Arlington,
TX76019 Arlington, United States
14:20
LE.52
GC-IMS-QTOF-MS – A NEW
HYPHENATED SEPARATION
TECHNIQUE FOR THE ANALYSIS OF
COMPLEX SAMPLES
Oliver J. Schmitz
University of Duisburg-Essen,
Universitaetsstr. 5, 45141 Essen, Germany
LE.57
UNDERSTANDING PORE STRUCTURE IN
CHROMATOGRAPHIC PARTICLES USING
FOCUSED ION BEAM/SCANNING
ELECTRON MICROSCOPY (FIB/SEM) AND
ADVANCED COMPUTER MODELING
1
2
Mark Schure , Taylor Shields , Brian M.
2
3
4
Wagner , Clare M. Wunder , Robert S. Maier ,
2
Joseph J. Kirkland
1
Kroungold Analytical Inc, 1299 Butler Pike,
PA 19422 Blue Bell United States
2
Advanced Materials Technology, Inc., 3521
Silverside Road, 19810 Wilmington, United
States
3
Dept of Chemical Engineering - University of
Delaware, 150 Academy Street, 19716
Newark, United States
4
Robert S Maier Consulting, Tucson, United
States
36
14:40
LE.53
PHOTOIONISATION-TOF MASS
SPECTROMETRY AS DETECTOR FOR
THERMOGRAVIMETRY COUPLED TO
FAST OPTICALLY HEATED GAS
CHROMATOGRAPHY OR GCXGC:
INVESTIGATION OF FLAVOR
FORMATION IN ROASTING OF
FOODSTUFFS AND ANALYSIS OF
PETROCHEMICAL FRACTIONS
1,2
1
Ralf Zimmermann , Thomas Gröger ,
1
1
Michael Fischer , Thorsten Streibel ,
3
Andreas Walte , Mohammad Saraji3
4
Bozorgzad , Thomas Denner , Sebastian
1
Wohlfahrt
1
Joint Mass Spectrometry
Centre/Cooperation Group Comprehensive
Molecular Analytics - Helmholtz Zentrum
München, Ingolstädter Landstrasse 1,
85764 Neuherberg, Germany
2
Institute of Chemistry - University of
Rostock, Dr.-Lorenz-Weg 1, 18051
Rostock, Germany
3
Photonion Gmbh, Hagenowerstr 71,
19061 schwerin, Germany
4
Netzsch GmbH, Wittelsbacherstraße 42,,
95100 Selb, Germany
LE.58
METAL-ORGANIC FRAMEWORKS: NEW
MEANS TO PREPARATION OF
CHROMATOGRAPHIC MEDIA WITH
CONTROLLED SELECTIVITY
Frantisek Svec
Lawrence Berkeley Nat. Lab., Mail Stop
67R6110, CA 94720 Berkeley, United States
15:00
LE.54
SCREENING OF FLAME RETARDANTS
AND OTHER ADDITIVES IN
ELECTRONIC WASTE, PLASTICS AND
OTHER MATERIALS WITH DIRECT
PROBE COUPLED TO ATMOSPHERIC
PRESSURE CHEMICAL IONIZATIONHIGH RESOLUTION TIME-OF-FLIGHT
MASS SPECTROMETRY
Ana Ballesteros-Gomez, Jacob De Boer
IVM - VU University, De Boelelaan 1087,
1081HV Amsterdam, Netherlands
LE.59
HOW IMPORTANT IS STRUCTURAL
SIMILARITY IN QUANTITATIVE
STRUCTURE-RETENTION
RELATIONSHIPS
1
1
1
Paul Haddad , Soo H. Park , Maryam Taraji ,
1
1
1
Yabin Wen , Mohammad Talebi , Ruth Amos ,
1
2
Robert Shellie , Roman Szucs , John W.
3
4
Dolan , Christopher A. Pohl
1
School of Chemistry - ACROSS, University
Tasmania, Australia
2
Pfizer Global R&D, Sandwich, CT139NJ
Sandwich, United Kingdom
3
LC Resources, 1795 NM Wallace Rd, 97128
McMinnville, United States
4
ThermoFisher Scientific, Sunnyvale, 94085
Sunnyvale, United States
15:20
LE.55
IMPLEMENTATION OF AN ADVANCED
WORKFLOW TO ENHANCE THE
CONFIDENCE IN COMPOUND
IDENTIFICATION FOR NON-TARGETED
GC-HR-MS APPLICATIONS
Eric Dossin, Elyette Martin, Antonio
Castellon, Pierrick Diana, Pavel Pospisil,
Mark Bentley, Philippe Guy
Philip Morris International R&D - Philip
Morris Products S.A., Quai Jeanrenaud 5,
2000 Neuchatel, Switzerland
LE.60
POLYMERIC MONOLITHIC MATERIALS
FOR RAPID SAMPLE PREPARATION
1
2
3
Emily Hilder , Esme Candish , Robert Shellie ,
1
3
Sara Thomas , Hans-Juergen Wirth , Andrew
3
3
Gooley , Wei Boon Hon
1
University of South Australia, GPO Box
2471, 5001 Adelaide, Australia
2
University of Tasmania, ACROSS, 7001
Hobart, Australia
3
Trajan Scientific and Medical, 7 Argent
15:40 – 17:00
Coffee Break – Seminars – Exhibition – Posters M, O
15:45 – 16:45
Room 1000
Seminar
MERCK/SIGMA/ALDRICH/SUPELCO
Room 300
Seminar
RESTEK
Room 100
Seminar
CHROMALEONT
37
17:00 – 18.30
ISCC KEYNOTE LECTURES: SAMPLE
PREPARATION 2 AND GC- Room 1000
Chairperson:
Elena Ibanez
Instituto de Investigación en Ciencias de la
Alimentación-CIAL (CSIC), Madrid, Spain
ISCC KEYNOTE LECTURES:
MULTIDIMENSIONAL TECHNIQUES AND
MISCELLANEA - Room 300
Chairperson:
Ralf Zimmermann
Comprehensive Molecular Analytics, Munich,
Germany
17:00
KNL.15
DETERMINATION OF ACRYLAMIDE IN
ROASTED COFFEE POWDERS AND
BREWS AT TRACE LEVEL BY SOLID
PHASE MICROEXTRACTION WITH
POLYMERIC IONIC LIQUID-BASED
FIBERS AND GC-MS
1
1
Cecilia Cagliero , Chiara Cordero , Erica
1
1
Liberto , Barbara Sgorbini , Patrizia
1
2
1
Rubiolo , Jared L. Anderson , Carlo Bicchi
1
Dipartimento di Scienza e Tecnologia del
Farmaco - Università di Torino, Via Pietro
Giuria, 9, 10125 Torino, Italy
2
Department of Chemistry - Iowa State
University, 1605 Gilman Hall, 50011 Ames,
United States
KNL.21
EVALUATION AND FUNCTION OF DAMINOACID IN BRAIN TISSUE BY TWO
DIMENSIONAL LIQUID
CHROMATOGRAPHY
1
1
1
Choyce Weatherly , Siqi Du , Curran Parpia ,
2
2
Polan Santos , Adam Hartman , Daniel
1
Armstrong
1
The University of Texas at Arlington, 76019
Arlington, United States
2
Johns Hopkins Hospital, 1800 Orleans St,
21287 Baltimore, United States
17:15
KNL.16
NEW MATERIALS FOR MAGNETIC
SOLID PHASE EXTRACTION AND
ENRICHMENT OF PHOSPHORYLATED
PEPTIDES
Susy Piovesana, Anna Laura Capriotti,
Francesca Ferraris, Aldo Laganà
Dipartimento di Chimica - Sapienza
Università di Roma, Piazzale Aldo Moro 5,
185 Rome, Italy
KNL.22
FROM X-MS TO X×MS. HOW TO
TRANSFORM A HYPHENATED
TECHNIQUE TO A TWO DIMENSIONAL
SEPARATION USING SIMPLE
CHEMOMETRICS TOOLS
Guillaume L. Erny, Arminda Alves
Laboratory for Process Engineering,
Environment, Biotechnology and Energy Faculdade de Engenharia da Universidade do
Porto, Rua do Dr. Roberto Frias, s/n, 4200
465 Porto, Portugal
17:30
KNL.17
ANALYZE OF PESTICIDES IN FOOD
PRODUCT USING SFE-SFC-MSMS
1
2
Sigrid Baumgarten , Manasi Panov
1
Shimadzu Europa, Albert-Hahn-Straße 610, D-47269 Duisburg, Germany
2
Chem Analytical Services Ltd, 65A Cherni
Vrah blvd, 1407 Sofia, Bulgaria
KNL.23
HIGH EFFICIENCY MULTIDIMENSIONAL
GAS CHROMATOGRAPHY COUPLED TO
ISOTOPE RATIO MASS SPECTROMETRY
AND QUADRUPOLE MASS
SPECTROMETRY SIMULTANEOUS
DETECTION
1
1
Danilo Sciarrone , Antonino Schepis , Luigi
1,2
Mondello
1
Biologiche, Farmaceutiche ed Ambientali Università degli Studi di Messina, Viale
2
Chromaleont S..r.l. – Viale Boccetta 70,
98122 Messina, Italy
17:45
KNL.18
EXPLOITING THE VERSATILITY OF
VACUUM-ASSISTED HEADSPACE
SOLIDPHASE MICROEXTRACTION
1
1
Evangelia Yiantzi , Maria-Lito Glykioti ,
2
2
Maria Celeiro , Maria Llompart , Elefteria
1
Psillakis
1
Department of Environmental Engineering
- Technical University of Crete,
Polytechneioupolis, GR-73100 Chania
Crete, Greece
2
Department of Analytical Chemistry University of Santiago de Compostela,
University Campus, E-15782 Santiago de
Compostela, Spain
KNL.24
MULTIDIMENSIONAL GAS
CHROMATOGRAPHY HYPHENATED TO
ISOTOPIC RATIO MASS SPECTROMETRY
FOR CARBON DELTA VALUE
MEASUREMENTS AND QUADRUPOLE MS
FOR MOLECULAR CONFIRMATION IN THE
INVESTIGATION OF ENDOGENOUS
ANABOLIC STEROIDS IN URINE
1
2
Alessandro Casilli , Thomas Piper , Fabio A.
1
1
Oliveira , Monica Padilha , Henrique M.
1
2
Pereira , Mario Thevis , Francisco R. Aquino
1
Neto
1
LBCD-LADETEC - Universidade Federal do
Rio de Janeiro, Instituto de Química, 1281,
22941-909 Rio de Janeiro, Brazil
2
Center for Preventive Doping ResearchInstitute of Biochemistry - German Sport
University Cologne, Am Sportpark
Müngersdorf 6, 50933 Köln, Germany
38
18:00
KNL.19
IDENTIFICATION WITH HEADSPACE
SOLID PHASE MICROEXTRACTION
(SPME) AND GAS CHROMATOGRAPHYMASS SPECTROMETRY (GC-MS) OF
VOLATILE ORGANIC COMPOUNDS
PRODUCED IN-VITRO BY BACTERIA
ISOLATED FROM HUMAN FACE SKIN
MICROBIOTA
1
2
Chiara Carazzone , Marcela Tabares ,
2
3
Martha Vives , Mario I. Ortiz , Jorge
3
Molina
1
Department of Chemistry - Universidad de
los Andes, Carrera 1# 18A-10, 111711
Bogota, Colombia
2
Centro de Investigaciones Microbiologicas
- Universidad de los Andes, Carrera 1#
18A-10, 111711 Bogota, Colombia
3
Centro de Investigaciones en
Microbiologia y Parasitologia Tropical Universidad de los Andes, Carrera 1# 18A10, 111711 Bogota, Colombia
KNL.25
CHARACTERIZATION AND
QUANTIFICATION OF ULTRA-THIN
POLYMER FILMS BY HYPHENATED MASS
SPECTROMETRIC TECHNIQUES
1
1
Valentina Gianotti , Diego Antonioli , Katia
1
1
Sparnacci , Michele Laus , Tommaso J.
2
2
Giammaria , Monica Ceresoli , Gabriele
2
2
Seguini , Michele Perego
1
DISAV Dipartimento di Scienze
dell'Ambiente e della Vita - University of
Piemonte Orientale, Viale T. Michel 11, 15121
Alessandria, Italy
2
Laboratory MDM - IMM-CNR, Agrate
Brianza, 20864 Agrate Brianza, Italy
18:15
KNL.20
INNOVATIVE SOLID-PHASE
MICROEXTRACTION COATINGS FOR
THE SUPRAMOLECULAR DETECTION
OF BTEX IN AIR
Federica Bianchi, Nicolò Riboni, Enrico
Dalcanale, Maria Careri
Dipartimento di Chimica, Università di
Parma, Parco Area delle Scienze 17/A,
43124 Parma
KNL.26
PEAK DECONVOLUTION TO CORRECTLY
AND COMPLETELY ASSESS THE TRUE
BAND BROADENING OF
CHROMATOGRAPHIC COLUMNS
Yoachim Vanderheyden, Gert Desmet, Ken
Broeckhoven
Universiteit Brussel, Pleinlaan 2, 1050
Brussels, Belgium
21:00 – 23:00
Discussion - Comprehensive Techniques, Conference Centre - Room 1000
39
Friday, June 3, 2016
08:30 – 10:30
ISCC Session 12 - CAPILLARY GC 2 Room 1000
Chairperson:
Robert Synovec
University of Washington, Seattle, WA,
United States
ISCC Session 13 – MICRO LC 2 - Room 300
08:30
LE.61
MICROFABRICATED AND FIELDPORTABLE GC FOR AIR POLLUTION
MEASUREMENTS
Alastair Lewis, Rachel E. Dunmore,
Stephen J. Andrews, Michelle Wang,
Jacqui F. Hamilton, Marvin Shaw, Martyn
Ward
York, Heslington, Y010 5DD York, United
Kingdom
LE.67
SMALL BUGS - BIG IMPACT.
METABOLOMICS INVESTIGATION OF THE
MICROBIOME
Katja Dettmer
Institute of Functional Genomics - University
of Regensburg, Am Biopark 9, 93053
Regensburg, Germany
08:50
LE.62
DETERMINATION OF ALLERGY
SUBSTANCES IN FRAGRANCE BY
CAPILLARY GAS CHROMATOGRAPHY /
LASER IONIZATION MASS
SPECTROMETRY USING A
FEMTROSECOND LASER AS AN
IONIZATION SOURCE
1
2
Shinpei Shibuta , Tomoko Imasaka , Totaro
1
Imasaka
1
Department of Applied Chemistry,
Graduate School of Engineering - Kyushu
University, 744 Motooka, Nishi-ku, 8190395 Fukuoka, Japan
2
Graduate School of Design - Kyushu
University, 4-9-1 Shiobaru, Minami-ku, 8158540 Fukuoka, Japan
LE.68
NOVEL STRATEGY TO SCREEN AND
PROFILE STEVIOL GLYCOSIDES OF
NATURAL SWEETENERS IN FOOD USING
MICROFLUIDIC UPLC ION MOBILITY MASS
SPECTROMETRY
1
1
Eimear McCall , Ramesh Rao , Michael
1
1
McCullagh , David Douce , Severine
2
Goscinny
1
Food and Environmental - Waters, Stamford
Avenue, SK9 4AX Wilmslow, United Kingdom
2
Wetenschappelijk Instituut VolksgezondheidInstitut Scientifique de Santé Publique, Rue
Juliette Wytsmans, 1050 Brussels, Belgium
09:10
LE.63
DIODE ARRAY DETECTION WITH GAS
CHROMATOGRAPHY
1,2
1,3
Ronda Gras , Jim Luong , Robert A.
2,4
Shellie
1
Analytical Technology Centre - Dow
Chemical Canada, PO BAG 16, Highway
15, T8L2P4 Fort Saskatchewan, AB,
Canada
2
ARC Training Centre for Portable
Analytical Separation Technologies
(ASTech) - University of Tasmania, Private
Bag 75, 7001 Hobart, Australia
3
Australian Centre for Research on
Australia
4
Trajan Scientific & Medical, 7 Argent
LE.69
ADVANTAGES OF PACKED
MICROFLUIDIC SEPARATION CHANNELS
FOR VERY HIGH-PRESSURE LIQUID
CHROMATOGRAPHY - MASS
SPECTROMETRY ANALYSES
Fabrice Gritti, Thomas McDonald, Martin Gilar
Instrument/Core Research/Fundamental Waters Corporation, 34 Mapple Street, 01157
Milford, United States
09:30
LE.64
FINALLY A SIGNIFICANT IMPROVED
CHROMATOGRAPHIC SEPARATION
FOR ARGON AND OXYGEN, USING
NEW PLOT COLUMN PHASE AND
DEPOSITION TECHNOLOGIES
1
2
Jaap de Zeeuw , Bill Bromps , Ashlee
2
2
Reese , Roy Lautamo
1
New products group - Restek Corp.,
weerhaan 9, 4336 KT 4336 KT Middelburg,
Netherlands
2
Restek corp, 4211 Business Dr, 95682
Shingle springs, United States
LE.70
ELECTRON IONIZATION LC-MS WITH
SUPERSONIC MOLECULAR BEAMS - THE
NEW SYSTEM, ADVANTAGES AND
BENEFITS
Alexander B. Fialkov, Boaz Seemann,
Svetlana Tsizin, Tal Alon, Aviv Amirav
Chemistry - Tel Aviv University, Ramat Aviv,
69978 Tel Aviv, Israel
Chairperson:
Peter Myers
Liverpool, Liverpool, United Kingdom
40
09:50
LE.65
GET THE BEST PEAK SHAPE
PERFORMANCE AND CONSISTENCY
WITH ULTRA INERT WAX COLUMN
1
2
Laura Provoost , Yun Zou
1
Agilent Crosslab Group - Agilent
Technologies, Herculesweg 8, 4338 PL
Middelburg, Netherlands
2
Agilent Crosslab Group - Agilent
Technologies, 412 Ying Lun Road, 200131
Shanghai, China
LE.71
AUTOMATED LIBRARY-BUILDING OF
METABOLITES IN COMPLEX SAMPLES
1
1
Albert Robbat , Nicole Kfoury , Amanda
1
2
2
Kowalsick , Yuriy Gankin , Eugene Baidakov
1
Department of Chemistry - Tufts University,
62 Talbot Ave, 02155 Medford, United States
2
EPAM Systems, 41 Univesity Drive, 18940
Newtown, United States
10:10
LE.66
MICROFABRICATED GAS
CHROMATOGRAPHY COLUMNS WITH
STATIONARY PHASES BASED ON SOLGEL PROCESS
1
2
Elodie Lussac , Florence Ricoul , Bertrand
2
2
3
Bourlon , Eric Ollier , Regis Barattin ,
1
1
Valerie PeulonAgasse , Pascal Cardinael
1
Sciences et Méthodes Séparatives University of Rouen, rue Tesnière, 76821
Mont saint aignan, France
2
CEA, LETI - University of Grenoble Alpes,
MINATEC Campus, 38054 Grenoble,
France
3
APIX Analytics, Miniparc Polytec Immeuble Tramontane, 60 rue des Berges,
38000 Grenoble, France
LE.72
INVESTIGATIONS ON THE
METABOLIZATION OF XENOBIOTICS IN
PLANTS
Christian W. Klampfl, Lisa Emhofer, Markus
Himmelsbach, Wolfgang Buchberger
Johannes Kepler-University, Austria,
Altenbergerstr 69, 4040 Linz, Austria
10:30 – 11:00
11:00 – 12:40
ISCC Session 14 – MISCELLANEOUS Room 1000
Chairperson:
Paola Dugo
ISCC Session 15 – SAMPLE
PREPARATION 3 - Room 300
Chairperson:
Frank David
R.I.C., Kortrijk, Belgium
11:00
LE.73
FOOD INGREDIENTS, FOODOMICS AND
CANCER
Alejandro Cifuentes
Foodomics Lab, CIAL, CSIC, Nicolas
Cabrera 9, 28049 Madrid, Spain
LE.78
DYNAMIC HEADSPACE SAMPLING IN THE
ANALYSIS OF SOLID MATRICES OF
VEGETABLE ORIGIN
Carlo Bicchi, Cecilia Cagliero, Chiara
Cordero, Erica Liberto, Patrizia Rubiolo,
Barbara Sgorbini
Dipartimento di Scienza e Tecn. del Farmaco University of Torino, Via Pietro Giuria 9, 10125
Torino, Italy
11:20
LE.74
MICRO-PLATE ARRAY COLUMNS FOR
GC
1
2
Sander Jespers , Frederic Lynen , Gert
1
Desmet
1
Department of Chemical Engineering Vrije Universiteit Brussel (VUB), Pleinlaan
2, 1050 Brussel, Belgium
2
Separation Science Group, Universiteit
Gent (Ugent), Krijgslaan 281, B-9000 Gent,
Belgium
LE.79
SOLID-PHASE MICROEXTRACTION
ARROW SYSTEM – A GREAT POTENTIAL
FOR SAMPLING AND SAMPLE
PREPARATION
1
1
Marja-Liisa Riekkola , Hangzhen Lan , Tuukka
1
1
Rönkkö , Jevgeni Parshintsev , Kari
1
1
2
Hartonen , Luis Barreira , Markku Kulmala
1
Laboratory of Analytical Chemistry,
Helsinki, P.O. Box 55, 00014 Helsinki, Finland
2
Division of Atmospheric Sciences,
Department of Physics - University of Helsinki,
P.O. Box 64, 00014 Helsinki, Finland
41
11:40
LE.75
A FASCINATING CHROMATOGRAPHIC
JOURNEY THROUGH THE FLOWER
KINGDOM
Elena Stashenko
Cenivam-Chemistry - Industrial University
of Santander, Building 45, Carrera 27 calle
9, 680002 Bucaramanga, Colombia
LE.80
POLYMERIC IONIC LIQUIDS AND
MAGNETIC IONIC LIQUIDS IN
ANALYTICAL CHEMISTRY
Jared L. Anderson
Department of Chemistry - Iowa State
University, 1605 Gilman Hall, 50010 Ames,
United States
12:00
LE.76
INTRODUCTION OF MOMENT ANALYSIS
THEORY TO KINETIC STUDY OF
INTERMOLECULAR INTERACTION BY
AFFINITY CAPILLARY
ELECTROPHORESIS
Kanji Miyabe
Rikkyo University, 171-8501 Tokyo, Japan
LE.81
ON-LINE COMBINATION OF SAMPLE
PREPARATION-LIQUID
CHROMATOGRAPHYTANDEM MASS
SPECTROMETRY FOR AUTOMATED
DETERMINATION OF RESIDUES AND
CONTAMINANTS IN FOOD SAMPLES
Fernando M. Lancas
Institute of Chemistry at Sao Carlos University of Sao Paulo, Postal Code 780,
13560-970 Sao Carlos, Brazil
12:20
LE.77
COMPARISON OF GC-QMS WITH GCQTOFMS FOR THE NON-TARGETED
ANALYSIS OF VOLATILE COMPOUNDS
FORMED IN MEAT AND MODEL
SYSTEMS
1
1
James B. Addison , Lewis Jones , Kathy
2
2
Ridgway , Nathan Hawkins
1
Flavour Chemistry - Waltham Centre for
Pet Nutrition, Freeby Lane, LE14 4RT
Melton Mowbray, United Kingdom
2
Anatune Ltd, Wellbrook Court, CB3 0NA
Cambridge, United Kingdom
LE.82
EXTRACTION, CONCENTRATION AND
SEPARATION OF dsDNAS USING AN
OPEN CAPILLARY WITHOUT AN APPLIED
ELECTRIC FIELD
1
2
Sarah Friedrich , Jeffrey M. Burke , Kelvin
2
1
3
Liu , Tza-Huei Wang , Cornelius F. Ivory
1
Mechanical Engineering - Johns Hopkins
University, 108 Latrobe Hall, 21218 Baltimore,
United States
2
Circulomics, Inc., , 810 Wyman Park Drive,
21211 Baltimore, United States
3
Chemical Engineering - Washington State
University, Wegner 111, Pullman WA, 991646515, United States
12:40 – 13:00
Presentation of the Leslie S. Ettre Award sponsored by PERKINELMER, Inc.
Presentation of the Best Poster Award sponsored by SHIMADZU Europa GmbH and
SPRINGER
Closing Address
13:00
Farewell Cocktail, offered by Waters Corporation, Conference Center
42
-VENDOR SEMINARSTuesday, May 31, 2016
Timing
Location
Vendor seminar by
15:45 – 16:45
Room 1000
SHIMADZU:
Smart solutions for complex samples
- Dual and capillary liquid chromatography coupled to tandem mass spectrometry for
enhanced throughput and sensitivity
Presenter:
Gerard Hopfgartner, University of Geneva, Switzerland
- SFE-SFC-MS -The latest addition to the chromatography toolbox
Presenter:
Gesa Schad, Shimadzu Europa Gmbh
- Comprehensive 2D gas chromatography combined with a triple-quadrupole mass
spectrometer and a useful quali/quantitative tool
Presenter:
Mariosimone Zoccali, Chromaleont S.r.l., Messina, Italy
15:45 – 16:45
Room 300
LECO
- LECO technology development – technical update
Presenter:
Joe Binkley, LECO Corporation, USA
- Statistical comparisons of beer types using GC×GC-(HR) TOFMS
Presenter:
Jean-Francois F. Focant, Department of Chemistry – University of Liege, Belgium
- Spices – are they authentic and safe ? Seeking answer by GC TOFMS
Presenter:
Jana Haislova, Jaromir Hradecky, Department of Food Analysis and Nutrition,
University of Chemistry and Technology, Prague, Czech Republic
15:45 – 16:45
Room 100
ZOEX
- Developments in thermal and flow modulators in GC×GC: a tailored solution for
every analytical challenge
Presenter:
Daniela Peroni, Zoex Europe, Netherlands
18:45-20:00
Room 100
AGILENT TECHNOLOGIES Users meeting
43
Wednesday, June 01, 2016
Timing
Location
Vendor seminar by
10:45 – 11:45
Room 1000
AGILENT TECHNOLOGIES
Advance Your Laboratory Power with Agilent’s Innovative Analytical
Separation and Detection in Analytical Measurement
- Differential Flow Modulated GC×GC-qMS - how to make friendly a complex task
Presenter:
Chiara Cordero, Dipartimento di Scienza e Tecnologia del Farmaco Università degli
Studi di Torino, Turin – Italy
- The four separation dimensions of 2D-LC-IM-qTOF-MS as an optimal tool for nontarget analysis
Presenter:
Oliver J. Schmitz, University of Duisburg-Essen. Faculty of Chemistry, Applied
Analytical Chemistry, Essen, Germany
10:45 – 11:45
Room 300
DANI
- Advances in separation and detection systems for demanding applications: solid
phase deposition GC/FTIR and LN2-free modulator for GC×GC TOFMS
Presenter:
Albino Sironi, DANI Instruments
Alessandro Casilli, LBCD-LADETEC, Instituto de Química, Universidade Federal do
Rio de Janeiro, Brasil
10:45 – 11:45
Room 100
PEAK SCIENTIFIC
- Switching GC carrier gas – How to set up your GC using hydrogen
Presenter:
Edward Connor, Peak Scientific, UK
11:45 – 12:45
Room 1000
WATERS
- Identification and quantitation of (mixed) halogenated dioxins and furans using
atmospheric pressure chemical ionisation quadrupole time of flight mass
spectrometry
Presenter:
Karl Jobst, Department of Chemistry and Chemical Biology, McMaster University,
Ontario, Canada
- New MS Technologies for Screening and Quantification of Contaminants
Presenter:
Steve Preece, Waters, Senior Manager MS Business, Europe and India
11:45 – 12:45
Room 300
MARKES INTERNATIONAL
- Tandem Ionisation for GC-MS and GC×GC-MS
Presenters:
Laura McGregor, Markes International
Nick Bukowski, Markes International
- Forensic blood VOC characterisation by TD–GC×GC–TOF MS with variable-energy
electron ionisation
Presenter:
Katelynn Perrault, University of Liege, Belgium
44
11:45 – 12:45
Room 100
ELEMENTAR/ISOPRIME
- Advanced chromatographic interfaces for the detection of isotopic ratios in complex
matrixes
Presenters:
Filip Volders, Christian Schmidt - Elementar Analysensysteme GmbH
Eugen Federher, Paul Wheeler - Isoprime Ltd
15:45 – 16:45
Room 1000
PERKINELMER
- Pushing the Technology and Application Frontiers in Compact High-performance
GC-MS
Presenters:
Milton Lee, Brigham Young University, UT, USA
Philip Marriott, Monash University, Australia
15:45 – 16:45
Room 300
GERSTEL
-Extractables and Leachables Analysis using Thermal Desorption and SBSE with
GC Single Quad and GC Time-of-Flight Mass Spectrometric Detection
Presenters:
Andreas Hoffmann , T. Albinus - Gerstel GmbH & Co.KG, Mülheim, Germany
E.Almasi, Agilent Technologies, Santa Clara, USA
Kurt Thaxton, Gerstel, Inc., Linthicum, USA
- SBSE in a routine environment, does it really work? A testimonial.
