hisham abass
Transcription
hisham abass
Winter 2014 Saudi Aramco A quarterly publication of the Saudi Arabian Oil Company Contents Shale Gas Characterization and Property Determination by Digital Rock Physics 2 Anas M. Al-Marzouq, Dr. Tariq M. Al-Ghamdi, Safouh Koronfol, Dr. Moustafa R. Dernaika and Dr. Joel D. Walls Chemically Induced Pressure Pulse: A Novel Fracturing Technology for Unconventional Reservoirs 14 Ayman R. Al-Nakhli, Dr. Hazim H. Abass, Mirajuddin R. Khan, Victor V. Hilab, Ahmed N. Rizq and Ahmed S. Al-Otaibi Integrating Intelligent Field Data into Simulation Model History Matching Process 25 Bevan B. Yuen, Dr. Olugbenga A. Olukoko and Dr. Joseph Ansah Borehole Casing Sources for Electromagnetic Imaging of Deep Formations 34 Dr. Alberto F. Marsala, Dr. Andrew D. Hibbs and Prof. Frank Morrison Laboratory Study on Polymers for Chemical Flooding in Carbonate Reservoirs 41 Dr. Ming Han, Alhasan B. Fuseni, Badr H. Zahrani and Dr. Jinxun Wang Sweet Spot Identification and Optimum Well Planning: An Integrated Workflow to Improve the Sweep in a Sector of a Giant Carbonate Mature Oil Reservoir 52 Dr. Ahmed H. Alhuthali, Abdullah I. Al-Sada, Abdullah A. Al-Safi and Mohamed T. Bouaouaja Innovation in Approach and Downhole Equipment Design Presents New Capabilities for Multistage Stimulation Technology 61 Mohammed A. Al-Ghazal, Saad M. Al-Driweesh, Mustafa R. Al-Zaid and Fadel A. Al-Ghurairi Deploying Global Competition by Innovation Network for Empowering Entrepreneurship, Venturing and Local Business Development: A Case Study — Desalination Using Renewable Energy Dr. M. Rashid Khan 70 Journal of Technology THE SAUDI ARAMCO JOURNAL OF TECHNOLOGY Shale Gas Characterization and Property Determination by Digital Rock Physics Authors: Anas M. Al-Marzouq, Dr. Tariq M. Al-Ghamdi, Safouh Koronfol, Dr. Moustafa R. Dernaika and Dr. Joel D. Walls ABSTRACT Unconventional shale reservoirs differ largely from conventional sandstone and carbonate reservoirs in their origin, geologic evolution and current occurrence. Shale comprises a wide variety of rocks that are composed of extremely fine-grained particles with very small porosity values on the order of a few porosity units and very low permeability values in the nanodarcy (nD) range. Shale formations are very complex at the core scale: they exhibit large vertical variations in lithology and total organic carbon (TOC) at a scale so small that it renders core characterization and sweet spot detection very challenging. Shale formations are also very complex at the nano-scale level, where pores having different porosity types are detected within the kerogen volume. These complexities have led to further research and the development of an advanced application of high resolution X-ray computed tomography (XCT) scanning on full-diameter core sections to characterize shale mineralogy, porosity and rock facies so that accurate evaluation of the sweet spot locations can be made for further detailed petrophysical and petrographic studies. In this work, argillaceous shale gas cores were imaged using high resolution dual-energy XCT scanning. This imaging technique produces continuous whole core scans at 0.5 mm spacing and derives accurate bulk density (BD) and effective atomic number (Zeff) logs along the core intervals, logs that are crucial in determining lithology, porosity and rock facies. Additionally, integrated X-ray diffraction (XRD) data and energy dispersive spectroscopy (EDS) analysis results were acquired to confirm the mineral framework composition of the core. Smaller core plugs and subsamples representing the main variations in the core then were extracted for much higher resolution XCT scanning and scanning electron microscopy (SEM) analysis. Porosity, mainly found in organic matter, was determined from 2D and 3D SEM images by the image segmentation process. Horizontal fluid flow was only possible through the organic matter and the simulations of 3D focused ion beam (FIB)-SEM volumes by solving the Stokes equation using the Lattice Boltzmann method (LBM). A clear trend was observed between porosity and permeability, correlating with identified facies in the core. Silica-rich facies gave higher porosity-permeability relationship characteristics 2 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY compared to the clay-rich facies. This is mainly caused by the pressure compaction effect on the soft clay-rich samples. High percentages of organic matter were not found to be a good indication for high porosity or permeability in the clay-rich shale samples, while the depositional facies was found to have a great effect on the pore types, rock fabric and reservoir properties. The results and interpretations in this study provide further insights and enhance our understanding of the heterogeneity of the organic-rich shale reservoir rock. INTRODUCTION Hydrocarbon recovery factors from unconventional organicrich shale have always been at the lower end of historic figures from conventional reservoirs1. The reason for this is the ultralow permeability of the rock, which requires massive hydraulic fracturing to enhance connectivity, and therefore, permeability for the flow. The fracturing technique should have the potential to lead to economical hydrocarbon production by creating a complex fracture network that is made up of many interconnected fractures in close proximity to one another. To choose the right fracturing technique, one must have a good understanding of the reservoir characteristics at multiple scales. The evaluation of shale, however, is complicated by the structurally heterogeneous nature of the fine-grained strata and their intricate pore networks, which are interdependent on many geologic factors, including total organic carbon (TOC) content, mineralogy, maturity and grain size. In this work, full-diameter whole core samples from a shale gas reservoir in the Middle East were characterized at the core and pore scale levels. The core samples were analyzed using the dual-energy X-ray computed tomography (XCT) scanning technique to locate potentially high quality rock intervals with high porosity and high TOC. Data acquired from 2D scanning electron microscopy (SEM) and 3D focused ion beam (FIB)SEM analysis were studied to characterize the kerogen content in the samples, together with (organic and inorganic) porosity and rock fabric. The mineral framework of the samples was determined from energy dispersive spectroscopy (EDS) analysis. The FIB-SEM images in 3D were used to determine porosity and TOC by segmentation and to determine directional permeability by the Lattice Boltzmann method (LBM). Trends were obtained among the computed data, in addition to the TOC and rock fabric values that are necessary for proper shale evaluation and completion considerations. A clear trend was observed between porosity and permeability in relation to identified facies in the core. Silica-rich facies gave higher poroperm characteristics compared to the clay-rich facies. The depositional facies was found to have a profound effect on the pore types, rock fabric and reservoir properties. DUAL-ENERGY COMPUTED TOMOGRAPHY IMAGING XCT imaging is a powerful nondestructive technique used in the oil industry to evaluate the internal structures of cores. The acquisition of high resolution continuous images along the core length is essential in complex reservoirs to characterize reservoir heterogeneity and optimize sample selection for further detailed analysis. Dual-energy computed tomography (CT) scanning involves imaging the core at two energy levels at the same location. This dual-energy imaging provides two distinct 3D images of the core by using a high and a low energy setting. The high energy images are slightly more sensitive to bulk density (BD) — Compton scattering effect — and the low energy images are slightly more sensitive to mineralogy — photoelectric absorption effect2. The high resolution computed BD values and effective atomic number (Zeff), or photoelectric factor (PEF), values can be used in shale formations to interpret and quantify porosity, organic content (for identifying sweet spots) and mineralogy. When combined with other commonly available information, such as core spectral gamma data, more complex analyses can be performed. For example, the elastic properties and brittleness index can be determined3. Recently, the technique has been used in complex carbonate and sandstone reservoirs in the Middle East to characterize reservoir heterogeneity and optimize the sample selection for special core analysis testing4-6. In cases of poor core recovery and drilling mud invasion, it becomes more practical to correlate the CT data to density logs or photoelectric logs instead of the natural gamma ray logs. presented in green. In this perspective, low PEF values (around 1.8) and low BD (<2.4) would indicate silica-rich shale with low clay content and high porosity. Five different facies were detected and highlighted in Fig. 1b. Figure 2 plots the BD data vs. PEF with the highlighted facies. Reference lines for the main minerals are shown in the figure to indicate mineralogy variations in the core. It is clear from Fig. 2 that this core contains no calcite minerals. The five different color facies were identified as follows and summarized in Table 1: • Green facies: Data with low density and low PEF. When Fig. 1. Dual-energy CT data along 49 discontinuous 1 ft core sections: (a) BD, (b) identified facies, (c) PEF, (d) PEF with reversed BD, and (e) radial crosssectional images. CORE CHARACTERIZATION AND SAMPLE SELECTION Dual-energy CT scanning was performed on a total of 49 ft of core (49 discontinuous 1 ft sections) from a shale source rock reservoir in the Middle East. The dual-energy logs in Figs. 1a and 1c provided accurate BD and PEF data, respectively, along core lengths that were used to characterize the core sections and to efficiently identify sweet spots for the representative selection of plug sampling locations. Shale formations are often composed of stacked para-sequences7 that are quite thin and difficult to detect from well logs. This high resolution data from the whole core therefore provides a powerful tool to define these para-sequences. Figure 1d plots the PEF data with reversed scale BD to highlight the best quality shale intervals, with the largest gap Fig. 2. BD vs. PEF for all dual-energy CT data. Color cutoffs were identified from Fig. 1d to highlight variations in shale properties. Reference lines for the main minerals are shown in the figure to indicate mineralogy variations in the core. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 3 Color Facies Porosity Organic Matter Silica Clay Carbonate Green High High High Low Low Red Low High Low High Low Black Very low Low High Low Low Blue/ Yellow Very low Low Low High Low (a) green facies, large green fill (low PEF, low BD) Table 1. Potential description of each identified facies in the cores based on PEF and BD values from dual-energy CT data BD is reversed as in Fig. 1d, it creates the largest gap between the PEF and ROHB curves. This identifies the potential regions for silica-rich shale with high porosity/organic matter and low clay content (sweet spots). This behavior is clearly shown in one of the zoomed intervals as represented by Fig. 3a. • Red facies: Data with medium density and medium PEF. When BD is reversed, it creates a small gap between the curves. This identifies potential regions for clay-rich shale with low porosity/high organic matter and low silica content. This behavior is clearly shown in one of the zoomed intervals as represented by Fig. 3b. • Black facies: Data with high density and low-to-medium PEF. When BD is reversed, it creates no gap between the curves. This identifies potential regions for silica-rich shale with very low porosity/low organic matter and low clay content. This behavior is clearly shown in one of the zoomed intervals as represented by Fig. 3c. • Blue/yellow facies: Data with high density and medium PEF. When BD is reversed, it creates a large gap between the curves filled with blue. This identifies potential regions for clay-rich shale with very low porosity/low or ganic matter and low silica content. The larger gap in this group indicates denser layers, which are indicated with yellow; the layers are otherwise blue, as can be clearly seen in the “facies” and “radial image” columns in Fig. 3d. Table 1 provides only qualitative indications for the facies variations in the cores and should be confirmed by further detailed analysis using X-ray diffraction (XRD), EDS and SEM. It should also be noted that (in this analysis) each color facies has a range of dual-energy data that allows for shale property variations within the same facies. Therefore, the description