SFA SA3000-5000D newpump

Transcription

SKALAR
SEGMENTED FLOW ANALYZER
SA3000/5000 CHEMISTRY UNIT
USER MANUAL
SEGMENTED FLOW ANALYZER
SA3000/5000 CHEMISTRY UNIT
USER MANUAL
Publication No: 0101063D.US
Issue date: February 2013
 Copyright Skalar Analytical B.V.
P.O Box 3237
4800 DE Breda
The Netherlands
Tel:
+31 (0)76 5 486 486
Fax:
+31 (0)76 5 486 400
E-mail: [email protected]
Internet: http://www.skalar.com
Welcome to the SA3000/5000 Chemistry unit
This manual guides you through the complete definition of the chemistry unit, to help
you quickly gain the necessary knowledge and confidence to use the chemistry unit
to its optimum efficiency.
This manual is divided in 5 chapters:
1.
2.
3.
4.
5.
Introduction
Unpacking and installation
Maintenance
Technical information
Spare parts
Please read this manual (and the other manuals, that are incorporated in the SANplus
analyzer system) carefully before the instrument is put into operation, pay special
attention to the Safety precautions in chapter 1.2
If despite the information given in this manual, any problems should arise, please do
not hesitate to call your local Skalar representative or the Skalar head office at the
address given below.
Skalar Analytical B.V.
P.O Box 3237
4800 DE Breda
The Netherlands
Tel:
+31 (0)76 5 486 486
Fax:
+31 (0)76 5 486 400
E-mail: [email protected]
Internet: http://www.skalar.com
TABLE OF CONTENTS
1
INTRODUCTION............................................................................................. 1-1
1.1
1.2
1.3
1.4
2
The SA3000/5000 chemistry unit .................................................................. 1-1
Safety precautions ........................................................................................ 1-3
WARRANTY REGISTRATION FORM .......................................................... 1-5
CUSTOMER ACCEPTANCE FORM............................................................. 1-7
UNPACKING AND INSTALLATION .............................................................. 2-1
2.1 Unpacking ..................................................................................................... 2-1
2.1.1 Location ................................................................................................ 2-1
2.2 Laboratory requirements ............................................................................... 2-1
2.3 Instrument requirements ............................................................................... 2-2
2.4 Installation ..................................................................................................... 2-3
3
MAINTENANCE .............................................................................................. 3-1
3.1
3.2
3.3
3.4
3.5
3.6
3.7
4
Scheduled maintenance................................................................................ 3-1
Changing the air tubing ................................................................................. 3-2
Moving the bridges or replacing the pump tubing ......................................... 3-2
Tubing connections ....................................................................................... 3-4
Replacing the pump deck springs ................................................................. 3-6
Adjustment of the air-pressure ...................................................................... 3-6
Changing pre-mount membranes ................................................................. 3-7
TECHNICAL INFORMATION ......................................................................... 4-1
4.1 Technical specifications ................................................................................ 4-1
4.2 Housing ......................................................................................................... 4-2
4.3 Proportioning pump ....................................................................................... 4-4
4.4 Air injector ..................................................................................................... 4-6
4.5 Membrane pump ........................................................................................... 4-6
4.6 Reactor and control unit ................................................................................ 4-7
4.6.1 Adjusting the pre-set temperature ........................................................ 4-8
4.6.2 Error messages .................................................................................... 4-8
5
SPARES AND CONSUMABLES .................................................................... 5-1
SA3000/5000 Chemistry unit
Chapter 1
1
INTRODUCTION
1.1
The SA3000/5000 chemistry unit
Introduction
1-1
Figure 1.1 Chemistry unit with integrated back panel
The chemistry unit incorporates Skalar’s years of experience in automating wetchemistry analysis with our latest innovations.
The chemistry unit can accommodate (depending on the applied chemistries) up to
five chemistry modules and detection channels for running five chemistries
simultaneously using one chemistry unit.
The samples coming from a sampler and the reagents from the canisters are drawn
to the chemistry unit by the multi-speed pump. The built-in air-injector provides air
segmentation of the samples. On the chemistry module the required reagents are
added to the samples and mixed in coils. Special in-line treatments of the reaction
mixtures are possible: UV digestion, distillation, hydrolysis, dialysis, ionexchange/reduction, heating and cooling. The reaction mixtures are subsequently
transferred to the built-in detection heads or separate external detectors (depending
on the chemistry to be measured). After detection the reaction mixture is transferred
to a waste receptacle, which must be connected to a waste facility. The measured
signals are collected on a computer, where the data are processed.
Chapter 1
Introduction
1-2
The multi-speed pump with standby, analysis and fast rinse position takes care for a
fast start-up and shutdown of the analyzer by pumping the reagents or rinsing
solution at an elevated speed.
For chemistries that need reactors (which are placed under the chemistry module
plate), these reactors are connected to reactor controllers with clearly visible
temperature displays, which are integrated at the front and/or the back of the pump in
the chemistry unit.
For chemistries with in-line distillation a back panel is integrated on the chemistry
unit.
Leak detectors are placed at the bottom of the chemistry unit. When a system
controller is present and a leak is detected, the system will shut down.
The chemistry can be built-up from left to right as well as from right to left (see Figure
1.2), which is an advantage (it keeps the sampling lines short and ease maintenance)
when more chemistry channels are to be run simultaneously on a second
SA3000/5000 chemistry unit.
The chemistry unit can be run fully automatic in combination with a SA1050, SA1074
or SA1077 autosampler, electrical reagent valves, system controller and
FlowAccessTM software.
The SA3000 and SA5000 are identical chemistry units, except for the proportioning
pump. The pump of the SA3000 is provided with one pump deck and roller cage that
is equipped for 16 pump tubing’s, while the SA5000 is provided with a pump with two
pump decks and roller cages and is equipped for 32 pump tubing’s.
Figure 1.2 Example of system with SA1074 sampler and two chemistry units
1.2
Chapter 1
Introduction
1-3
Safety precautions
Only qualified personnel should carry out repair of the exposed equipment.
1. The instrument is designed for laboratory use.
2. Before the instrument is connected to the mains and switched on, check whether
the required voltage (indicated on the type plate at the back of the instrument)
corresponds with the line voltage.
3. The instrument power cord must only be plugged into a line supply outlet with
ground protector (earth). If an extension cord is used, make sure that the protector
line is not interrupted.
4. Opening of the instrument or disassembling of parts of the instrument can set free
voltage carrying parts while the instrument is connected to the mains. Also
connectors could carry voltage. Before any service, repair or change of parts, the
instrument has to be disconnected from all power supplies. Service and repair
work on voltage carrying open instruments should be avoided whenever possible.
If such work is absolutely necessary, qualified personnel, who are aware of the
hazards of this work, should carry it out.