Presenters:
C. Devos, B. Tienpont, F. David, and P. Sandra, RIC, Pres Kennedypark 26, B-8500
Kortrijk, Belgium
S. Vonckx, European Quality Center, Coca-Cola Services, Brussels, Belgium
15:45 – 16:45
Room 100
VUV Analytics
- New Tools for Qualitative and Quantitative GC Analysis using VUV Spectroscopy
Presenter:
Kevin Schug, Department of Chemistry and Biochemistry, University of Texas at
Arlington, Texas, USA
- More Selectivity for Complex Samples: Comprehensive Two-dimensional Gas
Chromatography – VUV Absorption Spectroscopy
Presenter:
Thomas Groger, Helmholtzentrum München, Oberschleiheim, Germany
45
Thursday, JUNE 02, 2016
Timing
Location
Vendor seminar by
10.45 – 11.45
Room 1000
THERMO SCIENTIFIC
Life in the Lab using Thermo Scientific Chromatography and Mass
Spectrometry.
- Challenges in Doping Control Analyses:
LC-Orbitrap for fast screening of peptides and small molecules
GC/C/IRMS measurements of endogenous anabolic steroid in urine
Presenter:
Alessandro Casilli, LBCD-LADETEC, Instituto de Química, Universidade Federal do
Rio de Janeiro, Brasil
- A Deeper Look into the Life of a Dioxins and POPs Lab
Presenter:
Dave Hope, Pacific Rim Laboratories
10:45 – 11:45
Room 300
BRECHBUEHLER
- Advances in automation using the PAL RTC
Presenters:
Philippe Mottay, Brechbuehler, Switzerland
Roger Simon, Brechbuehler, Switzerland
10:45 – 11:45
Room 100
JEOL
Introduction of the JEOL JMS-T200GC (AccuTofGCx) with the Photoionization
source, the ultimate tools for Comprehensive Two-dimensional GC (GC×GC)
and High-Resolution TOFMS.
Presenters: Professor Jean-Francois Focant and his science group from University of
Liege
Featuring :
- Introduction of the AccuTofGCx and its basic performance
- Separation without Fragmentation
- Photoionization as a Soft Ionization Source for Comprehensive Two-dimensional
GC (GCxGC) and High-Resolution TOFMS
- Application with Photoionization as a Soft Ionization Source
Presenters:
Chip Cody - JEOL USA
Junichi Osuga - JEOL Europe
Masaaki Ubukata - JEOL Japan
Bram van Meer - JEOL Europe
15:45 – 16:45
Room 1000
MERCK/SIGMA-ALDRICH/SUPELCO
- New developments in ionic liquid capillary GC column technology
Presenter:
Len Sidisky - Merck/Sigma-Aldrich/Supelco, Bellefonte, PA, USA
- New developments in sample preparation
Presenter:
Len Sidisky - Merck/Sigma-Aldrich/Supelco, Bellefonte, PA, USA
46
15:45 – 16:45
Room 300
RESTEK
- Optimize separation and reduce run times using a new FREE software tool in GC:
EZ-GC Method Translator. Learn how to get exact the same peak elution order when
changing carrier gas, column dimensions, moving from FID to MS or changing the
column flow
Presenter:
Jaap de Zeeuw, Restek Corporation
- Shoot and Dilute GC": Get more analysis and reduced maintenance by smart use of
split injection.
Presenter:
Jack Cochran, Restek Corporation
15:45 – 16:45
Room 100
CHROMALEONT
- Powerful supporting tools for a reliable identification of cumbersome samples
Presenter:
Margita Utczas, Chromaleont S.r.l., Messina, Italy
- Flow modulator: a new generation of GC×GC system with a comprehensive
software
Presenter:
Giorgia Purcaro, Chromaleont S.r.l., Messina, Italy
- Development of novel hyphenated techniques for characterization of complex
samples
Presenter:
Mariosimone Zoccali, Chromaleont S.r.l., Messina, Italy
47
48
-POSTER LIST-
49
50
_____________________________________________________________________________
A. FUNDAMENTALS
_____________________________________________________________________________
A.01
EFFECTS OF DYNAMIC MODIFICATION OF STATIONARY PHASES BY ANALYTES IN GAS
CHROMATOGRAPHY. PARTIAL SEPARATION OF ENANTIOMERS
Igor G. Zenkevich, Alexander A. Pavlovskii
Chemical - State University, Universitetskii prosp., 26, 198504 St. Petersburg, Russia (Russian Fed.)
A.02
EVALUATING SEPARATION PROPERITIES OF THERMAL GRADIENT GC
H. Dennis Tolley1, Luke T. Tolley2, Samuel E. Tolley2, Abhijit Ghosh2, Milton L. Lee2
Department of Statistics - Brigham Young University, 206 TMCB, 84602 Provo, UT, United States
Department of Chemistry, Brigham Young University, 84602 Provo, UT, United States
1
2
A.03
ANALYSIS OF LONGITUDINAL AND RADIAL HOMOGENEITY OF MONOLITHIC SILICA IN
CAPILLARIES BY VARIATION OF CAPILLARY INNER DIAMETER
Rafael Meinusch1, Kristof Hormann2, Ulrich Tallarek2, Bernd M. Smarsly1
1 Institute of Physical Chemistry - Justus-Liebig-University Giessen, Heinrich-Buff-Ring 17, 35392 Giessen,
Germany
2 Department of Chemistry - Philipps-University Marburg, Hans-Meerwein-Strasse, 35032 Marburg, Germany
A.04
PAPAIN-FUNCTIONALIZED GOLD NANOPARTICLES AS HETEROGENEOUS
BIOCATALYST IN BIOANALYSIS
Siyao Liu, Markus Höldrich, Michael Lämmerhofer
Pharmaceutical (Bio)Analysis - Institute of Pharmaceutical Sciences, University of Tuebingen, Auf der
Morgenstelle 8, 72076 Tübingen, Germany
A.05
STUDY OF THE SURFACE DIFFUSION CHARACTERISTICS OF HYPERCARB FOR POLAR
ANALYTES
Daniel Lunn, Young J. Yun, James W. Jorgenson
Department of Chemistry - UNC-Chapel HIll, 125 South Road, 27599 Chapel Hill, United States
A.06
ASSURING QUALITY IN THE ANALYTICAL LAB: CERTIFIED REFERENCE MATERIALS
FOR GAS CHROMATOGRAPHY
Frank Michel1, Christine Hellriegel2, Alexander Rueck2
1 R&D - Sigma-Aldrich/Supelco, Eschenstr. 5, 82024 Taufkirchen, Germany
2 Sigma-Aldrich Chemie GmbH, Industriestrasse 25, 9471 Buchs SG, Switzerland
_____________________________________________________________________________
B. COLUMN TECHNOLOGY
_____________________________________________________________________________
B.01
CONDENSATION AND CHAIN-GROWTH POLYMERIZED IONIC LIQUIDS AS HIGH
TEMPERATURE STABLE STATIONARY PHASE IN GAS CHROMATOGRAPHY
Kevin Roeleveld1, Frank David2, Frédéric Lynen1
1 Separation Science Group - Ghent University, Krijgslaan 281, 9000 Gent, Belgium
2 Research Institute for Chromatography, President Kennedypark 26, 8500 Kortrijk, Belgium
51
B.02
NEW DEFINITION FOR MAXIMUM ALLOWABLE OPERATING TEMPERATURE OF WAX GC
COLUMNS
John Oostdijk, Ngoc-A Dang
Agilent Crosslab R&D group - Chemical Applications - Agilent Technologies, Herculesweg 8, 4338 PL
Middelburg, Netherlands
B.03
IMPROVED INERTNESS IONIC LIQUID CAPILLARY COLUMNS
Len Sidisky, Gustavo Serrano, Greg A. Baney, James L. Desorcie, Xin Zheng, Michael D. Buchanan
Sigma Aldrich/ Supelco, 595 North Harrison Road, 16823 Bellefonte, United States
B.04
A SIMPLE AND CONVENIENT WAY TO PACK CAPILLARY LC COLUMNS
Hans-Jurgen Wirth1, Robert A. Shellie1,2, Harry Ritchie1, Mike Bailey1
1 Trajan Scientific and Medical, 7 Argent Place, 3134 Ringwood, Australia
2 ASTech - University of Tasmania, Private Bag 75, 7001 Hobart, Australia
B.05
CHARACTERISATION OF THREE NEW ETHYLVINYLBENZENE-DIVINYLBENZENE BASED
CAPILLARY COLUMNS EXHIBITING ION-EXCHANGE AND HYDROPHOBIC PROPERTIES
USING BIOGENIC NEUTRAL AND CHARGED SOLUTES
Yan Li1, Pavel N. Nesterenko1, Roger Stanley2, Brett Paull1, Mirek Macka3
School of Physical Sciences and Australian Centre for Research on Separation Science (ACROSS) - University
of Tasmania, Private Bag 75, 7001 Hobart, Australia
2 Centre for Food Innovation, University of Tasmania, Locked Bag 1370, 7052 Launceston, Australia
3 Chemistry - ACROSS - University of Tasmania (UTAS), Private Bag 75, 7001 Hobart, Australia
1
B.06
UNIQUE SELECTIVITY: THE POWER OF IONIC LIQUID CAPILLARY COLUMNS
Len Sidisky, Gustavo Serrano, James L. Desorcie, Greg A. Baney, Daniel L. Shollenberger, Katherine K.
Stenerson, Michael D. Buchanan
B.07
EVALUATION AND APPLICATIONS OF A HIGHLY INERT POLYETHYLENE GLYCOL BASED
CAPILLARY COLUMN TECHNOLOGY
Taylor Hayward1, Ronda Gras1, Gary Lee2, Allen Vickers2, Ngoc-A Dang2, Jim Luong1,3
1 Dow Chemical Canada ULC, PO Bag 16, Highway 15, T8L 2P4 Fort Saskatchewan, Canada
2 Agilent Technologies, 91 Blue Ravine Rd, 95630 Folsom, United States
3 Australian Centre for Research on Separation Science (ACROSS) - University of Tasmania, Private Bag 75,
7001 Hobart, Australia
_____________________________________________________________________________
C. SAMPLE PREPARATION
_____________________________________________________________________________
C.01
PREPARATION OF IMMOBILIZED ENZYME REACTOR USING A HYDROPHILIC,
MONOLITHIC BED AS A SUPPORT
Kinga Meller, Michal Szumski, Boguslaw Buszewski
Department of the Environmental Chemistry and Bioanalytics - Faculty of Chemistry, Nicolaus Copernicus
University in Torun, 7 Gagarin St., 87-100 Torun, Poland
52
C.02
APPLICATION OF HOLLOW FIBERS AS EFFECTIVE PHASES FOR FLOATING SAMPLING
TECHNOLOGY - THE ROLE ON THE SORPTION-DESORPTION STEPS
Alexandra M. Fernandes, Samir M. Ahmad, Nuno R. Neng, José M. Nogueira
Centro de Química e Bioquímica - Faculdade de Ciências da Universidade de Lisboa, Campo Grande Edifício
C8 piso 2 lab 8.2.48, 1749-016 Lisboa, Portugal
C.03
QUANTIFICATION OF PESTICIDES IN FOOD SAMPLES BY MEANS OF MINIATURIZED
QuEChERS APPROACH COUPLED TO FAST GC-QqQ MS
Antonino Schepis1, Mariosimone Zoccali2, Giorgia Purcaro2, Peter Q. Tranchida1, Luigi Mondello1,2
1 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - Università degli studi di Messina,
Viale Annunziata, 98168 Messina, Italy
2 Chromaleont S.r.L., viale Boccetta, 70, 98122 MESSINA, Italy
C.04
NEW GENERATION BAµE DEVICES FOR MICROEXTRACTION ANALYSIS
Alessandra H. Ide1,2, Samir M. Ahmad1, Nuno R. Neng1, José M. Nogueira1
1 Centro de Química e Bioquímica - Faculdade de Ciências da Universidade de Lisboa, Campo Grande, Ed C8,
1749-016 Lisboa, Portugal
2 CAPES Foundation - Ministry of Education of Brazil, SBN, Quadra 02, Lote 06, Bloco L, 70040-020 Brasília,
Brazil
C.05
BAR ADSORPTIVE MICROEXTRACTION (BAµE): AN OUTSTANDING ANALYTICAL TOOL
FOR TRACE ANALYSIS
Nuno R. Neng1, Alexandra M. Fernandes1, A.M. Segurado1, Alessandra H. Ide1,2, Samir H. Ahmad1, José M.
Nogueira1
1 Centro de Química e Bioquímica - Faculdade de Ciências, Universidade de Lisboa, Campo Grande ed. C8
lab.8.2.48, 1749-016 Lisbon, Portugal
2 CAPES Foundation - Ministry of Education of Brazil, SBN, Quadra 02, lote 06, Bloco L, 70040-020 Brasília DF, Brazil
C.06
"GREEN" EXTRACTION TECHNIQUE IN THE DETERMINATION OF PESTICIDES IN THE
AQUATIC ENVIRONMENT BY GC-MS
Agnesa Páleníková, Svetlana Hrouzková, Silvia Zichova
Department of Analytical Chemistry - Faculty of Chemical and Food Technology, STU Bratislava, Radlinského 9,
81237 Bratislava, Slovakia
C.07
DIRECT IMMERSION SOLID PHASE MICROEXTRACTION OF PESTICIDES FROM
SPAGHETTI SAUCE USING A NEW OVERCOATED FIBER
Len Sidisky1, Katherine K. Stenerson1, Robert E. Shirey1, Yong Chen1, Tyler Young2
1 Gas R&D - Sigma Aldrich/ Supelco, 595 North Harrison Road, 16823 Bellefonte, United States
2 R&D Intern - Sigma Aldrich/ Supelco, 595 North Harrison Road, 16823 Bellefonte, United States
C.08
AN IMPROVED SAMPLE CLEANUP APPROACH FOR THE GC/MS ANALYSIS OF PAHS IN
BUTTER
Olga Shimelis1, Katherine Stenerson1, Caitlin Brown2, Jennifer Claus1, Klaus Buckendahl3, Frank Michel3,
Anders Fridstrom4, Mike Buchanan1
Sigma-Aldrich/Supelco, 595 N. Harrison Rd., 16823 Bellefonte, United States
2 Pennsylvania State University, ., 16801 State College, United States
3 Sigma-Aldrich Chemie GmbH, Eschenstraße 5, 82024 Taufkirchen, Germany
4 Sigma-Aldrich International GmbH, Wassergasse 7, CH-9000 St. Gallen, Switzerland
1
53
C.09
EVALUATION OF MATRIX-COMPATIBLE SPME COATING AND ITS APPLICATION TO GCBASED FOOD ANALYSIS
Erica A. Souza-Silva1, Emanuela Gionfriddo2, Janusz Pawliszyn2
1 Instituto de Quimica - Universidade Federal do Rio Grande do Sul, Avenida Venancio Aires, 306 - ap 204,
90040-190 Porto Alegre, Brazil
2 University of Waterloo, 200 University Ave W, N2L 3G1 Waterloo, Canada
C.10
HOW DOES ETHANOL CONTENT DISTURB SPME ADSORPTION OF VOLATILE WINE
COMPOUNDS?
Erica A. Souza-Silva, Karine P. Nicolli, Janaina A. Barbara, Claudia A. Zini, Elina B. Caramão
Instituto de Quimica - Universidade Federal do Rio Grande do Sul, Avenida Venancio Aires, 306 - ap 204,
90040-190 Porto Alegre, Brazil
C.11
GC/MS/MS ANALYSIS OF PESTICIDE RESIDUES IN CANNABIS USING QUECHERS
EXTRACTION AND CLEANUP WITH AND IMPROVED SORBENT MIXTURE
Len Sidisky, Katherine K. Stenerson, Patrick Myers, Olga Shimelis, Michael Ye
C.12
BAµE - A NEW APPROACH FOR THE ANALYSIS OF PSYCHOACTIVE CATHINONES IN
ORAL FLUID
A.M. Segurado, Samir M. Ahmad, C.R. Queirós, Nuno R. Neng, H.M. Gaspar, Josè M. Nogueira
Centro de Química e Bioquímica - Faculdade de Ciências, Universidade de Lisboa, Campo Grande ed. C8
lab.8.2.48, 1749-016 Lisbon, Portugal
C.13
COMPARISON OF DIFFERENT SPME FIBER COATING MATERIALS AND FIBER
GEOMETRIES FOR THE ANALYSIS OF VOLATILE ORGANIC COMPOUNDS IN DRINKING
WATER ACCORDING DIN METHOD 38407-41
Peter Egli1, Beat Schilling1, Guenter Boehm2
1 BGB Analytik AG, Webereistrasse 56, 8134 Adliswil, Switzerland
2 CTC Analytics AG, Industriestrasse 20, 4222 Zwingen, Switzerland
C.14
FULLY AUTOMATED SAMPLE PREPARATION FOR THE DETERMINATION OF
PLASTICIZERS IN PVC FROM FOOD CONTACT MATERIALS AND TOYS
Maurus Biedermann1, Reto Bolliger2, Beat Schilling3, Guenter Boehm2
1 Official Food Control Authority - of the Canton of Zurich, Fehrenstrasse 15, 8032 Zurich, Switzerland
2 CTC Analytics AG, Industriestrasse 20, 4222 Zwingen, Switzerland
3 BGB Analytik AG, Webereistr. 56, 8134 Adliswil, Switzerland
C.15
REPLACING DISPERSIVE SPE WITH STANDARD SPE FOR QUECHERS BASED
AUTOMATED SAMPLE PREPARATION
Norbert Helle1, Franziska Chmelka1, Ilka Karrenbrock1, Jochen Vandenberg2, Andreas Hoffmann2,2
1 TeLA GmbH Bremerhaven, Handelspark 4-6, 27624 Geestland, Germany
2 Gerstel GmbH & Co.KG, Eberhard-Gerstel-Platz 1, 45473 Mülheim an der Ruhr, Germany
C.16
SAMPLE PREPARATION METHODS BASED ON MICROPOROUS ORGANIC POLYMERS
FOR TRACE ANALYSIS OF COMPLICATED SAMPLES
Gongke Li, Jialiang Pan, Chengjiang Zhang, Langjun Zhou, Yuling Hu, Zhuomin Zhang
School of Chemistry and Chemical Engineering - Sun Yat-sen University, 135 Xingang Xi Road, 510275
Guangzhou, China
54
C.17
DISPERSIVE SOLID PHASE EXTRACTION OF ESTROGENIC COMPOUNDS IN WATER BY
POLYDOPAMINE COATED MAGENTIC NANOPARTICLES AND LIQUID
CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY
Chiara Cavaliere, Giorgia La Barbera, Susy Piovesana, Salvatore Ventura, Riccardo Zenezini Chiozzi, Aldo
Laganà
Dipartimento di Chimica - Sapienza Università di Roma, Piazzale Aldo Moro 5, 185 Rome, Italy
C.18
PERFECT SAMPLE PREPARATION – IS COMPLETE HOLISTIC EXTRACTION OF
VOLATILE ORGANIC COMPOUNDS FROM FOODS POSSIBLE?
Lewis L. Jones1, Samuel Wordsworth2, Nathan Hawkins3, Kathy Ridgway3
1 Feeding Performance - Flavour Chemistry - Mars Petcare, Waltham Centre for Pet Nutrition, Freeby Lane,
LE14 4RT Waltham-on-the-Wolds, United Kingdom
2 The University of Nottingham, University Park, NG7 2RD Nottingham, United Kingdom
3 Anatune, Wellbrook Court, CB3 0NA Cambridge, United Kingdom
C.19
INVESTIGATION OF DIFFERENT CATION-EXCHANGE POLYMERS AS A NEW APPROACH
FOR THE DETERMINATION OF BASIC DRUGS IN URINE BY SOLID PHASE EXTRACTIONLIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY
Giacomo Musile1, Lucia Cenci2, Elena Piletska3, Rossella Gottardo1, Alessandra M. Bossi2, Federica Bortolotti1
1 Department of Diagnostics and Public Health - University of Verona, p.le L.A. Scuro, 10, 37134 Verona, Italy
2 Department of Biotechnology - University of Verona, strada le Grazie, 37134 Verona, Italy
3 Chemistry Department - Leicester University, University Road, LE1 7RH Leicester, United Kingdom
C.20
EFFICIENT MAGNETIC CARBON NANOTUBES METHOD FOR THE DETERMINATION OF
COCAINE AND BENZOYLECGONINE IN BREAST MILK BY GAS CHROMATOGRAPHY /
MASS SPECTROMETRY
Rosimeire R. Santos1, Helvecio C. Menezes1, Ana Paula C. Teixeira1, Maria J. Paiva2, Julio C. Veloso2, Zenilda
L. Cardeal1
1 Department of Chemistry - Universidade Federal de Minas Gerais, Av. Antonio Carlos, 6627, 31270901 Belo
Horizonte, Brazil
2 Universidade Federal de São João Del Rey, Av. Sebastião Gonçalves Coelho, 400, 35501-296 Divinopolis,
Brazil
C.21
DEVELOPMENT OF A DYNAMIC HEADSPACE TECHNOLOGY BASED VACUUM
EXTRACTION METHOD FOR IMPROVED GAS CHROMATOGRAPHIC ANALYSIS OF FOOD
AROMA COMPONENTS IN LIPOPHILIC MATRICES
Elvira Paulus1, Birgit Kohlenberg2, Eike Kleine-Benne3, Egon Gross2, Peter Schieberle1, Johannes Kiefl2
1 Lehrstuhl fuer Lebensmittelchemie - Technische Universitaet Muenchen, Lise-Meitner-Straße 34, 85354
Freising, Germany
2 R&T Flavors Division - Symrise AG, Muehlenfeldstrasse 1, 37603 Holzminden, Germany
3 Gerstel GmbH & Co.KG, Eberhard-Gerstel-Platz 1, D-45473 Muelheim an der Ruhr, Germany
C.22
OPTIMIZATION OF IN-PIPETTE SOLID-PHASE EXTRACTION FOR DETERMINATION OF
MINOR COMPONENTS IN VEGETABLE OILS BY GC×GC-FID/MS
Giorgia Purcaro1, Flavio A. Franchina1, Laura Barp2, Peter Q. Tranchida2, Luigi Mondello2,1
1 Chromaleont S.r.L., viale Boccetta 70, 98122 Messina, Italy
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, viale
C.23
GRAPHENE SHEETS SUPPORTED ON AMINOPROPYL SILICA AS SORBENT FOR
DETERMINATION OF PARABENS IN WATER SAMPLES BY MICROEXTRACTION BY
PACKED SORBENT
Bruno H. Fumes, Fernando M. Lanças
Institute of Chemistry of São Carlos - University of São Paulo, Av. Trab. São-Carlense, 400, 13566-590 São
Carlos, Brazil
55
C.24
GRAPHENE OXIDE SUPPORTED ON AMINOPROPYL SILICA AS SORBENT FOR IN-TUBE
SPME DETERMINATION OF TRIAZINES
Ana L. Toffoli, Bruno H. Fumes, Fernando M. Lancas
Institute of Chemistry of São Carlos - University of São Paulo, Av. Trab. São-Carlense, 400, 13566-590 São
Carlos, Brazil
C.25
DEVELOPMENT OF A RAPID MINIATURIZED DISPERSIVE LIQUID/LIQUID
MICROEXTRACTION METHOD (DLLME) FOR THE DETERMINATION OF THC-COOH IN
BIOLOGICAL FLUIDS BY GC-MS
Sara Odoardi, Valeria Valentini, Sabina Strano-Rossi
Institute of Public Health, Sction of Legal Medicine - Catholic University of Sacred Heart, L.go F. Vito, 1, 00168
Rome, Italy
C.26
SUB-PART PER TRILLION HEADSPACE ANALYSIS OF ODOR PRODUCING
HALOANISOLES, GEOSMIN, AND 2-METHYLISOBORNEOL IN WATER AND WINE BY
GCMS WITHOUT THE NEED TO CONTACT THE LIQUID SAMPLE
Daniel B. Cardin, Thomas X. Robinson
Analytical Instrumentation - Entech Instruments, Inc., 2207 Agate Ct., 93065 Simi Valley, United States
_____________________________________________________________________________
D. SAMPLING SYSTEMS
_____________________________________________________________________________
D.01
AUTOMATED CONSECUTIVE GAS SAMPLE TRANSFER SYSTEM FROM POLYMER BAGS
AND HIGHLY PRESSURIZED CYLINDERS TO A GAS CHROMATOGRAPH
Namgoo Kang
Center for Gas Analysis - Korea Research Institute of Standards and Science, 267 Gajeong-ro, Yuseong-gu,
34113 Daejeon, Korea, (South) Republic of
D.02
USING TDU-GC-MS TO INVESTIGATE THE VOCS EMISSION OF BRASSICA NAPUS L .