in Table 1 should be used only to locate potentially high quality shale for sampling and further analysis. Facies-based Sample Selection Figure 4 combines wireline log data with the dual-energy XCT derived data. In column (c) the BD data from dual-energy CT shows a reasonable match with the wireline density log. Column (h) shows the percentage of quartz obtained from the XRD analysis performed in selected locations in the core to 4 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY (b) red facies, small green fill (medium PEF, medium BD) (c) black facies, small blue fill (medium PEF, high BD) (d) blue/yellow facies, large blue fill (medium PEF, high BD) Fig. 3. Example of color facies based on the dual-energy CT data from Fig. 1d. confirm the facies distribution determined from dual-energy CT and described in Table 1. High quartz percentages from the XRD data confirmed the green facies in the core and the facies description in Table 1. Similarly, column (j) shows high clay concentrations from the XRD data for the red and yellow facies, which are characterized by medium-to-high PEF values, thereby confirming the descriptions in Table 1. The nine arrows in Fig. 4. (a) wireline gamma ray, (b) total gamma, (c) wireline density vs. duel-energy density, (d) identified facies from dual-energy CT, (e) PEF from dual-energy CT, (f) PEF with reversed BD from dual-energy CT, (g) recommended sampling locations, (h) % quartz from XRD data, (i) wireline neutron/density, (j) % clay minerals from XRD data, (k) potassium log, (l) thorium log, and (m) uranium log. Arrows in column (g) indicate selected plug locations for further porosity, permeability and TOC characterization. Arrow colors refer to identified facies from dual-energy CT. Fig. 4g indicate the selected plug sampling locations in the core for further shale characterization. Five samples were cut from the green facies (identified sweet spot), three from the red facies and one from the yellow facies. The goal of this facies analysis and sample selection is to explore the possible links between shale depositional facies and pore types in shale rocks. This will enhance our understanding of the overall reservoir quality. It is also our goal to quantify the relationship between porosity and matrix permeability for each identified facies in the core. Identifying such trends of poroperm data and facies would facilitate upscaling, reserves estimation and well-to-well correlation. PETROPHYSICAL PROPERTIES Laboratory-based core analysis data on shale rocks are very difficult to obtain due to the tight nature of these rocks. Traditional laboratory evaluation methods may not be applicable to shale, and therefore the continued development of laboratory methods is required to help characterize and understand challenging shale reservoir behaviors. In recent years, digital imaging technology has been extensively used in the petroleum industry, including in shale formations8, to obtain fast and reliable core data such as porosity and permeability. The new emerging technology has been called digital rock physics (DRP) and has contributed reliably to the computations of reservoir properties through image segmentation in 3D and direct simulation4, 9-11. Micro XCT Imaging Each selected plug sample from the nine whole cores was scanned with a micro XCT scanner at a resolution of 40 microns per voxel. A series of multiresolution scans was then acquired, down to 4 microns per voxel, to evaluate the microscale heterogeneity and to scout for an optimal location in the sample for further SEM analysis. These micro XCT scans were combined with X-ray fluorescence readings to characterize the elemental composition of the sample and to locate a region that could adequately represent the sample. Figure 5 presents an example of such images from Sample #1. 2D SEM In Fig. 5d, a representative region (outlined in red) was selected for 2D SEM overview. The 2D SEM area was extracted and polished with a broad ion beam, resulting in a smooth surface of approximately 1,000 by 500 microns. That surface was imaged at a resolution of approximately 250 nanometers (nm) per pixel. Then a series of high resolution SEM images was acquired perpendicular to the lamination at a resolution of 10 SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 5 Fig. 5. Multiresolution XCT images from whole core at (a) 500 microns/voxel down to (d) XCT at 4 microns/voxel. Fig. 6. 2D SEM images from plug Sample #1: (e) 2D SEM overview image at 250 nm/pixel selected from the XCT image at 4 microns/pixel (d); (f) a set of 10 high resolution 2D SEM images at 10 nm/pixel; (g) one representative high resolution 2D SEM image chosen for 3D FIB-SEM (the 3D area of interest is outlined in red). nm per pixel. It is at this resolution that we were able to observe and quantify porosity and organic matter content. Figure 6 shows a representation of this analysis. Images were segmented for total porosity, porosity in organic matter, organic matter and high density. These results were used to choose one representative image with high porosity and high organic matter for 3D FIB-SEM. The segmented data for all the nine plug samples are shown in Table 2. The identified facies from the nine samples link very well with the segmented porosity and organic matter percentages. As described in Table 1 from the dual-energy CT data in the core, Table 2 shows that the green facies has the highest porosity, the red facies has low porosity, and the yellow facies has very low porosity. The pictures of 6 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY selected 2D SEM images from the different facies shown in Fig. 7 confirm the obtained data in Table 2. 3D FIB-SEM The area of interest in Fig. 6g was imaged in 3D at a resolution of 15 nm per voxel using FIB-SEM imaging and digital reconstruction techniques. Rock matrix materials, organic matter and porosity were individually identifiable via their unique gray scale signatures. Each of the 3D volumes from the plug samples was digitally analyzed, and volumetric percentages of organic matter and total porosity were determined. The porosity was further analyzed and quantified as connected, Plug Sample # Core Facies Porosity (%) Organic Matter (%) Porosity in Organic Matter (%) High Density Material (%) 1 Red 1.58 8.16 1.33 2.06 2 Red 1.51 9.91 1.34 1.74 0.88 4.24 3 Red 1.17 16.37 4 Green 3.09 13.48 2.73 2.99 5 Green 5.36 8.75 4.05 0.57 6 Green 3.95 6.02 2.66 0.53 13.56 3.92 0.82 7 Green 4.80 8 Green 2.63 5.01 1.84 2.46 9 Yellow 0.29 0.75 0.08 0.37 Table 2. Average values from the 10 2D SEM images for each plug sample Fig. 7. Example 2D SEM images (at 10 nm/pixel) representing different facies that were identified at core scale. non-connected and associated with organic matter. The connected porosity was used to compute absolute permeability directly in the 3D digital rocks in the horizontal and (whenever possible) vertical directions using the LBM12. Porosity associated with organic matter can be an indicator of organic matter maturity and flow potential. Table 3 gives the segmented values from the 3D FIB-SEM volumes. The table also gives calculations of the conversion ratio, and the organic porosity and total porosity in percentages. The conversion ratio percent would represent the porosity within the organic matter with respect to the organic matter volume, while the organic-to-total porosity percent would represent the percentage of pores in the organic matter with respect to the total porosity in the 3D volume. The 3D volume data in Table 3 is a clear confirmation of the potential relationship among facies, pore type, porosity and flow characteristics in shale. Both the red and green facies have high percentages of organic matter, but the red facies are at the lower range of porosity, which influenced the flow properties and thereby yielded much lower matrix permeabilities than the green facies samples. This can be quantified in Table 3 by the conversion ratio values, which show higher than 30% for the green facies and lower than 20% for the red facies. These findings suggest that further analysis of the organic matter and mineral framework in the red facies samples is required to determine the reasons behind the lower conversion ratios. Sample #9 was excluded from the 3D FIB-SEM analysis because the sample showed no flow potential due to the very low porosity in the 2D SEM image in Fig. 7 and Table 2. Figure 8 shows video snapshots from the different facies with their different permeability values. This figure serves as a good visual means to evaluate the simulated directional permeability values in Table 3. Sample #1 has low horizontal permeability with low porosity in the organic matter. Sample #5 has higher horizontal permeability and gave rise to flow in the vertical direction as well. Sample #8 has the highest horizontal permeability value, and the reason is clearly seen to be an unrepresentative streak of organic matter with relatively large pore sizes. The permeability in these shale facies seem to be controlled SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 7 Core Facies Porosity (%) NonConnected Porosity (%) Organic Matter (%) Porosity in Organic Matter (%) Absolute Permeability (Kh) (nD) Absolute Permeability (Kv) (nD) Conversion Ratio (%) Porosity in OM/ Total Porosity (%) 1 Red 2.2 0.9 14.8 2.1 40 0 12.4 95.5 2 Red 2.5 0.8 9.3 2.2 19 0 19.1 88.0 3 Red 3.2 0.8 18.5 3.0 50 0 14.0 93.8 4 Green 6.1 1.5 11.4 5.1 102 0 30.9 83.6 5 Green 5.0 0.8 7.1 4.2 131 32 37.2 84.0 6 Green 6.4 1.2 9.3 5.6 348 21 37.6 87.5 7 Green 5.3 0.6 9.2 4.9 786 0 34.8 922.5 8 Green 7.7 1.2 10.1 6.8 6,111 0 40.2 88.3 Plug Sample # Table 3. Values from 3D FIB-SEM volumes for each plug sample the EDS mineralogy results. Table 5 gives the XRD data and confirms the EDS analysis. Figure 9 presents schematic comparisons between the EDS and XRD analyses for Sample #1 from the red facies and Sample #6 from the green facies. EDS is represented by the mineral distribution map and XRD by the pie chart. EFFECTS OF DEPOSITIONAL FACIES ON PORE TYPES, ORGANIC MATTER, ROCK FABRIC AND RESERVOIR PROPERTIES Fig. 8. Example 3D FIB-SEM video snapshots (at 15 nm/pixel) representing directional flow for different samples. Shale pore systems may generally be described and classified as inter-granular (between grains), intra-granular (within grains) or organic matter13. Porosity within organic matter would be formed by the shrinkage of kerogen during maturation. The inter-granular and intra-granular pores are inorganic and so by the organic matter distribution and the porosity associated with the organic matter. MINERALOGY Areas of interest for the EDS analysis were selected to include the analyzed 2D SEM images and the 3D area of interest. The SEM-EDS area of interest is imaged at a resolution of approximately 200 nm per pixel and covers an area of approximately 200 by 150 microns. Table 4 gives the mineral volume percentages for all plug samples analyzed by EDS. The EDS results confirm a clear link between mineralogy and the core facies as analyzed from dual-energy CT data on the whole cores and as previously described in Table 1. The red and yellow facies are clay-rich shale with less than 25% silica, while the green facies are silica-rich shale with less than 25% clay. One would then be tempted to think of a link between mineralogy and porosity when comparing the red and green facies. These two facies have similar fractions of organic matter but different porosity. The reason for this could be either maturation of kerogen or the mineral framework of the samples. XRD analysis was performed on all nine samples to confirm 8 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Fig. 9. Comparisons between EDS (top) and XRD (bottom) analyses for Sample #1 (red facies) and Sample #6 (green facies). EDS is represented by the mineral distribution map and XRD by pie chart. Reference mineral phase is given for the EDS mineral maps, and legend is given for the XRD pie charts. Plug # Core Facies PlaSilica gioclase KFeldspar Clay Calcite Dolomite Siderite Anhydrite Pyrite Rutile Apatite Other Total 1 Red 13.7 5.0 0.0 72.1 1.0 0.2 0.0 0.0 4.7 0.5 0.0 2.9 100 2 Red 21.3 5.4 0.3 62.4 0.1 2.5 0.0 0.0 4.7 0.5 0.0 2.8 100 3 Red 25.6 9.8 0.0 44.5 0.0 6.1 0.0 0.0 7.6 0.8 0.2 5.5 100 4 Green 57.5 5.6 0.0 29.1 0.0 1.7 0.0 0.0 3.2 0.3 0.9 1.6 100 5 Green 64.8 2.3 0.0 18.7 0.1 3.9 0.0 0.0 1.3 0.1 0.0 8.8 100 6 Green 74.4 1.6 0.5 20.6 0.1 0.2 0.0 0.0 1.0 0.1 0.0 1.6 100 7 Green 73.0 5.0 0.0 19.1 0.1 0.0 0.0 0.0 1.3 0.4 0.0 1.1 100 8 Green 63.4 4.4 0.0 25.3 0.1 2.1 0.0 0.0 1.3 0.5 0.3 2.7 100 9 Yellow 20.2 8.3 0.0 67.0 0.0 0.0 0.0 0.0 0.5 0.5 0.3 3.1 100 Table 4. Volume percent mineralogy from EDS analysis Sample Core Facies Illite/ Smectite Illite+ Mica Kaolinite Chlorite