5. Whenever it is likely that safe operation is impaired, the instrument must be made
inoperative and secured against unintended operation. The appropriate servicing
personnel must then be informed.
6. The instrument must be disconnected from all electrical sources when a fuse is to
be replaced.
7. Keep the chemistry unit and all incorporated components dry and clean.
8. Keep hands, jewelry, hair etc. from the inside of the instrument whenever it is in
operation.
Skalar Analytical B.V. does not accept liability for any consequences caused by
irresponsible use or irresponsible handling of the chemistry unit, nor for the effects
and consequences induced by its use.
Chapter 1
Introduction
1-5
1.3
WARRANTY REGISTRATION FORM
The warranty period is 12 months and starts on the date of shipment. To activate the
warranty, please return the signed warranty registration form by the Skalar Service
Desk. The warranty registration form should be received within 2 months from the
shipment date.
Warranty is ex Skalar Analytical BV and does not include traveling, expenses and
working hours at customer’s location.
Warranty is subject to the following exception(s): Glassware breakage. Consumable
products, brokerage and transport costs for the replacement parts replaced under the
warranty are to the client’s account. Skalar will not be responsible for malfunctioning
of the instrument if third party components are used in the instrument.
All Skalar contracts are according “General terms and conditions for the Instrument
branch as issued by FHI Het Instrument”, which are available on request.
REGISTRATION FOR WARRANTY:
Purchase order no.:
Serial no.:
Date of purchase:
Distributor:
Company name:
Address:
Post code/ZIP
City
Country:
Contact person:
Telephone number:
Fax number:
E-mail address:
Company stamp:
Name:
Signature:
The warranty registration form will only be valid when accompanied by the signed
customer acceptance form.
Please return this form to:
SKALAR ANALYTICAL B.V.
PO Box 3237
4800 DE Breda
The Netherlands
Attn.: Service desk
Date:
1.4
Chapter 1
Introduction
1-7
CUSTOMER ACCEPTANCE FORM
Company name:
Address:
Post code/ZIP code:
City:
Country:
Date:
The undersigned authorized officer confirms that the performance of the instrument,
as per the purchase order number as mentioned on the warranty registration form, is
according to the specifications as submitted by the manufacturer.
YES
NO
Remarks:
Signature
Name
2
Chapter 2
2-1
UNPACKING AND INSTALLATION
2.1
Unpacking
To protect the chemistry unit against damage during transport the chemistry unit is
safely foamed in a wooden crate. The best will be to do the unpacking with two
persons.
While unpacking do not discard any packing materials, till all parts have been
unpacked and checked against the packing list to insure all items are accounted for.
If any item is missing first check the packing. If it still can not be found, make a note
of it giving as clear a description as possible using part numbers from the manual
and immediately inform the forwarder and the supplier (see delivery conditions).
Even when you think that all items have been accounted for, check the packing.
Should there be any damaged or broken parts, repack it in the original packing, and
immediately inform the forwarder and the supplier who will give further instructions. If
the goods are supplied on trial, the original packing material must be used for return
shipment unless better is available.
1. Open the chest with a crowbar.
2. Remove the plastic sheet wrapped foam mould. The chemistry unit will now
become visible.
3. Lift, with two persons, the chemistry unit out of the chest, keeping it straight.
4. Place the chemistry unit on the required place.
Note: Some (partly) loose parts are secured with tape. Do not release these parts
until the instrument is installed.
2.1.1 Location
The instrument should only be placed on a level, clean, dry and sturdy surface with
sufficient space for all components. The ambient temperature should be between
+10ºC and +40ºC, humidity 20% to 80%, non-condensing.
Do not locate the instrument:
• In direct sunlight.
• Near an air conditioning unit.
• Near any heat or cooling source.
• Near equipment that generates intensive magnetic or electric fields.
• Near equipment that generates high frequency.
2.2
-
Laboratory requirements
Space for the storage of the required reagents in the vicinity of the analyzer
system to provide short liquid supply lines.
Waste facility for collection of the reaction products from the analyzer system.
These products can be of an aggressive or volatile nature and adequate
recipients for them must be provided (use different facilities if the wastes are noncompatible). Make sure that the waste can be disposed regularly and safely.
2.3
2-2
Instrument requirements
A.
B.
-
C.
Chapter 2
Power supply; the chemistry unit can be used at 220-240 Volt or 110-120 Volt.
The unit must only be connected to a line supply with ground protector (earth). If
an extension lead is used make sure the ground protector line is not interrupted.
Max. power consumption: 530 VA.
The instrument is provided with the power cable for the voltage as requested.
Also the fuses are installed for the requested voltage. If the instrument is
connected to a different power supply, the fuses have to be replaced.
Fuses for 220 - 240 V: 2.5 A and for 100 -110 V: 5 A
Power outlets or power extension bar for a minimum of 6 power connections to
accommodate power for the total analyzer. Power connections are required for:
Sampler
Interface
Computer
Computer screen
Printer
If a water bath, UV digestion or one or more external detectors are present
more power outlets must be available. However, if a system controller is
present, these devices can be connected to system controller bars.
(Optional) Bottle with compressed air or Nitrogen gas (dependent on the
chemistries) with a gas-reducing valve for 200 kPa.
2.4
Chapter 2
2-3
Installation
Important notes:
• Connect the power cables only after all other connections have been made.
• All cables and tubing to be connected should be labeled.
• Use lubricant for tubing-tubing and glass-tubing connections if necessary, except
for connections on the TOC module.
• Do not use lubricant for connections on Perspex manifolds and heat exchangers.
Here the installation of a complete analyzer system is described. You can skip the
instructions for the parts that are not included in your analyzer system.
Procedure: (Skip an instruction if the item is not present)
1. Place the sampler on the left side of the available bench space. Check if the
voltage selector on the sampler is set on the proper voltage and for the SA1000
check if 50 or 60 Hz is used. Adjust if necessary.
2. Connect the supplied RS232 cable (not for SA1000 sampler) and power cable to
the sampler.
3. Place the chemistry unit right from the sampler; place the (optional) rinsing valves
between the sampler and the chemistry unit. Save if possible enough space for
the reagents (and the water bath*, if present) between sampler and chemistry
unit. (If not enough space is available on the bench, place the reagents (and
water bath) under the bench, but as high as possible to reduce the backpressure
and to keep the reagent lines as short as possible).
* A water bath may not be placed beside the electronics (interface, detectors, etc.)
4. Place the (optional) air scrubber at the back of the analyzer.
5. Lead the tubing from the water bath under the back door of the chemistry unit till
under the chemistry module. Lift the module and connect the tubing to the heat
exchanger. Fill the water bath (preferably with distilled water) until about 2 cm
under the cover plate. Place the thermometer.
6. Connect the power cable and (optional, only if a system controller is present) the
system controller cable (9-p sub D connector) to the back of the chemistry unit.