PLANTLETS CULTIVATED IN VITRO AND EXPOSED TO CADMIUM ABIOTIC STRESS
Bastien Durenne1, Alodie Blondel1, Philippe Druart1, Marie-Laure Fauconnier2
1 Department of Life Sciences, Bioengineering unit - CRA-W, Chaussée de Charleroi 234, 5030 Gembloux,
Belgium
2 Chimie Générale Organique - Université de Liège - Gembloux Agro-Bio Tech, 2, Passage des Déportés, 5030
Gembloux, Belgium
D.03
EVALUATION OF VARIOUS COATING MATERIALS FOR SPME AND THE NOVEL SPME
ARROW FOR THE EXTRACTION OF 1,1,6-TRIMETHYL-1,2-DIHYDRONAPHTHALENE AND
VITISPIRANE IN WINE USING MULTIPLE HEADSPACE SOLID PHASE MICROEXTRACTION
Michael Ziegler1, Hans-Georg Schmarr1,2
1 Institute for Wine Research - DLR Rheinpfalz, Breitenweg 71, 67435 Neustadt a.d. Weinstraße, Germany
2 Instrumental Analytical Chemistry - University Duisburg-Essen, Universitätsstraße 5, 45141 Essen, Germany
D.04
DEVELOPMENT OF NOVEL SAMPLING SYSTEM FOR METABOLOMIC PROFILING OF
HUMAN BREATH
Mari Päiviö, Hanna-Mari Salmia, Tuulia Hyötyläinen
Turku Centre for Biotechnology - University of Turku, Tykistökatu 6 A, 20520 Turku, Finland
56
D.05
XAD-2 AS ALTERNATIVE ADSORBENT FOR THE ANALYSIS OF VOCs BY GC/MS AFTER
THERMODESORPTION
Andrea C. Marcillo1, Anja Widdig2, Claudia Birkemeyer1
1 Mass Spectrometry Group, Institute of Analytical Chemistry, Faculty of Chemistry and Mineralogy - University of
Leipzig, Linnestr. 3, 04103 Leipzig, Germany
2 Institute of Biology, Faculty of Bioscience, Pharmacy and Psychology - University of Leipzig, Talstrasse 3,
D-04103 Leipzig, Germany
D.06
USE OF AN “INTELLIGENT KNIFE” (IKNIFE), BASED ON THE RAPID EVAPORATIVE
IONISATION MASS SPECTROMETRY TECHNOLOGY, FOR AUTHENTICITY ASSESSMENT
OF PISTACHIO SAMPLES
Francesca Rigano1, Sara Stead2, Renata Jandova2, Davy Petit3, Sara Farnetti4, Nino Marino5, Luigi Mondello6,1
1 Chromaleont SrL, Viale Boccetta 70, 98122 Messina, Italy
2 Waters Corporation, Stamford Avenue, Altrincham Road, SK9 4AX Wilmslow, United Kingdom
3 Waters Corporation, Waters S.A.S., BP 608, 78056 Saint-Quentin En Yvelines Cedex, France
4 Diabetes Research Institute, Division of Cellular Transplantation of Surgery - University of Miami, 1450 NW
10th Avenue, 33136 Miami, United States
5 Pistì – Antichi Sapori dell’Etna S.r.L, Viale J. F. Kennedy / Zona artigianale 12-13, 95034 Bronte (CT), Italy
6 Dipatimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina - Polo
Annunziata, Viale Annunziata, 98168 Messina, Italy
_____________________________________________________________________________
E. CAPILLARY GAS CHROMATOGRAPHY
_____________________________________________________________________________
E.01
ANALYSIS OF CHLORINATED, SULFOCHLORINATED DERIVATIVES OF LAURATE
METHYL ESTER BY ELECTRON IONIZATION
Amel Asselah1,2, Ammal Tazerouti2
Département du Génie de l'Environnment, Faculté des Sciences de l'Ingénieur-FSI - Université de M'Hamed
Bougara-UMBB, Avenue de l'indépendance, 35000 Boumerdes, Algeria
2 Laboratoire de Chimie Organique Appliquée- Faculté de Chimie - Université des Sciences et de la TechnologieUSTHB, BP32, Cité El Alia, 16000 Bab Ezzouar, Algeria
1
E.02
HUMAN BLOOD VS. ANIMAL BLOOD – PROFILING THE SCENT OF TRAINING AIDS FOR
BLOOD-DETECTION DOGS
Latara Rust, Miroslava Ross, Katie D. Nizio, Shari L. Forbes
Centre for Forensic Science - University of Technology Sydney, PO Box 123, 2007 Sydney, Australia
E.03
GAS CHROMATOGRAPHIC CHARACTERIZATION OF MONO-ESTERS OF DICARBOXYLIC
ACIDS
Igor G. Zenkevich, Lilia N. Fakhretdinova
Chemical - State University, Universitetskii prosp., 26, 198504 St. Petersburg, Russia (Russian Fed.)
E.04
GC FLOW PATH INERTNESS ENSURING RELIABLE RESULTS
Laura Provoost1, Yun Zou2
1 Agilent Crosslab Group - Agilent Technologies, Herculesweg 8, 4338 PL Middelburg, Netherlands
2 Agilent Crosslab Group - Agilent Technologies, 412 Ying Lun Road, 200131 Shanghai, China
57
E.05
VUV SPECTRA DATABASE OF FATTY ACIDS DERIVATIZED COUPLED WITH LINEAR
RETENTION INDEX APPROACH: RELIABLE IDENTIFICATION TOOL FOR COMPLEX
SAMPLES
Mariosimone Zoccali1, Margita Utczas1, Giorgia Purcaro1, Luigi Mondello1,2
1 Chromaleont S.r.L., Viale Boccetta 70, 98122 Messina, Italy
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, Viale
E.06
NEW CROSS-LINKED STATIONARY PHASES FOR GC BASED ON POLY(OLIGO
ETHYLENGLYCOL DIACRYLATE): KINETIC PERFORMANCE AND THERMODYNAMIC
SELECTIVITY
Alexander Kurganov, Alexander Korolev, Anastasiya Kanateva, Tamara Popova, Valeriya Shiryaeva
Institute of Petrochemical Synthesis - Academy of Sciences, Lenin Avenue 29, 119991 Moscow, Russia (Russian
Fed.)
E.07
AGILENT J&W DB-WAX ULTRA INERT GC COLUMN, A NEW PEG GC COLUMN WITH
IMPROVED INERTNESS RELIABILITY AND COLUMN LIFETIME
Ngoc-A T. Dang1, Roy Lensen1, Frans Biermans1, Allen K. Vickers2, Liying Yu2
1 R&D - Agilent Technologies, Herculesweg 8, 4338 PL Middelburg, Netherlands
2 Supply Chain Folsom - Agilent Technologies, Blue Ravine Rd 91, 95630 CA Folsom, United States
E.08
THE QUANTITATIVE MEASUREMENT OF WATER BY GC USING IONIC LIQUID CAPILLARY
COLUMNS
Len Sidisky, Gustavo Serrano, James L. Desorcie, Greg A. Baney, Katherine K. Stenerson, Michael Halpenny,
Michael D. Buchanan
E.09
ANALYSIS OF BIOMARKERS IN CRUDE OILS FROM COLOMBIA´S EASTERN PLAINS AND
MIDDLE MAGDALENA VALLEY BASINS BY GC-QQQ-MS
Andrés F. González1,2, Taylor S. Motta1,2, Ivama S. Calles1,2, Jairo R. Martínez1,2, Elena E. Stashenko1,2
1 Department of Chemistry - Universidad Industrial de Santander, Carrera 27 calle 9 UIS, 680002 Bucaramanga,
Colombia
2 Centro de Investigación en Biomoléculas-CIBIMOL - Centro de Investigación de Excelencia CENIVAM, Carrera
27 calle 9 UIS Ed-45, 680002 Bucaramanga, Colombia
E.10
NEW HIGH TEMPERATURE PEG GC COLUMN WITH ULTRA-LOW BLEED LEVEL
Ngoc-A Dang, John Oostdijk, Frans Biermans
R&D - Agilent Technologies, Herculesweg 8, 4338 PL Middelburg, Netherlands
E.11
THE QUANTIFICATION OF TRACE WATER IN PETROLEUM AND PETROLEUM PRODUCTS
Lillian A. Frink, Daniel W. Armstrong
Department of Chemistry and Biochemistry - University of Texas at Arlington, Arlington, 76019 Arlington, United
States
E.12
REDUCE ANALYSIS TIME AND OPTIMIZE SEPARATIONS, WHILE MAINTAINING THE
SAME PEAK ELUTION ORDER: A NEW FREE SOFTWARE TOOL IN GC: EZ-GC METHOD
TRANSLATOR
Jaap de Zeeuw
New products group - Restek Corp., weerhaan 9, 4336 KT 4336 KT Middelburg, Netherlands
58
E.13
WHY DON’T MORE PEOPLE USE GUARD COLUMNS IN CAPILLARY GAS
CHROMATOGRAPHY? AN INVESTIGATION INTO THE ADVANTAGES AND
DISADVANTAGES OF AVAILABLE TECHNIQUES
Remko van Loon, Matthew Giardina
Gas Phase Separations Division - Agilent Technologies, Herculesweg 8, 4338 PL Middelburg, Netherlands
E.14
ANALYSIS OF 1,4-DIOXANE, DIOXANES AND DIOXOLANES IN WATER BY SOLID PHASE
EXTRACTION AND GAS CROMATOGRAPHY TANDEM MASS SPECTROMETRY (GC-MS/
MS)
Guillem Carrera Ruiz, Lida Vegué Garrich, Rosa Boleda Vall-Llobera
Department of Organic Chemistry - Aigües de Barcelona, Empresa Metropolitana de Gestió del Cicle Integral de
l'Aigua S.A., General Batet 1-7, 08028 Barcelona, Spain
E.15
STUDY OF A NEW CHIRAL BIOACTIVE AND CHOLESTERIC GC COLUMN
Ouassila Ferroukhi
LABORATOIRE DE CHROMATOGRAPHIE - FACULTE DE CHIMIE USTHB, BP32 ELAALIA, BEZ, ALGER,
16017 ALGER, Algeria
E.16
INFLUENCE OF DIFFERENT ARYL GROUPS ON THE SELECTIVITY OF POLYSILOXANES
IN GAS CHROMATOGRAPHY
Helmut Riering, Natalie Bilmann, Giovanna Cozzupoli, Astrid Wirtz
GC - Macherey-Nagel GmbH & Co. KG, Neumann-Neander-Str. 6-8, D-52355 Düren, Germany
E.17
NON-MS SIDA QUANTIFICATION OF LOW MOLECULAR WEIGHT SULFUR VOLATILES
AFTER HS-SPME-GC-PFPD ANALYSIS
Sylvia K. Neef, Sebastian Ullrich, Hans-Georg Schmarr
Viticulture and Enology - DLR Rheinpfalz, Breitenweg 71, 67431 Neustadt an der Weinstrasse, Germany
E.18
NOVEL MID-POLARITY CYANOPROPYL PHASES WITH SILARYLENE TECHNOLOGY FOR
LOWEST BLEED CAPILLARY GC COLUMNS
Stefan Hilken, Tanja Harst, Tobias Schäpers, Helmut Riering, Martin Rödel, Andreas Bohne, Dirk Rieger
MACHEREY-NAGEL Gmbh & Co. KG, Neumann-Neander-Str. 6-8, 52355 Dueren, Germany
E.19
RAPID ANALYSIS OF 32 VOLATILE SULFUR COMPOUNDS (VSCs) IN WINE BY HEADSPACE SOLID PHASE MICROEXTRACTION GAS CHROMATOGRAPHY TANDEM MASS
SPECTROMETRY (HS-SPME-GC-MS/MS)
Davide Slaghenaufi, Sergio Moser, Loris Tonidandel, Roberto Larcher
CTT - Fondazione Edmund Mach, via E. Mach, 1, 38010 San Michele all'Adige, Italy
E.20
THE CRITICAL ASSESSMENT OF GC-HRMS BASED METHODS FOR WHISKY
AUTHENTICATION
Michal Stupak1, Monika Tomaniova1, Ian Goodall2, Jana Hajslova1
1 Food Analysis and Nutrition - UCT, Technicka 3, 166 28 Prague 6, Czech Republic
2 The Scotch Whisky Research Institute, Research Avenue North, EH14 4AP Edinburgh, United Kingdom
E.21
CHROMATOGRAPHIC EVALUATION OF THERMODYNAMIC AND KINETIC PROPERTIES
OF NEW MEMBRANE POLYMERS WITH INTRINSIC POROSITY AS STATIONARY PHASES
IN GC
Alexander Kurganov, Anastasiya Kanateva, Alexander Korolev, Elena Yakubenko, Maxim Bermeshev, Pavel
Chapala
Institute of Petrochemical Synthesis - Academy of Sciences, Lenin Avenue 29, 119991 Moscow, Russia (Russian
Fed.)
59
E.22
GAS CHOROMATOGRAPHY-VACUUM ULTRAVIOLET ABSORBANCE SPECTROSCOPY
FOR QUANTITATION OF TRACE AND BULK WATER IN ORGANIC SOLVENTS: AN
EMERGING ALTERNATIVE TO KARL FISCHER TITRATION
Lindsey Shear1, Dale Harrison1, Jonathan Smuts1, Len Sidisky2
1 VUV Analytics, 715 Discovery Blvd., 78613 Cedar Park, United States
2 Supelco, 595 North Harrison Road, 16823 Bellefonte, United States
E.23
ISOTOPIC SEPARATION ON A PLOT COLUMN ALLOWS A NON-MS STABLE ISOTOPE
DILUTION ASSAY FOR ACETALDEHYDE ANALYSIS USING HS-GC-FID
Hans-Georg Schmarr
E.24
QUANTIFYING OF THE DELTA-9-TETRAHYDROCANNABINOL IN UNCONVENTIONAL
MATRIXES
Ludmila Komorousova, Michael Roman, Lukas Franek
Department of Chemistry - Institute of Criminalistics Prague, P.O.Box 62/KUP, Strojnicka 27, 17089 Prague 7,
Czech Republic
E.25
FAST PESTICIDE ANALYSIS IN FOOD USING FLOW FIELD THERMAL GRADIENT GAS
CHROMATOGRAPHY AND TOF-MS WITH SOFT ELECTRON IONIZATION
Jan Leppert1, Kai Schütt1, Gerhard Horner2, Peter Boeker1
1 Institute of Agricultural Engineering - University of Bonn, Nussallee 5, 53115 Bonn, Germany
2 five technologies GmbH, Frauenstraße 22, 80469 München, Germany
E.26
VALIDATION OF THE METHOD CAPILARY GAS CHROMATOGRAPHY (GC-FID) FOR THE
QUANTITATIVE DETERMINATION OF SYNTHETIC CANNABINOIDS IN FORENSIC
PRACTICE
Ivo Beroun
Depatment of Chemistry - Institute of Criminalistics Prague, Strojnická 27, P.O.Box 62/KÚP, 170 89 Prague,
Czech Republic
E.27
DECONVOLUTION AND IDENTIFICATION OF COELUTING ISOMERS OF
DIMETHYLNAPHTHALENE USING GAS CHROMATOGRAPHY - VACUUM ULTRAVIOLET
SPECTROSCOPY
Kevin A. Schug1, Jamie Schenk1, Xiaojian Mao1, Jonathan Smuts2, Phillip Walsh2, Peter Kroll1
1 Chemistry and Biochemistry - University of Texas at Arlington, 700 Planetarium PI., Box 19065, TX 76019-0065
2 VUV Analytics, Inc., 715 Discovery Blvd Suite 502, 78613 Cedar Park, United States
_____________________________________________________________________________
F. (MICRO)LIQUID CHROMATOGRAPHY
_____________________________________________________________________________
F.01
DIRECT-EI LC-MS: A NEW CONFIGURATION TO ENHANCE PERFORMANCE AND
STABILITY
Maurizio Piergiovanni, Giorgio Famiglini, Pierangela Palma, Veronica Termopoli, Achille Cappiello
DiSPeA - University of Urbino, Piazza Rinascimento 6, 61029 Urbino, Italy
60
F.02
DETERMINATION OF ANTI-TB DRUGS IN BIOLOGICAL FLUIDS BY LIQUID
CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY (LC/MS/MS) FOR OPTIMIZATION
TUBERCULOSIS TREATMENT
Liudmila A. Kartsova, Elena A. Bessonova, Svetlana A. Soloveva
Institute of Chemistry - Saint-Petersburg St. Univ., Universitetskii pr. 26, Peterhof, 198504 Saint-Petersburg,
Russia (Russian Fed.)
F.03
DEVELOPMENT OF HPLC AND MEKC METHODS FOR THE ANALYSIS OF SULFUR
MUSTARD CYCLIC DEGRADATION PRODUCTS
Heidi Lees, Mihkel Kaljurand, Merike Vaher
Institute of Chemistry - Tallinn University of Technology, Akadeemia tee 15, 12618 Tallinn, Estonia
F.04
CHARACTERIZATION OF FREE FATTY ACID PROFILE IN MUSSELS BY NANOLC
DIRECTLY COUPLED TO ELECTRON IONIZATION MASS SPECTROMETRY
Francesca Rigano1, Ambrogina Albergamo2, Danilo Sciarrone2, Marco Beccaria1, Giorgia Purcaro1, Luigi
Mondello2,1
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina - Polo
F.05
NANOLC-EI-MS FOR A RELIABLE CHARACTERIZATION OF POLYMETOXYFLAVONES
ISOLATED FROM COLD-PRESSED MANDARIN ESSENTIAL OIL BY MEANS OF A
MULTIDIMENSIONAL PREPARATIVE HPLC SYSTEM
Marina Russo1,2, Francesca Rigano3, Adriana Arigò2, Danilo Sciarrone2, Maria L. Calabrò2, Paola Dugo2,3, Luigi
Mondello2,3
1 Unit of Food Science and Nutrition, Department of Medicine - University Campus Bio-Medico of Rome, Via
Alvaro del Portillo 21, 00128 Rome, Italy
F.06
LIPIDOMICS-TYPE ANALYSIS BY UHPLC-Q-MS WITH ESI AND APCI INTERFACES
Marco Beccaria1, Veronica Inferrera2, Francesca Rigano1, Giorgia Purcaro1, Paola Dugo2,1, Luigi Mondello2,1
1 Chromaleont s.r.l., viale Boccetta, 70, 98122 Messina, Italy
F.07
BUILDING OF A LINEAR RETENTION INDEX SYSTEM IN LIQUID CHROMATOGRAPHY
Francesca Rigano1, Danilo Sciarrone2, Luigi Mondello2,1
_____________________________________________________________________________
G. SUPERCRITICAL FLUID CHROMATOGRAPHY AND EXTRACTION
_____________________________________________________________________________
G.01
SFC-MS METHOD SCOUTING FOR NOVEL CHIRAL COMPOUNDS
Gesa Schad
Shimadzu Europa GmbH, Albert-Hahn-Str. 6-11, 47269 Duisburg, Germany
61
G.02
REALISING THE BENEFITS OF CONVERGENCE CHROMATOGRAPHY IN FOOD TESTING
Eimear McCall, Ramesh Rao, Jinchuan Yang
Food and Environmental - Waters, Stamford Avenue, SK9 4AX Wilmslow, United Kingdom
G.03
"IMPACT OF CONVERGENCE CHROMATOGRAPHY COUPLED TO TIME-OF-FLIGHT MASS
SPECTROMETRY ON LIPID ANALYSIS: APPLICATIONS TO TRIACYLGLYCEROL
FINGERPRINTING IN EDIBLE OILS"
Veronica Inferrera1, Paola Donato2, Francesco Cacciola2, Paola Dugo1,3, Luigi Mondello1,3
Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, Viale
2 Dipartimento di Scienze Biomediche, Odontoiatriche e delle Immagini Morfologiche e Funzionali - University of
Messina, Viale Consolare Valeria, 98165 Messina, Italy
3 Chromaleont S.r.L., Viale Boccetta, 70, 98122 Messina, Italy
1
G.04
ON-LINE COUPLING OF CO2 SUPERCRITICAL FLUID EXTRACTION AND SUPERCRITICAL
FLUID CHROMATOGRAPHY COUPLED TO TRIPLE QUADRUPOLE MASS
SPECTROMETRY
Mariosimone Zoccali1, Giorgia Purcaro1, Masayuki Nishimura2, Luigi Mondello1,3
2 Shimadzu Scientific Instruments, Inc., Riverwood Drive, 21046 Columbia, United States
G.05
SUPERCRITICAL FLUID CHROMATOGRAPHY (SFC) AS ORTHOGONAL TECHNIQUE FOR
IMPROVED DETECTION OF POLAR ANALYTES IN ANTI-DOPING CONTROL
Marica Barbieri1, Maria K. Parr2, Bernhard Wüst3, Edgar Nägele3, Francesco Botre4
1 Agilent Technologies - , Via Vincenzo Lamaro 13, 00173 Roma, Italy
2 Institut of Pharmacy - Freie Universität Berlin, Kaiserswerther Str. 16-18, 14195 Berlin, Germany
3 Agilent Technologies, Hewlett-Packard-Straße 8, 76337 Waldbronn, Germany
4 Laboratorio Antidoping FMSI, Largo Giulio Onesti, 1, 00197 Rome, Italy
_____________________________________________________________________________
H. ELECTROMIGRATION METHODS
_____________________________________________________________________________
H.01
DISTRIBUTION CONSTANTS OF LOCAL ANESTHETICS BETWEEN AQUEOUS AND
LIPOSOME PHASES
Suvi-Katriina Ruokonen1, Filip Dusa1, Paula Holma1, Alexandra Robciuc2, Antti H. Rantamäki1, Juha
Holopainen2, Susanne K. Wiedmer1
1 Department of Chemistry - University of Helsinki, A.I. Virtasen aukio 1, 00014 Helsinki, Finland
2 Department of Ophthalmology - University of Helsinki and Helsinki University Hospital, Haartmanninkatu 4,
H.02
NEW APPROACHES FOR ELECTROPHORETIC DETERMINATION OF BIOLOGICALLY
ACTIVE COMPOUNDS
Elena A. Bessonova, Liudmila A. Kartsova, Valeria F. Gallyamova, Andrey V. Nikolaev, Ekaterina V. Obedkova
Department of Chemistry - Saint-Petersburg St. Univ., Universitetskii pr. 26, Peterhof, 198504 Saint-Petersburg,
Russia (Russian Fed.)
62
H.03
INTERACTION OF GLAUCOMA DRUGS WITH BIOMIMETIC MEMBRANES USING
LIPOSOME ELECTROKINETIC CHROMATOGRAPHY
Antti H. Rantamäki1, Suvi-Katriina Ruokonen1, Joanna Witos1, Alexandra Robciuc2, Juha M. Holopainen2,
Susanne K. Wiedmer1
1 Department of Chemistry - University of Helsinki, A.I. Virtasen Aukio 1, 00014 Helsinki, Finland
2 Helsinki Eye Lab, Department of Ophthalmology - University of Helsinki and Helsinki University Hospital,
Haartmaninkatu 4C, 00290 Helsinki, Finland
H.04
APPLICATION OF OLIGOSACCHARIDE-CROWNED HYPERBRANCHED POLY(ETHYLENE
IMINE)S AS CHIRAL SELECTORS IN HIGH PERFORMANCE LIQUID CHROMATOGRAPHY
(HPTLC) AND AS COATING MATERIALS IN CAPILLARY ELECTROPHORESIS (CE)
Daria V. Dzema, Liudmila A. Kartsova, Diana A. Kapizova
Department of Chemistry - Saint-Petersburg State University, Universitetskii pr. 26, Peterhof, 198504 SaintPetersburg, Russia (Russian Fed.)
H.05
IONIC LIQUIDS BASED ON IMIDAZOLIUM ARE MODIFIERS OF ELECTROPHORETIC
SYSTEMS AND EXTRACTANTS AT DETERMINATION OF AMINO ACIDS AND STEROID
HORMONES IN URINE
Ekaterina A. Kolobova, Liudmila A. Kartsova, Elena A. Bessonova
Institute of Chemistry - Saint-Petersburg State University, Petrodvorets, Universitetskii pr. 26, 198504 SaintPetersburg, Russia (Russian Fed.)