Chert Quartz K Feldspar Plagioclase Calcite Dolomite Siderite Pyrite Total 1 Red 19.9 31.6 15.8 11.2 0.0 10.5 TR 2.1 1.2 1.2 0.0 6.4 100 2 Red 20.2 31.9 12.1 10.0 0.0 12.7 TR 2.9 0.0 1.8 0.0 8.6 100 3 Red 23.9 27.5 0.0 3.5 0.0 21.0 TR 3.6 0.0 2.0 0.0 18.5 100 4 Green 14.8 25.4 0.0 0.2 0.0 42.0 TR 4.2 0.0 4.5 0.0 8.9 100 5 Green 0.0 15.8 0.0 0.0 0.0 76.4 TR 2.3 0.0 1.5 0.0 4.1 100 6 Green 0.4 17.3 0.0 0.0 0.0 74.7 TR 2.8 0.0 1.6 0.0 3.1 100 7 Green 0.2 20.2 0.0 2.6 0.0 69.4 TR 2.0 0.0 0.8 0.0 4.8 100 8 Green 0.2 25.1 0.0 4.0 0.0 58.9 TR 2.3 TR 3.1 2.3 4.0 100 9 Yellow 25.7 35.5 0.0 10.4 0.0 19.3 TR 3.2 0.0 0.0 5.9 0.0 100 Table 5. XRD analysis would normally be located in the matrix. The organic matter itself may also be classified as nonporous, spongy or pendular8. In this study, each area of the 2D SEM produced two images: Secondary electron (SE2) micrographs that are used to quantify porosity and organic matter, and backscattered electron (BSE) micrographs that better display the contrast between the solid components of the rock. Red Facies Figure 10a presents examples of such images for the red facies — Sample #1. In this sample, in the SE2 image, the organic matter appears to be compacted between the delicate clay mineral layers and elongated in the horizontal direction. This compaction must have led to the compaction of the pores within the organic matter. The BSE image clearly shows the clay minerals oriented in the horizontal direction due to overborne pressure. The pores in this facies are almost all in the organic matter, and the porosity value of Sample #1 is around 2% with only 1% porosity connected in the 3D FIB-SEM volume. This has led to a very low matrix permeability of 40 nano-darcy (nD). Green Facies Figure 10b presents examples from the green facies — Sample #7. In this sample, in the SE2 image, the organic matter appears to be protected from severe pressure compaction between the strong quartz grains and the microcrystalline silica particles. The organic matter in this facies seems to have an irregular shape with a spongy type of porosity at 5%. Therefore, the pore space within the organic matter was preserved and gave good connectivity in 3D, which yielded a very high permeability value at 786 nD. The BSE image in Fig. 10b clearly shows the grainy structure of the quartz particles around the organic matter that is spread out in the whole image. The pores in this facies are almost all in the organic matter. The poroperm characteristics of these shale facies are plotted from the Table 3 data and are shown in Fig. 11. The green SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 9 Fig. 12. Organic matter vs. porosity for the red and green facies: The green facies have larger porosity but less organic matter. for North American shale plays, the data from this Middle East shale gas fell within the upper and lower bounds of Eagle Ford shale in the United States. Figure 12 plots organic matter vs. porosity, both derived from the 3D FIB-SEM volumes, and shows that the red facies have more organic matter with lower conversion ratios. EFFECTS OF HETEROGENEITY Fig. 10. Different pore types detected in different facies. Fig. 11. Poroperm characteristics of the red and green facies with Eagle Ford upper and lower bounds. facies samples are at the higher poroperm range. It is interesting to note that the red facies samples have higher concentrations of the organic matter — 10% to 20% — and yet gave lower poroperm values compared to the green facies samples with only 7% to 11% organic matter. These organic matter figures were derived from the 3D FIB-SEM volumes. In this perspective, flow properties of this shale formation are controlled more by the rock fabric, the mineralogy and the resultant porosity within the organic matter. As an initial comparison of these poroperm results to those 10 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Shales are heterogeneous at millimeter to centimeter scales. Figure 13 compares the segmented porosity and organic matter data from the 2D SEM image with those from the 3D FIBSEM volume. The figure shows that analyzed samples show porosity variations that could be larger than those of the organic matter at different scales. Porosity estimations from the 3D volume could double the initial estimations from the 2D SEM images. Figure 14 serves as a visual comparison of the 2D and 3D SEM images, where the porosity in this example (Sample #7) decreased from 6.2% in the 2D image to 5.3% in the 3D image, and the organic matter decreased from 15.1% in the 2D image to 9.2% in the 3D image. The average results from all 10 of the 2D SEM images from this sample were 4.8% porosity and 13.6% organic matter. Close inspection of all 10 of the 2D SEM images acquired for every sample in this study revealed the porosity variation — within each set of the 10 2D SEM images — to be less than 3% porosity unit and the organic matter variation to be less than 5%. VALIDATION OF CORE FACIES FROM DUAL-ENERGY XCT The initial plug sample selection in the core was based on accurate application of a dual-energy XCT imaging technique that produced continuous BD and PEF data along the core lengths. The sample selection targeted three different facies (green, red and yellow) in the core identified from the Fig. 13. Comparison between the data obtained from the selected 2D SEM image for 3D FIB-SEM and the 3D volume data: porosity (left) and organic matter (right) — heterogeneity effect. and organic matter values derived from high resolution SEM images and through EDS and XRD analyses. Figure 15 is a nice representation of the excellent match in porosity, mineralogy and organic matter between core facies described by dualenergy CT and by high resolution SEM images. This would assist in more efficient upscaling, improved reserves estimation and enhance well-to-well correlation. CONCLUSIONS Fig. 14. Comparison between the data obtained from the selected 2D SEM image (left) from Sample #7 and the 3D FIB-SEM volume (right) — heterogeneity effect. Fig. 15. Analysis of reservoir shale characteristics (porosity, mineralogy and organic matter) from core dual-energy CT scanning and SEM. dual-energy CT data. The shale characteristics — porosity, organic matter and mineralogy — of the selected samples from the core facies were then confirmed through segmented porosity Initial core facies characteristics — porosity, organic matter and mineralogy — of a shale formation in the Middle East were computed using the dual-energy CT scanning technique. This core facies analysis was used to locate potential sweet spots in the core for optimum sample selection. The selected plugs, following a well-defined DRP workflow, underwent multiresolution scanning to construct 3D FIB-SEM volumes for the determination of shale porosity, organic matter and mineralogy. The objectives of the study were to explore possible links between shale depositional facies and pore types as well as to quantify the relationship between porosity and matrix permeability for each identified facies in the core. The objectives of the study were fulfilled and the following is a summary of the key findings in this shale play. 1. A robust dual-energy CT scanning technique was used to characterize a shale gas core and to identify potential facies intervals for DRP analysis. 2. Absolute shale matrix permeability was determined in horizontal and vertical directions in 3D FIB-SEM volumes. 3. Only two samples (out of eight) gave 3D connectivity in the vertical direction for permeability simulation in the silicarich samples. This is consistent with a shale depositional environment and anisotropy considerations. 4. Almost all the porosity was found within the organic matter volume. Consequently, flow was only possible through organic matter within the 3D volumes. 5. The silica-rich facies gave higher poroperm characteristics SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 11 compared to the clay-rich facies. This is due to the pressure compaction effect on the soft clay-rich samples, which caused the organic matter to be squeezed within a clay mineral framework, leading to closure of the pore space. 6. A very high permeability value (6,000+ nD) was simulated in one of the samples, which a visual examination determined was caused by an unrepresentative porous organic matter layer along the horizontal direction. Such an observation has led to the recognition of the importance of the visuals in explaining the petrophysical data in the samples. 7. A higher percentage of organic matter was not found to be a good indication for high porosity or permeability in the clay-rich shale samples in this study. The conversion ratios of organic matter should be taken into consideration when judging porosity or permeability. 8. A clear trend was observed between porosity and permeability in relation with the identified facies in the core. 9. The depositional facies was found to have a great effect on the pore types, rock fabric and reservoir properties. Of particular importance are the mineralogy and clay in the samples. 10. Shale heterogeneity in this formation showed larger effects on porosity variability than organic matter variations at different scales. 11. The results and interpretations in this study enhanced our understanding of the complexity of unconventional shale reservoir quality. NOMENCLATURE K Kh Kv Zeff Ø permeability horizontal permeability vertical permeability effective atomic number porosity ACKNOWLEDGMENTS The authors would like to thank the management of Saudi Aramco for their support and permission to publish this article. Ingrain Inc. conducted the measurements discussed in this article. This article was presented at the SPE-SAS Annual Technical Symposium and Exhibition, al-Khobar, Saudi Arabia, April 2124, 2014. REFERENCES 1. Butler, J.A., Bryant, J.E. and Allison, D.B.: “Hydrocarbon Recovery Boosted by Enhanced Fracturing Technique,” SPE paper 167182, presented at the SPE Unconventional Resources Conference-Canada, Calgary, Alberta, Canada, November 5-7, 2013. 2. Wellington, S.L. and Vinegar, H.J.: “X-ray Computerized Tomography,” Journal of Petroleum Technology, Vol. 39, No. 8, 1987, pp. 885-898. 12 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY 3. Walls, J. and Armbruster, M.: “Shale Reservoir Evaluation Improved by Dual-energy X-ray CT Imaging: Technology Update,” Journal of Petroleum Technology, November 2012. 4. Amabeoku, M.O., Al-Ghamdi, T.M., Mu, Y. and Toelke, J.: “Evaluation and Application of Digital Rock Physics (DRP) for Special Core Analysis in Carbonate Formations,” IPTC paper 17132, presented at the International Petroleum Technology Conference, Beijing, China, March 26-28, 2013. 5. Al-Owihan, H., Al-Wadi, M., Thakur, S., Behbehani, S., Al-Jabari, N., Dernaika, M., et al.: “Advanced Rock Characterization by Dual-Energy CT Imaging: A Novel Method for Complex Reservoir Evaluation,” IPTC paper 17625, presented at the International Petroleum Technology Conference, Doha, Qatar, January 20-22, 2014. 6. Al Mansoori, M., Dernaika, M., Singh, M., Al Dayyani, T., Kalam, Z. and Bhakta, R.: “Application of Digital and Conventional Techniques to Study the Effects of Heterogeneity on Permeability Anisotropy in a Complex Middle East Carbonate Reservoir,” SPWLA paper, presented at the SPWLA 55th Annual Logging Symposium, Abu Dhabi, UAE, May 18-22, 2014. 7. Passey, Q.R., Bohacs, K.M., Esch, W.L., Klimentidis, R. and Sinha, S.: “From Oil-Prone Source Rock to Gas Producing Shale Reservoir — Geologic and Petrophysical Characterization of Unconventional Shale Gas Reservoirs,” SPE paper 131350, presented at the International Oil and Gas Conference and Exhibition in China, Beijing, China, June 8-10, 2010. 8. Walls, J.D. and Sinclair, S.W.: “Eagle Ford Shale Reservoir Properties from Digital Rock Physics,” First Break, Vol. 29, No. 6, June 2011, pp. 97-101. 9. De Prisco, G., Toelke, J. and Dernaika, M.: “Computation of Relative Permeability Functions in 3D Digital Rocks by a Fractional Flow Approach Using the Lattice Boltzmann Method,” SCA2012-36 paper, presented at the International Symposium of the Society of Core Analysts, Aberdeen, Scotland, U.K., August 27-30, 2012. 10. Mu, Y., Fang, Q., Baldwin, C., Toelke, J., Grader, A., Dernaika, M., et al.: “Drainage and Imbibition Capillary Pressure Curves of Carbonate Reservoir Rocks by Digital Rock Physics,” SCA2012-56 paper, presented at the International Symposium of the Society of Core Analysts, Aberdeen, Scotland, U.K., August 27-30, 2012. 11. Grader, A., Kalam, M.Z., Toelke, J., Mu, Y., Derzhi, N., Baldwin, C., et al.: “A Comparative Study of Digital Rock Physics and Laboratory SCAL Evaluations of Carbonate Cores,” SCA2010-24 paper, presented at the International Symposium of the Society of Core Analysts, Halifax, Nova Scotia, Canada, October 4-7, 2010. 