Connect the tubing of the air scrubber to the air inlet at the back of the instrument.
Optional: Connect the cable for connection to a second SA5000 chemistry unit
and/or the system controller socket bench(es)(only in combination with SA8505
interface) to the required connection(s). Each type of device requires its own
socket bench (pumps, heaters, detectors).
7. Place the back panel with the distillation unit (and flow meter) in the holes on the
back panel of the chemistry unit.
8. Connect the inlet (lower connection) of the flow meter to a nitrogen gas cylinder.
Connect the inlet of the distillation unit to the outlet (upper connection) of the flow
meter.
9. Place the measuring heads as required for the application in the chemistry unit.
Open the right side door in the chemistry unit and connect the connection cables
to the measuring heads. Close the door with the cables led outside at the bottom
of the door. For a measurement with the SA6280, SA6310 or SA6850 no
measuring head is placed in the chemistry unit. For these measurements the
detection head is situated on its electronics section.
Chapter 2
2-4
10. Place the electronics housing of the analogue detector (SA6280 IR detector,
SA6310 Fluorimeter, SA6850 UV detector, etc.) at the right of the chemistry unit.
11. Place the interface (SA8502, SA8503 or SA8505) right from the photometer unit.
Connect the RS232 cable coming from the sampler to the required RS232
connection on the interface. Also connect the RS232 cable for the connection to
the PC and the power cable on the interface. For SA8502 and SA8503: Connect
the (optional) system controller cable from the chemistry unit with the 9-p sub D
connector and leak detection plugs to the interface (system 1). Connect the
automatic rinsing valves (cat.no. 21530902-21530909) to the connections at
system 1 on the interface. If a system controller power bar is required, connect
this power bar to connector ‘System 2’ on the interface. For SA8505: Connect the
(optional) system controller cable from the chemistry unit with the 9-p sub D
connector plugs to the system controller bracket on the interface. Connect the
automatic rinsing valves (cat.no. 21530912-21530919) to the connections at the
system controller bracket on the interface.
12. Connect the cable(s) of the analogue detection head(s) to the electronics housing
and connect the output cables from the electronics housing to the required
channel connection on the interface (for SA8505 connect the cable to the correct
channel on the connection box, which is connected to the analog insert board on
the interface). Connect the power cable to the electronics section. Refer also to
the provided manuals of the interface and detector(s).
Remark: If a digital detector is present connect the cables of the detection heads
directly to the required channel on the interface. All connections on the
interface must be connected; otherwise the not connected PCB’s must be
removed from the interface.
13. Place the PC on the interface (SA8505 can also be placed upright; in this case
place the PC beside the interface) and the printer right from the interface.
Connect the connection cables between screen and PC and printer and PC.
Connect the RS232 cable coming from the interface. Connect the power cables
on PC, screen and printer.
Figure 2.1 Example of a setup analyzer system
14. Release the tapes that were used for securing parts on the chemistry unit.
15. Connect the sample tubing coming from the sampler to the splitter on the
chemistry unit (check the labeling).
16. Connect the pump tubing to the outlets of the valves. Check the labeling on the
inlet tubing of the valves and on the pump tubing for the proper connections.
17. Connect the tubing to and from the distillation unit to the required module (refer to
method diagram in the corresponding method sheet). Place the waste tubing from
the distillation unit in a waste container.
Chapter 2
2-5
18. If nitrogen is used for segmentation, connect the supply tubing from the gas
cylinder to the inlet at the backside of the chemistry unit. If a distillation unit is
present use a T-piece.
19. Place the interference filters in the measuring head(s). Refer to the method sheet
for the required filter.
20. Place the required flow cell (refer to the corresponding method sheet) and
connect the tubing to the flow cell (for proper connection see the manual for the
SA62xx or interface).
21. Place the waste tubing, coming from the waste receptacles in the chemistry unit
and from the rinsing vessel on the sampler, in a waste container(s). See also
chapter 2.2.
22. Place the rinsing water supply tubing (check the labeling) on the sampler and the
reagent supply tubing (to the valves) in distilled water.
23. Connect the power cables of the sampler, the chemistry unit, the interface, the PC
and printer to the mains. Connect all other power cables to the mains, or to the
required part of the system controller power bar, if required.
24. Now first the chemistry unit is checked.
25. Slightly grease the pump decks and close them.
26. If nitrogen is used, turn on the gas supply; adjust the pressure valve on the bottle
until it indicates 0.9 -1 bar (90 - 100 kPa).
27. If a column is present on the module, by-pass it from the stream by turning the tap
on the module.
28. Lift the air bars by their rings and turn them counter clockwise, then release the
rings to place the bars square over the air tubing.
29. Switch on the sampler and the chemistry unit only. (If the reactor control units are
on, switch them off, see chapter 4.6). The pump starts in normal mode.
30. Let the system run during 30 minutes with distilled water on low, normal and high
speed (use the switch at the front of the chemistry unit) and check the system for
leaks. Repair any leaks found.
31. When everything is working satisfactory, switch off the sampler and the chemistry
unit.
Note: If the unit is not used anymore during the day, close the gas supply and open
the pump decks.
32. The installation is continued with the installation of the software. Switch on the PC
and let Windows start up.
33. Install the FlowAccessTM software. Refer to the installation instructions.
34. Copy the supplied .mdb file with the system setup into the FlowAccessTM
directory.
35. To run an analysis refer to the manuals supplied with the system.
3
Chapter 3
Maintenance
3-1
MAINTENANCE
3.1
Scheduled maintenance
The following preventative maintenance procedures are recommended to assure
continued reliable operation of the Skalar Flow Analyzer system.
A. Daily:
1. Check all tubing for loose connections and leaks.
2. Check the reagents and standards, prepare new if required (see method sheets).
3. Perform the rinsing procedure as recommended for the method at the end of the
operation.
4. Clean all spillage with a water-dampened cloth. If it is necessary to use a cleaning
solution, first check the method for possible interaction with the reagents in use.
5. At the end of the operations, release the pump decks. If the system will be off for
more than 48 hours, lift the air bars and turn them anti clockwise until the air
tubing are released. This prevents premature occluding of the tubes.
Note: The pump decks cannot be lifted if the ‘Time program’ is used in the software.
B. Weekly
1. Check the reagent absorbance and primer sensitivity at least every week or
whenever a new reagent or standard is used. Check the values obtained against
previously obtained values.
2. Check if the pump decks at the inside contain a thin film of grease. Smoothen a
fingertip of grease over the full plate and remove any overdose at the edges.
3. While the pump is running, take each silicone air tubing on both sides of the air
injector and slide it slightly in either direction so that a new section is under the air
bars.