H.06
NEW METHODOLOGY FOR CAPILLARY ELECTROPHORESIS WITH ESI-MS
DETECTION: ELECTROPHORETIC FOCUSING ON INVERSE ELECTROMIGRATION
DISPERSION GRADIENT FOR HIGH SENSITIVITY ANALYSIS OF SULFONAMIDES IN
WATERS
Zdena Malá, Petr Gebauer, Petr Bocek
Institute of Analytical Chemistry of the CAS, v. v. i., Veveri 97, 60200 Brno, Czech Republic
H.07
MONITORING BIOMASS DEGRADATION, ISOMERIZATION OF GLUCOSE TO FRUCTOSE
AND CONVERSION TO 5-HMF IN IONIC LIQUIDS BY CE
Tiina Aid, Margus Lopp, Merike Vaher
H.08
COMPARISON OF LIPOSOME- AND OCTANOL-WATER DISTRIBUTION CONSTANTS OF
ANTIOXIDANTS
Jana Vanova1,2, Petr Cesla1, Susanne K. Wiedmer2
1 Department of Analytical Chemistry - Faculty of Chemical Technology, University of Pardubice, Studentská 573,
532 10 Pardubice, Czech Republic
2 Department of Chemistry - University of Helsinki, POB 55, 00014 University of Helsinki Helsinki, Finland
H.09
RAPID CAPILLARY ELECTROPHORESIS METHOD WITH LED-INDUCED NATIVE
FLUORESCENCE DETECTION FOR THE ANALYSIS OF AMPHETAMINE AND COCAINE
DERIVATIVES IN ORAL FLUID
Anastassia Tretjakova, Jekaterina Mazina, Merike Vaher, Maria Kulp
Institute of Chemistry - Tallinn University of Technology, Ehitajate tee 5, 12816 Tallinn, Estonia
H.10
VARIOUS CAPILLARY COATINGS IN CAPILLARY ELECTROPHORESIS-BASED
ENZYMATIC ASSAY OF CHLOROPHYLLASE
Pawel M. Nowak1, Michal Wozniakiewicz1, Maciej Michalik2, Leszek Fiedor2, Pawel Koscielniak1
1 Department of Analytical Chemistry, Faculty of Chemistry - Jagiellonian University in Kraków, ul. Ingardena 3,
30-060 Kraków, Poland
2 Department of Plant Physiology and Biochemistry, Faculty of Biochemistry, Biophysics and Biotechnology Jagiellonian University in Kraków, ul. Gronostajowa 7, 30-387 Kraków, Poland
63
H.11
DIBLOCK COPOLYMERS STUDIED BY CAPILLARY ELECTROPHORESIS AND
ASYMMETRICAL FLOW FIELD FLOW FRACTIONATION
Joanna Witos, Erno Karjalainen, Heikki Tenhu, Susanne K. Wiedmer
Department of Chemistry - University of Helsinki, A.I. Virtasen Aukio 1, 00014 Helsinki, Finland
H.12
SYSTEMATIC OVERVIEW OF UV LIGHT-MEDIATED SYNTHESIS LUMINESCENT AQUEOUS
QUANTUM DOTS CHARACTERIZED BY CE-LEDIF
Lukas Nejdl1,2, Pavel Kopel1,2, Marketa Vaculovicova1,2, Vojtech Adam1,2
Department of Chemistry and Biochemistry - Mendel University in Brno, Zemendelska 1, 61300 Brno, Czech
Republic
2 Central European Institute of Technology - Brno University of Technology, Purkynova 123, 61200 Brno, Czech
Republic
1
_____________________________________________________________________________
I. INSTRUMENTATION AND AUTOMATION
_____________________________________________________________________________
I.01
OPEN PROBE FAST GC-MS - REAL TIME ANALYSIS WITH SEPARATION
Alexander B. Fialkov, Uri Keshet, Tal Alon, Aviv Amirav
Chemistry - Tel Aviv University, Ramat Aviv, 69978 Tel Aviv, Israel
I.02
WARPING-BASED STRATEGY FOR THE SYSTEMATIC DETERMINATION OF
DISCRIMINATIVE FEATURES IN GC-MS DATA
Clement Truan1,2, Said Abouelkaram2, Nathalie Kondjoyan2, Jérémy Ratel2, Christophe Peres3, Erwan Engel2
1 ANALYTISS, 89 rue des poissonniers, 75018 PARIS, France
2 INRA - UR370 Qualité des Produits Animaux, theix, 63122 saint genes champanelle, France
3 Laboratoire Parfums - CHANEL, 135 avenue Charles de Gaulle, 92200 Neuilly sur seine, France
I.03
AUTOMATED MICRO SOLID PHASE CLEAN-UP OF QUECHERS EXTRACTS FOR
PESTICIDE ANALYSIS
Hans-Joachim Huebschmann1, Guenter Boehm1, Reto Bolliger1, Mark Hayward2
1 APAC - CTC Analytics AG, Industriestrasse 20, 4222 Zwingen, Switzerland
2 ITSP Solutions Inc., Northlake Drive, 212 Hartwell, United States
I.04
CHEMSNIFF – A PORTABLE DIGITAL MS-BASED SNIFFER INSTRUMENT
Sjaak de Koning1, Edwin Beekwilder1, Boris Brkic2, Sarfaraz Syed3
1 Da Vinci Laboratory Solutions, Cairostraat 10, 3047BC Rotterdam, Netherlands
2 Q-Technologies, Brownlow Hill, L69 3GJ Liverpool, United Kingdom
3 Amsterdam Scientific Instruments, Science Park 105, 1098XG Amsterdam, Netherlands
I.05
SEGMENTED TOTAL ION SPECTRA (STIS): A PRE-PROCESSING STEP FOR GC-MS DATA
FOR CHEMOMETRIC ANALYSIS OF ARSON DATA
Lawrence A. Adutwum, James J. Harynuk
Chemistry - University of Alberta, 11227 Saskatchewan Drive, T6G2G2 Edmonton, AB, Canada
64
I.06
255 nm AND 280 nm UV-LED BASED PHOTOMETRIC DETECTION INTEGRATED WITH ZCELL FOR CAPILLARY LC
Yan Li1, Pavel N. Nesterenko1, Roger Stanley2, Brett Paull1, Mirek Macka3
School of Physical Sciences and Australian Centre for Research on Separation Science (ACROSS) - University
of Tasmania, Private Bag 75, 7001 Hobart, Australia
2 Centre for Forensic Science - University of Tasmania, Locked Bag 1370, 7052 Launceston, Australia
3 Chemistry - ACROSS - University of Tasmania (UTAS), Private Bag 75, 7001 Hobart, Australia
1
I.07
THE USAGE OF A DIRECT INLET PROBE IN COMBINATION WITH HIGH RESOLUTION
MASS SPECTROMETRY FOR THE FAST ANALYSIS OF SOLID AND LIQUID SAMPLES
Juergen Wendt
Leco EATC, Berlin, D-10589 Berlin, Germany
I.08
DETERMINATION OF THE FAT CONTENT PROFILE OF DIFFERENT CHOCOLATE
PRODUCTS USING AN AUTOMATED WORKFLOW FOR THE GENERATION OF FATTY
ACID METHYL ESTERS (FAME)
Guenter Boehm, Reto Bolliger, Hans-Joachim Huebschmann
CTC Analytics AG, Industriestrasse 20, 4222 Zwingen, Switzerland
I.09
RAPID PORTABLE GC-MS ANALYSIS FOR ON-SITE SCREENING OF PHYTOCHEMICAL
LEAF OILS IN AN AUSTRALIAN NATIVE BOTANIC GARDEN
Yong Foo Wong1, Dandan Yan2,3, Humberto Bizzo4, Philip J. Marriott1
1 Monash University, Wellington Rd, 3800 Clayton, Australia
2 School of Physical Sciences - University of Tasmania, Sandy Point Road, 7001 Hobart, Australia
3 School of Chemistry - Monash University, Wellington Road, 3800 Clayton, Australia
4 Embrapa, Av. das Américas, 29501, 23020-470 Rio de Janeiro, Brazil
I.10
A SIMPLE AND FLEXIBLE METHANIZER SOLUTION FOR LOW LEVEL CO/CO2 GAS
ANALYSIS BY GAS CHROMATOGRAPHY
Jaap de Zeeuw
I.11
COMPACT ULTRAHIGH PRESSURE NANOFLOW LC SYSTEM
Luke Tolley1, Milton Lee2, Xiaofeng Zhao2, Xiaofeng Xie2, Sonika Sharma2, Alex Plistil3, Hal Barnett3, Martin
Brisbin3, Stanley D. Stearns3, Paul Farnsworth2, H. Dennis Tolley2
1 Chemistry - Southern Illinois University, 1245 Lincoln Dr., 62901 Carbondale, United States
2 Brigham Young University, Department of Chemistry, 84602 Provo, United States
3 VICI Valco Instruments, 8300 Waterbury, 77055 Houston, United States
I.12
ON-LINE LIQUID ANALYSIS WITH A NEW GENERATION OF FAST MICRO-ANALYZER
Adrien Maniquet
Process Experimentation - IFPEN, Rond point de l'echangeur de Solaize, les levees, 69360 SOLAIZE, France
I.13
SPECTRAL PROPERTIES OF ALLERGY SUBSTANCES IN FRAGRANCE CALCULATED
FOR USE IN MULTIPHOTON IONIZATION MASS SPECTROMETRY
Tomoko Imasaka1, Totaro Imasaka2
Graduate School of Design - Kyushu University, 4-9-1 Shiobaru, Minami-ku, 815-8540 Fukuoka, Japan
2 Department of Applied Chemistry, Graduate School of Engineering - Kyushu University, 744 Motooka, Nishi-ku,
819-0395 Fukuoka, Japan
1
65
_____________________________________________________________________________
J. COUPLED AND MULTIDIMENSIONAL TECHNIQUES
_____________________________________________________________________________
J.01
CHALLENGING GC-MS APPLICATIONS ACHIEVED WITH COLD EI
Aviv Amirav, Alexander B. Fialkov, Uri Keshet, Tal Alon
Department of Chemistry - Tel Aviv University, Ramat Aviv, 69978 Tel Aviv, Israel
J.02
SEPARATION, DETECTION, AND QUANTITATION OF INTACT PROTEINS BASED ON
MULTIPLE REACTION MONITORING TRIPLE QUADRUPOLE MASS SPECTROMETRY
Kevin A. Schug1, Evelyn H. Wang1, Frances Carroll2, Peter C. Combe3
Chemistry and Biochemistry - University of Texas at Arlington, 700 Planetarium PI., Box 19065, TX 76019-0065
2 Restek Corporation, 110 Benner Circle, 16823 Bellefonte, United States
3 Shimadzu Scientific Instruments, Inc., 7102 Riverwood Drive, 21046 Columbia, United States
1
J.03
DIRECT SPECIFIC ISOTOPIC ANALYSIS OF COMPOUNDS RELEASED BY PYROLYSIS
(Py-CSIA): NOVEL APPLICATIONS IN PALEOENVIRONMENTAL STUDIES
José M. De La Rosa1, Nicasio T. Jiménez-Morillo1, Ana Z. Miller1, Gonzalo Almendros2, José A. GonzálezPérez1
1 Instituto de Recursos Naturales y Agrobiología de Sevilla (IRNAS-CSIC), Reina Mercedes Av. 10., 41012
Seville, Spain
2 Museo Nacional de Ciencias Naturales (MNCN-CSIC), Serrano Street, 115b., 28006 Madrid, Spain
J.04
IMPROVED QUANTITATIVE ANALYSIS OF PESTICIDES IN COMPLEX MATRICES
THROUGH REDUCTION OF MATRIX SUPPRESSION AND INTERFERENCES BY MULTIDIMENSIONAL LIQUID CHROMATOGRAPHY COUPLED TO MASS SPECTROMETRY
Nicola Cimino1, Stephan Buckenmaier2, Thomas Glauner2
Italia, Via V. Lamaro, 13, 00173 Roma, Italy
2 Agilent Technologies, Hewlett Packard Strasse 8, 76337 Waldbronn, Germany
1 Agilent
J.05
COUPLING OF ION MOBILITY SPECTROMETRY AS DETECTOR TO A MICRO GAS
CHROMATOGRAPH FOR ENHANCED DETECTION LIMITS AND APPLICABILITY
Remko van Loon1, Nuria Sabugo Garcia2, Daniel Sanders2
Gesellschaft für Analytische Sensorsysteme, Otto-Hahn-Str. 15, 44227 Dortmund, Germany
1
2
J.06
HYDROCARBON CONTAMINANTS IN PIZZA BOXES FROM THE ITALIAN MARKET
Sabrina Moret1, Claudia Picon2, Chiara Conchione2, Renzo Bortolomeazzi2
1 Food Science - University of Udine, Via Sondrio 2A, 33100 Udine, Italy
2 Department of Agricultural, Food, Environmental, Animal Sciences - University Udine, Via Sondrio 2A, 33100
Udine, Italy
J.07
AUTOMATED SOLID PHASE EXTRACTION FOLLOWED BY ON-LINE LC-GC FOR CLASS
SEPARATION OF AROMATICS IN EDIBLE OILS
Sabrina Moret1, Chiara Conchione2, Lanfranco S. Conte2
1 Food Science - University of Udine, Via Sondrio 2A, 33100 Udine, Italy
2 Department of Agricultural, Food, Environmental, Animal Sciences - University Udine, Via Sondrio 2A, 33100
Udine, Italy
66
J.08
MZMINE AS A TOOL FOR THE OPTIMIZATION OF CHROMATOGRAPHIC AND MASSSPECTROMETRIC CONDITIONS TO IDENTIFY PHENOLIC COMPOUNDS IN COMPLEX
PHYTOCHEMICAL MIXTURES
Giorgia La Barbera, Anna Laura Capriotti, Patrizia Foglia, Susy Piovesana, Riccardo Zenezini Chiozzi, Aldo
Laganà
J.09
USE OF MULTIDIMENSIONAL GC AND SIMULTANEOUS SELECTIVE DETECTION TO
RESOLVE COMPLEX MIXTURES
Benjamin L'Homme, Erik Ritzen, John Mommers
DSM Resolve, Urmonderbaan 22, 6167 Geleen, Netherlands
J.10
A NOVEL MULTIDIMENSIONAL GAS CHROMATOGRAPHY SYSTEM FOR ON-LINE
POSITION SPECIFIC STABLE ISOTOPE ANALYSIS OF ENVIRONMENTAL ORGANIC
CONTAMINANTS
Caroline Gauchotte-Lindsay1, Bryan White2
1 School of Engineering - University of Glasgow, Oakfield Avenue, G12 8LT Glasgow, United Kingdom
2 JSB United Kingdom and Ireland, Cedar Court Grove Park Business Est. White Waltham, SL6 3LW
Maidenhead, United Kingdom
J.11
USING THE SELF-CLEANING ION SOURCE TO EXTEND MAINTENANCE FREE GC/MS
OPERATION
Bruce Quimby1, Elizabeth Almasi1, Ken Brady2
Technologies, 2850 Centerville Road, 19808-1610 Wilmington, United States
2 Marketing Programs - Agilent Technologies, 5500 Lakeside, SK8 3GR Cheadle, United Kingdom
1 Agilent
J.12
EFFICIENT REMOVAL OF OLEFIN INTERFERENCES BY ON-LINE LIQUID-LIQUID
CHROMATOGRAPHY PRIOR TO THE GAS CHROMATOGRAPHY DETERMINATION OF
MINERAL OIL CONTAMINATION IN VEGETABLE OILS
Mariosimone Zoccali1, Giorgia Purcaro1, Laura Barp2, Marco Beccaria1, Danilo Sciarrone2, Luigi Mondello1,2
J.13
ISOLATION OF UNKNOWN MOLECULES FROM PLANT EXTRACTS EXPLOITING A
MULTIDIMENSIONAL GC-PREP SYSTEM FOLLOWED BY NMR, MS AND FTIR FOR
STRUCTURAL IDENTIFICATION
Danilo Sciarrone1, Luigi Mondello1,2
1 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - Università degli studi di Messina,
J.14
SILICA MODIFIED WITH POLYMERIC AMPHIPHILIC NANOPARTICLES AS FIRST
DIMENSION FOR MULTIDIMENSIONAL SEPARATION TECHNIQUES
Rodrigo N. Padovan1, Anderson L. Luiz1, Maraíssa S. Franco1, Christopher Palmer2, Fernando M. Lancas1
Institute of Chemistry at Sao Carlos - University of Sao Paulo, 780, 13560-970 Sao Carlos, Brazil
Department of Chemistry and Biochemostry - University of Montana, 32 Campus Drive Missoula, 59812
Montana, United States
1
2
J.15
DETERMINATION OF OCHRATOXIN A IN WINE BY IN-TUBE SOLID PHASE
MICROEXTRACTION AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY WITH
SEQUENTIAL MASS SPECTROMETRY DETECTION
Mariane A. Andrade, Fernando M. Lancas
Institute of Chemistry at Sao Carlos - University of Sao Paulo, Postal Code 780, 13560-970 Sao Carlos, Brazil
67
J.16
PHTHALIC ACID ESTERS DETERMINATION IN VEGETABLE OILS BY USING SPME
FOLLOWED BY FAST GC COUPLED WITH TRIPLE QUADRUPOLE MS
Flavio A. Franchina1, Laura Barp2, Mariosimone Zoccali1, Giorgia Purcaro1, Danilo Sciarrone2, Peter Q.
Tranchida2, Luigi Mondello2,1
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, Polo
_____________________________________________________________________________
K. COMPREHENSIVE GC
_____________________________________________________________________________
K.01
IMPACT OF DIVERSE MATRICES ON STANDARD METHODS EVALUATED BY OFFLINE
HYPHENANTION OF HPLC-RI WITH GCxGC-TOFMS
Maximilian K. Jennerwein1,2, Markus Eschner2, Thomas Gröger1, Thomas Wilharm2, Ralf Zimmermann1
1 Comprehensive Molecular Analytics - Helmholtz Zentrum München, Ingolstadter Landstraße 1, 85764 Munich,
Germany
2 R&D - ASG Analytik Service Gesellschaft, Trentiner Ring 30, 86356 Neusäss, Germany
K.02
TWO DIMENSIONAL GAS CHROMATOGRAPHY: A POWERFUL TOOL TO UNRAVEL WINE
VOLATILES
Katja Suklje1, Silvia Carlin2, Jan Stranstrup2, Guillaume Antalick1, Alain Deloire1, Urska Vrhovsek2, Leigh M.
Schmidtke1
1 National Wine and Grape Industry Centre, Charles Sturt University, Locked Bag 588, 2678 Wagga Wagga,
Australia
2 Department of Food Quality and Nutrition Department - Edmund Mach Foundation, Via E. Mach 1, 38010 San
Michele a/A, Italy
K.03
A NEW PASSIVE SAMPLER USING SILICONE RUBBER FOR THE ANALYSIS OF SURFACE
WATER BY COMPREHENSIVE GAS CHROMATOGRAPHY – TIME OF FLIGHT MASS
SPECTROMETRY
Yvette Naudé1, Peter Gorst-Allman2, Egmont Rohwer1
Department of Chemistry - University of Pretoria, c/o Lynnwood Rd and Roper St, 83 Hatfield, Pretoria, South
Africa
2 Separation Science - LECO Africa, Vuurslag Avenue, 1620 Kempton Park, South Africa
1
K.04
POTENTIAL OF GCxGC-ToF MS WITH SCRIPT FILTERS FOR THE IDENTIFICATION OF
PERSISTENT ORGANOHALOGENATED POLLUTANTS IN TUNA SAMPLES
Juan Escobar-Arnanz, Lourdes Ramos
Dpt Instrum Anal & Environ Chem - IQOG-CSIC, Juan de la Cierva 3, 28006 Madrid, Spain
K.05
COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY COUPLED TO TIMEOF-FLIGHT MASS SPECTROMETRY FOR THE ANALYSIS OF VAPOUR PHASE
MAINSTREAM CIGARETTE SMOKE
Benjamin Savareear1, Radoslaw Lizak1, Jean-Francois Focant1, Michal Brokl2, Christopher Wright2
1 Organic & Biological Analytical Chemistry Group - University of Liege, Allée du Six Août, 11, 4000 Liege,
Belgium
2 British American Tobacco, Southampton, SO158TL Southampton, United Kingdom
68
K.06
GC×GC-TOF-MS BASED URINE METABOLOMICS IN PROSTATE CANCER
Marta Kordalewska1, Renata Bujak1, Tomás Kovalczuk2, Agnieszka Ulanowska3, Grzegorz Straczynski3, Michal
J. Markuszewski1
1 Department of Biopharmaceutics and Pharmacodynamics - Medical University of Gdansk, Hallera 107, 80-416
Gdansk, Poland
2 LECO Instrumente Plezen, Plaska 66, 32300 Plezen, Czech Republic
3 LECO Poland, Czarna 4, 43-100 Tychy, Poland
K.07
COMPARISON OF GCXGC TOF MS AND GCXGC-HR MS FOR THE ANALYSIS OF
ENVIRONMENTAL SAMPLES
Els Van Meenen1, Thomas Groger2, Pieter Joos1,3, Benedikt Weggler2, Ralf Zimmermann2,4
1 Laboratory - water-link, Mechelsesteenweg 66, 2018 Antwerp, Belgium
2 Comprehensive Molecular Analytics, Ingolstaedter Landstrasse 1, 85764 Oberschleissheim, Germany
3 Department of Bioengineering - University of Antwerp, Groenenborgerlaan 171, 2020 Antwerpen, Belgium
4 Chair of Analytical Chemistry - Uinversity of Rostock, Dr. Lorenz Weg 1, 18051 Rostock, Germany
K.08
PROFILING OF VOLATILE ORGANIC COMPOUNDS FROM CANOLA BY GCxGC-TOFMS
James J. Harynuk1, Paulina A. de la Mata1, Chaminda S. Weeraddana2, Maya L. Evendon2, Lawrence A.
Adutwum1
1 Department of Chemistry - University of Alberta, 11227 Saskatchewan Drive, T6G2G2 Edmonton, AB, Canada
2 Biological Sciences - University of Alberta, CW 405 Biological Sciences Bldg, T6H 3M8 Edmonton, AB, Canada
K.09
LOW RESOLUTION, HIGH RESOLUTION, ACCURATE MASS, DECONVOLUTION! A
COMPARISON OF LOW AND HIGH RESOLUTION GAS CHROMATOGRAPHY – TIME OF
FLIGHT MASS SPECTROMETRY AND COMPREHENSIVE GAS CHROMATOGRAPHY –
TIME OF FLIGHT MASS SPECTROMETRY
Charles P. Gorst-Allman
Separation Science - LECO Africa (Pty) Ltd, 3 Vuurslag Avenue, 1620 Spartan Ext.7, Kempton, South Africa
K.10
GCXGC AS A TOOL FOR DISENTANGLING PETROLEUM REFINERY PROCESSES: 2STAGE HYDROTREATING_HYDROCRACKING
Asger B. Hansen1, Asbjorn S. Andersen2, Rasmus G. Egeberg2
1 R&D Chemical Analytical - Haldor Topsoe AS, 55 Nymollevej, 2800 Lyngby, Denmark
2 R&D Refinery Processes, Haldor Topsoe AS, 55 Nymollevej, 2800 Kgs. Lyngby Copenhagen, Denmark
K.11
MONITORING VOCS DURING BLOOD DEGRADATION BY TD-GC×GC-TOFMS WITH
VARIABLE-ENERGY ELECTRON IONISATION
Lena M. Dubois1, Katelynn A. Perrault1, Pierre-Hugues Stefanuto1, Stefan Koschinski2, Matthew Edwards3,
Laura McGregor3, Jean-François Focant1
1 Department of Chemistry - University of Liège, Allée du 6 Août 11, B6c, 4000 Liège, Belgium
2 Markes International GmbH, Schleussnerstrasse 42, 63263 Frankfurt, Germany
3 Markes International Ltd., Gwaun Elai Medi-Science Campus, RCT Llantrisant, United Kingdom
K.12
INVESTIGATION OF EMISSIONS FROM HEATED TOBACCO WITH COMPREHENSIVE
TWO-DIMENSIONAL GAS CHROMATOGRAPHY WITH MASS SPECTROMETRY
DETECTION
Radek Lizak1, Benjamin Savareear1, Michal Brokl2, Christopher Wright2, Jean-Francois Focant1
1 Organic and Biological Analytical Chemistry - University of Liege, Allée du 6 août, 11, B6c, Quartier Agora,
B-4000 Liège (Sart-Tilman), Belgium
2 ADC Group Research and Development - British American Tobacco, Regents Park Road, Millbrook,
Southampton, SO15 Southampton, United Kingdom
69
K.13
APPLICATION OF COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY-TIME
OF FLIGHT MASS SPECTROMETRY FOR CHARACTERIZATION AT MOLECULAR LEVEL
OF BRAZILIAN OIL
Gabriela Vanini1, Vinícius B. Pereira1, Wanderson Romão2, Lize Mirela S. Oliveira3, Júlio César M. Dias3,
Débora A. Azevedo1
1 Institute of Chemistry - Federal University of Rio de Janeiro, Av. Horácio Macedo, 1281, 21941598 Rio de
Janeiro, Brazil
2 Federal Institute of Espírito Santo, Av. Ministro Salgado Filho, 1000, 29106010 Vila Velha, Brazil
3 Cenpes - Petrobrás, Ilha do Fundão, 21941915 Rio de Janeiro, Brazil
K.14
UNDERSTANDING THE COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHIC DISCRIMINATION OF PETROLEUM HYDROCARBON STRUCTURES
Daniela Franca, Bruno Q. Araújo, Jaakko Laakia, Francisco R. Aquino Neto, Debora A. Azevedo
Institute of Chemistry - Federal University of Rio de Janeiro, Av. Horacio Macedo 1281, 21941598 Rio de
Janeiro, Brazil
K.15
SEPARATION AND QUANTIFICATION OF HYDROCARBON CLASSES IN CRUDE OIL
USING COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY UNDER
REVERSED-PHASE COLUMN SYSTEM
Dayane M. Coutinho1, Daniela França1, Vinícius B. Pereira1, Lize Mirela S. de Oliveira2, Júlio César M. Dias2,
Debora A. Azevedo1
1 Institute of Chemistry - Federal University of Rio de Janeiro, Av. Horácio Macedo 1281, 21941598 Rio de
Janeiro, Brazil
2 Cenpes - PETROBRAS, Av. Horácio Macedo 950, 21941915 Rio de Janeiro, Brazil
K.16
COMBINING MULTIDIMENSIONAL GAS CHROMATOGRAPHY-MASS SPECTROMETRY
WITH HEART-CUTTING AND COMPREHENSIVE TWO DIMENSIONAL GAS
CHROMATOGRAPHY FOR VOLATILE SAMPLE CHARACTERIZATION
Davide Mendes1, Sofia Branco2, Eduardo Mateus2, Maria R. Paiva2, Marco Gomes da Silva1
1 LAQV, REQUIMTE, Departamento de Química - Faculdade de Ciências e Tecnologia da Universidade Nova de
Lisboa, Campus da Caparica, 2829-516 Caparica, Portugal
2 CENCE - Faculdade de Ciências e Tecnologia da Universidade Nova de Lisboa, Campus da Caparica,