12. Tolke, J., Baldwin, C., Mu, Y., Derzhi, N., Fang, Q., Grader, A., et al.: “Computer Simulations of Fluid Flow in Sediment: From Images to Permeability,” The Leading Edge, Vol. 29, No. 1, January 2010, pp. 68-74. 13. Loucks, R.G., Reed, R.M., Ruppel, S.C. and Hammes, U.: “Preliminary Classification of Matrix Pores in Mudrocks,” Gulf Coast Association of Geological Societies Transactions, Vol. 60, April 2010, pp. 435-441. BIOGRAPHIES Anas M. Al-Marzouq is a Petroleum Engineer in Saudi Aramco’s Reservoir Description Division. He joined Saudi Aramco in 2004 and is currently working in the Exploration Petrophysical Unit. Anas is a member of the Tight Gas Assessment team, the Unconventional Gas Petrophysical team and the Northwest Unconventional Gas Operation team. He has published and coauthored many papers and journal articles. Anas’s recent work involves integration of the core and petrophysical measurements to evaluate unconventional gas resources. He received his B.S. degree from King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia, in 2004, and his M.S. degree from Texas A&M University, College Station, TX, in 2010, both in Petroleum Engineering. Dr. Tariq M. Al-Ghamdi is a Reservoir Engineer working in Saudi Aramco’s Reservoir Description and Simulation Department. His responsibilities include management and petrophysical evaluation of exploration and gas fields. Tariq is currently leading the Unconventional Shale Shal Gas team in Saudi Aramco. His main interests are optimizing petrophysical evaluation, permeability modeling and modeling saturation height function; recently Tariq has been involved in digital core analysis and numerical simulations of special core analysis and nuclear magnetic resonance. He has published and coauthored numerous papers and journals. Tariq received his B.S. degree from the University of Tulsa, Tulsa, OK, his M.S. degree from Heriot-Watt University, Edinburgh, U.K., and his Ph.D. degree from the University of New South Wales, Kensington NSW, Australia, all in Petroleum Engineering. Safouh Koronfol joined Ingrain Inc. in May 2012 and is the Operations Manager. He has 10 years of special core analysis experience. Safouh was the Head of the Special Core Analysis Department at Weatherford Laboratories Abu Dhabi and later became the b h SCAL coordinator between Weatherford Labs globally and Shell/Petroleum Development Oman in Muscat, Oman. Safouh received his B.S. degree in Industrial Chemistry from University of Aleppo, Aleppo, Syria. He is an active member of Society of Petrophysicists and Well Log Analysts (SPWLA), the Society of Petroleum Engineers (SPE) and the Society of Core Analysts (SCA). Safouh has authored and coauthored seven technical papers on both conventional SCAL and digital rock physics. Dr. Moustafa R. Dernaika has been the Manager of Ingrain Inc. Abu Dhabi since 2010. Before he joined Ingrain, he worked for Emirates Link ResLab LLC (Weatherford Laboratories) as the Regional Special Core Analysis (SCAL) Manager in Abu Dhabi. Dh bi He H has h 15 years of routine and SCAL experience with special interest in business development, project management and data interpretation. Moustafa has written 26 technical papers. His current research areas include digital rock physics, dual energy coiled tubing applications and the variations of petrophysical and flow properties with rock types and wettability. Moustafa received his B.S. and M.S. degrees in Chemical Engineering from the Middle East Technical University, Ankara, Turkey, and his Ph.D. degree in Petroleum Reservoir Engineering from the University of Stavanger, Stavanger, Norway. Dr. Joel D. Walls is a Geophysicist focused on research, development, and commercialization of advanced digital rock physics services for unconventional reservoirs. He joined Ingrain Inc. in 2010, and as the Director of Technology, JJoel guides the development and commercialization of services focused on shale plays. Joel was a co-founder and the first president of the Society of Core Analysts (SCA). He is a member of the Society of Economic Geologists (SEG), Society of Petroleum Engineers (SPE) and the Society of Petrophysicists and Well Log Analysts (SPWLA). Joel is the author of numerous publications in several geophysical and petrophysical journals, and holds four U.S. patents in the rock physics and reservoir characterization. He received his B.S. degree in Physics from Texas A&M University, College Station, TX. Joel received his M.S. and Ph.D. degrees in Geophysics from Stanford University, Stanford, CA. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 13 Chemically Induced Pressure Pulse: A Novel Fracturing Technology For Unconventional Reservoirs Authors: Ayman R. Al-Nakhli, Dr. Hazim H. Abass, Mirajuddin R. Khan, Victor V. Hilab, Ahmed N. Rizq and Ahmed S. Al-Otaibi ABSTRACT The huge resources of unconventional gas worldwide, along with the increasing oil demand, make the contribution of unconventional gas critical to the world economy; however, one of the major challenges that operators face with production from unconventional resources is finding a commercial stimulation technique that creates sufficient stimulated reservoir volume (SRV). Unconventional reserves trapped within very low permeability formations, such as tight gas or shale formations, exhibit little or no production, and are therefore economically undesirable to develop with existing conventional recovery methods. Such reservoirs require a large fracture network with high fracture conductivity to maximize well performance. One commonly employed technique for stimulating low productivity wells is multistage hydraulic fracturing, which is costly and typically involves the injection of high viscosity fluids into the well. Fracturing fluid by itself could be a damaging material for the fracture due to the high capillary forces involved. Therefore, the need exists for another more economical method to enhance production within a tight gas formation. This article discusses a new stimulation method to increase SRV around the wellbore and fracture area, thereby improving unconventional gas production. The method entails triggering an exothermic chemical reaction in situ to generate heat, gas and localized pressure sufficient to create fractures around the wellbore. In a controlled experiment, chemical reactants were separately injected into core samples with a mini-hole, and upon their mixing inside the core, an exothermic chemical reaction occurred and the resultant heat and gas pressure caused macrofractures. Nuclear magnetic resonance (NMR) porosity imaging showed a significant increase in macropores throughout the core. Additionally, large-scale experiments using cement blocks with a simulated wellbore cavity were performed. Once the wellbore was filled with the chemicals and a triggering catalyst was introduced, an in situ chemical reaction took place, which generated heat and gas with sufficient pressure to cause shear fractures in the surrounding rock. These experiments, which showed extensive fractured and shattered pieces, also provided preliminary design requirements for a field test. The chemical reactants were then incorporated into a fracturing gel that simulated additional fractures created from the main induced hydraulic 14 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY fracture. The results were very encouraging, and the generated high-pressure/high temperature caused the gel to break. Therefore, it was concluded that this technique effectively contributes to fracture cleanup in addition to creating the required SRV. The experiments were very successful in proving the new concept for generating SRV in a tight gas well, and the developed stimulation technique is fairly easy to implement in the field. INTRODUCTION There is tremendous potential for tight gas plays to provide long-term energy throughout the world because of the vast resource base that these formations represent. Horizontal drilling and multistage hydraulic fracturing technologies have allowed significant gas to be produced from shale gas and tight sand formations. Yet the primary recovery factors have been less than 20%, which implies the compelling need for advanced technologies. The goal of this research effort is to provide a cost-effective stimulation technique that potentially replaces costly multistage hydraulic fracturing in shale gas and tight sand formations. Water scarcity in the Kingdom requires a new look at fracturing treatments. Energized and waterless fracturing is an evolving and promising technology that eliminates the polymer residue within the created fracture and the water phase trapping within the rock matrix — both of these damaging mechanisms are associated with conventional water-based fracturing stimulation of tight gas wells. Additionally, the conventional fracturing must be carefully applied to stimulate tight gas plays because it is not the single, conductive, and long fracture that one is after; rather what one wants is the stimulated volume connected to the well, needed to make it a commercial producer. The current costly multistage fracturing is helping, but there is a desperate need for cost-effective stimulation techniques. New alternatives to hydraulic fracturing are being researched, including tailored gas fracturing, with the ultimate objective of replacing the current costly fracturing with a more cost-effective and environmentally friendly treatment that could significantly reduce stimulation costs. Several articles have been presented on introducing a pressure pulse loading into a given well to induce near wellbore fracture1-3. The technique is based on loading a well with a high-pressure pulse over a short period of time so that the pressure exceeds all in situ stresses, causing multiple fractures to propagate in all directions. The fast expanding pulse generates stress waves, which travel through the rock medium, creating fractures in the reservoir. A new technique discussed in this article is based on generating a pressure pulse but via an in situ exothermic chemical reaction. The pressurization time is the main parameter that determines the fracture pattern. The number of fractures initiated increases with an increase in loading rate, for loading rates above the onset pressure. There are three main categories of fracturing techniques. First is hydraulic fracturing, with the longest pressure rise time (P ≤ 1 MPa/s), which creates a single radial fracture. A second technique is using explosives downhole, which has the shortest rise time (P ≥ 107 Mpa/s) and generates compacted zones with multiple radial fractures. The third technique is using propellant to generate multiple radial fractures, which has an intermediate pressure rise time (p ≈ 102 MPa/s ~106 MPa/s). In general, the number of fractures initiated increases with an increase in pressurizing rate for the intermediate pressurizing rate techniques1-3. Controlling the pressurizing rate is a key factor for controlling the fracture pattern. The new invention describes a new rock fracturing technique, which has significant advantages over the three methods just described. With this novel invention, pressurizing time can be controlled, so a fracturing pattern can also be optimized1. The damaging effect of the fracturing technique is another key factor considered during the fracturing selection process. Detonating an explosive in a wellbore generally creates a damaged zone surrounding the wellbore wall that impairs permeability and communication with the reservoir. The pressurization rate is very high, which causes compressive stresses in the wellbore area that are much higher than the in situ stress state. This stress environment can cause compaction or pulverization of a finite zone around the wellbore to such a degree that permeability is decreased significantly. CONCEPT Unconventional gas requires an extensive fracturing network to create commercially producing wells. One commonly employed technique is multistage hydraulic fracturing in horizontal wells, which is very costly and may not provide the required stimulated reservoir volume (SRV). Therefore, a need exists for an economical method to enhance production within tight gas formations. A new technique has been developed to increase SRV around the wellbore and fracture area, and therefore improve unconventional gas production. The method entails triggering an exothermic chemical reaction in situ to generate heat, gas and localized pressure sufficient to create fractures around the wellbore. In a controlled experiment, chemical reactants were separately injected into core samples with a mini-hole, and upon their mixing inside the core, an exothermic chemical reaction occurred and the resultant