4. Clean the rinsing liquid vessel on the sampler with a syringe and check for dirt.
5. Check the sample tubing. Replace if clogged or dirty.
6. Check the sample needle by pricking through the needle. Replace if blocked.
7. Rinse the system as recommended in the method sheet.
C. Monthly
1. Use an alcohol-moisten cloth to wipe of the inside of the pump decks and then
grease the plate with new grease.
2. Replace the silicon air tubing (SA3150/SA5150) with new tubing, see chapter 3.2.
3. Shift all pump tubing one bridge or, if this was already done, replace the tubing
(see chapter 3.3). If the analyzer is not used daily for more than 5 hours, this
stretching or replacement can be done after 2 months.
4. Use a clean soft cloth to wipe the sample needle.
5. Clean the interference filter using lens tissue. Replace if delaminated.
6. Replace, if present, the dialysis membrane(s) (see chapter 3.5).
7. Remove the syringe from the diluter and clean the inside of the syringe after
removing the plunger with a soft brush and distilled water. If algae persist on the
wall and the plunger, clean with 1:10 diluted hypo chlorite solution and rinse then
thoroughly with distilled water.
Chapter 3
Maintenance
3-2
D. 6 Monthly
1. Check the pump decks for wear every six months, or after 1000 hours of pumping
time, and replace if worn.
2. Check the pump rollers and clean with a dry soft clean cloth.
3. If applicable, replace the CO2 absorbent cartridge.
E. Yearly
1. Replace the halogen detector lamp yearly, or after 3500 hours of use.
2. Check the interference filters if they are dark around the edges. If so, replace
them.
3. Clean all coils, waste vessels, glass tubing, distillation unit, flow cells and Perspex
manifolds and replace all tubing as described in chapter 3.2, 3.3, 3.4 and 3.5.
For replacement procedures in the optional equipment see their respective manuals.
3.2
Changing the air tubing
Note: Always replace all air tubing at the same time and replace them one by one to
prevent mixing up.
Required: Silicon tubing 0.5 ID: cat. no. SA3150 or 1.0 ID cat. no SA5150
Procedure:
1. Switch off the power of the
SA3000/5000.
2. Pull and turn the rings fixed to the
bars clockwise, so that the tubing’s
are released (see Figure 3.1).
3. Disconnect the first mounted
silicone air tubing from the
manifold, combs and air supply pin.
4. Take new silicone tubing. Cut off
straight a piece at the same length
as the removed tubing by means of
Figure 3.1
a razor blade.
5. Connect this tubing to the appropriate air supply pin, air injector combs and
manifold.
6. Repeat step 3 – 5 for all air tubing on the air injector, one by one.
7. Replace any short-circuited pieces of tubing on the air supply pins by new pieces.
8. Pull and turn the rings counter clockwise until the air tubing’s are tensioned under
the bars.
3.3
Moving the bridges or replacing the pump tubing
Note: Preferably move or replace all pump tubing at the same time and replace them
one by one to prevent mixing up.
Procedure for moving the bridges:
1. Make sure the tubing’s are empty (preferred) or filled with distilled water (no
reagents!).
2. Switch off the power of the SA3000/5000.
Chapter 3
Maintenance
3-3
3. Pull up the handle of the pump
deck. Pull the locking pins towards
each other (see Figure 3.2).
4. Pull up the pump deck until the
locking pins can rest on the side,
when the locking pins are released
(see Figure 3.3). Remove the pump
deck by pulling it away from the
pump (see arrows in Figure 3.3).
5. Check if the clamp at the side of
the sampler has moved up when
the pump deck was opened. If not
pull the clamp up a bit by hand.
Now the tension on the pump
tubing is a bit released.
Figure 3.2
6. Loosen the bridge of the pump
tubing from the clamp at the side of
the module.
7. Loosen the bridge of the pump
tubing from the clamp at the side of
the sampler and place this bridge
on the clamp at the side of the
module.
8. Place the extra bridge on the clamp
at the side of the sampler.
9. Cut off the tubing at the side of the
module to the length required for
the connection to the manifold on
the module and dry the module with
a cloth. Avoid leakage and/or
Figure 3.3
spillage.
10. Repeat step 6 – 9 for all pump tubing.
11. Slightly grease the pump deck(s) and replace the decks.
12. Close the decks by pushing them down while pulling the locking pins together
until the pins can lock the deck. The clamp is pushed down with the deck, thus
stretching the pump tubing on the roller cage. Lower the handle
Procedure for replacing the pump tubing:
Required: Pump tubing in the sizes mentioned in the method sheets, sleeves.
Note: If a column is present on the module, bypass it.
1. Let the system rinse with distilled water and then let the system run empty.
2. Switch off the power.
3. Pull up the handle of the pump deck. Pull the locking pins towards each other
(see Figure 3.2).
4. Pull up the pump deck(s) until the locking pins can rest on the side, when the
locking pins are released (see Figure 3.3). Remove the pump deck(s) by pulling it
away from the pump (see arrows in Figure 3.3).
Chapter 3
Maintenance
3-4
5. Loosen the first pump tubing from the clamps and its connections.
6. Take a pump tubing of the same size and make a connection with the supply
tubing or the valve. Use a sleeve if necessary. For the connection with the valve a
piece of SA3035 tubing is used for pump tubing smaller than SA3032. Use a little
lubricant.
7. Place the bridges on the clamps, leaving the extra bridge at the side of the
sampler.
8. Connect the pump tubing to the manifold.
9. Repeat step 5 – 8 for all pump tubing.
10. Slightly grease the pump deck(s) and replace the decks.
11. Close the decks by pushing them down while pulling the locking pins together
until the pins can lock the deck. The clamp is pushed down with the deck, thus
stretching the pump tubing on the roller cage. Lower the handle.
3.4
Tubing connections
Examples for sleeving:
Perspex-tubing connection:
The dialyzers and some manifolds
have perspex connectors on which no
lubricant may be used.
1. Required: Diluted (0.3 0/00) Brij 35,
lubricant, sleeves, a small pipette
and a scalpel
2. With a sharp scalpel blade score
the sleeve to no more then half
the thickness of the sleeve (see
Figure 3.4).
3. Score the sleeve down its full
length; avoid any contact with the
Perspex connector.
4. Use your thumb nails to pry open
the sleeve (see Figure 3.5).
5. When the sleeve is fully open it can
be removed.
6. Use lubricant to ease the new
sleeve back onto the tubing (see
Figure 3.6).
7. Position the tubing so that it is half
way into the sleeve.
Figure 3.4
Figure 3.5
Figure 3.6
Chapter 3
Maintenance
3-5
8. Use a few drops of Brij 35 (0.3 0/00)
in water to lubricate the open half
of the sleeve (see Figure 3.7).
Figure 3.7
9. Position the sleeve back onto the
Perspex connector, making sure
there are no gaps (see Figure 3.8).