2829-516 Caparica, Portugal
K.17
BIOMARKER DETECTION AND CHARACTERIZATION OF SMOKE FLAVORINGS BY HSSPME-GC×GC-TOF MS
Anupam Giri1,2, Zuzana Zelinkova2, Thomas Wenzl2
1 Department of Chemistry - University of Liège, Allée du 6 août, 11, B6c, Quartier Agora, B-4000 Liège, Belgium
2 Institute for Reference Materials and Measurements - European Commission, Joint Research Centre,
Retieseweg 111, B-2440 Geel, Belgium
K.18
COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY COMBINED WITH
HIGH-RESOLUTION MASS SPECTROMETRY: EXPLORING MASS DEFECT INFORMATION
TO CHARACTERIZE BASE OIL
Anupam Giri1, Marion Courtiade2, Amandine Racaud2, Jean-François Focant1
2 Centre de Recherche de Solaize - Total Marketing Services, Chemin du Canal, BP 22, 69360 Solaize, France
70
K.19
TWO-DIMENSIONAL GAS CHROMATOGRAPHY TIME-OF-FLIGHT MASS SPECTROMETRY
FOR THE INVESTIGATION OF PARTICULATE MATTER-BOUND ORGANIC COMPOUNDS
DEPOSITED ON URBAN VEGETATION
Ana Castanheiro1, Roeland Samson1, Pieter Joos2,3
1 Department of Bioscience Engineering - University of Antwerp, Groenenborgerlaan 171, 2020 Antwerp,
Belgium
2 Laboratory - water-link, Mechelsesteenweg 64, 2018 Antwerp, Belgium
3 Department of Bioengineering - University of Antwerp, Groenenborgerlaan 171, 2020 Antwerpen, Belgium
K.20
PEAK DISPERSION EVALUATION AND OPTIMIZATION IN GC×GC
Pierre-Hugues Stefanuto1, Jean-Marie Dimandja2, Jean-François Focant1
1 Organic and Biological Analytical Chemistry Group, CART, Chemistry Department - University of Liège, Allée du
six août B6c, 11, Quartier Agora, B-4000 Liège, Belgium
2 Department of Chemistry and Biochemistry - Spelman College, 350 Spelman Lane, 30314-4399 Atlanta, United
States
K.21
MULTIPLEXED DUAL DIMENSIONS COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHY (2GC × 2GC) WITH CONTRA-DIRECTIONAL THERMAL
MODULATION AND FLOW CONTROL
Dandan Yan, Robert A. Shellie
Australian Centre for Research on Separation Science - School of Physical Sciences, University of Tasmania,
Private Bag 75, 7001 Hobart, TAS, Australia
K.22
ANALYSIS OF CONTAMINANTS IN SURFACE WATER USING SPE–GC×GC–HR-TOF MS
Sjaak de Koning1, Juergen Wendt2
1 Da Vinci Laboratory Solutions, Cairostraat 10, 3047BC Rotterdam, Netherlands
2 LECO Instruments, Marie-Bernays-Ring 31, 41199 Mönchengladbach, Germany
K.23
ANALYSIS OF PYROLYSIS OILS ON GC-QTOF AND GCxGC-QTOF
Mette Kristensen, Peter Christensen, Jan Christensen
Department of Plant and Environmental Sciences - University of Copenhagen, Thorvaldsensvej 40, 1871
Frederiksberg C, Denmark
K.24
POTENTIALS OF THE REVERSED-INJECT DIFFERENTIAL FLOW MODULATOR
COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY IN THE QUANTITATIVE
PROFILING OF SUSPECTED FRAGRANCE ALLERGENS
Chiara Cordero1, Davide Bressanello1, Patrizia Rubiolo1, Luigi Cobelli2, Armando Miliazza3, Matthew Giardina4,
Carlo Bicchi1
1 Dipartimento di Scienza e Tecnologia del Farmaco - University of Turin, Via Pietro Giuria, 9, I-10125 Turin, Italy
2 SRA Intruments SpA, Via alla Castellana 3, 20063 Cernusco sul Naviglio (Milan), Italy
3 Agilent Technologies, Cernusco sul Naviglio, 20063 Cernusco sul Naviglio (Milan), Italy
4 Gas Phase Separations Division - Agilent Technologies, 2850 Centerville Road, 19808 Wilmington, United
States
K.25
EXAMINATION OF HAFTING ADHESIVES ON PALEOLITHIC STONE TOOLS USING GC×
GC-QTOFMS
Katelynn A. Perrault1, Lena Dubois1, Pierre-Hugues Stefanuto1, Benjamin L'Homme2, Dries Cnuts3, Veerle
Rots3, Jean-François Focant1
1 Organic and Biological Analytical Chemistry Group - University of Liège, Allée du 6 Août 11, B6c, Quartier
Agora, 4000 Liège, Belgium
2 DSM Resolve, Urmonderbaan 22, 6167 Geleen, Netherlands
3 Prehistoric Archaeology/Traceolab - University of Liège, Quai Roosevelt 1B (Bât. A4), 4000 Liège, Belgium
71
K.26
OPTIMIZATION OF CADAVERIC INTERNAL GAS MONITORING BY GC×GC-HR ToF MS
FOR USE IN POSTMORTEM EXAMINATIONS
Katelynn A. Perrault1, Pierre-Hugues Stefanuto1, Lena Dubois1, Silke Grabherr2, Vincent Varlet3, Jean-François
Focant1
1 Organic and Biological Analytical Chemistry Group - University of Liège, Allée du 6 Août 11, B6c, Quartier
Agora, 4000 Liège, Belgium
2 Forensic Imaging Unit - University Center of Legal Medicine, Chemin de la Vulliette 4, CH-1000 Lausanne 25,
Switzerland
3 Forensic Toxicology and Chemistry Unit - University Center of Legal Medicine, Chemin de la Vulliette 4,
CH-1000 Lausanne 25, Switzerland
K.27
GCxGC-QTOF: A COMPREHENSIVE APPROACH TO THE IDENTIFICATION CHALLENGES
IN COMPLEX FOOD MATRICES
Daniela Peroni1,2
1 Zoex Europe, Traamstraat 15, 5611CM Eindhoven, Netherlands
2 JSB Nederland, Apolloweg 2B, 8239DA Lelystad, Netherlands
K.28
DETAILED CHARACTERIZATION OF PETROCHEMICAL SAMPLES BY GCxGC-HR-TOF
WITH ADVANCED DATA PROCESSING
Tomas Kovalczuk
LECO, Plaska 66, 32300 Plzen, Czech Republic
K.29
TWO-DIMENSIONAL GAS CHROMATOGRAPHY FOR THE ANALYSIS OF ATMOSPHERIC
HALOCARBONS
Chang-Feng Ou-Yang1,2, Scott Hua2, Ming-Kai Teng2, Yu-Chieh Chou2, Wen-Tzu Liu2, Chieh-Heng Wang2, JiaLin Wang2
1 Department of Atmospheric Sciences - National Central University, No. 300, Zhongda Rd., 32001 Taoyuan,
Taiwan
2 Department of Chemistry - National Central University, No. 300, Zhongda Rd., 32001 Taoyuan, Taiwan
K.30
ANALYSIS OF PETROLEUM PRODUCTS USING COMPREHENSIVE TWO-DIMENSIONAL
GAS CHROMATOGRAPHY (GC×GC) WITH BOTH TIME OF FLIGHT MS AND FLAME
IONIZATION DETECTORS
Joe Binkley, Christina N. Kelly, Jonathan D. Byer
LECO Corporation, 3000 Lakeview Avenue, 49085 Saint Joseph, MI, United States
K.31
COMPARISON OF METABOLIC PROFILES OF LIVER BIOPSY SAMPLES AND MATCHING
SERUM SAMPLES BY GC×GC-TOF
Ismo Mattila1, Matej Oresic1, Hannele Yki-Järvinen2, Panu Luukkonen2, Sanja Sädevirta2, Marja Leivonen2,
Johanna Arola2, Tuulia Hyötyläinen1
1 Steno Diabetes Center, Niels Steensens Vej 2, 2820 Gentofte, Denmark
2 University of Helsinki, Haartmaninkatu 8, 00290 Helsinki, Finland
K.32
ANALYSIS OF VOLATILE AND SEMIVOLATILE FLAVOUR COMPONENTS IN CIGARETTES
BY HS-SPME AND GCxGC-QTOF-MS
Jorge Regueiro, Anupam Giri, Zuzana Zelinkova, Thomas Wenzl
Standards for Food Bioscience - European Commission, Joint Research Centre, Retieseweg 111, 2440 Geel,
Belgium
K.33
GC-MS/MS ROUTINE QUANTITATION AND GC×GC-MS SCREENING FOR EMERGING
POLLUTANTS IN ONE SINGLE INJECTION
Philippe Mottay1, Jiri Ondrus2, Roger Simon1
Brechbuehler, Steinwiessenstrasse 3, 8952 Schlieren, Switzerland
service de l'energie et de l'environnement de l'etat de Neuchatel, Rue du Tombet 24, 2034 Peseux, Switzerland
1
2
72
K.34
ANALYSIS OF URINE SRMS USING SOLID PHASE MICRO EXTRACTION, DYNAMIC
HEADSPACE AND LIQUID INJECTION WITH COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHY (GC×GC)-HIGH RESOLUTION TIME-OF-FLIGHT MASS
SPECTROMETRY
Joe Binkley, David E. Alonso, Jonathan D. Byer
LECO Corporation, 3000 Lakeview Avenue, 49085 Saint Joseph, MI, United States
K.35
NOVEL ANALYSIS METHOD OF VARIOUS ENVIRONMENTAL SAMPLES USING GC×GCHRMS WITH ENCODED FREQUENT PULSING™
Scott Pugh, Viatcheslav Artaev, Mark F. Merrick
LECO Corporation, 3000 Lakeview Avenue, 49085 St. Joseph, MI, United States
K.36
MULTIWAY TOOLS OF NON TARGET COMPOUNDS USING GC × GC-TOFMS DATA TO
MODELING CRUDE OIL PROPERTIES
Daniela L. Vale1, Paula F. de Aguiar1, Lize Mirela S. de Oliveira2, Julio Cesar M. Dias2, Debora Azevedo1
Institute of Chemistry - Federal University of Rio de Janeiro, Avenida Athos da Silveira Ramos, 149, 21941-909
Rio de Janeiro, Brazil
2 Petrobras/Cenpes, Av. Horácio Macedo, 21941-909 RIO DE JANEIRO, Brazil
1
K.37
ANALYSIS OF AROMATIC AMINES IN HUMAN URINE USING COMPREHENSIVE MULTIDIMENSIONAL GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC×GC-QMS)
Nerea Lorenzo Parodi, Torsten C. Schmidt
Instrumental Analytical Chemistry - Faculty of Chemistry, Universitätsstraße 5, S05 V02 E31, 45141 Essen,
Germany
K.38
FAST AND SLOW PYROLYSIS OF COFFEE RESIDUES: CHARACTERIZATION OF THE BIOOIL BY GC×GC/qMS
Ariel O. Celestino1, Nayna L. Sampaio1, Anne Raquel T. Cardoso1, Jaderson K. Schneider2, Maria Elisabete
Machado2, Laiza C. Krause1, Elina B. Caramao2
1 Programa de Pós Graduação em Biotecnologia Industrial - Universidade Tiradentes, UNIT, av. Murilo Dantas,
300, 49032490 Aracaju, Brazil
2 Instituto de Quimica - UFRGS, av.Bento Goncalves,9500, 91510-960 Porto Alegre, Rs, Brazil
K.39
INVESTIGATION OF THE POSSIBLE EFFECT OF SAMPLING ON HUMAN EXHALED
BREATH SAMPLE INTEGRITY
Romain Pesesse1, Pierre-Hugues Stefanuto1, Florence Shleich2, Marie-Alice Meuwis3, Edouard Louis3, Renaud
Louis2, Jean-François Focant1
1 Organic and Biological Analytical Chemistry Group, CART - University of Liège, Allée du six août B6c, B-4000
Liège, Belgium
2 Pneumology and Allergology Unit - University Hospital Center, Avenue de l'hopital, 4000 Liège, Belgium
3 Gastroenterology, Hepatology and Digestive Oncology Unit - University Hospital Center, Avenue de l'hopital,
4000 liège, Belgium
K.40
PHOTOIONIZATION AS A SOFT IONIZATION SOURCE FOR COMPREHENSIVE TWODIMENSIONAL GC (GC×GC) AND HIGH-RESOLUTION TOFMS
Masaaki Ubukata1, Robert B. Cody1, A. J. Dane1, Toshiyuki Kato2, Masahiro Ito2, Bram van der Meer3, Junichi
Osuga4, Jean-François Focant5
1 JEOL USA, Inc., 11 Dearborn Road, 01960 Peabody, United States
2 JEOL Ltd,., 3-1-2 Musashino, 196-8558 Akishima, Japan
3 JEOL (Europe) BV, Lireweg 4, 2153 Nieuw-Vennep, Netherlands
4 JEOL (Europe) SAS, Espace Claude Monet-1, allee de Giverny, 78290 Croissy-Sur-Seine, France
5 University of Liège, Bâtiment B6b, 4000 Liège, Belgium
73
K.41
INTERACTIVE TOOLS FOR OPTIMIZING BLOB DETECTION AND TEMPLATE
MATCHING FOR COMPREHENSIVE TWO-DIMENSIONAL CHROMATOGRAPHY
Qingping Tao1, Chase Heble1, Stephen Reichenbach2,1, Chiara Cordero3
1 GC Image, LLC, PO Box 57403, 68505-7403 Lincoln, United States
2 Computer Science & Engineering - University of Nebraska, 260 Avery, 68588-0115 Lincoln, United States
3 Universita degli Studi di Torino, Via Pietro Giuria, 9, I-10125 Torino, Italy
K.42
CHARACTERIZATION OF SULFUR AND NITROGEN COMPOUNDS IN BRAZILIAN
PETROLEUM DERIVATIVES USING IONIC LIQUID COLUMNS IN COMPREHENSIVE TWODIMENSIONAL GAS CHROMATOGRAPHY AND MASS SPECTROMETRIC DETECTION
Fernando C. Fontanive1, Érica S. Silva1, Juliana M. da Silva2, Elina B. Caramão3, Claudia A. Zini1
Chemistry Institute - UFRGS, Bento Goncalves, 9500, 91501-970 Porto Alegre, Brazil
2 Fundação Escola Técnica Liberato Salzano Vieira da Cunha, Rua Inconfidentes 395, 93340140 Novo
Hamburgo, Brazil
3 UNIT, Avenida Murilo Dantas 300, 49032-490 Aracaju, Brazil
1
K.43
VOLATILES PROFILING FROM HIGH QUALITY COCOA SAMPLES AT EARLY STAGES OF
TECHNOLOGICAL TREATMENT BY TWO-DIMENSIONAL COMPREHENSIVE GAS
CHROMATOGRAPHY - MASS SPECTROMETRY
Federico Magagna1, Erica Liberto1, Stephen E. Reichenbach2, Qingping Tao3, Carlo Bicchi1, Chiara Cordero1
1 Dipartimento di Scienza e Tecnologia del Farmaco - University of Turin, Via Pietro Giuria, 9, I-10125 Turin, Italy
2 Computer Science and Engineering Department, University of Nebraska, 1400 R Street, 68504 Lincoln, United
States
3 GC Image LCC, 1400 R Street, 68504 Lincoln, United States
K.44
COMPREHENSIVE GC×GC ANALYSIS OF HYDRAULIC FRACTURING ADDITIVES IN
WASTEWATER FROM UNCONVENTIONAL GAS PRODUCTION
Aileen Melsbach, Martin Elsner
Institute of Groundwater Ecology - Helmholtz Zentrum München, Ingolstädter Landstrasse 1, D-85764
Neuherberg, Germany
K.45
EFFICIENT GC×GC DATA TREATMENT WITH BARCHAN ALGORITHM (BLOB ALIGNMENT
FOR ROBUST CHROMATOGRAPHIC ANALYSIS) AND ANCHOR POINTS
Camille Couprie1, Maxime Moreaud1, Laurent Duval1, Sophie Hénon2, Vincent Souchon2
1 Mechatronics, Computer Science and Applied Mathematics Division - IFP Energies nouvelles, 1 et 4 avenue de
Bois-Préau, 92852 Rueil-Malmaison, France
2 Physics and Analysis Division - IFP Energies nouvelles, Rond-point de l'échangeur de Solaize - BP3, 69360
Solaize, France
K.46
GC×GC WITH SIMULTANEOUS MASS SPECTROMETRY/FLAME IONIZATION DETECTION
FOR ROUTINE PETROCHEMICAL ANALYSES
Nick Bukowski, Laura McGregor, Matthew Edwards, Massimo Santoro
Markes International, Gwaun Elai Medi-Science Campus, CF72 8XL Llantrisant, United Kingdom
K.47
COMPREHENSIVE CHARACTERISATION OF ESSENTIAL OILS BY FLOW-MODULATED
GC×GC–TOF MS
Laura McGregor, Matthew Edwards, Nick Bukowski, Massimo Santoro
Markes International, Gwaun Elai Medi-Science Campus, CF72 8XL Llantrisant, United Kingdom
K.48
WHAT'S IN YOUR MORNING DRINK? COMPREHENSIVE CHARACTERISATION OF
COFFEE EXTRACTS BY GCxGC-TOF MS
Laura McGregor1, Massimo Santoro1, Eligio Sebastiani2, Steve Smith1
1 Markes International, Gwaun Elai Medi-Science Campus, CF72 8XL Llantrisant, United Kingdom
2 SRA Instruments S.p.A, Via alla Castellana 3, 20063 Milan, Italy
74
K.49
USE OF COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY WITH MASS
SPECTROMETRIC DETECTION TO IDENTIFY MISCELANEOUS AROMA DESCRIPTORS
OBTAINED BY GAS CHROMATOGRAPHY-OLFACTOMETRY OF MERLOT WINES FROM
CAMPANHA GAÚCHA
Karine P. Nicolli1, Laura O. Lago2, Elina B. Caramão3, Celito C. Guerra4, Henrique P. dos Santos4, Aline B.
Marques5, Juliane E. Welke1, Claudia A. Zini1
1 Chemistry Institute - UFRGS, Bento Goncalves, 9500, 91501-970 Porto Alegre, Brazil
2 Instituto de Ciência e Tecnologia de Alimentos - UFRGS, Av. Bento Gonçalves 9500, 91501-970 Porto Alegre,
Brazil
4 Embrapa Uva e Vinho, Rua Livramento, n? 515, 95700-000 Aracaju, Brazil
5 Embrapa Semi-Árido, BR 428, km 152, Zona Rural, 56302-970 Petrolina, Brazil
K.50
COMPREHENSIVE CHARACTERIZATION OF E-LIQUID VOLATILES BY SPME-GC×GCHRTOF/MS
Anupam Giri1,2, Jorge Regueiro2, Thomas Wenzl2
2 Institute for Reference Materials and Measurements - European Commission, Joint Research Centre,
Retieseweg 111, B-2440 Geel, Belgium
K.51
PRODUCT CONTROL USING DIFFERENTIAL GC/MS AND COMPREHENSIVE GCxGC/MS
Marco Ruijken
R&D - MsMetrix, Doornhoecklaan 81, 3601JT maarssen, Netherlands
K.52
CANADIAN CRAFT BEER CHARACTERIZATION USING TD-GC×GC-TOFMS
Pierre-Hugues Stefanuto1, Katelynn A. Perrault1, Lena Dubois1, Benjamin L'Homme1, Catherine Allen1, Caitriona
Loughnane1, Nobuo Ochiai2, Jean-François Focant1
2 Gerstel, 2-13-18 Nakame, Meguro-ku, Tokyo 152-0031, Japan
K.53
PRESSURE TUNING OF THE FIRST DIMENSION COLUMN IN GC×GC
Mohammad Sharif Khan, Sung-Tong Chin, Chadin Kulsing, Philip J. Marriott
Department of Chemistry - Monash University, 17 Rainforest walk, 3800 Clayton, Australia
K.54
USE OF COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY AND TANDEM
MASS SPECTROMETRY FOR THE TARGETED AND UNTARGETED ANALYSIS OF
PETROCHEMICAL SAMPLES
Maria Elisabete Machado1,2, Marco Piparo3, Flavio A. Franchina4, Claudia Zini1, Elina B. Caramao1,2, Peter Q.
Tranchida3, Luigi Mondello3,4
1 Instituto de Química - Universidade Federal do Rio Grande do Sul, Av. Bento Gonçalves, 9500 Porto Alegre,
Brazil
2 Programa de Pós Graduação em Biotecnologia Industrial - Universidade Tiradentes, av. Murilo Dantas,
49032490 Aracaju, Brazil
75
K.55
(LOW-)FLOW MODULATION COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHY EXPERIMENTS UNDER DIFFERENT OUTLET PRESSURE
CONDITIONS
Thiago R. Bjerk1, Mariarosa Maimone2, Flavio A. Franchina3, Giorgia Purcaro3, Danilo Sciarrone2, Claudia Zini1,
Peter Q. Tranchida2, Luigi Mondello2,3
1 Instituto de Química - Universidade Federal do Rio Grande do Sul, Av. Bento Gonçalves, 9500 Porto Alegre,
Brazil
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, Polo
Annunziata - viale Annunziata, 98168 Messina, Italy
K.56
INNER AND OUTER INFLUENCES ON WHITE WINE AGEING: REVEALING THEIR IMPACT
BY MULTIVARIATE STATISTICAL PROFILING OF WINE AROMA COMPOUNDS BASED ON
HS-SPME-GC×GC-qMS
Ann-Katrin Walther1, Thomas Roos1, Christof Steingass2, Hans-Georg Schmarr1, Dominik Durner1,3
1 Institute for Viticulture and Oenology - Dienstleistungszentrum Ländlicher Raum Rheinpfalz, Breitenweg 71,
67435 Neustadt, Germany
2 Institute of Food Science and Biotechnology - Hohenheim University, Garbenstraße 25, 70599 Stuttgart,
Germany
3 Department of Applied Logistics and Polymer Sciences - Hochschule Kaiserslautern, Carl-Schurz-Straße
10-16, 66953 Pirmasens, Germany
K.57
GC×GC-HRTOFMS TO BETTER UNDERSTAND CLOAK-AND-DAGGER ACTIVITIES OF
MADAGASCAR MANTELLA FROGS
Pierre-Hugues Stefanuto1, Catherine Brasseur1, Cecchini Harisoa2, Marta Andriantsiferana2, Jean-Francois
Focant1
2 University of Antananarivo, Antananarivo, 1001 Antananarivo, Madagascar
K.58
HIGH-TEMPERATURE GCXGC-TOFMS ANALYSIS AND TWO-DIMENSIONAL SIMULATED
DISTILLATION OF CRUDE OILS
Maximilian K. Jennerwein1,2, Markus Eschner2, Thomas Gröger1, Thomas Wilharm3, Ralf Zimmermann1
1 Comprehensive Molecular Analytics - Helmholtz Zentrum München, Ingolstadter Landstraße 1, 85764 Munich,
Germany
2 R&D - ASG Analytik Service Gesellschaft, Trentiner Ring 30, 86356 Neusäss, Germany
3 Management - ASG Analytik Service Gesellschaft, Trentiner Ring 30, 86356 Neusäss, Germany
K.59
CHARACTERIZATION OF SAFFRON AROMA PROFILE: COMPARISON AMONG PTR-TOFMS, HS-SPME-GC-MS AND HS-SPME-2DGC-MS/TOF
Francesca Ieri1, Pamela Vignolini1, Fabio Villanelli2,3, Eligio Sebastiani2, Luca Calamai4, Elisa Masi5, Stefano
Mancuso5, Annalisa Romani1,3
1 PHYTOLAB laboratory -DiSIA, University of Florence, 50100 Firenze, Italy
2 SRA INSTRUMENTS, Viale Assunta 101, 20063 Cernusco S/N Milano, Italy
3 QuMAP laboratory - PIN Polo Universitario Prato, Prato, 50019 Prato, Italy
4 CNR Consiglio Nazionale delle Ricerche, Sesto Fiorentino, 50019 Sesto Fiorentino, Italy
5 DISPAA, University of Florence, 50100 Firenze, Italy
K.60
QUANTITATIVE AND QUALITATIVE NON-TARGETED ENVIRONMENTAL APPLICATIONS
UTILIZING COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY - TIME-OFFLIGHT MASS SPECTROMETRY
Matias Kopperi, Marja-Liisa Riekkola
Department of Chemistry - University of Helsinki, A.I.Virtasen aukio 1, P.O.BOX 55, FI-00014 Helsinki, Finland
76
K.61
APPLICATION OF MULTI-DIMENSIONAL GAS CHROMATOGRAPHY MASS
SPECTROMETRY TECHNIQUES TO EXPLAIN THE INCREASED SENSITIVITY OF
ATLANTIC HADDOCK EMBRYOS TO CRUDE OIL POLLUTION
Lisbet Soerensen1,2, Steven J. Rowland3, William Robson3, Andy M. Booth4, Svein A. Mjøs2, Sonnich Meier1
1 Department of Environmental Chemistry - Institute of Marine Research, P.O 1870 Nordnes, 5817 Bergen,
Norway
2 Department of Chemistry - University of Bergen, P.O. 7800, 5020 Bergen, Norway
3 Petroleum & Environmental Geochemistry Group, Biogeochemistry Research Centre - University of Plymouth,
Devon, PL4 8AA Plymouth, United Kingdom
4 Environmental Technology - SINTEF Materials and Chemistry, P.O. Box 4760 Sluppen, 7465 Trondheim,
Norway
K.62
GC-MS AND 2DGC-MS/TOF VOLATILE PROFILE OF MONOVARIETAL EXTRA VIRGIN
OILVE OILS
Luca Calamai1, Fabio Villanelli2, Francesca Ieri3, Stefano Mulas3, Eligio Sebastiani4, Annalisa Romani2,3
DISPAA, University of Florence, 50100 Firenze, Italy
QuMAP Laboratory, PIN Polo Universitario Città di Prato, 59100 Prato, Italy
3 PHYTOLAB laboratory - DiSIA - University of Florence, Viale Morgagni 65, 50100 Firenze, Italy
4 SRA INSTRUMENTS, Viale Assunta 101, 20063 Cernusco S/N Milano, Italy
1
2
K.63
TOWARD DEVELOPING A TB BREATHALYZER
Theodore R. Mellors1, Joanne L. Flynn2, Jaime Tomko2, Melanie O'Malley2, Charles A. Scanga2, Philana L. Lin3,
Jane E. Hill1
1 School of Engineering - Dartmouth College, 14 Engineering Drive, 03755 Hanover, United States
2 University of Pittsburgh, 3501 5th Avenue, 15261 Pittsburgh, United States
3 Children's Hospital of UPMC, 4401 Penn Avenue, 15224 Pittsburgh, United States
K.64
LOW EV FRAGMENTATION AS A COMPLEMENTARY TOOL FOR THE EXTENDED LIST OF
SUSPECTED ALLERGENS BY GC×GC-TOFMS – APPLICATION TO ESSENTIAL OILS