heat and gas pressure caused macrofractures. Nuclear magnetic resonance (NMR) porosity imaging showed a significant increase in macropores throughout the core. Additionally, large-scale experiments using cement blocks with a simulated wellbore cavity were performed. Once the wellbore was filled with the chemicals and a triggering catalyst was introduced, an in situ chemical reaction took place, which generated heat and gas with sufficient pressure to cause shear fractures in the surrounding rock. These experiments, which showed extensive fractured and shattered pieces, also provided preliminary design requirements for a field test. The chemical reactants were then incorporated into a fracturing gel that simulated additional fractures created from the main induced hydraulic fracture. The results were very encouraging, and the generated high-pressure/high temperature (HPHT) caused the gel to break. Therefore, it was concluded that this technique effectively contributes to fracture cleanup in addition to creating the required SRV. The experiments were very successful in proving the new concept of generating SRV in tight gas wells, and the developed stimulation technique is fairly easy to implement in the field. AUTOCLAVE REACTOR TESTING Two autoclave reactors, Fig. 1, were used to study the reaction kinetics of the selected chemicals. One system was rated up to 10,000 psi and 500 °C with a total volume of 3 liters, and the other was rated up to 20,000 psi. Experiments were carried out in a dedicated specialized HPHT laboratory equipped with the required safety features. The experimental parameters were controlled and PC monitored remotely. Real-time pressure and temperature data were recorded every 2 seconds to observe the resulting pressure-temperature behavior during the chemical reaction. This testing phase was performed to simulate the pressure and temperature anticipated to occur in a given wellbore as a result of injecting the chemicals and triggering the reaction. There was one critical assumption; that the well is drilled in a zero permeability formation to match that of the autoclave reactor. Although this is not a practical assumption, Fig. 1. Autoclave systems rated up to 10,000 psi and 20,000 psi. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 15 it is an approximation of the extremely low permeability when a well is drilled in a shale formation. There were two independent variables considered in these tests; the molarity of the chemicals, and the initial pressure and ratio of the chemical’s volume to the autoclave reactor vessel’s volume. ENVIRONMENTAL SCANNING ELECTRON MICROSCOPY (ESEM) The rock samples were examined in the environmental scanning electron microscope (ESEM) with an integrated energy dispersive X-ray system. The ESEM equipment was operated at 15 kV, 0.4 Torr water vapor pressure and around 8 mm working distance. Useful and insightful textural information on the two formations was obtained by acquiring surface images from different parts of the examined samples. The samples were mounted on ESEM holders using double-sided carbon tape, and then the samples were inserted into the ESEM chamber for analysis. fracturing gel. The fracturing gel was water-based WG-17, with a loading of 40 lb/Mgal. The viscosity of this fluid was about 1,600 centipoise (cP) at a share rate of 81 s-1 at room temperature. The concentrations of the exothermic chemicals varied from 3 molar to 5 molar and were used immediately after preparation. The injection rate was about 30 cc/min to 100 cc/min. Samples were tested with and without confinement. For the confined stress testing, samples were loaded in a biaxial cell with equal horizontal stresses of 2,000 psi for one test and 4,000 psi for another test. If we consider a well depth of 2,570 ft, these stresses represent gradients of 0.78 psi/ft and 1.56 MR-CT MICROSCOPE A magnetic resonance and computed tomography (MR-CT) microscope is a new suite of core analysis tools that utilizes NMR combined with X-ray CT to improve the description of pore property changes as a result of coreflooding with different types of fluids4. The MR-CT microscope allows the observation of microscopic events within reservoir porous media and provides fluid-rock interaction with proper mineralogy quantification information. Both a medical CT scan and a micro CT scan were also used to evaluate the chemical treatment on the carbonate cores. ROCK BLOCK TESTING A series of laboratory experiments were conducted to provide insight on applying the concept of chemically induced pulse fracturing in the field. Rock samples used in these experiments were rectangular blocks with dimensions of 8” x 8” x 8” and 10” x 10” x 10”. Each rock sample was made to have a 1½” x 3” cavity to simulate a wellbore. The tested rocks were Indiana limestone, Berea sandstone, shale and cement. The man-made rock samples were cast by mixing water and cement with a weight ratio of 31/100, respectively. The physical and mechanical properties of the rock samples were: porosity = 29%, bulk density = 1.82 gm/cc, Young’s modulus = 1.92 x 106 psi, Poisson’s ratio = 0.26, uniaxial compressive strength = 3,299 psi, cohesive strength = 988 psi and internal friction angle = 28°. The breakdown pressure for this test was 5,400 psi. A vertical open hole was cast or drilled in the center of the block. For the unconfined test, the simulated wellbore was 3” long and 1½” in diameter, Fig. 2. For the confined test, the vertical open hole was cast all the way through the center of the block, Fig. 3. The exothermic chemicals were used with a 16 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Fig. 2. Block design for unconfined tests. Fig. 3. Block design for confined tests. UNCONFINED CONDITION TESTING 1.82 gm/cc, Young’s modulus = 1.92 x 106 psi, Poisson’s ratio = 0.26, uniaxial compressive strength = 3,299 psi, tensile strength = 271 psi, cohesive strength = 1,067 psi and internal friction angle = 23°. Tests 1 and 2 Test 4 The samples for this type of test, which simulated an open hole vertical well, were man-made cement blocks. The rock samples were preheated to 200 °F. Then reactive chemicals were injected in the rock at atmospheric pressure and at a rate of 15 cc/min. As chemical injection was completed and the reaction took place, multiple fractures were created, as shown in Figs. 4 and 5. The created fractures were longitudinal and perpendicular with respect to the vertical wellbore. The fracture geometry indicates that fractures propagated from the wellbore to the end of the sample. This indicates that the pressure generated was greater than the compressive strengths of the samples. The breakdown pressure for these tests was 5,400 psi. A shale block sample from Mancos was used for this test with a drilled hole 2” long and 1½” in diameter, to simulate a vertical open hole well. In this test, the reactive chemicals were injected first, then the block was placed in a 200 °F oven. After 3 hours, a chemical reaction took place and multiple fractures were created, Fig. 7. The time interval for the reaction to be activated simulated the downhole temperature recovery of the wellbore. The breakdown pressure for this test was 6,600 psi. The physical and mechanical properties of the shale rock samples were: porosity = 3.8%, bulk density = 2.50 gm/cc, Young’s modulus = 2.66 x 106 psi, Poisson’s ratio = 0.20, uniaxial compressive strength = 4,965 psi, cohesive strength = 1,268 psi and internal friction angle = 36°. psi/ft, respectively. The reactive chemicals were injected in the block and heat was applied using the biaxial plates. Test 3 The Indiana limestone block sample was used for this test with a drilled hole 3” long and 1½” in diameter, to simulate a vertical open hole well. The block was preheated to 200 °F, then reactive chemicals were injected in the rock at atmospheric pressure and at a rate of 15 cc/min. As chemical injection was completed and the reaction took place, multiple fractures were created within two minutes, Fig. 6. The created fractures were two longitudinal and one perpendicular with respect to the vertical wellbore. The breakdown pressure for this test was 4,700 psi. The physical and mechanical properties of the Indiana limestone rock samples were: porosity = 28%, bulk density = CONFINED CONDITION TESTING Samples for this test simulated a vertical open hole well with a hole drilled in the center of an 8” x 8” x 8” cube, Fig. 8. The hole was 1½” in diameter, extending throughout the whole length of the sample, as previously shown in Fig. 3. The test sample was then placed in a biaxial loading frame where two horizontal stresses of a given stress were applied while the vertical stress was controlled by mechanical tightening of the Fig. 6. Pre- and post-treatment views of Indiana limestone block sample, using chemically pulsed fracturing. Fig. 4. Pre- and post-treatment views of white cement block sample, using chemically pulsed fracturing. Fig. 5. Pre- and post-treatment views of portrait cement block sample, using chemically pulsed fracturing. Fig. 7. Pre- and post-treatment views of shale block sample, using chemically pulsed fracturing. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 17 Fig. 8. 8” x 8” x 8” cement block. base and top platens, Fig. 9. Then reactive chemicals were injected in the rock at atmospheric pressure and room temperature at a rate of 15 cc/min. The sample was then heated for 2 to 3 hours until the reaction took place and fractures were created. Two tests were performed as follows. Fig. 9. Biaxial system for confined condition tests. Test 5 and 6 For Test 5, the applied horizontal stress was 2,000 psi at both directions, Fig. 10. The reaction was triggered at 167 °F. Upon triggering the reaction, three longitudinal and one perpendicular fractures were created with respect to the vertical hole, Fig. 11. The applied horizontal stress in Test 6 was 4,000 psi at both directions, Fig. 12. Almost the same behavior was observed for this test. Four longitudinal fractures were created with respect to the vertical hole, Fig. 13. The fracture geometry shows that the created fracture was longitudinal with respect to the vertical wellbore. The fracture geometry indicates that two sets of fractures propagated from the wellbore to the end of the sample. This indicates that the pressure generated was greater than 8,000 psi. Each created planar fracture propagated in the direction of one σH and perpendicular to the direction of the other σH, as the applied stress is equal in both horizontal directions. REACTOR TESTING An autoclave reactor, rated up to 10,000 psi, was used to test the chemical reaction. Figure 14 shows a typical reaction behavior with pressure and temperature pulses. In this test, 18 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Fig. 10. Pulsed fracturing under 2,000 psi biaxial stress. reactive chemicals were placed in the autoclave at room conditions. Then the temperature was increased until reaction was triggered at 120 °F. The pressure rise time was less than 2 seconds, which is the machine’s low limit. So, depending on the pressurizing rate, multiple fractures were expected to be generated in the rock samples. The initial pressure does not have a negative impact on the Fig. 11. Fractured cement block under 2,000 psi biaxial stress. Fig. 14. Chemical reaction at zero psi initial pressure and 2X solution volume. Fig. 12. Pulsed fracturing under 4,000 psi confined stress. Fig. 15. Chemical reaction at different initial pressure. Fig. 13. Fractured cement block under 4,000 psi biaxial stress. generated pressure pulse. As can be seen in Fig. 15, the final pressure is a function of the initial pressure. In other words, final pressure is the summation of initial reactor pressure and reaction generated pressure; however, the temperature was almost constant with the changes in initial pressure at fixed chemical concentration and volume. In another test, reactive chemicals were prepared with crosslinked fracturing gel (40 lb/1,000 gal), Fig. 16. The solution’s pH was adjusted to 9.7. Then the gel was injected into the reactor, which was preset at 200 °F. The reaction was not triggered for 1 hour, not until the gel breaker was injected. When the gel breaker was injected, which reduces the solution pH, the pressure pulse was generated. This characteristic can give more control over the reaction behavior for field applications. Fig. 16. Activation of cross-linked gel containing reactive chemicals using a breaker. EFFECT OF CONCENTRATION AND VOLUME The chemicals were tested using an autoclave at different concentrations and solution volumes. The results showed that pressure is a function of chemical concentration and volume. The greater the solution volume used, the greater the generated