10. Run the analyzer and check to
make sure there are no leaks
Figure 3.8
Tubing-glass connection:
A tubing-glass connection is made when connecting a tubing to a coil. The ID of the
coil is the same as the ID of the tube. The OD’s however differ and so an extra
sleeve is used to connect them (see Figure 3.9).
1. Slide a piece of SA 5401
(2.4 mm ID) sleeve over
the SA 5142 (1.5 mm ID)
tubing; use some lubricant
to ease the sliding.
2. Cut off straight the tubing,
so that the sleeve has the
length of one centimeter.
3. Then take a piece of 2 cm
Figure 3.9
of SA 5400 (3.2 mm ID)
sleeve, slide one end over
the sleeve just made and
the other end over the end
of the glass coil.
Glass-glass connection:
1. Make sure that the glass
Figure 3.10
ends are touching each
other and the connection is the center of the sleeve (see Figure 3.10).
2. Use SA 5400 for all glass-glass connections except for reactors (use SA 5192
acidflex) and distillation units (use SA 5194 acidflex).
Chapter 3
Maintenance
3-6
3.5
Replacing the pump deck springs
1. Close the pump deck and lower the
handle.
2. Push the locking pin (see arrow in
Figure 3.11) out of the handle.
3. Firmly press the deck down by hand
and carefully pull the locking pins
towards each other.
4. Gradually release the pressure of
your hand on the deck until the tension
is away.
Figure 3.11
5. Now the deck is divided in two parts
and the upper part can be taken away.
6. Replace the six springs and replace the upper deck.
7. Push the deck down until the deck can be locked with the locking pins.
8. Replace the handle and drive in the locking pin.
3.6
Adjustment of the air-pressure
Warning: Only qualified personnel, who are aware of the hazards when working with
open equipment, should perform this work.
1. The membrane pump with air-reducing valve is located behind the front cover
with the On/Off switch and pump speed control (see Figure 3.12).
Figure 3.13
Figure 3.12
2. Set the speed control to normal speed.
3. Release the hexagonal screw at the bottom of the front cover (see arrow in Figure
3.12), pull the cover carefully to the front and lay it down (see Figure 3.13).
4. Turn the locking ring of the air-reducer a quarter turn counter clockwise (see left
arrow in Figure 3.13) to release it.
Chapter 3
Maintenance
3-7
5. Then turn the knob (see right arrow in Figure 3.13) until the air bubbles are at the
size as required (size between 2 and 5 mm without the meniscus at both sides).
More pressure creates bigger air bubbles; less pressure smaller air bubbles.
6. When the air bubbles are at the required size, tighten the locking ring by turning it
clockwise (make sure not to turn the knob with it).
7. Close the front cover and replace and tighten the screw.
3.7
Changing pre-mount membranes
Required: Membranes with the cat.no. SA5282 or SA5283.
Remark: For Teflon and pergamin membranes follow the procedure as described in
the corresponding method sheet.
1. Loosen and remove the
dialyzer mounting bolts with a
hexagonal wrench (see Figure
3.14). Start with the middle
bolts and work out.
Figure 3.14
2. Gently lift off the top half of the
dialyzer and remove the old
membrane (see Figure 3.15).
3. Clean the dialyzer block on
both sides with water and dry
with a cloth; make sure that
both surfaces are free of dirt.
4. Take a new membrane, open
the package by cutting the
plastic package at three sides
to avoid any damage to the
membrane (see Figure 3.16)
5. Open the flap you created and
take out the membrane
carefully by the white plastic
surroundings.
6. Rinse the new membrane with
distilled water to remove the
conservation fluid. Center the
membrane on the dialyzer
bottom plate (see Figure 3.17).
Make sure that the flat side is
under (carton side up).
Figure 3.15
Figure 3.16
Figure 3.17
Chapter 3
Maintenance
3-8
7. Make a cross incision with a
blade in the membrane on the
2 center holes of the dialyzer
bottom plate. Make also cross
incisions on the holes for the
mounting bolts (for this size of
dialyzer 4, see Figure 3.18).
8. Carefully position the dialyzer
top plate on the bottom plate
(see Figure 3.19).
Figure 3.18
9. Carefully push the mounting
bolts through the membrane
and tighten the bolts until
Figure 3.19
finger tight (see Figure 3.20).
10. Then tighten the bolts with an
Allen key (starting with the
inside bolts), carefully tighten
down in stages to hand tight.
Rinse the system several
minutes with distilled water
and check if there are no leaks
Figure 3.20
Important notes:
1. When the analyzer is not in operation the membrane should remain in contact
with the rinsing liquid/distilled water. Never leave the membrane dry.
2. If the membrane frequently breaks during rinsing, it is advisable to use 1 drop of
wetting agent per liter in the rinsing liquid of the unit (not in the rinsing liquid of the
sampler!).
Chapter 4
4
TECHNICAL INFORMATION
4.1
Technical specifications
4-1
SA3000/5000
Material housing:
Housing:
Power supply:
Dimensions:
With integrated rack:
Weight:
Power consumption:
Fuses:
Capacity:
Waste:
Detection:
Performance:
Safety:
Air supply:
External gas supply:
Air injector:
Capacity air injector:
Injection:
Fan:
Reactor control:
Pump:
Pump speed:
Motor pump:
Pump decks:
Roller cage:
Capacity:
Polypropylene
According CE and CSA regulations
100-240 V
27 cm (H) x 54 cm (D) x 84 cm (W)
67 cm (H) x 54 cm (D) x 84 cm (W)
± 25 kg
650 VA max.
3.15 A (230 V), 6.3 A (115 V)
5 chemistry module positions
5 separate glass waste receptacles
4 positions for dual detection heads and 5 positions
for detection heads with matrix correction
Software controlled hardware on/off switching (with
system controller)
Leak detection (with system controller)
Membrane pump with pressure regulator
1 bar (100 kPa)
Mechanical, dual bar
10 channels
30 air bubbles/min. at normal pump speed
24 V DC
Built-in dual channel controllers, max. 2, if required
for the application(s) installed
Multi-speed (off, standby, normal, high)
1 rpm. (standby), 6 rpm. (normal) and 10 rpm. (high)
Stepper motor
2, fully removable*
2 x 10 stainless steel rollers*
2 x 16 channels*
* SA3000 has the same specifications as model SA5000, except that the
proportioning pump is provided with 1 pump deck, 1 x 10 stainless steel rollers and 1
x 16 channels
Chapter 4
4-2
4.2
Housing
The chemistry unit consists of three compartments (see Figure 4.4).
Compartment 1 houses the power supply board, the proportioning pump, the
membrane pump with air-reducing valve, the reactor control unit(s) and the
electronics for the reactor control unit(s) and pump.
• Compartment 2 houses the chemistry modules (up to five).
• Compartment 3 houses the detection heads and the waste receptacles.