Thomas Dutriez1, Laetitia Duffour1, Diane Pétermann1, Laura McGregor2, Nick Bukowski2, Neil Owen3, Greg
Adamson4
1 RAPS Analytical Laboratory - Givaudan, Chemin de la parfumerie 5, 1214 Vernier, Switzerland
2 Markes International Ltd, Gwaun Elai Medi-Science Campus, CF72 8XL Llantrisant, United Kingdom
3 Givaudan UK Ltd, Kennington Road Ashford Kent, TN24 0LT Ashford, United Kingdom
4 Givaudan Fragrances Corp., 717 Ridgedale Avenue, 07936 East Hanover Ridgedale, United States
K.65
MULTIDIMENSIONAL GAS CHROMATOGRAPHIC ANALYSIS OF TRACE OXIDISED
SPECIES IN THERMALLY STRESSED JET FUELS
Renee Webster1,2
1 Australian Centre for Research on Separation Science, School of Chemistry - Monash University, Wellington
Rd, 3800 Clayton, Australia
2 Defence Science Technology Group, 506 Lorimer St, 3207 Fisherman's Bend, Australia
K.66
GC×GC-TOFMS FOR FORENSIC BLOOD VOC PROFILING
Lena M. Dubois, Katelynn A. Perrault, Pierre-Hugues Stefanuto, Jean-François Focant
Department of Chemistry - University of Liège, Allée du 6 Août 11, B6c, 4000 Liège, Belgium
K.67
APPLICATION OF GC×GC-TOF/MS TO THE ASSESSMENT OF THE BIOACCESSIBILITY OF
PCBs IN MEAT AFTER DIGESTION
Christelle Planche1,2, Jérémy Ratel1, Frédéric Mercier1, Cheng Zhang1, Laurent Debrauwer2, Erwan Engel1
1 MASS group - INRA, UR370 QuaPA, 63123 Saint-Genes-Champanelle, France
2 MetaToul-MetaboHUB-AXIOM platform - INRA, UMR1331 TOXALIM, Research Centre in Food Toxicology,
31027 Toulouse, France
77
K.68
IDENTIFICATION OF FOOD CONTAMINANTS FROM HOT-MELT ADHESIVES BY GCXGCMS
Martin Lommatzsch1, Maurus Biedermann2, Konrad Grob2, Thomas J. Simat1
1 Chair of Food Science and Food Contact Materials - TU Dresden, Bergstr. 66, 01062 Dresden, Germany
2 KLZH, Fehrenstr. 15, 8032 Zurich, Switzerland
K.69
COMBINING UNI-AND MULTIVARTIATE STATISTICS FOR THE GAIN OF COMPREHENSIVE
INSIGHT IN THE MOLECULAR COMPOSITION OF PARTICULATE MATTER FROM WOOD
COMBUSTION USING TWO DIMENSIONAL GAS CHROMATOGRAPHY TIME-OF-FLIGHT
MASS SPECTROMETRY
Benedikt Weggler1, Saray LyVerdu1, Maximilian Jennerwein2, Ahmed A. Reda1, Juergen Orasche1, Thomas
Groger1, Ralf Zimmermann1,3
1 Joint Mass Spectrometry Centre/Cooperation Group Comprehensive Molecular Analytics - Helmholtz Zentrum
München, Ingolstädter Landstrasse 1, 85764 Neuherberg, Germany
2 Joint Mass Spectrometry Centre/Cooperation Group Comprehensive Molecular Analytics - Analytical Service
Group, Trentiner Ring 30, 86356 Augsburg, Germany
3 Division of Analytical and Technical Chemistry - University of Rostock, Dr.-Lorenz-Weg 1, 18059 Rostock,
Germany
K.70
GC×GC-TOFMS FOR THE ANALYSIS OF ESPRESSO COFFEE VOLATILE COMPOUNDS:
FROM POWDER TO THE BREW, FROM GLOBAL TO PARTICULAR
Guido R. Lopes1, Andreia S. Ferreira1, Mariana Pinto1, Cláudia P. Passos1, Elisabete Coelho1, Carla
Rodrigues2, Cláudia Figueira2, Manuel A. Coimbra1, Sílvia M. Rocha1
1 QOPNA - Department of Chemistry - University of Aveiro, Campus Universitário de Santiago, 3810-193 Aveiro,
Portugal
2 Diverge, Grupo Nabeiro Innovation Center, Alameda dos Oceanos 65, 1.1, 1990-208 Lisboa, Portugal
K.71
R2D2: AN R PACKAGE FOR THE AUTOMATIC PROFILING OF GC×GC-MS SAMPLES IN
UNTARGETED METABOLOMICS
Xavier Domingo-Almenara1, Alexandre Perera2, Gabriel Vivó-Truyols3, Jesus Brezmes1
1 Metabolomics Platform - DEEEA - Universitat Rovira i Virgili, c/ Paisos Catalans, 26, 43007 Tarragona, Spain
2 B2SLAB, Automatic Control Department - Universitat Politècnica de Catalunya, Campus Diagonal Sud, 08028
Barcelona, Spain
3 Analytical Chemistry Group, Van't Hoff Institute for Molecular Sciences - Universiteit van Amsterdam, Science
Park 9046, 1098 WV Amsterdam, Netherlands
K.72
FUNCTIONALIZED OCTATETRAYNE AS NOVEL CARBON MEDIA FOR COMPREHENSIVE
TWO-DIMENSIONAL GAS CHROMATOGRAPHY
Jiayi Liu1, Susan V. Olesik1, Matthew Giardina2
Department of Chemistry and Biochemistry - The Ohio State University, 100 West 18th Avenue, 43210
Columbus, United States
2 GC&Workflow Automation - Agilent Technologies, 2850 Centerville Rd, 19808 Wilmington, United States
1
K.73
PYROLYSIS TWO-DIMENSIONAL GAS CHROMATOGRAPHY MASS SPECTROMETRY FOR
IDENTIFICATION AND QUANTIFICATION OF POLYOLEFINS
Eric Brander
Analytical Technology - SABIC, Plasticslaan 1, 4600 AC Bergen op Zoom, Netherlands
K.74
APPLICATION OF COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATORGAPHY
MASS SPECTROMETRY FOR POLYMERS USING DIFFERENT SAMPLE INTRODUCTIONS
Eric Brander
Analytical Technology - SABIC, Plasticslaan 1, 4600 AC Bergen op Zoom, Netherlands
78
K.75
THE ANALYSIS OF VOCs IN INDOOR AIR SAMPLES USING TD-GC×GC-TOF-MS INVESTIGATION OF THE ORIGINS OF THE "SICK-BUILDING SYNDROME"
Matyas Ripszam1, Ingrid Liljelind1, Peter Haglund2
1 Department of Occupational and Environmental Medicine - Umeå University, Norrlands Univeristetssjukhus
Building 6B and 6H, 901 85 Umeå, Sweden
2 Department of Chemistry - Umeå University, Linnaeus väg 6, 901 87 Umeå, Sweden
K.76
NEW EXPERIMENTS TO SHOW A PREDICTION MODEL FOR SIMULATION OF A CONTOUR
PLOT FOR GC×GC ANALYSIS
Jan Henk Marsman1,2, Gert-Jan Boer2, Léon Rohrbach1, Hero J. Heeres1
Chem. Engineering - University Groningen, Nijenborgh 4, 9747 AG Groningen, Netherlands
2 University Labs - CS Aspa, Hoevenkamp 5, 9461 HE Gieten, Netherlands
1
K.77
ANALYSIS OF AQUEOUS ENDOCRINE-DISRUPTING PESTICIDES BY GC-ECD WITH STIR
BAR SORPTIVE EXTRACTION USING ELECTROSPUN NANOFIBER
Jen F. Jen
Department of Chemistry - National Chung Hsing University, , 402 Taichung City, Taiwan
K.78
A NEW APPROACH TO CREATING MICROFLUIDIC FLOW SWITCHING DEVICES FOR
COMPLEX CAPILLARY GC APPLICATIONS
James McCurry, Heng He, Matthew Giardina
Gas Phase Division - Agilent Technologies, 2850 Centerville Road, 19808 Wilmington, United States
K.79
GAS VELOCITY CALCULATIONS IN A CHROMATOGRAPHIC SYSTEM: A CRITICAL TOOL
TO OPTIMIZE MODULATION TIMES IN COMPREHENSIVE GAS CHROMATOGRAPHY
USING FORWARD AND REVERSE FILL/FLUSH FLOW MODULATORS
Marie Vaccaro1, Laurence Levacher2, Gaelle Jousset-Semard2, Valerie Agasse-Peulon1, Pascal Cardinael1
1 Sciences et Méthodes Séparatives - University of Rouen, rue Tesnière, 76821 Mont saint aignan, France
2 Total Research & Technology Gonfreville, BP 27, 76700 Harfleur, France
K.80
ORGANOPHOSPHORUS PESTICIDE AND ESTER ANALYSIS BY USING COMPREHENSIVE
TWO-DIMENSIONAL GAS CHROMATOGRAPHY WITH FLAME PHOTOMETRIC DETECTION
Xiangping Liu1, Dengkun Li1, Gavin Rose2, Philip J. Marriott3
Department of Pysical and Chemical Analysis - Nanjing municipal center of disease control and prevention, No
2, Street Zizhulin, Gulou district, Nanjing, Jiangsu, 210003 Nanjing, China
2 Department of Primary Industry Macleod Centre, Ernest Jones Drive, Macleod, 3085 Victoria, Australia
3 School of Chemistry - Monash University, Wellington Rd, 3800 Victoria, Australia
1
K.81
A STANDARDIZED STATIC IN VITRO DIGESTION PROTOCOL FOR THE ASSESSMENT OF
THE BIOACCESSIBILITY OF FOOD CONTAMINANTS BY GCXGC-TOF/MS
Jeremy Ratel1, Christelle Planche1,2, Cheng Zhang1, Frédéric Mercier1, Patrick Blinet1, Laurent Debrauwer2,3,
Erwan Engel1
1 MASS Group - UR370 QuaPA - INRA, Centre INRA de Theix, 63122 Saint-Genes-Champanelle, France
2 Research Centre in Food Toxicology - MetaToul-MetaboHUB-AXIOM platform - UMR1331 TOXALIM - INRA,
180 Chemin de Tournefeuille, 31027 Toulouse, France
3 INPT - UPS - UMR 1331 - Université de Toulouse, 118 Route de Narbonne, 31062 Toulouse, France
K.82
THE USE OF ACCURATE MASS SCRIPTING FUNCTIONS TO DETECT AND IDENTIFY NEW
DISINFECTION BYPRODUCTS IN SWIMMING POOLS AND SPAS
Jonathan D. Byer1, Eric J. Daiber2, Sridevi A. Ravuri2, Joe Binkley1, Susan D. Richardson2
1 LECO Corporation, 3000 Lakeview Avenue, 49085 Saint Joseph, United States
2 Department of Chemistry and Biochemistry - University of South Carolina, 631 Sumter Street, 29208 Columbia,
United States
79
K.83
BREATH GAS MONITORING DURING AN ORAL GLUCOSE TOLERANCE TEST BY A
COMBINED PTR-QUAD-MS/GC×GC–TOFMS APPROACH FOR THE VERIFICATION OF
POTENTIAL VOLATILE BIOMARKERS
Beate Gruber1, Stefan Keller2, Thomas Groger1,3, Georg Matuschek2, Ralf Zimmermann1,3
Comprehensive Molecular Analytics - HelmholtzZentrum münchen, Ingolstaedter Landstrasse 1, 85764
Neuherberg, Germany
2 Research Unit Medical Radiation Physics and Diagnostics - Helmholtz Zentrum München, Ingolstädter Landstr.
1, 85764 Neuherberg, Germany
3 Joint Mass Spectrometry Centre - University of Rostock, Dr. Lorenz Weg 1, 18059 Rostock, Germany
1
K.84
FLOW-MODULATED COMPREHENSIVE 2D GAS CHROMATOGRAPHY COMBINED WITH
VACUUM ULTRAVIOLET DETECTOR FOR THE ANALYSIS OF COMPLEX MIXTURE
Mariosimone Zoccali1, Margita Utczas1, Giorgia Purcaro1, Peter Q. Tranchida2, Kevin A. A. Schug3, Luigi
Mondello1,2
3 Chemistry and Biochemistry - University of Texas at Arlington, 700 Planetarium PI., Box 19065, TX 76019-0065
_____________________________________________________________________________
K*. OTHER COMPREHENSIVE TECHNIQUES
_____________________________________________________________________________
K*.01
COMPREHENSIVE TWO DIMENSIONAL LIQUID CHROMATOGRAPHY IN DETERMINATION
OF PHOSPHOLIPIDS ISOLATED FROM EGG YOLK
Justyna Walczak1, Szymon Bocian2, Boguslaw Buszewski2
Department of the Environmental Chemistry and Bioanalytics - Faculty of Chemistry, 7 Gagarin St., 87-100
Torun, Poland
2 Department of the Environmental Chemistry and Bioanalytics - Faculty of Chemistry, Nicolaus Copernicus
University in Torun, 7 Gagarin St., 87-100 Torun, Poland
1
K*.02
COMPREHENSIVE LIPID PROFILING IN MUSSEL SAMPLES BY COMPREHENSIVE LIQUID
CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY
Paola Donato1, Francesca Rigano2, Ambrogina Albergamo3, Francesco Cacciola1, Marco Beccaria2, Paola
Dugo3,2, Luigi Mondello3,2
Messina, Viale Consolare Valeria, 98125 Messina, Italy
K*.03
COMPREHENSIVE TWO-DIMENSIONAL LIQUID CHROMATOGRAPHY FOR
CHARACTERIZATION OF FOOD CAROTENOIDS
Domenica Mangraviti1, Francesco Cacciola2, Daniele Giuffrida2, Margita Utczas3, Paola Donato2, Paola Dugo1,3,
Luigi Mondello1,3
Annunziata, Polo Annunziata, 98168 Messina, Italy
Messina, via Consolare Valeria, 98125 Messina, Italy
80
K*.04
ON-LINE COUPLING OF ULTRA PERFORMANCE CONVERGENCE CHROMATOGRAPHY
AND ULTRA HIGH PRESSURE LIQUID CHROMATOGRAPHY FOR BOOSTING
ORTHOGONALITY IN COMPREHENSIVE SEPARATIONS
Paola Donato1, Veronica Inferrera2, Daniele Giuffrida1, Francesco Cacciola1, Paola Dugo2,3, Luigi Mondello2,3
Messina, Via Consolare Valeria , 98125 Messina, Italy
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, viale
_____________________________________________________________________________
L. TRACE ANALYSIS
_____________________________________________________________________________
L.01
SOLVENT EVOLUTION ASSESSMENT IN BLOCK COPOLYMER ULTRATHIN FILMS FOR
NANO-TECHNOLOGICAL APPLICATIONS
Valentina Gianotti1, Diego Antonioli1, Katia Sparnacci1, Michele Laus1, Tommaso J. Giammaria2, Monica
Ceresoli2, Gabriele Seguini2, Michele Perego2
1 DISAV Dipartimento di Scienze dell'Ambiente e della Vita - University of Piemonte Orientale, Viale T. Michel 11,
15121 Alessandria, Italy
2 Laboratory MDM - IMM-CNR, Agrate Brianza, 20864 Agrate Brianza, Italy
L.02
OCURRANCE OF ANTIHYPERTENSIVE DRUGS BY SPE-GC/MS-MS IN SURFACE WATER
IN SOUTH REGION OF BRAZIL
Rodrigo A. Osawa1,2, Alessandra H. Ide1,3, Júlio César R. De Azevedo4
1 Department of Chemistry and Biochemistry - Faculty of Sciences University of Lisbon, R. Ernesto de
Vasconcelos, 1749-016 Lisbon, Portugal
2 Graduate Program on Water Resources and Environmental Engineering - Federal University of Paraná, Caixa
Postal 19011 – Jardim das Américas, 81531-990 Curitiba, Brazil
3 CAPES Foundation- Ministry of Education of Brazil, SBN, Quadra 02, Lote 06, Bloco L,, 70040-020 Brasília,
Brazil
4 Graduate Program Environmental Science and Technology - Federal University of Technology - Paraná,
Deputado Heitor de Alencar Furtado, 5000, 81280-340 Curitiba, Brazil
L.03
FAST SCREENING, IDENTIFICATION AND QUANTIFICATION OF PESTICIDE RESIDUES IN
BABY FOOD USING GC ORBITRAP MS TECHNOLOGY
Dominic Roberts1, Cristian Cojocariu2, Richard Fussell2, Paul Silcock2, Mike Hetmanski3
1 GC-MS - Thermo Fisher Scientific, Tudor Road, WA7 1TA Runcorn, United Kingdom
2 Thermo Fisher Scientific, Manor Park, WA7 1TA Runcorn, United Kingdom
3 FERA, Sand Hutton, YO41 1LZ York, United Kingdom
L.04
INSTRUMENT PERFORMANCE STANDARDS: QUICK AND EFFICENT TESTING OF GC/MS
SENSITIVITY AND PERFORMANCE FOR THE ANALYSIS OF DIOXINS AND FURANS
Dirk Krumwiede, Heinz Mehlmann
Marketing - Thermo Fisher Scientific, Hanna-Kunath-Str. 11, 28199 Bremen, Germany
L.05
USING GC-MS/MS AS A CONFIRMATORY METHOD FOR DIOXIN-LIKE PCBS IN FOOD AND
FEED
Dominic Roberts1, Esteban A. Holgado2, Cristian Cojocariu1, Inge d. Dobbeleer1
1 Thermo Fisher Scientific, Tudor Road, WA7 1TA Runcorn, United Kingdom
2 CSIC - Spanish Council for Scientific Research (CSIC), c/ Jordi Girona, 18-26, 08034 Barcelona, Spain
81
L.06
DOUBLED SAMPLE TROUGHPUT FOR DIOXINS AND OTHER POPS: THE DUAL DATA
CONCEPT ON THE BASIS OF A DUAL GC MASS SPECTROMETER
Heinz Mehlmann, Dirk Krumwiede
POPs Center of Excellence - Thermo Fisher Scientific, Hanna-Kunath-Str. 11, 28199 Bremen, Germany
L.07
IDENTIFICATION OF LEACHABLE IMPURITIES FROM PHARMACEUTICAL CONTAINER
CLOSURE MATERIALS USING ORBITRAP BASED GC-MS
Dominic Roberts1, Andrew Feilden2, Paul Silcock3, Kyle DSilva1, Richard Barlow2
1 GC-MS - Thermo Fisher Scientific, Tudor Road, WA7 1TA Runcorn, United Kingdom
2 Smithers RAPRA, Shawbury, SY4 4NR Shawbury, United Kingdom
3 Thermo Fisher Scientific, Tudor Road, WA7 1TA Runcorn, United Kingdom
L.08
DETERMINATION OF THCCOOH TRACE IN HAIR WITH GCQQQ ACCORDING TO THE
LOWEST LIMIT REQUESTED BY THE REGULATION
Elena Ciceri, Inge de Dobbeleer, Tommaso Albertini, Andrea Caruso
Thermo, Strada Rivoltana, 20090 Rodano (MI), Italy
L.09
ANALYSIS OF MOSH AND MOAH IN PAPER-BASED PACKAGING MATERIAL USING GC–
VUV
Sjaak de Koning, Larissa Ram
Da Vinci Laboratory Solutions, Cairostraat 10, 3047BC Rotterdam, Netherlands
L.10
STUDY OF BIOGENIC VOLATILE ORGANIC COMPOUNDS (BVOCs) EMMITED FROM
MYRTUS COMMUNIS L. GROWING IN ALGERIA
Yazid Foudil-Cherif1, Noureddine Yassaa1,2
1 Faculté de Chimie, - USTHB, BP32, 16111 Bab-Ezzouar, Alger, Algeria
2 Centre de Développement des Energies Renouvelables - CDER, BP62 Route de l'Observatoire, Bouzareah,
16000 Algiers, Algeria
L.11
RAPID HPLC DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAHS) IN
CHESTNUTS FLOUR
Chiara Conchione1, Sabrina Moret1, Lanfranco S. Conte1, Jean Daniel Coisson2, Marco Arlorio2
1 Department of Agricultural, Food, Environmental and Animal Sciences - University of Udine, Via Sondrio 2A,
33100 Udine, Italy
2 Department of Pharmaceutical Sciences - University of Piemonte Orientale A. Avogadro, Largo Donegani 2,
28100 Novara, Italy
L.12
GC-MS ANALYSIS OF PIMPINILLA ANISUM BIOACTIVE EXTRACTS: ANTIOXIDANT AND
ANTIBACTERIAL ACTIVITIES
Ali Boudina, Kaouthar Ayache, Soumia Boulahlib, Yazid Foudil-Cherif
Chemistry - USTHB, El-Alia, BP 32 Bab-Ezzouar, Alger, Algeria
L.13
TOWARDS ULTIMATE SENSITIVITY FOR THE ANALYSIS OF PERSISTENT ORGANIC
POLLUTANTS (POPs)
Francesca Rigano1, Jody Dunstan2, Francisco Ferron3, Davy Petit4, Luigi Mondello5,1
2 Waters Corporation, Stamford Avenue, Altrincham Road, SK9 4AX Wilmslow, United Kingdom
3 Waters S.p.A., Viale dell'Innovazione 3, 20126 Milan, Italy
4 Waters S.A.S., BP 608, 78056 Saint-Quentin En Yvelines Cedex, France
82
_____________________________________________________________________________
M. ENVIRONMENTAL APPLICATIONS
_____________________________________________________________________________
M.01
DETERMINATION OF PCBs AND DDT IN BIOTA OF LAKE BAIKAL
Olga V. Kustova, Alexander G. Gorshkov
Laboratory of Chromatography - Limnological Institute Siberian Branch of Russian Academy of Sciences, 3,
Ulan-Batorskaya St., P.O. Box 278, 664033 Irkutsk, Russia (Russian Fed.)
M.02
UNRAVELLING THE PRESENCE OF ORGANIC COMPOUNDS IN MOONMILK FROM A
LAVA CAVE BY ANALYTICAL PYROLYSIS (Py-GC/MS)
Ana Z. Miller1, José M. De La Rosa1, José A. Gonzalez-Perez1, Nicasio T. Jiménez-Morillo1, Octavio
Fernández2, Cesareo Saiz-Jimenez1
Instituto de Recursos Naturales y Agrobiología de Sevilla (IRNAS-CSIC), Reina Mercedes Av. 10., 41012
Seville, Spain
2 Grupo de Espeleología Tebexcorade La Palma, Santa Catalina, 14, 38700 S.C. La Palma, Spain
1
M.03
IDENTIFICATION OF EMERGING CONTAMINANTS IN THE ENVIRONMENT BY LC/Q-TOF
MS USING SUSPECT AND NON-TARGET SCREENING WORKFLOWS COMBINED WITH
COMMERCIAL AND OPEN-SOURCE MS/MS LIBRARIES
Nicola Cimino1, Sascha Lege2, Jean Daniel Berset3, Thomas Glauner4, Christian Zwiener2
1 Agilent Italia, Via V. Lamaro, 13, 00173 Roma, Italy
2 Eberhard Karls University, Hölderlinstraße 12, 72074 Tuebingen, Germany
3 Water and Soil Protection Laboratory, Reiterstrasse 11, 3011 Bern, Switzerland
4 Agilent Technologies, Hewlett Packard Strasse 8, 76337 Waldbronn, Germany
M.04
GC/MS SCREENING OF WATER SAMPLES FOR ORGANIC POLLUTANTS BY STIR BAR
SORPTIVE EXTRACTION (SBSE)
Oliver Lerch1, Jasmin Zboron1, Andreas Hoffmann1, Chris Sandy2
2 Agilent Technologies, 5500 Lakeside, Cheshire SK8 3GR Cheadle, United Kingdom
M.05
DETERMINATION OF SOME EMERGING CONTAMINANTS IN FRESHWATER
INVERTEBRATES USING A DEVELOPED QUECHERS EXTRACTION TECHNIQUE AND AN
ADVANCED ORBITRAP SYSTEM
Jalal T. Althakafy1,2, Chadin Kulsing1, Erinn Richmond3, Michael R. Grace3, Philip J. Marriott1
1 Australian Centre of Research on Separation Science, School of Chemistry, Faculty of Science - Monash
University, VIC, 3800 Clayton, Australia
2 Department of Chemistry, Faculty of Applied Sciences - Umm Al-Qura University, Makkah, 21955 Makkah,
Saudi Arabia
3 Water Studies Centre, School of Chemistry, Faculty of Science - Monash University, VIC, 3800 Clayton,
Australia
M.06
SPE-GC-MS/MS FOR THE DETERMINATION OF PHARMACEUTICAL AND PERSONAL
CARE PRODUCTS IN BRAZILIAN WATERS
Alessandra H. Ide1,2, Rodrigo A. Osawa2, Júlio César R. Azevedo3
1 Departamento de Química e Bioquímica - Faculdade de Ciências da Universidade de Lisboa, Campo Grande,
Ed C8, 1749-016 Lisboa, Portugal
2 CAPES Foundation - Ministry of Education of Brazil, SBN, Quadra 02, Lote 06, Bloco L, 70040-020 Brasília,
Brazil
3 UTFPR, Deputado Heitor Alencar Furtado, 4900, 81280-340 Curitiba, Brazil
83
M.07
DEVELOPMENT OF A LC-MS/MS METHOD FOR THE DETERMINATION OF NINE
PHARMACEUTICAL COMPOUNDS IN SURFACE WATER SAMPLES
Rodrigo A. Osawa1,2, Maria Helena Florêncio1, Maria Rosário Bronze3,4
1 Department of Chemistry and Biochemistry - Faculty of Sciences University of Lisbon, R. Ernesto de
Vasconcelos, 1749-016 Lisbon, Portugal
2 CAPES Foundation- Ministry of Education of Brazil, SBN, Quadra 02, Lote 06, Bloco L, 70040-020 Brasília,
Brazil
3 Institute for Experimental Biology and Technology, Apartado 12, 2780-901 Oeiras, Portugal
4 Faculty of Pharmacy University of Lisbon, Av. Prof. Gama Pinto, 1649-019 Lisbon, Portugal
M.08
ENVIRONMENTAL FRIENDLY METHOD FOR MYCOTOXINS (AFB1 AND ZEA)
DETERMINATION IN SOIL
Nathalie Zamariola, Mary R. Marchi
Department of Analitycal Chemistry - Institute of Chemistry, Unesp, Rua Prof. Francisco Degni, 55. Quitandinha,
14800-060 Araraquara, Brazil
M.09
DETERMINATION OF TOTAL PETROLEUM HYDROCARBONS IN RUBBLE AND SOILS BY
ACCELERATED SOLVENT EXTRACTION AND GC-FID
Fabrizio Galbiati1, Luca Teli2, Inge d. Dobbeleer1
1 Thermo Fisher Scientific, Im Steingrund, 63303 Dreieich, Germany
2 Consulenze Ambientali SpA, Via A. Moro 1, 24020 Bergamo, Italy
M.10
DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) IN SOILS AND SOLID
WASTE BY ACCELERATED SOLVENT EXTRACTION AND GC-MS/MS
Elena Ciceri1, Fabrizio Galbiati2, Luca Teli3
1 Thermo, Strada Rivoltana, 20090 Rodano (MI), Italy