pressure, Fig. 17. At 50 vol%, the pressure increased from 988 psi to 6,100 psi and then to 16,600 psi, as the concentration SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 19 was increased from 1x to 3x and then to 4x, respectively. These are actual data measured using the autoclave system. Tests also showed that the greater the concentration, the higher the generated pressure was. As the solution volume was increased from 50 vol% to 100 vol%, the generated pressure that was measured increased from 988 psi to 20,000 psi. It is anticipated that the pressure can exceed 45,000 psi using chemicals at high concentrations and large volumes. TRIGGERING TEMPERATURE Figure 18 shows that the reaction triggering temperature was around 200 °F at zero initial reactor pressure and a 6.5 pH solution. Once this temperature was reached, the reaction progressed vigorously and reached maximum pressure and temperature in milliseconds. The minimum limit of the autoclave system was 2 seconds, so it was not possible to record the reaction pulse duration. During experiments with an initial reactor pressure of 350 psi and higher, the triggering temperature was stabilized round 122 °F. When the solution pH was increased from 6 to 9, the triggering temperature increased from 200 °F to 230 °F, at zero initial pressure. At an initial pressure of 500 psi, the triggering temperature was increased from 122 °F to 184 °F, as the pH increased from 6.5 to 9. SYNTHETIC SWEET SPOT Microscopic analysis of a sample treated with the reactive chemicals showed that no damaged zone was formed around the treated area; however, a synthetic sweet spot was created, Figs. 19 and 20. A tight core sample with an air permeability of 0.005 nano-darcy was chemically treated using the coreflood system. The chemical was injected through a drilled hole within the core sample, two-thirds of the total core sample length, 3.2”. The core diameter was 1½” with porosity of 1.35%. Pre- and post-treatment CT scan analysis shows significant density reduction, also seen in Figs. 19 and 20. Voids are scattered around the treated area throughout the core sample. The change in slice colors from red and green to green and blue indicates a reduction around the treated area, which reflects an increase in porosity. ESEM analysis shows that microfractures were created along the core sample. The MR-CT microscope image also shows visible voids and high porosity around the treated hole, Fig. 20, which was confirmed by ESEM analysis. Several backscattered electron topographical Fig. 17. Effect of chemical concentration and volume on pressure pulse. Fig. 19. Pre-treatment tight core sample (MR-CT, ESEM and CT scan). Fig. 18. Reaction triggering temperature behavior. Fig. 20. Post-treatment tight core sample with synthetic sweet spot, (MR-CT, ESEM and CT scan). 20 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY images were taken at different magnifications from different parts of the samples, but mainly from the center of the rock samples. The acquired images show submicron pores and microcracks. The sizes of the pores were measured and found to be in the range of less than 1 micron to 50 microns. The concentration of the cracks and pores was mainly in the center of the rock, where the epicenter of the treatment took place. The exothermic reaction treatment thereby led to the initiation of micro-cracks and pores in the rock samples4, 5. MR-CT MICROSCOPE The pre- and post-treatment MR-CT microscope results show a significant increase in macropores throughout the core and suggest communication among an otherwise isolated system of micro-, miso- and macropores of the core, with an overall permeability increase. Figure 20 also shows the isolated porosity system of the pre-treatment core sample, where the micro-, miso- and macropores are clearly not communicating with each other; however, post-treatment results show strong communication among all pore sizes6. CT-SCAN OF RM9 AND RM13 Fig. 21. Reactive gel with proppant. The pre- and post-treatment medical CT scan images of the treated core samples show a significant porosity increase and numerous created fractures due to the chemical reaction, previously seen in Figs. 19 and 20. The red color represents high density and low porosity sites, while the blue color represents a low density and high porosity system. Pre- and post-treatment images of a tight core sample show the creation of fractures perpendicular to the flow of injection. A clear reduction of density and porosity is noted. Fractures and voids are clearly shown in black in both samples. VISCOSITY AND COMPATIBILITY WITH FRACTURING FLUID The reactive chemicals were prepared and showed compatibility with the cross-linked fracturing fluid, Fig. 21. The gel, containing reactive chemicals, was also prepared with proppant and again showed compatibility, Fig. 22. The gel was activated in the autoclave system by heating to the triggering temperature. The heat generated by the reaction broke the gel viscosity, even without injecting the gel breaker, Fig. 23. Therefore, this type of treatment can help clean up the well after a fracturing job. Using a Chandler viscometer, the viscosity of the cross-linked gel, containing reactive chemicals, was measured pre- and post-reaction. The gel viscosity was reduced from 1,600 cP to 10 cP, Fig. 24. This indicates the reactive chemicals can fully break the gel viscosity, which can help in fracture cleanup. Fig. 22. Pre-reaction gel. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 21 Fig. 24. Reaction effect on breaking cross-linked gel viscosity. Fig. 23. Post-reaction gel. Fig. 25. Cooling effect of preflush on downhole temperature. REACTION ACTIVATION METHOD FOR FIELD APPLICATION Injecting a preflush reduced the downhole temperature from 250 °F to 100 °F, Fig. 25. The cooling effect and heat recovery of the treated well can be used to self-activate the reactive chemicals. By selecting the optimum pH, the reactive chemicals can take from 1 to 3 hours to be activated, depending on the designed procedures and required need. From Fig. 25, results show it took around 4 hours for the downhole temperature to reach 184 °F, which is the triggering temperature of the reactive chemicals using a 9 pH solution. This gives sufficient time to place and self-activate the gel downhole. CONCLUSIONS 1. A new shale or tight gas stimulation technique has been developed using chemical reaction and has been proven through laboratory experiments. This new approach is based on pulsed fracturing. 2. Multiple fractures were created using the new technique in shale, Indiana limestone, Berea sandstone and cement block samples. Fracturing was also tested, using cement 22 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY block samples, under a stress level of 4,000 psi. 3. This technique can be used to increase SRV in shale or tight gas wells. The technology can also be applied to stimulate limestone and sandstone formations. 4. The simplicity of this technique makes it very attractive to implement. The applicability of this technique has been demonstrated in the laboratory and a field trial is being planned. There is no special tool required to apply the technology in the field, compared to propellant techniques. 5. The reactive chemicals are compatible with the fracturing fluid and can be activated by either reservoir thermal effect or pH reduction. 6. A synthetic sweet spot is created around the treated area of tight rock samples using the new chemical treatment method. This confirms that no damaged zone will be formed. 7. The new technology can enable fracture cleanup. ACKNOWLEDGMENTS The authors would like to thank the management of Saudi Aramco for their support and permission to publish this article. This article was presented at the Unconventional Resources Technology Conference, Denver, Colorado, August 25-27, 2014. REFERENCES 1. Swift, R.P. and Kusubov, A.S.: “Multiple Fracturing of Boreholes by Using Tailored-Pulse Loading,” Society of Petroleum Engineers, Vol. 22, No. 6, 1982, pp. 923-932. 2. Cuderman, J.F.: “Tailored-Pulse Fracturing in Cased and Perforated Boreholes,” SPE paper 15253, presented at the SPE Unconventional Gas Technology Symposium, Louisville, Kentucky, May 18-21, 1986. 3. Yang, D.W. and Risnes, R.: “Experimental Study on Fracture Initiation by Pressure Pulses,” SPE paper 63035, presented at the SPE Annual Technical Conference and Exhibition, Dallas, Texas, October 1-4, 2000. 4. Al-Nakhli, A.R., Abass, H.H., Kwak, H.T., Al-Badairy, H., Al-Ajwad, H.A., Al-Harith, A., et al.: “Overcoming Unconventional Gas Challenges by Creating Synthetic Sweet Spot and Increasing Drainage Area,” SPE paper 164165, presented at the SPE Middle East Oil and Gas Show and Conference, Manama, Bahrain, March 10-13, 2013. 5. Al-Ajwad, H.A., Abass, H.H., Al-Nakhli, A.R., Al-Harith, A.M. and Kwak, H.T.: “Unconventional Gas Stimulation by Creating Synthetic Sweet Spot,” SPE paper 163996, presented at the SPE Unconventional Gas Conference and Exhibition, Muscat, Oman, January 28-30, 2013. 6. Kwak, H.T., Funk, J.J., Yousef, A.A. and Balcom, B.J.: “New Insights into Microscopic Fluid/Rock Interaction: MR-CT Microscopy Approach,” SPE paper 159194, presented at the SPE Annual Technical Conference and Exhibition, San Antonio, Texas, October 8-10, 2012. BIOGRAPHIES Ayman R. Al-Nakhli is a Petroleum Scientist with the Production Technology team of Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC), where he is involved in the study of His main research interest is unconventional reservoirs. reserv developing new technologies in the field of fracturing, stimulation, heavy oil recovery, unconventional gas and smart fluids. Ayman has generated several patents and published several papers related to production technology. He has also published a book about self-development. He received his B.S. degree in Industrial Chemistry from King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia, and an MBA from Open University Malaysia, Bahrain. Dr. Hazim H. Abass was a Senior Consultant at Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC). He has advanced the geomechanics discipline by developing practical applications to solve li i l petroleum related problems. Hazim has pioneered advanced techniques related to oriented perforation, fracturing horizontal wells, acid fracture closure, sanding tendency, gas hydrate and water coning. Before joining Saudi Aramco in 2001, he worked for the Northern Petroleum Organization in Iraq, the Halliburton Research Center in Oklahoma and the PDVSA Research Center in Venezuela. Hazim is the recipient of the 2008 SPE Middle East Regional Award, Production Operations; the 2009 SPE International Award, Distinguished Member; the 2012 SPE International Award, Completion Optimizations and Technology; and the 2012 SPE Middle East Regional Award, Completion Optimizations and Technology. He was one of the SPE Distinguished Lecturers for the 2011/2012 season, educating professionals around the globe on “the use and misuse of applied rock mechanics in petroleum engineering.” Hazim holds 10 U.S. patents, has authored more than 40 technical papers and contributed to three industrial books. He is a member of the Society of Petroleum Engineers (SPE) and the Technical Editor of its journal Production & Facilities, and he is a member of the International Society for Rock Mechanics (ISRM). In 1977, Hazim received his B.S. degree in Petroleum Engineering from the University of Baghdad, Baghdad, Iraq. He received his M.S. and Ph.D. degrees in 1987 in Petroleum Engineering from the Colorado School of Mines, Golden, CO. He retired from Saudi Aramco in September 2014. Mirajuddin R. Khan joined Saudi Aramco in 1991. He is a Geologist working in Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC). His interests are rock mechanics’ applications in petroleum engineering. Mirajuddin is a petro member of the Society of Petroleum Engineers (SPE) and has published several technical papers. Before joining Saudi Aramco, Mirajuddin worked as a Teaching Assistant for 1 year and then received a scholarship to work as a Research Scholar for 2 years at the University of Karachi. His awards include the 2004 Recognition Award of the Engineering & Operations Services of Saudi Aramco. Mirajuddin received his B.S. degree in 1984 and his M.S. degree in 1985, both in Petroleum Geology from the University of Karachi, Karachi, Pakistan. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 23 Victor V. Hilab is a Petroleum Engineer with the Production Technology team of Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC). He has 36 years of experience working in chemistry laboratories, h i l b i of which 26 years has been with Saudi Aramco. Victor’s areas of interest are research in formation damage analysis and remediation, scale problems, wastewater disposal, and injection water quality and fracturing. He is currently working in laser and heavy oil research. Victor is a member of the Society of Petroleum Engineers (SPE) and the American Chemical Society (ACS). He has authored and coauthored many papers throughout his career. Victor also has one granted U.S. patent. He received his B.S. degree in Chemical Engineering from FEATI University, Manila, Philippines. Ahmed N. Rizq is a Lab Technician with the Production Technology team of Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC). He has several years of experience, working with the Geochemistry Division Divisio for 3 years, the R&D Division for 1 year and the Geology Technology team for 2 years. Ahmed’s interests include unconventional resources and reducing the cost of production. He received his B.S. degree in Chemical Engineering from Jubail Industrial University, Jubail, Saudi Arabia. Ahmed S. Al-Otaibi joined the Industrial Training Center in 2008, for a 2 year program. He then went on to study at Jubail Industrial College for 10 months, graduating in July 2011. Ahmed then joined Saudi Aramco as a Lab Technician with the Production Technology T chnology Team Te T am of Saudi Aramco’s Exploration and Te Petroleum Engineering Center –Advanced Research Center (EXPEC ARC). 24 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Integrating Intelligent Field Data into Simulation Model History Matching Process Authors: Bevan B. Yuen, Dr. Olugbenga A. Olukoko and Dr. Joseph Ansah ABSTRACT The advent of digital oil field technology initiated a new era of real-time data acquisition, which facilitated continuous field monitoring and swift intervention. Although yesterday’s or the last hour’s real-time data is not “real time,” it can be classified as intelligent field data. Raw intelligent field data is usually recorded and stored in second or minute intervals, and the volume of the data has been continuously increasing. Yet the added value of the intelligent field data so far has outweighed the challenges in the storage, validation and summarization of such huge amounts of data. While reservoir engineers often struggle with historical well data that is limited in nature and is measured at different time intervals, the continuous and synchronized data stream emerging from the intelligent field provides unique opportunities to improve the history matching process of reservoir simulation models. In this article, we present the data utilization and the workflows adopted to integrate such data into reservoir simulation modeling. The workflow was devised to manage data quality, consistency, conversion and reconciliation with allocation data. Challenges lie in the selection of the intelligent field data to match, and in simulator reported pressure and time stepping. Continuous and synchronized data streaming in real time means that data is available to the engineer almost instantly or within a short time frame from acquisition. The wealth of data enables the simulation engineer to appropriately diagnose and account for critical reservoir phenomena, such as well interference and subsurface well responses to surface well actions. Successful integration of intelligent field data into reservoir simulation significantly enhances the quality and predictability of our models. This builds on the success of our high resolution geological models that attempt to capture all spatial heterogeneities. In much the same way, high resolution temporal data attempts to capture all dynamic actions and reactions within the reservoir to further improve the reservoir simulation models. INTRODUCTION systems has been developed to measure, capture, store, process, manage and visualize massive amounts of data for real-time decision making2, 3. The boundary of the technology is always being pushed to get systems to provide more subsurface multi-station, multivariable, multiphase real-time measurements along a wellbore. The availability of such large amounts of complex data has been a challenge for the industry to handle, and companies are developing a growing number of applications to transform this data into useful information. Al-Mulhim et al. (2010)4 and AbdulKarim et al. (2010)1 both described the application of intelligent field data in the area of real-time control in oil and gas field operations. Yuen et al. (2011)5 described intelligent field data as one of the four major evolving technological developments influencing advanced reservoir simulation practices in the oil and gas industry; the other three are high resolution geological modeling, Thomeer pore description and high performance computing clusters. High resolution reservoir modeling attempts to capture significant heterogeneities on a small physical scale. The high resolution temporal data generated by intelligent field operations capture pressure responses on a small time scale, yet in reservoir simulation practice, reservoir engineers are often encouraged to use algorithms that enable simulators to take large time steps during the computation to reduce computing time and resources. This is even more so the case with models that are spatially high resolution — with hundreds of millions of cells. Confronted with high frequency real-time data, engineers face the dilemma of either running the simulator in smaller time steps, in line with the high frequency data, or adhering to the large time step practice. Some prefer to reduce the high frequency well rate data to a lower frequency to decrease the computing time. Others choose to ignore the real-time data and only use it qualitatively to guide the simulation study. In Saudi Aramco, our preferred approach is to run the simulation models at daily average time steps, which is made possible by our in-house GigaPOWERS simulator — Saudi Aramco’s gigacell parallel reservoir simulator. This lets us take full advantage of intelligent field data and high resolution models without compromising on quality. Digital oil field technology is now mainstream and its deployment by oil and gas companies has been going on for some years1. A robust platform comprising hardware and software SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 25 INTELLIGENT FIELD DATA TYPES FOR SIMULATION MODEL HISTORY MATCHING By design, intelligent fields are equipped to gather and store massive amounts of different types of data in real time from sensors that monitor reservoir response and the operation history of the production equipment installed in individual wells and surface facilities. The rationale behind this effort is that different entities within an organization or company use different sets of the same data. By applying a diverse set of software and tools, these different groups within the organization can analyze the real-time data to ensure efficient oil and gas production, as well as optimize fluid injection systems that support this production. In reservoir simulation, only a subset of the intelligent field data is essential for proper history matching of the simulation models that will be used to monitor reservoir performance and forecast future production and injection requirements: • Oil, gas and water production rates. • Water and/or gas injection rates. • Reservoir pressure. In a typical intelligent field, production wells are equipped with multiphase flow meters (MPFMs) that provide oil, gas and water production rates in real time. These production wells are additionally equipped with wellhead pressure (WHP) and temperature sensors that measure and store real-time pressures and temperatures. In some fields, pressure and temperature gauges are installed downhole to enable pressure and temperature measurements closer to the reservoir, ensuring accurate reservoir pressure data gathering, especially during production. The wellhead is also equipped with a choke system that remotely regulates fluid production from individual wells. In this system, choke position sensors provide real-time choke position, which is one of the key parameters for verifying the status of a well — open or closed. Fig. 1. Tabulated intelligent field data types relevant to reservoir simulation. 26 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY All injection wells are equipped with wellhead water rate meters that provide fluid injection rate data in real time. In addition, injectors are equipped with pressure and temperature gauges that provide real-time injection pressures and temperatures at the wellhead. These wells are further equipped with surface chokes to enable the injection of precise volumes of fluid. Static reservoir pressures are provided by dedicated observation wells located in key sectors of the field. These observation wells are equipped with permanent downhole measurement systems (PDHMS) that continually measure and transmit realtime downhole static pressures and temperatures via the field supervisory control and data acquisition system to intelligent field servers, where they are stored. These static pressures, in combination with flowing and static reservoir pressures determined from the production and injection wells, are keys for history matching reservoir simulation models. The raw intelligent field data from different sources are filtered through special software tools to remove any outliers and then summarized on an hourly or daily basis, together with calculated parameters, such as water cut and gas-oil ratio (GOR), into a usable format, Fig. 1. The data is also plotted to observe trends and identify logical and consistent data responses, especially when the wells are flowing or shut-in. Sample plots of the intelligent field data for oil producers and water injectors are shown in Figs. 2 and 3, respectively. In these plots, oil production, water production and water injection rates, together with flowing bottom-hole pressure (FBHP) and WHP, are plotted in real time. KEY CONSIDERATIONS FOR INTELLIGENT FIELD DATA INTEGRATION INTO RESERVOIR MODELING The availability of high frequency intelligent field data is beneficial for reservoir simulation modeling. The continuous pressure and rate stream, however, needs to be carefully incorporated Fig. 2. Intelligent field data — oil and water production rate and FBHP profiles. Fig. 3. Intelligent field data — water injection rate and WHP profiles. into the history matching process. The following are some key steps to be considered for the utilization of intelligent field data in history matching when compared to conventional data. Data Quality Prior to utilizing the intelligent field data for history matching, it is important to ensure data quality and consistency between the datasets, such as checking that buildups/falloffs correspond to zero production/injection periods. Data quality degradation is usually due to instruments malfunctioning, breaking down or being down for operational reasons. This can happen to gauges, meters, data relay units and servers. Data missing over a short period of a few days may not have a big impact on simulation model history matching. For longer durations and wider fluctuation, the missing data must be backfilled and filtered by well models, expert systems or smart algorithms. Data consistency problems typically manifest as illogical responses between pressure and rate data, such as getting non-zero production rate measurements while the pressure gauge data indicates a well is shut-in, or vice versa. Figure 4 shows an example of inconsistent data; the FBHP of an oil producer is rising toward the end with zero production rates, but the choke position shows that the well is still open. This was resolved through an integration of data and well rules. Tools that can quickly ensure quality assurance/quality control of the large amount of data are indispensable. Data Summarization and Conversion As previously seen in Figs. 2 and 3, the measurement frequency of intelligent field rates and pressures (hours: minutes: seconds) is often impractical for reservoir simulation purposes. On the other hand, conventional monthly production rates and infrequent wireline static pressure measurements are sometimes too far from reality. A compromise of daily average rates and pressures may be sufficient, depending on simulation hardware availability. Intelligent field data cannot be used directly and SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 27 Fig. 4. Producer missing data and inconsistent data. must go through a conversion process prior to being used in reservoir model history matching. In reservoir simulation, well FBHP at top perforation and static well pressure at datum are calculated from dynamic flow and well equations. During history matching, the calculated pressures need to be compared to the measured pressures