In Compartment 1 the proportioning pump (4) is mounted on top of the bracket
above the electronic boards. The electronic boards are mounted upside down against
the bracket and can, if necessary, be reached from the bottom side after removing
the cover of the bracket. The multi-speed proportioning pump has two pump decks,
divided by the air injector and is provided with a drain to compartment 2 in the case
that the pump tubing are leaking. (The SA3000 has a pump with one pump deck).
The membrane pump with reducing valve for the air supply is placed just behind the
front cover (5, membrane pump not visible on Figure 4.4, see Figure 3.13).
In the front cover (see Figure 4.1), the On/Off switch and the speed selector for the
multi-speed proportioning pump is placed. Also a dual channel reactor control unit is
mounted here. If no reactors are present a blind plate covers the opening.
•
Figure 4.1 Front cover
Figure 4.2 Back cover
Figure 4.3
In the back cover (see Figure 4.2 and no. 6 in Figure 4.4) the power entry, the fan,
the connector (9-p sub-D) for the system controller, the reactor control unit (only if
more than two reactors are present on the chemistry modules), the air inlet and 4
mini DIN connectors for external connections are placed. When more than 4 reactors
and/or other devices (as UV digesters, analogue detectors and external pumps) are
present, and the system is equipped with a system controller, these devices are
connected to an external system controller power bar (cat. no. 28505940, see Figure
4.3), which is connected to the required DIN connector on the interface. Each type
requires its own socket bench. The DIN connector called ‘second CFA’ is used to
connect a second SA5000 chemistry unit to be controlled by the same system
controller (cable is connected to 9-p sub D on second chemistry unit).
Chapter 4
4-3
In Compartment 2 up to five module plates can be placed (max. 3 with a width of 83
mm and 2 with a width of 105 mm) complete with reactors and UV digesters (placed
under the module plate). The connectors for the reactors are placed in the wall
between compartment 1 and 2. Dialyzers, heat exchangers and ionexchange/reduction columns can be part of the chemistry module. Two doors (one at
the front side and one at the back side) provide access under the module plates,
where the leak detectors are placed on the bottom. The back door is provided with
openings for tubing and cables (i.e. for water bath and UV digester). The
configuration with narrow and wide module plates is dependent on the requested
applications.
Figure 4.4 Housing SA 5000
In Compartment 3 the detection heads are placed. In principle up to four 2-channel
detection heads can be placed or up to 5 detection heads with matrix correction. Up
to five waste receptacles are mounted in clamps. The compartment is provided with a
door at the side with openings for detection cables and waste tubing. Optionally a
back panel is integrated on the chemistry unit for distillation parts (see Figure 1.1).
Chapter 4
4-4
4.3
Proportioning pump
The multi-speed proportioning pump (cat. no 22300360) with integrated air-bubble
injector is belt-driven by a stepper motor. The pump speed can be varied.
The pump has two roller cages (cat. no. 22300361 has one roller cage) that are
turned by a rotary axle with needle bearing. Up to 16 pump tubing can be mounted
over each roller cage on the combs by means of the bridges on the pump tubing. The
roller cages are closed by the pump decks. The pump decks are provided with
springs. When the pump handle is in its lower position, the inside of the deck pushes
against the tubing thus bringing pressure on the tubing at a calibrated level. The
inside of the pump deck is slotted in such a way (double radius) that the most
possible gradual flow is obtained. The sides of the pump deck rest, in closed position,
on a support. When the pump deck is closed (or opened) the pump tubing’s are also
stretched (or released) by the tightening mechanism fixed to one comb. When the
pump is operating the roller cages rotate and at least one of the rollers is pushing
against the tubing’s. When the roller cages are turning the tubing’s are held taut and
the liquid is drawn into the tubing’s and then pushed forward.
Figure 4.5 Proportioning pump
To prevent premature wearing, the pump decks should always be slightly greased
and opened when the analyzer system is not in use. Only when a system controller is
present on the analyzer system it is not necessary to open the pump decks (see also
the FlowAccessTM manual).
Chapter 4
4-5
The Cross-sections of air-injector and pump are shown in Figure 4.6 and Figure 4.7.
Figure 4.6
Figure 4.7
The pump speed is changed by the speed selector in the front panel. Four modes are
possible:
1. Off
2. Standby (1 rpm). This speed can be used to save reagents between two analyses
and keeps the system in fast start-up condition
3. Normal (6 rpm). This speed is used during analysis.
4. High (10 rpm). This speed can be applied for fast rinse at the end of the analysis
before shutdown
By pressing shortly on the selector, one can toggle between the speed options. To
switch the pump off, press the selector during a few seconds.
When the power switch is put on, the pump starts automatically at normal speed,
even if the chemistry unit was switched off in another mode.
Any liquid that is leaking from the pump tubing in the pump is collected under the
pump and drained to the chemistry compartment. If a system controller is present,
the leak will be detected and the system is shut down.
4.4
Chapter 4
4-6
Air injector
The air-injector is assembled in the proportioning pump and is driven by the motor of
the proportioning pump, so the air bubble supply is synchronous parallel with the
liquid supply. The air-injector pump is supplied with air by the membrane pump. The
membrane pump supplies air continuously when the proportioning pump is on. The
air tubes are laying on top of the air-injector under two bars.
A wheel, with five bars, connected with the main axle of the roller cages, turns at the
same speed as the roller cages. Above the wheel two rollers are located that are
pushed up each time one of the five rollers passes beneath it. These rollers are
located under a tumbler that pushes one bar up and the other bar down each time
the rollers go up. This mechanism results in a precise uniform up and down
movement of the bars, creating a regular pattern of 30 air bubbles per minute at
normal speed (6 rpm). This working principle allows automatic injection of air bubbles
in the manifolds through which the samples enter the chemistry modules. Up to ten
air tubing’s (cat. no. SA3150 or SA5150) can be connected to the air pins on the air
block. If not all air pins are used the remaining pins should be short-circuited by
pieces of tubing.
When releasing the air tubes always switch off the power. Pull the rings and turn
them a quarter of a turn.
Figure 4.8 Air pump
4.5
Membrane pump
The membrane air pump operates with an electromagnetic drive and is suitable for
permanent use. The air pump is placed in compartment 1 of the chemistry unit below
the proportioning pump and just behind the front cover. The pump takes the air
directly from the atmosphere and provides a constant airflow. The input of the air
pump is connected with the air inlet nipple in the back cover, providing fresh air
supply. The output of the air pump is connected to the reducing valve and then to the
air block of the air injector.
When the use of nitrogen or clean compressed air is necessary, the air pump can be
connected at the back of the instrument with a nitrogen (or compressed air) supply.
The nitrogen (or compressed air) supply must be adjusted prior to the inlet of the
chemistry unit with a regulator valve at 0.9 to 1 bar (14-15 psi or 90 – 100 kPa).