2 Thermo Fisher Scientific, Schweiz, 4153 AG, Reinach, Switzerland
3 Consulenze Ambientali SpA, Via Aldo Moro, 24020 Scanzorosciate, Italy
M.11
SOURCE IDENTIFICATION OF BEACHED OIL AT AL ZUBARAH, NORTWESTERN QATAR
Mette Kristensen1, Nasser S. Al-Kaabi2, Jan H. Christensen1
1 Department of Plant and Environmental Sciences - University of Copenhagen, Thorvaldsensvej 40, 1871
Frederiksberg C, Denmark
2 Department of Environmental Science - Qatar University, Al Tarfa, 2713 Doha, Qatar
M.12
DETERMINATION OF PM2.5-BOUND POLYCYCLIC AROMATIC HYDROCARBONS AND
OXYGENATED POLYCYCLIC AROMATIC HYDROCARBONS IN AN URBAN ENVIRONMENT
Zoltán Nyiri1, Tamás Szigeti2, Márton Novák1, Bálint Sámuel Szabó1, Zsuzsanna Eke1,3
1 Joint Research and Training Laboratory on Separation Techniques - Eötvös Loránd University, Pázmány Péter
sétány 1/A, 1117 Budapest, Hungary
2 Cooperative Research Centre for Environmental Sciences - Eötvös Loránd University, Pázmány Péter sétány
1/A, 1117 Budapest, Hungary
3 WESSLING International Research and Educational Center, Fóti út 56., 1047 Budapest, Hungary
M.13
DETERMINATION OF BENZOTHIAZOLES, BENZOTRIAZOLES AND
BENZENESULFONAMIDES IN MARINE ORGANISMS BY GAS CHROMATOGRAPHY-ION
TRAP-TANDEM MASS SPECTROMETRY
Laura Trabalón1, Martí Nadal2, Jose Luis Domingo2, Francesc Borrull1, Eva Pocurull1
Chemistry and Organic Chemistry - University Rovira i Virgili, Marcel-li Domingo s/n, 43007
Tarragona, Spain
2 Laboratory of Toxicology and Environmental Health - Universitat Rovira i Virgili, Sant Llorenç, 21, 43201 Reus,
Spain
1 Analytical
84
M.14
INTERLABORATORY STUDY ON THE ANALYSIS OF CHLORINATED PARAFFINS IN
ENVIRONMENTAL MATRICES
Louise van Mourik1,2, Ike van der Veen1, Steven Crum3, Wim Cofino3, Jacob de Boer1
1 Institute for Environmental Studies (IVM) \ Chemistry & Biology - VU University, De Boelelaan 1087, 1081HV
2 National Research Centre for Environmental Toxicoligy (ENTOX) - University of Queensland, 39 kessels road,
4108 Coopers Plains, Australia
3 QUASIMEME Laboratory Performance Studies - Wageningen University and Research Centre, PO box 8005,
6700EC Wageningen, Netherlands
M.15
INVESTIGATIONS ON THE METABOLISM OF PHARMACEUTICALS IN PLANTS
Lisa Emhofer, Wolfgang Buchberger, Christian W. Klampfl
Institute of Analytical Chemistry - Johannes Kepler-University, Austria, Altenbergerstr 69, 4040 Linz, Austria
M.16
VERSATILE MAGNETIC CARBON NANOTUBES METHOD FOR THE DETERMINATION OF
PESTICIDES IN REAL WATER SAMPLES BY GC/MS
Frederico H. Barbosa1, Helvécio C. Menezes1, Ana Paula C. Teixeira1, Philippe Serp2, Zenilda L. Cardeal1
Department of Chemistry - Universidade Federal de Minas Gerais, Av. Antonio Carlos, 6627, 31270901 Belo
Horizonte, Brazil
2 Université de Toulouse, UPS-INP-LCC 4 allée Emile Monso BP 44362, 31030 Toulouse, France
1
M.17
PASSIVE COLLECTION OF VOLATILE AND SEMI-VOLATILE COMPOUNDS IN AIR USING A
NOVEL ADSORBENT SAMPLER WITH DIRECT, RAPID INJECTION INTO A CAPILLARY GCMS WITHOUT SECONDARY FOCUSING
Daniel B. Cardin, Daniel J. Cardin, Thomas X. Robinson
Analytical Instrumentation - Entech Instruments, Inc., 2207 Agate Ct., 93065 Simi Valley, United States
M.18
IMPLEMENTATION AND VALIDATION OF AN ANALYTICAL PLATFORM TO ASSESS THE
IMPACT OF TOBACCO PRODUCTS ON INDOOR AIR QUALITY
Manuel Tharin, Emmanuel Rouget, Nicolas Mottier
R&D - Philip Morris International, Quai Jeanrenaud 5, 2000 Neuchatel, Switzerland
_____________________________________________________________________________
N. ENERGY, PETROCHEMISTRY AND INDUSTRIAL APPLICATIONS
_____________________________________________________________________________
N.01
HPLC-MS AS IMPORTANT TOOL FOR THE ANALYSIS OF THE ANTIOXIDATIVE
MECHANISM OF STABILIZERS IN ENGINE OILS
Georg Kreisberger, Wolfgang Buchberger, Christian Klampfl
Institue of Analytical Chemsitry - Johannes Kepler University, Altenbergerstrasse 69, 4040 Linz, Austria
N.02
DEVELOPMENT OF ORIGINAL ANALYTICAL STRATEGIES FOR THE MONITORING OF
GASEOUS EMISSIONS FROM SOLVENTS USED FOR CO2 CAPTURE PILOT PLANTS
Lorena Cuccia1,2, José Dugay1, Domitille Bontemps3, Véronique Bellosta4, Myriam Louis-Louisy3, Jérôme Vial1
1 Laboratoire Sciences Analytiques Bioanalytiques et Miniaturisation (LSABM) - ESPCI ParisTech, 10 rue
Vauquelin, 75005 Paris, France
2 ADEME, 20 avenue du Grésillé, 49004 Angers, France
3 EDF R&D, 6 quai Watier, 78401 Chatou, France
4 Laboratoire de Chimie Organique - ESPCI ParisTech, 10 rue Vauquelin, 75005 Paris, France
85
N.03
HPLC-MS AS A TOOL FOR STUDYING INTERACTIONS BETWEEN STABILIZERS USED IN
PLASTIC MATERIALS
Leila Maringer1, David Nitsche2, Wolfgang Buchberger1
1 Institute of Analytical Chemistry - Johannes Kepler University Linz, Altenberger Str. 69, 4040 Linz, Austria
2 AGRU Kunststofftechnik GmbH, Ing.-Pesendorfer-Straße 31, 4050 Bad Hall, Austria
N.04
PDMS OVERCOATED SOLID PHASE MICRO EXTRACTION FILM IN DIRECT IMERSION
MODE FOR THE CHARACTERIZATION OF PHENOLS IN AQUEOUS PHASE ORIGINATED
FROM RESIDUAL BIOMASS PYROLYSIS
Francieli M. Mayer1, Erica A. Souza-Silva1, Elina B. Caramão2, Claudia A. Zini1
N.05
PYROLYSIS OF MINERAL COAL: CHARACTERIZATION OF N-COMPOUNDS BY GC×GC/
qMS
Jaqueline Franciele d. Teles1, Jefferson C. Almeida1, Bruna Onorevoli2, Juliana M. da Silva2, Maria Elisabete
Machado2, Elina B. Caramao2
1 Programa de Pós Graduação em Biotecnologia Industrial - Universidade Tiradentes, UNIT, av. Murilo Dantas,
300, 49032490 Aracaju, Brazil
N.06
SAMPLE FLOW PATH DEACTIVATION FOR ANALYSIS OF LOW-PPM LEVELS OF ACTIVE
SULFUR COMPOUNDS USING MICRO GAS CHROMATOGRAPHY
Remko van Loon1, Coen Duvekot2
2 Micro GC Product Marketing - Agilent Technologies, Herculesweg 8, 4338 PL Middelburg, Netherlands
1
N.07
HYPHENATION OF GC AND APCI-FT-ICR-MS FOR ANALYSIS OF PYROLYSIS OILS FROM
A GERMAN BROWN COAL
Jan Zuber, Marius Kroll, Philipp Rathsack, Matthias Otto
Faculty of Chemistry and Physics - Institute of Analytical Chemistry, Leipziger Strasse 29, 09599 Freiberg,
Germany
N.08
DIATOSORB W, A NEW HIGH PERFORMANCE CHROMATOGRAPHIC DIATOMACEOUS
EARTH USED AS SUPPORT IN PACKED COLUMNS
Jaap de Zeeuw
N.09
PYROLYSIS OF AGRO-INDUSTRIAL RESIDUES OF COFFEE, SUGARCANE STRAW AND
COCONUT-FIBERS IN A SEMI-PILOT PLANT FOR PRODUCTION OF BIO-OILS: GASCHROMATOGRAPHIC CHARACTERIZATION
Elina B. Caramao1, Mozart D. Bispo2, Laiza C. Krause2
2 Unit, av. Murilo Dantas, 300, 49032-490 Aracaju, Brazil
86
_____________________________________________________________________________
O. BIOMEDICAL AND PHARMACEUTICAL APPLICATIONS
_____________________________________________________________________________
O.01
NEW LIQUID PHASE MICROEXTRACTION METHOD TO ANALYZE BISPHENOL A AND
PLASTICIZERS METABOLITES IN URINE SAMPLES USING GAS CHROMATOGRAPHY /
MASS SPECTROMETRY
Miriany Moreira1, Leiliane Andre2, Zenilda Cardeal1
1 Departament of Chemistry - UFMG, Av. Antonio Carlos, 6627, 31270010 Belo Horizonte, Brazil
2 Department of Clinical and Toxicological Analysis - UFMG, Av. Antonio Carlos, 6627, 31270010 Belo Horizonte,
Brazil
O.02
DISCRIMINATION AMONG DIFFERENT FORMS OF CANCER BASED ON URINARY
VOLATOMIC COMPOSITION. THE CASE STUDY OF BREAST AND LUNG CANCERS
Carina Cavaco1, Michael Caldeira1, Fernando Aveiro2, Jorge Pereira1, José S. Câmara1,3
Chemistry and Enology Lab - Centro de Química da Madeira, Universidade da Madeira, Campus da
Penteada, 9000-390 Funchal, Portugal
2 Centro Hospitalar do Funchal, Serviço de Hematoncologia, Avda. Luís de Camões, Nº 57, 9050-514 Funchal,
Portugal
3 Faculdade de Ciências Exactas e da Engenharia - Universidade da Madeira, Campus da Penteada, 9000-390
Funchal, Portugal
1 Analytical
O.03
EXTRACTABLES AND LEACHABLES ANALYSIS OF IV BAG SYSTEMS USING THERMAL
DESORPTION AND STIR BAR SORPTIVE EXTRACTION WITH GC SINGLE QUAD AND GC
TIME-OF-FLIGHT MASS SPECTROMETRIC DETECTION
Andreas Hoffmann1, Thomas Albinus1, Elizabeth Almasi2, Kurt Thaxton3
2 Agilent Technologies, 5301 Stevens Creek Boulevard, 95051 Santa Clara, United States
3 Gerstel, Inc., 701 Digital Drive, Suite J, 21090 Linthicum, United States
O.04
FULLY AUTOMATED GC/MS DETERMINATION OF THC, CBN AND CBD IN HAIR BY GC/MS
Oliver Lerch, Carlos Gil
Analytical Services - Gerstel GmbH & Co.KG, Eberhard-Gerstel-Platz 1, 45473 Mülheim an der Ruhr, Germany
O.05
RAPID DETERMINATION OF DRUG PROTEIN BINDING AFFINITY USING SOLID PHASE
MICROEXTRACTION (SPME)
Len Sidisky, Emily Barrey, Craig Aurand
O.06
ANALYSIS OF LIPID PROFILE IN HUMAN LIPID STORAGE MYOPATHIES
Marco Beccaria1, Giorgia Purcaro1, Marianna Oteri2, Giuseppe Micalizzi1, Paola Dugo2,1, Luigi Mondello2,1
1 Chromaleont s.r.l., viale Boccetta, 70, 98122 Messina, Italy
87
O.07
SALIVARY VOLATOMIC PROFILES AS A POWERFUL AND NON-INVASIVE APPROACH TO
DISCRIMINATE DIFFERENT FORMS OF CANCERS. A PRELIMINARY STUDY WITH
BREAST AND LUNG CANCER PATIENTS
Carina Cavaco1, Michael Caldeira1, Fernando Aveiro2, Jorge A. Pereira1, José S. Câmara1,3
1 Analytical Chemistry and Enology Lab - Centro de Química da Madeira, Universidade da Madeira, Campus da
2 Centro Hospitalar do Funchal, Serviço de Hematoncologia, Avda. Luís de Camões, Nº 57, 9050-514 Funchal,
Portugal
Funchal, Portugal
O.08
APPLICATION OF ZIC-HILIC AND RP MONOLITHIC SILICA CAPILLARIES IN LC-MS
ANALYSIS OF BIOMOLECULES
Vanessa Flink1, Stephan Altmaier1, Egidijus Machtejevas1, Klaus Buckendahl2, Frank Michel2, Anders
Fridstrom3, Mike Buchanan4
Merck KGaA, Frankfurter Str. 250, 64293 Darmstadt, Germany
3 Sigma-Aldrich International GmbH, Wassergasse 7, CH-9000 St. Gallen, Switzerland, CH-9000 St. Gallen,
Switzerland St. Gallen, Switzerland, Switzerland
4 Sigma-Aldrich/Supelco, 595 N. Harrison Rd., 16823 Bellefonte, United States
1
O.09
HUMAN URINARY METABOLIC SIGNATURES BY PARALLEL DUAL SECONDARY
COLUMN-DUAL DETECTION TWO-DIMENSIONAL COMPREHENSIVE GAS
CHROMATOGRAPHY: RELIABLE TARGETED AND UNTARGETED COMPARATIVE
ANALYSIS
Davide Bressanello1,1, Erica Liberto1, Davis W. Rempe2, Qingping Tao3, Stephen E. Reichenbach2, Stefano
Balducci4, Elisa Benetti1, Carlo Bicchi1, Chiara E. Cordero1
1 Dipartimento di Scienza e Tecnologia del Farmaco - University of Turin, Via Pietro Giuria, 9, I-10125 I-10125,
Italy
2 Computer Science and Engineering Department - University of Nebraska, R Street, 1400 Lincoln, United States
3 GC Image LCC, PO Box, 57403 Lincoln, United States
4 La Sapienza University, Piazzale Aldo Moro 5, 00185 Roma, Italy
O.10
ANALYTICAL METHODOLOGIES INVOLVED IN COMPREHENSIVE IDENTIFICATION OF
GLYCANS IN HUMAN URINARY EXOSOMES
Helena Soini, Guozhang Zou, Solomon T. Gizaw, Milos V. Novotny
Department of Chemistry - Indiana University, 800 E Kirkwood Avenue, 47405-4001 Bloomington, IN, United
States
O.11
SCREENING OF TARGET BINDING OF IRREVERSIBLE JNK3 INHIBITORS ON PEPTIDE
AND INTACT PROTEIN LEVEL BY MICROFLOW LC-QTOF-MS
Adrian Sievers-Engler1, Felix Muth2, Silke M. Bauer2, Stefan Laufer2, Michael Lämmerhofer2
1 Institute of Pharmacy, Lämmerhofer Group - University of Tübingen, Auf der Morgenstelle 8, 72076 Tübingen,
Germany
2 Institute of Pharmaceutical Sciences - University of Tübingen, Auf der Morgenstelle 8, 72076 Tübingen,
Germany
O.12
OBETICHOLIC ACID BIODISTRIBUTION AND METABOLISM IN CIRROTHIC RATS BY
MEANS OF LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY ANALYSIS
Aldo Roda1, Rita Aldini2, Cecilia Camborata1, Silvia Spinozzi1, Placido Franco1, Massimiliano Cont3, Antonietta
D'Errico4, Francesco Vasuri4, Alessio Degiovanni4, Lorenzo Maroni4, Emanuele Porru1, Luciano Adorini5
1 Department of Chemistry - University of Bologna, Via Selmi 2, 40126 Bologna, Italy
2 Department of Pharmacy and Biotechnology - University of Bologna, Via S. Donato 15, 40126 Bologna, Italy
3 INBB, Viale delle Medaglie D'Oro, 305, 00136 Roma, Italy
4 DIMES Department - University of Bologna, Via Massarenti 9, 40138 Bologna, Italy
5 Intercept Pharmaceuticals, 450 W 15th Street, 10011 New York, United States
88
O.13
DETERMINATION OF METOPROLOL ENANTIOMERS IN HUMAN PLASMA AND SALIVA
SAMPLES UTILIZING MICROEXTRACTION BY PACKED SORBENT AND LIQUID
CHROMATOGRAPHY–TANDEM MASS SPECTROMETRY
Hatem A. Elmongy, Mohamed Abdel-Rehim
Department of Environmental Science and Analytical Chemistry - Stockholm University, Svante Arrhenius väg
16C, SE-10691 Stockholm, Sweden
O.14
SIMPLE AND SENSITIVE METHOD FOR AMINO ACIDS ANALYSIS IN HUMAN CELLS
USING LIQUID CHROMATOGRAPHY-ION-TRAP-TIME-OF-FLIGHT MASS SPECTROMETRY
Eliane Nascimento1, Helvecio C. Menezes1, Rodrigo R. Resende2, Zenilda L. Cardeal1
1 Department of Chemistry - Universidade Federal de Minas Gerais, Av. Antonio Carlos, 6627, 31270901 Belo
Horizonte, Brazil
2 Department of Biology - Universidade Federal de Minas Gerais, Av. Antonio Carlos, 6627, 31270901 Belo
Horizonte, Brazil
O.15
HIGH-THROUGHPUT SCREENING FOR DRUGS OF ABUSE AND PHARMACEUTICAL
DRUGS IN HAIR BY LIQUID-CHROMATOGRAPHY-HIGH RESOLUTION MASS
SPECTROMETRY (LC-HRMS)
Sara Odoardi, Fabio De Giorgio, Sabina Strano-Rossi
Institute of Public Health, Sction of Legal Medicine - Catholic University of Sacred Heart, L.go F. Vito, 1, 00168
Rome, Italy
O.16
PERSPECTIVES ON TESTS AND MEASUREMENT FOR LEGAL PURPOSES: QUALITATIVE
VALIDATION FOR CONFIRMATION OF SEIZED DRUGS BY GC-MS
Adriaan A. Marais1, Johannes B. Laurens2
1 Forensic Chemistry Section - South African Police Service, 270 Pretoria Street, 0184 Pretoria, South Africa
2 Department of Chemistry - University of Pretoria, Lynnwood Road, 0002 Pretoria, South Africa
O.17
HPLC-ESI-QTOF-MS/MS BASED METABOLIC PROFILING OF MAMMALIAN CELL LINES
WITH DATA-INDEPENDENT SWATH ACQUISITION
Corinna Sanwald, Michael Lämmerhofer
Pharmaceutical (Bio)analysis - Institute of Pharmaceutical Sciences, University of Tuebingen, Auf der
Morgenstelle 8, 72076 Tuebingen, Germany
O.18
HPLC-MS TRACING OF SUBCLINICAL INFLAMMATION MOLECULAR MECHANISM IN
ETHIOPATOGENESIS OF DM2
Petr Kacer, Marek Kuzma
Department of Organic Technology - ICT-Prague, Technicka 5, 166 28 Prague 6, Czech Republic
O.19
A POWERFUL STRATEGY BASED ON HS-SPME/GC-MS TO ESTABLISH THE VOLATOMIC
PROFILE OF VACCINIUM PADIFOLIUM AT DIFFERENT RIPENING STAGES
José A. Figueira1, Priscilla Porto-Figueira1, Jorge A. Pereira1, José S. Câmara1,2
1 Analytical Chemistry and Enology Lab - Centro de Química da Madeira, Campus da Penteada, 9000-390
Funchal, Portugal
Funchal, Portugal
O.20
AN EFFICIENT ANALYTICAL METHOD FOR DETERMINATION OF SPHENYLMERCAPTURIC ACID (SPMA) IN URINE BY HPLC FLUORIMETRIC DETECTOR TO
ASSESSING BENZENE EXPOSURE
Michele Mendes, Josianne N. Silveira, Leiliane Andre
Department of Clinical and Toxicological Analysis - UFMG, Av. Antonio Carlos, 6627, 31270010 Belo Horizonte,
Brazil
89
_____________________________________________________________________________
P. ANALYSIS OF NATURAL PRODUCTS, FOOD, FLAVOURS AND
FRAGRANCES
_____________________________________________________________________________
P.01
STUDY OF WINE AROMA RELEASE THROUGH CONSECUTIVE EXTRACTIONS DHS-TDGC-MS
Yan Wen, Ricardo Lopez, Vicente Ferreira
Laboratory for Flavor Analysis and Enology, Department of Analytical Chemistry - University of Zaragoza, Calle
de Pedro Cerbuna, 12, 50009 Zaragoza, Spain
P.02
GC-MS AND LC-ESI(+)-TOF-MS ANALYSIS OF TWO CHEMOTYPES FROM Lippia
Origanoides ESSENTIAL OILS AND EXTRACTS
Yuri Córdoba Campo1, Anderson Arias1,2, Jairo Martínez1,2, Elena Stashenko1,2
1 Research Center of Excellence-CENIVAM - Universidad Industrial de Santander, Carrera 27, Calle 9, Edificio
2 Sede Bucaramanga - Universidad Industrial de Santander, Carrera 27, Calle 9, Edificio 45, 680002
Bucaramanga, Colombia
P.03
ANALYSIS OF VOLATILE AND SEMI-VOLATILE COMPOUNDS IN GROUND BLACK
PEPPER BY SOLID PROBE-GC/Q-TOF WITH NOVEL HIGH EFFICIENCY EI SOURCE
Jennifer Sanderson1, Peter Gautschi1, Ken Brady2
Technologies, 5301 Stevens Creek Blvd, 95051-8059 Santa Clara, United States
2 Marketing Programs - Agilent Technologies, 5500 Lakeside, SK8 3GR Cheadle, United Kingdom
1 Agilent
P.04
APPLICATION OF HS-SPME-GC-MS TO EVALUATE THE POSSIBLE INFLUENCE OF
ALTITUDE ON APPLE FLAVOR
Eugenio Aprea1, Maria Laura Corollaro2, Emanuela Betta1, Mathilde Charles1, Isabella Endrizzi1, Franco
Biasioli1, Flavia Gasperi1
1 Food Quality and Nutrition - Fondazione Edmund Mach, Via E. Mach, 1, 38010 San Michele all'Adige, Italy
2 Eurofins Qualis S.r.l., corso Unione Sovietica 612/15B, 10135 Torino, Italy
P.05
PHYTOCHEMICAL COMPOSITION BY SOLVENT FREE MICROWAVE EXTRACTION AND
ANTIOXIDANT ACTIVITY INVESTIGATION OF ALGERIAN LAURUS NOBILIS L. LEAVES
ESSENTIAL OILS
Tazerouti Firouz
Department of Chemistry - University of Science and Technology Houari Boumedien, LAOF, Fac Chemistry,
USTHB, BP 32 El Alia Bab Ezzouar, 16111 Algiers, Algeria
P.06
ON AQUEOUS REVERSED PHASE LIQUID CHROMATOGRAPHY-DIODE ARRAY
DETECTION-LINEAR ION TRAP MASS SPECTROMETRY FOR A LARGE-SCALE
PROFILING OF CAROTENOIDS IN SOME VARIETIES OF PEPPER (CAPSICUM ANNUUM
L.)
Alessandra Gentili, Virginia Perez-Fernandez, Roberta Curini
Department of Chemistry - University of Rome La Sapienza, Piazzale Aldo Moro 5, 00185 Rome, Italy
90
P.07
EXPOSURE ASSESSMENT TO TOXIC ALDEHYDES PRODUCED DURING SYRAH
WINEMAKING AND ANALYZED BY COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHY WITH TIME-OF-FLIGHT MASS SPECTROMETRIC DETECTION
Juliane E. Welke1, Karine P. Nicolli2, Laura O. Lago2, Aline B. Marques3, Elina B. Caramão4, Claudia A. Zini2
1 Instituto de Ciência e Tecnologia de Alimentos - UFRGS, Bento Goncalves, 9500, 91501-970 Porto Alegre,
Brazil
3 Embrapa Semi-Árido, BR 428, km 152, Zona Rural, 56302-970 Petrolina, Brazil
P.08
COMPARISON OF NEW SPME ARROW AND CONVENTIONAL SPME IN THE ANALYSIS OF
BEVERAGE FLAVOR PROFILE CHANGES
Hendrik J. Schulte, Hans-Ulrich Baier, Stephane Moreau
Product Marketing and Sales Support / MS Group - Shimadzu Europa GmbH, Albert-Hahn-Str. 6-10, 47269
Duisburg, Germany
P.09
AROMAOFFICE: APPLICATION OF A NOVEL LINEAR RETENTION INDICES DATABASE TO
A COMPLEX HOP ESSENTIAL OIL
Kevin MacNamara1, Kikuo Sasamoto1, Nobuo Ochiai1, Andreas Hoffmann2, Robert Shellie3
1 Gerstel K.K., 1-3-1 Nakane, Meguro-ku, 152-0031 Tokyo, Japan
2 Gerstel GmbH & Co. KG, Eberhard-Gerstel-Platz 1, 45473 Mülheim an der Ruhr, Germany
3 Trajan Scientific and Medical, 7 Argent Place Ringwood, 3134 Victoria, Australia
P.10
EFFECT OF ULTRASONIC PRE-TREATMENT ON AROMA-PROFILE OF APPLE SPIRITS
Tomas Bajer, Petra Bajerová, Daniel Kremr, Ales Eisner, Karel Ventura
Department of Analytical Chemistry - University of Pardubice, Faculty of Chemical Technology, Studentská 95,
53210 Pardubice, Czech Republic
P.11
STUDY OF THE CHEMICAL COMPOSITION OF THE ESSENTIAL OILS OF FIVE SPECIES
OF Lepechinia FROM COLOMBIA
Diego C. Durán1, Jairo R. Martínez1, José L. Fernández2, Elena Stashenko1
1 Department of Chemistry - Universidad Industrial de Santander, Carrera 27 calle 9 UIS, 680002 Bucaramanga,
Colombia
2 Institute of Natural Sciences - Universidad Nacional de Colombia, Carrera 30 calle 45 UNAL, 111321 Bogotá,
Colombia
P.12
QUANTITATIVE DETERMINATION OF PHYTOGENIC COMPOUNDS IN FEED BY GC-MS
Georg Weingart, Klaus Teichmann, Gerd Schatzmayr, Ilse Dohnal
Biomin Research Center - Biomin Holding GmbH, Technopark 1, 3430 Tulln, Austria
P.13
ANALYSIS OF PLANAR PESTICIDES FROM SPINACH AND OTHER FOOD MATRICES
USING QUECHERS CLEANUP WITH A NOVEL GRAPHITIZED CARBON BLACK AND
ZIRCONIA-BASED ADSORBENT
Patrick Myers1, Bill Betz1, Bill Ozanich1, Jennifer Claus1, Michael Ye1, Klaus Buckendahl2, Frank Michel2, Anders
Fridstrom3, Mike Buchanan1
1 Sigma-Aldrich/Supelco, 595 N. Harrison Rd., 16823 Bellefonte, United States
3 Sigma-Aldrich International GmbH, Wassergasse 7, CH-9000 St. Gallen, Switzerland
P.14
WHAT CAN WE SMELL FROM WOOD?