The tubing for the connections from and to the membrane pump is cat.no. SA 5133.
4.6
Chapter 4
4-7
Reactor and control unit
If a reactor is required for the chemistry module,
this reactor is placed under the module plate and
connected to the electronics by an amphenol
connector in the wall of the compartment. Several
different sizes of reactors with glass or metal
coils are available. For specific information about
the reactor refer to its separate manual.
A built-in reactor control unit controls the
temperature of the reactor. This control unit is
Figure 4.9
placed in the front cover and/or back cover and
each control unit can handle two reactors at the
same time. When the reactor is not switched on the display will show ‘OFF’, as soon
as the chemistry unit is switched on.
To switch on the control unit:
Press the Standby button during 2 seconds (most right button on the control unit).
When the control unit is to be switched off press the standby button again during
2 seconds.
Starting from SA3000 serial number 04115 and SA5000 serial number 04158 it is
possible to switch off one reactor independently by means of the control unit.
•
To switch off one reactor:
Press the button of the reactor to be switched off (S1 or S2) and the Standby
button at the same time during 2 seconds. The display of that channel will show
OFF.
Note: When the chemistry unit was switched off (or after a power cut), both reactors
are always switched on when the chemistry unit is switched on.
•
If a system controller is present on the chemistry unit:
The reactor can be switched on/off by means of the system controller (see the
FlowAccessTM manual). The control unit however stays on when the reactor is
switched off and will keep its settings when the chemistry unit is switched back on.
So when one reactor was switched off before an analysis and the system was
switched off after the analysis by the system controller, this reactor stays off when the
system is waked up and has to be switched on manually by keeping the
corresponding button and Standby button pressed simultaneously during 2 seconds.
Temperature display:
The control unit will be pre-set on the required temperature for the chemistry module.
When the control unit is switched on, the display will show the actual temperature of
the reactor as indicated by the light on the display (LED 1 ON = actual temperature of
S1 and LED 2 ON = actual temperature of S2). By default the temperature of S1 is
displayed.
To switch to the display of the actual temperature of the second reactor (S2) press
the S2 button during a moment.
To display the pre-set temperature of a reactor keep the corresponding button
pressed. As soon as the button is released the actual temperature is displayed again.
The pre-set temperature can be changed if required (see chapter 4.6.1).
Chapter 4
4-8
4.6.1 Adjusting the pre-set temperature
The pre-set temperature of the reactors can be adjusted if required by using a
combination of buttons.
To increase the pre-set temperature of reactor 1:
1. Press button S1 and keep it pressed (the current pre-set temperature is
displayed).
2. Press the arrow-up button until the required pre-set temperature is displayed.
Then release both buttons. The actual temperature is displayed.
3. The reactor will heat up until the pre-set temperature is achieved.
To decrease the pre-set temperature of reactor 1:
1. Press button S1 and keep it pressed (the current pre-set temperature is
displayed).
2. Press the arrow-down button until the required pre-set temperature is displayed.
Then release both buttons. The actual temperature is displayed.
3. The reactor will cool down until the pre-set temperature is achieved.
Use the same procedure for the adjustment of reactor 2 with button S2.
4.6.2 Error messages
The following messages can be displayed:
F1:
Caused by short circuit or crack in sensor 1. Check if the cable of reactor 1
was properly connected to the required connector in the separation wall
between compartment 1 and 2.
F2:
Caused by short circuit or crack in sensor 2. Check if the cable of reactor 2
was properly connected to the required connector in the separation wall
between compartment 1 and 2.
EP:
Lost of parameter settings. The control unit has to be sent to Skalar or your
local representative for repair.
5
Chapter 5
Spares and consumables
5-1
SPARES AND CONSUMABLES
For the cartridge components refer to the Method sheet provided for each chemistry
module and the accessory booklet.
Number
SA5703
SA5418
SA5419
SA2010
SA5204
SA5133
SA3150
SA5150
SA3142
SA5141
SA5142
SA5282
SA5283
SA5400
SA5401
SA5402
SA5406
SA5408
SA5414
SA5415
SA5410
SA5219
25200099
25300006
25300007
26990906
26990910
26001006
26001007
90037513
90028010
90040014
90040336
90028120
90028118
90020011
90024107
90020800
90028823
Description
Toolkit & Start up kit (for content see next page)
Lubricant
Glue
Grease for pump decks
Inlet connector H Glass 2 mm
Tygon tubing 3.2 x 6.4 mm
Silicon tubing 0.5 mm ID
Silicon tubing 1.0 mm ID
Polyethylene tubing 0.5 mm ID
Membranes pre-mount, small
Membranes pre-mount, large
Sleeve, tygon 3.2 mm ID
Sleeve, silicon 2.4 mm ID
Sleeve, polyethylene 1.5 mm ID
Sleeve, acidflex 1.90 mm ID
Acid resistant valve tubing
Pinners
Swivel for manifolds
Bolt for tube fitting on heat exchanger
Tube fitting for heat exchanger
Grey filters 0.6 O.D.
Diaphragm 0.5 mm
Diaphragm 1 mm
Mounting clip 30 mm ID
Cooling fan 24 V
Membrane pump 24 V
Reducing valve
Temperature controller
Power supply
Lamp indication power switch
Push button for speed selection
Motor for pump 22300360/61
Fuse slow 5x20 VDE 3.15 A
Quantity
1
1 bottle, 25 ml
1 bottle, 25 ml
1 pot, 50 ml
1
15 m
3m
15 m
5m
15 m
15 m
1 pack (12 pcs.)
1 pack (12 pcs.)
1 bag (50 pcs.)
1 bag (50 pcs.)
1 bag (50 pcs.)
1 bag (50 pcs.)
1 bag (50 pcs.)
1 bag (25 pcs.)
1 bag (25 pcs.)
1 set (5 pcs.)
1 set (2 pcs.)
1
1
1
set (6 pcs.)
set (6 pcs.)
1
1
1
1
1
1
1
1
1
1
1
1
Number
90028826
90039520
90039531
25120051
25121707
25121704
25121705
22300319
22300010
22300317
22300311
22300320
Chapter 5
Description
Fuse slow 5x20 VDE 6.3 A
O-ring 2.5x1 Buna
O-ring 4x1 Buna
Waste receptacle
Pump speed selector board
Heating control board A
Heating control board B
Pump deck complete
Handle for pump deck
Springs for pump deck
Bubble injector for pump
Needle block for bubble injector
Quantity
1
1
1
1
1
1
1
1
1
1
1
1
5-2
Chapter 5
Toolkit and Start up kit
Cat. no. SA 5703
Description
Grease for pump decks
Inlet connector H Glass 2 mm
Pinners for StSt needles
Sleeve tygon 3.2 mm ID
Sleeve tygon 2.4 mm ID
Sleeve silicone 2.0 mm ID
Acid resistant valve tubing
Lubricant
Swivel for manifolds
Bolt for tube fitting on heat exchanger
Tube fitting for heat exchanger
Hexagonal key 1.5 mm
Hexagonal key 2.5 mm
Hexagonal key 3 mm
Hexagonal key 5 mm
Lamp extractor
Reset rod for reactor
Bulb extractor tool
Open-end wrench
Screwdriver m 2.5
Scalpel holder type 4
Scalpel type 24 (broad blade)
File
Fuse slow 5x20 mm VDE 250mA
Fuse slow 5x20 mm VDE 1A
Fuse slow 5x20 mm VDE 3.15A
Fuse slow 5x20 mm VDE 6.3A
Fuse slow 5x20 mm CSA 400mA
Fuse slow 5x20 mm CSA 2 A
Fuse slow 5x20 mm CSA 6 A
Fuse slow 6.3x32 mm CSA 800mA
Screw M3 x 4 ck nylon PA6.6
O-ring 2.5x1 Buna
Quantity
1 (50 ml)
2 pcs.
1 set (2 pcs.)
10 pcs.
10 pcs.
10 pcs.
5 pcs.
6 pcs.
6 pcs.
1 (25 ml)
1 pc.
1 pc.
1 pc.
3 pcs.
3 pcs.
1 pc.
1 pc.
1 pc.
1 pc.
1 pc.
1 pc.
1 pc.
1 pc.
1 pc.
1 pc.
5 pcs.
1 pc.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
2 pcs.
1 pc.
1 pc.
5-3
Chapter 5
Description
O-ring 4x1 Buna
Tubing silicone 0.5x2.5 mm Raumedic
Tubing silicone 1.0x3.0 mm Raumedic
Tubing PE 1.0x2.7 mm PT53E
Tubing PE 1.5x2.7 mm PT54
Tubing PE 0.5x2.5 mm PT50A
Tubing FEP 1.0x2.0 mm
Quantity
1 pc.
1m
1m
1m
1m
1m
5m
5-4
Index
INDEX
A
Air ........................................................ 2-2
Air bars................................................. 2-5
Air injector .............................. 1-1, 4-2, 4-6
Air scrubber .......................................... 2-3
Autosampler ......................................... 1-2
B
Back panel .................................... 1-2, 2-3
C
Chemistry module ................................ 4-2
Chemistry modules............................... 1-1
Chemistry unit ........................ 1-1, 2-2, 2-3
Column .......................................... 2-5, 4-3
Computer ............................................. 2-2
Computer screen .................................. 2-2
Consumables ....................................... 5-1
Cooling ................................................. 1-1
Customer acceptance .......................... 1-7
D
Damage ............................................... 2-1
Detection .............................................. 1-1
Detection head ....................... 2-3, 4-2, 4-3
Dialysis ................................................. 1-1
Dialyzer ................................................ 4-3
Digital detector ..................................... 2-4
Distillation ...................................... 1-1, 2-3
F
Flow cell ............................................... 2-5
FlowAccessTM ................................ 1-2, 2-5
Fuses ................................................... 2-2
G
Gas-reducing valve ....................... 2-2, 2-5
Grease ................................................. 3-1
H
Heat exchanger ............................. 2-3, 4-3
Heating ................................................. 1-1
High speed ........................................... 4-5
Hydrolysis............................................. 1-1
I
Installation ..................................... 2-1, 2-3
Instrument requirements ................... 2-2
Laboratory requirements................... 2-1
Instrument requirements.... See Installation
Interface ........................................ 2-2, 2-4
Interference filters ................................. 2-4
Introduction ........................................... 1-1
Ion-exchange/reduction.................. 1-1, 4-3
L
Laboratory requirements .... See Installation
Leak detection ............................... 1-2, 2-4
Location ................................................ 2-1
Lubricant ............................................... 2-3
M
Maintenance ......................................... 3-1
6 Monthly .......................................... 3-2
Changing pre-mount membranes ...... 3-7
Changing the air tubing ..................... 3-2
Daily .................................................. 3-1
Dialyzer ............................................. 3-7
Monthly ............................................. 3-1
Replacing the pump deck springs ..... 3-6
Replacing the pump tubing................ 3-2
Scheduled ......................................... 3-1
Stretching the pump tubing ............... 3-2
Tubing connections ........................... 3-4
Weekly .............................................. 3-1
Yearly................................................ 3-2
Matrix correction ................................... 4-3
Membrane pump ............................ 4-2, 4-6
Method sheet ........................................ 2-4
Multi-speed pump ............ 1-1, 1-2, 4-2, 4-4
N
Nitrogen .................................. 2-2, 2-4, 4-6
Normal speed ....................................... 4-5
P
PC ........................................................ 2-4
Perspex manifold .................................. 2-3
Power consumption .............................. 2-2
Power supply ........................................ 2-2
Printer ............................................ 2-2, 2-4
Proportioning pump................. 4-2, 4-4, 4-6
Pump deck ..................................... 2-5, 4-4
Pump speed.......................................... 4-5
Pump tubing................................... 2-4, 4-4
R
Reactor .......................................... 4-3, 4-7
Reactor control
Adjusment ......................................... 4-8
Error messages................................. 4-8
Reactor controller............. 1-2, 2-5, 4-2, 4-7
Reactors ............................................... 1-2
Reagents ....................................... 2-1, 2-3
Roller cage ........................................... 4-4
S
SA3000/5000 .................. 1-1, 1-2, 2-2, 4-1
Housing ............................................ 4-2
Safety precautions................................ 1-3
Sampler ......................................... 2-2, 2-3
Segmentation ....................................... 2-4
Skalar ................................................... 1-5
Software ............................................... 2-5
Spares.................................................. 5-1
Speed selector .............................. 4-2, 4-5
Standby speed ..................................... 4-5
System controller........................... 1-2, 2-3
T
Technical drawings............................... 4-8
Technical information ........................... 4-1
Technical specifications........................ 4-1
Index
Time program ....................................... 3-1
Transport .............................................. 2-1
Tumbler ................................................ 4-6
U
Unpacking ............................................. 2-1
UV digester ........................................... 4-3
UV digestion ......................................... 1-1
V
Valves ............................................ 1-2, 2-4
Voltage selector .................................... 2-3
W
Warranty registration ............................. 1-5
Waste facility......................................... 2-1
Waste receptacle .................... 1-1, 2-5, 4-2
Water bath ............................................ 4-3

SFA SA3000-5000D newpump

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Animas® Insulin Pump Exposure to X-rays or

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Heavy duty PTO pump

Totally “Tube”ular Tweens

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a pdf of this case study

Stiletto Airless Pump - CSI - Cosmetic Specialties International