Daniel Kremr, Petra Bajerova, Tomas Bajer, Ales Eisner, Karel Ventura
Department of Analytical Chemistry - University of Pardubice, Faculty of Chemical Technology, Studentská 573,
53210 Pardubice, Czech Republic
91
P.15
QUANTITATIVE ANALYSIS AND ENANTIODIFFERENTIATION OF WHISKY- AND
COGNACLACTONE USING GAS CHROMATOGRAPHY WITH MASS SPECTROMETRIC
DETECTION
Hans-Georg Schmarr1, Marius S. Fraefel2, Maximilian Mathes1
1 Institute for Viticulture and Oenology - DLR Rheinpfalz, Breitenweg 71, 67435 Neustadt an der Weinstrasse,
Germany
2 Faculty of Biotechnology - Applied Science University Mannheim, Paul-Wittsack-Straße 10, 68163 Mannheim,
Germany
P.16
COMBINATION OF DIFFERENT EXTRACTION (SFE, MSPD, SPME) AND
CHROMATOGRAPHIC DETECTION TECHNIQUES (GC-MS, GC-MS/MS, LC-MS) FOR THE
ANALYSIS OF COCA FLOWER SECONDARY METABOLITES
Elena Stashenko, Deisy C. Bernal, Eduardo A. Solano, Fausto Prada, Jairo R. Martínez
Cenivam-Chemistry - Industrial University of Santander, Building 45, Carrera 27 calle 9, 680002 Bucaramanga,
Colombia
P.17
STUDY OF THE VOLATILE CHEMICAL COMPOSITION OF RED WINES PRODUCED WITH
PRE-FERMENTATION HEAT TREATMENT OF GRAPES
Ricardo Lopez1, Olivier Geffroy2, Jean-Luc Favarel3, Vicente Ferreira1
1 Quimica Analitica - Universidad de Zaragoza, Pz. San Francisco, Facultad Ciencias (Edif. D), 50009 Zaragoza,
Spain
2 Institut Français de la Vigne et du Vin Pôle Sud-Ouest, V'innopôle BP22, 81310 Lisle sur Tarn, France
3 Pera, Rue de la Métallurgie, 34510 Florensac, France
P.18
UNTARGETED ANALYTICAL METHOD FOR GLYCOSYLATED SIMPLE PHENOL
PROFILING BY ON-LINE SOLID PHASE EXTRACTION AND LC-HIGH RESOLUTION MASS
SPECTROMETRY (Q-ORBITRAP)
Chiara Barnaba, Tiziana Nardin, Davide Slaghenaufi, Giorgio Nicolini, Roberto Larcher
IASMA Fondazione Edmund Mach, via E. Mach 1, 38010 San Michel a/A, Italy
P.19
DETAILED ANALYSIS OF FAMES USING GC–VUV
Sjaak de Koning, Larissa Ram
Da Vinci Laboratory Solutions, Cairostraat 10, 3047BC Rotterdam, Netherlands
P.20
AROMA ANALYSIS OF BEVERAGE SAMPLES USING THE MULTI-VOLATILE METHOD
(MVM) FOR SEQUENTIAL DYNAMIC HEADSPACE GC/MS
Thomas Albinus1, Andreas Hoffmann1,1, Jun Tsunokawa2, Kikuo Sasamoto2, Nobuo Ochiai2
P.21
HUMAN SCENT SIGNATURE: AN OFF-LINE COUPLING OF GC WITH DOGS TO
DETERMINE THE SCENT COMPOSITION AND ANALYSIS OF HUMAN SCENT SAMPLES
BY GCXGC-MS
Petr Dolezal1, Jana Lnenickova2, Petra Vyplelova2, Ludvik Pinc2, Pavlina Kyjakova3, Irena Valterova3, Veronika
Skerikova1, Stepan Urban1
1 Department of Analytical Chemistry - University of Chemistry and Technology Prague (UCT Prague), Faculty of
Chemical Engineering, Technicka 5, 166 28 Prague 6, Czech Republic
2 Canine Behavior Research Center - Department of Animal Science and Ethology, Czech University of Life
Sciences Prague, Kamycká 129, 165 21 Prague, Czech Republic
3 Institute of Organic Chemistry and Biochemistry - Czech Academy Sciences, Flemingovo nám.2, 160 00
Prague 6, Czech Republic
P.22
AUTHENTICATION OF MEDICINAL CANNABIS BY ELECTROPHORETIC FINGERPRINTS
Jekaterina Mazina, Piret Saar-Reismaa, Maria Kuhtinskaja, Mihkel Kaljurand, Maria Kulp, Merike Vaher
92
P.23
VOLATILE PROFILE OF WOOD SPECIES FOR OENOLOGICAL PURPOSES BY PY-GC/MS
Raquel Garcia1, Sérgio Martins2, Ana Manhita2, Cristina Barrocas Dias2,3, Maria Cabrita4
ICAAM,IIFA,Universidade de Évora, ap 94, 7006-554 Evora, Portugal
Laboratório Hercules, Universidade de Évora, Largo Marques do Marialva, 7000-809 Evora, Portugal
3 Dep Quimica - Universidade de Evora, rua Romão Ramalho 59, 7000-671 Evora, Portugal
4 Instituto de Ciencias Agrárias e Ambientais Mediterranicas - Universidade Evora, Ap 94, 7002-554 Evora,
Portugal
1
2
P.24
COMPARATIVE STUDY OF EXTRACTION METHODS AND ESSENTIAL OIL COMPOSITION
FROM CARDAMOM SEEDS FROM FROM CARDAMOM FRUIT
Djamila Fouial-Djebbar1, Imane Ourabia1, Madina Yassa1, Amira N. Kasdi1, Reda Djebbar2
Department of Chemistry, Faculty of Chemistry, Laboratory of Functional Organic Analysis - Houari
Boumediene University of Sciences and Technology (U.S.T.H.B), BP 32 El-Alia, Bab-Ezzouar, 16111 Algiers,
Algeria
2 Faculty of Biological Sciences - , Laboratory of Biology and Physiology of Organisms, Houari Boumediene
University of Sciences and Technology (U.S.T.H.B), El Alia, BP 32, Bab Ezzouar, 16111 Algiers, Algeria
1
P.25
SCREENING FOR AROMA-ACTIVE COMPOUNDS IN THE AEREAL PARTS OF Heracleum
transcaucasicum BY MEANS OF GC-OLFACTOMETRY AND AROMA EXTRACT DILUTION
ANALYSIS
Mariarosa Maimone1,2, Martin Steinhaus2
Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - Università degli Studi di Messina,
2 Deutsche Forschungsanstalt für Lebensmittelchemie - German Research Center for Food Chemistry, LiseMeitner-Straße 34, 85354 Freising, Germany
1
P.26
DYNAMIC HEADSPACE MULTI-VOLATILE METHOD (DHS-MVM) FOR
CHARACTERIZATION OF AROMA COMPOUNDS IN BREAD AND BUTTER
Jun Tsunokawa1, Nobuo Ochiai1, Kikuo Sasamoto1, Andreas Hoffmann2
1 Gerstel K.K., 1-3-1, Nakane, Meguro-ku,, 152-0031 Tokyo, Japan
2 GERSTEL GmbH & Co. KG, Eberhard-Gerstel-Platz 1, 45473 1, Muelheim an der Ruhr, Germany
P.27
SOLVENT-ASSISTED STIR BAR SORPTIVE EXTRACTION (SA-SBSE) FOR WINE
ANALYSIS: APPLICATION TO AROMA, OFF-FLAVOR, AND PESTICIDES
Kikuo Sasamoto1, Nobuo Ochiai1, Frank David2, Pat Sandra2
2 Research Institute for Chromatography, Kennedypark 26, 8500 Kortrijk, Belgium
P.28
ANALYSIS OF WHISKEY LACTONE PRECURSORS IN OAK WOOD SAMPLES FROM THE
PALATINATE FOREST WITH UHPLC-QTOF-MS
Patricia Golombek1, Stefan Seegmüller2, Hans-Georg Schmarr1
2 Forschungsanstalt für Waldökologie und Forstwirtschaft RLP, Hauptstraße 16, 67705 Trippstadt, Germany
1
P.29
CYANOGENIC COMPOUNDS FROM MESOCARP AND EPICARP FLOURS OF PASSION
FRUIT ( Passiflora edulis flavicarpa )
Humberto R. Bizzo1, Rosemar Antoniassi1, Adelia F. Faria-Machado1, Andrea M. Guedes1, Allan E. Wilhelm1,
Eder D. Resende2, Simone V. Talma2
1 Embrapa Food Technology, Avenida das Américas, 29501, 23020-470 Rio de Janeiro, Brazil
2 CCTA/UENF, Av. Alberto Lamego, 2000, 28013-602 Campos, Brazil
93
P.30
SIMULTANEOUS DETERMINATION OF CAROTENOIDS AND TOCOCHROMANOLS FROM
PALM HYBRID OIL BY HPLC WITH PHOTODIODE ARRAY AND FLUORESCENCE
DETECTORS
Humberto R. Bizzo, Adelia F. Faria-Machado, Andrea M. Guedes, Allan E. Wilhelm, Sidney Pacheco, Ronoel L.
Godoy, Rosemar Antoniassi
Embrapa Food Technology, Avenida das Américas, 29501, 23020-470 Rio de Janeiro, Brazil
P.31
PURIFICATION AND IDENTIFICATION OF ENDOGENOUS ANTIOXIDANT AND ACEINHIBITORY PEPTIDES FROM DONKEY MILK BY MULTIDIMENSIONAL LIQUID
CHROMATOGRAPHY AND NANOHPLC-HIGH RESOLUTION MASS SPECTROMETRY
Riccardo Zenezini Chiozzi, Francesca Ferraris, Giorgia La Barbera, Susy Piovesana, Valentina Trionfera, Aldo
Laganà
P.32
GC-MS DETERMINATION OF CYCLOPROPANE FATTY ACIDS TO ASSESS BEEF QUALITY
Emanuele Sangiorgi, Elena Pellegrini, Ester C. Piccinelli
Reparto Chimica Applicata alle Tecnologie Alimentari, Lombardia Emilia Romagna - Istituto Zooprofilattico
Sperimentale, Via A. Bianchi 9, 25124 Brescia, Italy
P.33
COFFEE AROMA INVESTIGATION: A CHEMOMETRIC COMPARISON OF THE
INFORMATION PROVIDED BY THREE HCC SAMPLING TECHNIQUES ABLE TO
CHEMICALLY DESCRIBE THE SENSORY PROPERTIES OF THE CUP
Davide Bressanello1,1, Erica Liberto1, Patrizia Rubiolo1, Gloria Pellegrino2, Manuela R. Ruosi2, Carlo Bicchi1
1 Dipartimento di Scienza e Tecnologia del Farmaco - University of Turin, Via Pietro Giuria, 9, I-10125 I-10125,
Italy
2 Lavazza Spa, Strada Settimo 410, 10156 Turin, Italy
P.34
FATTY ACID AND ESSENTIAL OIL COMPOSITION OF PISTACIA TEREBINTHUS FRUITS
Samira f. Mecherara-Idjeri1,2, Fatima-zohra Zebboudj2, Nour el islam Lazib2
1 Laboratoire de Recherche sur les Produits Bioactifs et la Valorisation de la Biomasse - Ecole Normale
Supérieure (ENS), Vieux Kouba, 16000 Algiers, Algeria
2 Laboratoire d'Analyse Organique Fonctionnelle, Faculté de Chimie - USTHB, BP-32 El alia, 16004 Alger,
Algeria
P.35
APPLICATION OF AN IONIC LIQUID COLUMN TO THE ANALYSIS OF FLAVOR AND
FRAGRANCE INGREDIENTS
Nicole Curto, Nicholas Snow
Department of Chemistry and Biochemistry - Seton Hall University, 400 S Orange Ave,, 07079 South Orange,
United States
P.36
COMPARISON OF THE AROMA PROFILES OF HOPS BY TD-GC-TOF MS
Laura McGregor1, Massimo Santoro1, Nick Bukowski1, Gareth Roberts1, Stefan Koschinski2
1 Markes International, Gwaun Elai Medi-Science Campus, CF72 8XL Llantrisant, United Kingdom
2 Markes International GmbH, Schleussnerstrasse 42, 63263 Neu-Isenburg, Germany
P.37
HPLC-PDA/ESI-MS ANALYSIS OF PHENOLIC COMPOUNDS IN LYCIUM BARBARUM L.
FRUITS (GOJI BERRIES) AND EVALUATION OF ANTIOXIDANT ACTIVITY
Giusy Tripodo, Marina Russo, Laura Dugo, Chiara Fanali
Unit of Food Science and Nutrition, Department of Medicine - Campus Bio-Medico University, Via Alvaro del
Portillo 21, 00128 Rome, Italy
P.38
DIFFERENTIATING GOUDA TYPE CHEESES USING HEADSPACE GC-MS
Asger Geppel
Assays Department - Chr. Hansen A/S, Bøge Allé 10-12, DK-2970 Hørsholm, Denmark
94
P.39
DOES SEA LAMPREY HAVE A FATTY ACID SIGNATURE THAT REMAINS THROUGHOUT
THE LIFE CYCLE?
Eloi Martins1, Maria João Lança2, Pedro R. Almeida3, Marco Gomes da Silva1
1 Faculdade de Ciencias e Tecnologia - LAQV, REQUIMTE-DQ, Universidade Nova de Lisboa, 2829-516
Caparica, Portugal
2 ICAAM, Departamento de Zootecnia - Escola de Ciência e Tecnologia, Universidade de Évora, 7004-516
Évora, Portugal
3 MARE, Departamento de Biologia - Escola de Ciência e Tecnologia, Universidade de Évora, 7004-516 Évora,
Portugal
P.40
SCREENING FOR PESTICIDES RESIDUES IN COMPLEX FOOD MATRICES BY LC-MS/MS
WITH AN AUTOMATED MASS SPECTRAL LIBRARY CONFIRMATION
David R. Baker1, Neil Loftus1, Stephane Moreau2
Shimadzu Corporation, Trafford Wharf Road, Stretford, M17 1GP Manchester, United Kingdom
MS Group - SHIMADZU Europa Gmbh, Albert Hahn Strasse 6-10, 47269 DUISBURG, Germany
1
2
P.41
ULTRA-SENSITIVE AND RAPID ASSAY OF NEONICOTINOIDS, FIPRONIL AND SOME
METABOLITES IN HONEY BY UHPLC-MS/MS
Mikaël Levi1, Aurore Jaffuel1, Stephane Moreau2
1 SHIMADZU France, Bd Salvador Allende, Noisiel, 77448 Marne la Vallée Cedex 2, France
2 MS Group - SHIMADZU Europa Gmbh, Albert Hahn Strasse 6-10, 47269 DUISBURG, Germany
P.42
DEVELOPMENT AND VALIDATION OF AN HPLC-ES-MS/MS METHOD FOR THE STUDY OF
PHARMACOKINETICS AND MASS BALANCE OF BERBERINE AND BERBERRUBINE IN
RAT
Emanuele Porru1, Placido Franco1, Silvia Spinozzi1, Massimiliano Cont2, Marinella Roberti3, Cristiana Caliceti1,
Aldo Roda1
1 Department of Chemistry - University of Bologna, Via Selmi 2, 40126 Bologna, Italy
2 INBB, Viale delle Medaglie D'Oro, 305, 00136 Roma, Italy
3 Department of Pharmacy and Biotechnology - University of Bologna, Via Belmeloro, 6, 40126 Bologna, Italy
P.43
IMPACT OF GCMS ANALYSIS FOR STUDY THE INFLUENCE OF EXTRACTING METHOD
FOR THE EVALUATION OF THE ANTIOXIDANT ACTIVITY OF VOLATILE COMPOUNDS OF
ZINGIBER OFFICINAL
Lynda Boudarene, Lynda Boudarene, Sihem Aberrane, Sonia Amroun
Faculty of Chemistry, University of Science and Technology Houari Boumedienne - USTHB, BP32, El Alia , BAB
Ezzouar, 16111 Algiers, Algeria
P.44
AN IMPROVED HS-SPME MDGC-MS/MS METHOD FOR THE ANALYSIS OF 2AMINOACETOPHENONE IN WINE
Jutta Keiser, Susann Krautwald, Hans-Georg Schmarr
P.45
FAST ANALYSIS OF PHTHALATES IN FREEZE-DRIED BABY FOODS BY ULTRASOUNDVORTEX-ASSISTED LIQUID-LIQUID MICROEXTRACTION COUPLED WITH GC-IT/MS
Mario Vincenzo Russo1, Pasquale Avino2, Ivan Notardonato1
1 Dipartimento Agricoltura, Ambiente e Alimenti - Università Degli Studi Del Molise, via De Sanctis, 86100
Campobasso, Italy
2 INAIL Research Area, via R. ferruzzi 38/40, 00143 Rome, Italy
95
P.46
ALTERATIONS OF PAPAYA ( CARICA PAPAYA L. CV. ´SOLO') VOLATILES DURING PURÉE
PROCESSING
Christof B. Steingass1, Veronika Lieb1, Hans-Georg Schmarr2,3, Reinhold Carle1,4
1 Institute of Food Science and Biotechnology (150d) - Hohenheim University, Garbenstrasse 25, 70599
Stuttgart, Germany
2 Institute for Viticulture and Oenology - DLR Rheinpfalz, Breitenweg 71, 67435 Neustadt, Germany
3 Instrumental Analytical Chemistry - University Duisburg-Essen, Universitätsstr. 5, 45141 Essen, Germany
4 Biological Science Department, Faculty of Science - King Abdulaziz University, P.O. Box 80257, 21589 Jeddah,
Saudi Arabia
P.47
HIGH RESOLUTION ACCURATE MASS (HRAM) GC-MS MEASUREMENTS FOR
PHTHALATES CONTAMINATION ASSESSMENT IN WINE
Elena Ciceri1, Inge de Dobbeleer1, Flavio Ciesa2, Luca D'Ambrosio2
1 Thermo, Strada Rivoltana, 20090 Rodano (MI), Italy
2 Laboratory of Food Analysis, Provincial Environment Agency, Amba Alagi Street 5, 39100 Bolzano, Italy
P.48
METABOLOMIC PROFILING TO ASSESS ENVIRONMENTAL EFFECTS ON TEA QUALITY
Albert Robbat1, Nicole Kfoury1, Amanda Kowalsick1, Colin Orians2, Sean B. Cash3, Timothy Griffin3, Selena
Ahmed4, John R. Stepp5
1 Department of Chemistry - Tufts University, 62 Talbot Ave, 02155 Medford, United States
2 Department of Biology - Tufts University, 62 Talbot Ave, 02155 Medford, United States
3 Friedman School of Nutrition Science and Policy - Tufts University, 62 Talbot Ave, 02155 Medford, United
States
4 Health and Humand Development - Montana State University, 345 Reid Hall, 59717 Bozeman, United States
5 Anthropology - University of Florida, 337 Turlington Hall, 32611 Gainsville, United States
P.49
ASSESSMENT OF GC/MS BASED ANALYTICAL METHOD FOR 3-MCPD AND GLYCIDYL
ESTERS ANALYSIS WITH SPECIAL EMPHASIS ON ARTEFACT FORMATION AND
APPLICABILITY TO WIDE RANGE OF FOOD MATRICES
Zuzana Zelinkova, Thomas Wenzl
Standards for Food Bioscience - European Commission, Joint Research Centre, Retieseweg 111, 2440 Geel,
Belgium
P.50
DETERMINATION OF ESSENTIAL OIL COMPONENTS IN FEEDSTUFF ADDITIVES BY
PRESSURIZED LIQUID EXTRACTION FOLLOWED BY GAS CHROMATOGRAPHY-MASS
SPECTROMETRY
Maria T. Tena, Marta Jimenez-Salcedo
Department of Chemistry - University of La Rioja, Madre de Dios 53, E-26006 Logroño, Spain
P.51
STUDY OF AMINOACIDS IN MERLOT GRAPES AND THEIR CORRESPONDING WINES
USING LIQUID CHROMATOGRAPHY AND TANDEM MASS SPECTROMETRIC DETECTION
AND OF THEIR RELATED ALCOHOLS WITH COMPREHENSIVE TWO-DIMENSIONAL GAS
CHROMATOGRAPHY COUPLED TO TIME-OF-FLIGHT MASS SPECTROMETRIC
DETECTION
Karine P. Nicolli1, Laura O. Lago2, Celito C. Guerra3, Henrique P. dos Santos3, Rosângela A. Jacques1, Elina B.
Caramão4, Juliane E. Welke2, Claudia A. Zini1
2 Instituto de Ciência e Tecnologia de Alimentos - UFRGS, Bento Goncalves, 9500, 91501-970 Porto Alegre,
Brazil
3 Embrapa Uva e Vinho, Rua Livramento, nº 515, 95700-000 Bento Gonçalves, Brazil
96
P.52
ATMOSPHERIC PRESSURE GAS CHROMATOGRAPHY MASS SPECTROMETRY (APGCMS) BASED METABOLOMICS PROFILING OF GRAPE VOLATILES
Vladimir Shulaev1, Manoj Ghaste1, Fulvio Mattivi2
1 Biological Sciences - University of North Texas, 1155 Union Circle #305220, 76203 Denton, United States
2 Department of Food Quality and Nutrition, Research and Innovation Centre - Fondazione Edmund Mach
(FEM), Via E. Mach 1, 38010 San Michele all’Adige, Italy
P.53
GC-MS IDENTIFICATION OF THE SECONDARY METABOLITES OF ESSENTIAL OILS
OBTAINED FROM DAMIANA (TURNERA DIFFUSA) BY DISTILLATION TECHNIQUES
Yuri Córdoba Campo1, Gustavo Rodríguez1,2, Jairo Martínez1,3, Elena Stashenko1,2
1 Research Center of Excellence-CENIVAM - Universidad Industrial de Santander, Carrera 27, Calle 9, Edificio
2 Sede Bucaramanga - Universidad Industrial de Santander, Carrera 27, Calle 9, Edificio 45, 680002
Bucaramanga, Colombia
3 - Universidad Industrial de Santander, Carrera 27, Calle 9, Edificio 45, 680002 Bucaramanga, Colombia
P.54
ANALYTICAL COMPARISON OF THE DETERMINATION OF BISPHENOL A AND
BISPHENOL ANALOGUES IN PAPER PRODUCTS
Andrea Jurek, Erich Leitner
Institute of Analytical Chemistry and Food Chemistry - Graz University of Technology, Stremayrgasse 9/ II, 8010
Graz, Austria
P.55
DISCRIMINATION OF DIFFERENT PASSIFLORA L. VARIETIES BASED ON VOLATOMIC
PROFILE AND MULTIVARIATE ANALYSIS
Priscilla Porto-Figueira1, Ana Freitas1, Catarina J. Cruz1, José A. Figueira1, Jorge A. Pereira1, José S. Câmara1,2
Chemistry and Enology Lab - Centro de Química da Madeira, Campus da Penteada, 9000-390
Funchal, Portugal
Funchal, Portugal
1 Analytical
P.56
HS-SPME/GC-QMS COMBINED WITH MULTIVARIATE ANALYSIS AS A POWERFUL TOOL
TO DISCRIMINATE BETWEEN EUGENIA UNIFLORA L. VARIETIES
Priscilla Porto-Figueira1, José A. Figueira1, Jorge A. Pereira1, José S. Câmara1,2
1 Analytical Chemistry and Enology Lab - Centro de Química da Madeira, Universidade da Madeira, Campus da
Funchal, Portugal
P.57
APPLICATION OF GAS CHROMATOGRAPHY COUPLED TO OLFACTOMETRY (GC-O),
MASS SPECTROMETRY (GC/QMS) AND COMPREHENSIVE GAS CHROMATOGRAPHY
(GC×GC/TOFMS) AS COMPLEMENTARY TOOLS TO ACCESS THE VOLATILE
COMPOUNDS RESPONSIBLE FOR THE PECULIAR AROMA OF SYRAH WINE PRODUCED
IN THE VALE OF SAO FRANCISCO REGION IN BRAZIL
Janaína A. Barbará1, Érica S. Silva1, Elina B. Caramão2, Aline B. Marques3, Claudia A. Zini1
Chemistry Institute - UFRGS, Bento Goncalves, 9500, 91501-970 Porto Alegre, Brazil
UNIT, Avenida Murilo Dantas 300, 49020290 Aracaju, Brazil
3 Embrpa Semi-Árido, BR 428, km 152, Zona Rural, 56302970 Petrolina, Brazil
1
2
P.58
EMBEDDED OF THE LINEAR RETENTION INDEX INFORMATION WITHIN A DEDICATED
MS SPECTRA DATABASE TO BOOST THE IDENTIFICATION RELIABILITY OF COMPLEX
SAMPLES IN THE FLAVOUR AND FRAGRANCE FIELD
Margita Utczas1, Giuseppe Micalizzi1, Giorgia Purcaro1, Luigi Mondello1,2
1 Chromaleont SRL, Viale Boccetta 70, 98122 Messina, Italy
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, - Polo
97
P.59
EXPLOITATION OF DIFFERENT TECHNIQUES FOR A RELIABLE IDENTIFICATION OF
UNKNOWN COMPOUNDS TO BE ADDED INTO A DEDICATED DATABASE FOR THE
FLAVOUR AND FRAGRANCE FIELD
Giuseppe Micalizzi1, Margita Utczas1, Giorgia Purcaro1, Danilo Sciarrone2, Luigi Mondello1,2
1 Chromaleont SrL, viale Boccetta 70, 98122 Messina, Italy
2 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, - Polo
P.60
EVALUATION OF THE LIPID PROFILE OF DAIRY PRODUCTS DURING AND AFTER THEIR
SHELF-LIFE
Marianna Oteri1, Marco Beccaria2, Giorgia Purcaro2, Giuseppe Micalizzi2, Ivana L. Bonaccorsi1, Francesco
Cacciola3, Paola Dugo1,2, Luigi Mondello1,2
1 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - Università degli Studi di Messina,
3 Dipartimento di Scienze Biomediche, Odontoiatriche e delle Immagini Morfologiche e Funzionali - Università
degli Studi di Messina, Via Consolare Valeria, 98125 Messina, Italy
P.61
AZAPHILONES PIGMENTS FROM Talaromyces Albobiverticillius
Miroslava Zelena1, Laurent Dufosse2, Daniele Giuffrida3, Francesco Cacciola3, Mekala Venkat2, Mireille
Fouillaud2, Emmanuelle Girard-Valenciennes2, Lenka Ceslova1, Paola Dugo4,5, Luigi Mondello4,5
1 Department of Analytical Chemistry - Faculty of Chemical Technology - University of Pardubice, Studentská
573, 532 10 Pardubice, Czech Republic
2 Laboratoire de Chimie des Substances Naturelles et des Sciences des Aliments - LCSNSA EA 2212 Université de la Réunion, 15 Avenue René Cassin, CS 92003,Saint-Denis Cedex 9, F-97744 Ile de la Réunion,
France
Messina, via Consolare Valeria, 98125 Messina, Italy
4 Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali - University of Messina, Via SS.
P.62
CHEMICAL COMPOSITION OF ESSENTIAL OILS OF OLIVE LEAVES USING GC-MS AND
EVALUATION OF ANTIOXIDANT ACTIVITY OF THEIR CRUDE EXTRACTS
Linda Didaoui
Ecole Nationale Polytechnique - ENP, BP 182 El Harrach, 16000 Algiers, Algeria
P.63
HS-SPME-GC-MS METHOD FOR THE DETERMINATION OF EMERGING VOLATILE
CONTAMINANTS IN FRUITS.
Fabrizio Cincotta, Antonella Verzera, Concetta Condurso, Gianluca Tripodi
Department of Chemical, Biological, Pharmaceutical and Environmental Sciences - University of Messina, Viale
Stagno d'Alcontres 31, 98166 Messina, Italy
_____________________________________________________________________________
Q. MICROFABRICATED CHIPS
_____________________________________________________________________________
Q.01
CONVENTIONAL AND ENANTIOSELECTIVE GC WITH MICRO-FABRICATED PLANAR
COLUMNS FOR ANALYSIS OF REAL-WORLD SAMPLES OF PLANT VOLATILE FRACTION
Cecilia Cagliero1, Stefano Galli2, Mario Galli2, Chiara Cordero1, Erica Liberto1, Barbara Sgorbini1, Patrizia
Rubiolo1, Carlo Bicchi1
1 Dipartimento di Scienza e Tecnologia del Farmaco - Università di Torino, Via Pietro Giuria, 9, 10125 Torino, Italy
2 MEGA s.n.c., Via Plinio, 29, 20025 Legnano, Italy
98
Q.02
CHIP-BASED HIGH-TEMPERATURE LIQUID CHROMATOGRAPHY FOR HIGH SPEED
ANALYTICS
Josef J. Heiland1, Carsten Lotter1, Volkmar Stein2, Detlev Belder1
1 Faculty of Chemistry and Mineralogy, Institute of Analytical Chemistry, Workgroup Prof. Dr. Belder - University
of Leipzig, Linnéstrasse 3, 04177 Leipzig, Germany
2 Institute of Microtechnology Mainz (ICT-IMM) - Fraunhofer Institute for Chemical Technology, Carl-ZeissStrasse 18-20, 55129 Mainz, Germany
99

THE `40th INTERNATIONAL SYMPOSIUM ON CAPILLARY

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