to determine the quality of the match. To achieve this, the producer’s FBHP is corrected to top perforation, and the injector’s WHP is converted to FBHP. These conversions usually introduce some uncertainties, but to an acceptable degree. Further conversion of a well’s FBHP to static pressure may be carried out by introducing an assumed well productivity index (PI)/injectivity index (II), which involves additional uncertainties and is not recommended in instances where accurate static bottom-hole pressures (SBHP) are needed. case, the MPFM rate is close to the allocated rate, leading to high confidence in the MPFM data used for history matching. Data Reconciliation Since the field pressure data are instantaneous measurements at the well location, the well pressure output to be considered for the simulator should be based on the well average gridblock pressures rather than average drainage area pressures. This is because the latter attempts to mimic a field static pressure survey of a few hours or a couple of days for a shut-in period of a well by estimating the average drainage area pressure away from the well when the producing well is not actually shut-in, then use that estimation of static pressure in the model. For producer wells, however, a drainage area averaging method Intelligent field data provides individual well flow rate measurements. Reconciliation with the allocated monthly data for total field measurement is usually difficult. In theory, the whole is the sum of the parts, but in reality, there is usually a difference due to inexact meter calibration, missing data, out of range measurements and/or losses in the gathering and injection trunk lines. One analysis of producer rate data shows that the correction factor is centered on 1.0, Fig. 5. Therefore, in this 28 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Focus on Shut-in Periods for Static Pressure Match During the initial material balance step of the history matching, where the objective is matching the reservoir pressures while prescribed fluid volumes are withdrawn, the primary focus should be on the shut-in periods for producers and injectors, i.e., the buildup and falloff pressures, in addition to the observed well static pressures. Utilize Model Cell Average Static Pressures Rather than Drainage Area Pressures will usually estimate a higher well static pressure than the cell average technique, especially for low permeability reservoirs, Fig. 6. Today, such averaging is no longer required as the model will be run using the same (daily averaged) time steps as the intelligent field data, which includes actual shut-in time. Calibrate Well Index for FBHP Matching producing or injecting, i.e., using the FBHP, requires that the well’s PI/II be defined and/or calibrated in the model. These should be specified in the model input if measurements are available and thereafter tuned to match the FBHP data. It should be noted that the well’s PI/II may vary during a well’s producing life due to the changing operating conditions, e.g., acid stimulation, fines migration, thermal fracturing (for water injectors), etc. Utilization of the intelligent field pressure data while a well is Fig. 5. Well production rate reconciliation analyses. Fig. 6. Static cell pressure average and drainage area pressure average comparison. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 29 WORKFLOW FOR INTEGRATING INTELLIGENT FIELD DATA IN SIMULATION MODEL HISTORY MATCHING The workflow described here has been used in history matching several reservoir simulation models and is also being continuously used for updating the models. 1. Summarize the intelligent field data into daily interval time steps. This involves filtering, removing outliers and ensuring the consistency of the raw data. This can be done by an expert system, statistical algorithms, logical rules and mathematical models. 2. Reconcile the intelligent field rates with allocation rates. 3. Convert the oil, gas and water production and injection daily rates by wells into the reservoir simulator input format. 4. Convert the producer’s FBHP from gauge depth to the top of the perforation. Similarly, convert the WHP of the injectors to FBHP by using single-phase vertical flow equations. The observation well’s pressures are also converted from gauge depth to datum depth. More sophisticated well models can be used for the conversion. 5. Add new wells to the simulation model. 6. Perform the reservoir simulation with at least a weekly out put of well pressure, water cut and GOR. Pressure responses may be missed if done at a monthly interval. 7. Match the static pressure of observation wells and also the static pressures during the shut-in periods of producers and injectors. Fig. 7. Producer FBHP, oil production rate and water cut matches. 30 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY 8. Fine-tune the well’s PI/II as necessary to match FBHP. With reasonable permeability around the well after matching well static pressure, the well’s FBHP usually falls in place. If an extremely small or large PI or II is required to match a well’s FBHP, then the reservoir permeability is most likely incorrect. EXAMPLE RESULTS OF INTELLIGENT FIELD DATA INTEGRATION IN MODEL HISTORY MATCH By using the workflow just described, the high frequency rate and pressure data were incorporated in a simulation model. The history matching process was carried out the usual way using a combination of manual and assisted history match tools. Traditional history matching uses monthly average allocated rates with infrequent SBHP measurements, resulting in a wider uncertainty of the reservoir model. The averaged and nonsynchronized nature of non-intelligent field data means that the data do not capture the actual rates that correspond to the pressure responses from the well itself and from any well interference. A model that is matched to intelligent field data has reduced uncertainty due to the increased degree of constraints in the data. Most of the wells show a very good match with the high frequency pressure data and to a lesser degree with the water cut measured by MPFMs or from the allocation data. Figure 7 is an example of a history matched producer. The FBHP match, which is very good, was achieved by following the approach to match the shut-in pressure, then fine-tune the FBHP with modifications to the well’s PI. A calibrated well PI tuned to continuous FBHP measurements will give more credence to subsequent model predictions for this well as compared to predictions using a traditional model that is history matched to only conventional data. Water cut allocation issues are evident in the difference between the MPFM data and the allocated data, as previously shown in Fig. 7. In this example, we chose to match the intelligent field data water cut rather than the allocation data due to a decreasing trend in the latter — in the absence of any well intervention — which indicates that the allocated data is less reliable. Figure 8 shows a fairly good match of the SBHP during well shut-in as estimated from the intelligent field FBHP. The SBHP determined by the PDHMS is the most reliable data and requires very little processing and conversion. The SBHP match of an observation well is shown in Fig. 9, with pressure confirmation from wireline measurements (the period in the graph that shows a lot of erratic measurement was due to electric system glitches). Figure 10 shows the FBHP history Fig. 8. Producer SBHP match. Fig. 9. Observation well SBHP match. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 31 Fig. 10. Water injector FBHP match. match for a water injector. Daily water injection rates were specified as input to the simulation model and the goal was to match the FBHP derived from the WHP. Frozen flow meter data and differences with the allocation rates are evident. As most of the injectors were cleaned and not stimulated, a good match of the FBHP was achieved via modifications to model permeability rather than to the well’s II. ADVANTAGES OF INTEGRATING INTELLIGENT FIELD DATA The main advantage of integrating high frequency real-time intelligent field data for reservoir simulation modeling is the improvement in the model quality and reliability. Connectivity between wells can be calibrated more reliably using high resolution rate and pressure data. As long as the flow meters are frequently calibrated, the rate data is more reliable than the conventional data acquisition, which is often combined with infrequent well test data. Well examples previously shown clearly highlight the difference between intelligent field data and allocation data, which is the majority of data collected and stored in the past. In addition, high frequency pressure data should enhance the history match quality, as opposed to the data from conventional and infrequent wireline pressure surveys. CONCLUSIONS Our experiences in history matching several reservoir simulation models to intelligent field data show that: 32 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY 1. Filtering, processing, correction and conversion of the intelligent field data are required before it is usable for history matching. 2. Intelligent field data show that well rates and pressures vary considerably with time. Well events are accurately captured, which is impossible with monthly average rates and infrequent static shut-in pressure measurements. 3. A detailed workflow for history matching intelligent field data was developed. 4. The most accurate static pressure data is from observation wells and during producer/injector shut-in. These pressures should be given the highest priority during history matching. The FBHP matches can be fine-tuned using an individual well’s PI/II. 5. A reservoir simulation model history matched to intelligent field data is more reliable for both short-term and long-term prediction purposes since it is calibrated to a more extensive dataset than conventional monthly rates and infrequent static pressure data. ACKNOWLEDGMENTS The authors would like to thank the management of Saudi Aramco for their support and permission to publish this article. This article was presented at the SPE-SAS Annual Technical Symposium and Exhibition, al-Khobar, Saudi Arabia, April 2124, 2014. REFERENCES 1. AbdulKarim, A., Al-Dhubaib, T.A., Elrafie, E. and Al-Amoudi, M.: “Overview of Saudi Aramco’s Intelligent Field Program,” SPE paper 129706, presented at the SPE Intelligent Energy Conference and Exhibition, Utrecht, The Netherlands, March 23-25, 2010. 2. Al-Madi, S.M., Al-Aidarous, O., Al-Dhubaib, T.A., AhmadHusain, H.A. and Al-Amri, A.D.: “I-Field Data Acquisition and Delivery Infrastructure: Khursaniyah Field Best in Class Practices,” SPE paper 128659, presented at the SPE Intelligent Energy Conference and Exhibition, Utrecht, The Netherlands, March 23-25, 2010. 3. Alhuthali, A.H., Al-Ajmi, F.A., Shamrani, S.S. and Abitrabi, A.N.: “Maximizing the Value of the Intelligent Field: Experience and Prospective,” SPE paper 150116, presented at the SPE Intelligent Energy Conference and Exhibition, Utrecht, The Netherlands, March 27-29, 2012. 4. Al-Mulhim, W.A., Al-Faddagh, H.A., Al-Shehab, M.A. and Shamrani, S.S.: “Mega I-Field Application in the World,” SPE paper 128837, presented at the SPE Intelligent Energy Conference and Exhibition, Utrecht, The Netherlands, March 23-25, 2010. 5. Yuen, B.B., Abdel Ghani, R., Al-Garni, S., Olukoko, O. and Temaga, J.: “Utilizing New Proven Technologies in Enhancing Geological Modeling and Reservoir Simulation History Matching: Case Study of a Giant Carbonate Field,” paper 152, presented at the 20th World Petroleum Congress, Doha, Qatar, December 4-8, 2011. BIOGRAPHIES Bevan B. Yuen is a Petroleum Engineer Consultant with the Reservoir Simulation Division. He has built reservoir simulation models for ‘Ain Dar, Shedgum, Fazran, Abqaiq, Khurais, Abu Jifan and Mazalij production areas. Aramco in 1999, Bevan worked Prior to joining Saudi S for Amoco Canada, Computer Modeling Group, Canadian Occidental and Qatar Petroleum. He received his B.S. degree in Chemical Engineering from the University of Alberta, Edmonton, Alberta, Canada, in 1979 and his M.S. degree in Petroleum Engineering in 1982 and a MBA degree in 1990, both from the University of Calgary, Calgary, Alberta, Canada. Bevan’s interests are in complex well modeling, and fracture and streamline simulation. Dr. Olugbenga A. Olukoko is a Petroleum Engineering Consultant in the Reservoir Simulation Division, where he has been carrying out reservoir simulation studies to support field development and reservoir management activities. Prior to joining in SSaudi di Aramco A i 2005, 200 he worked for Shell and Pan Ocean Oil in Nigeria and the U.K. North Sea, holding various positions between 1988 and 2005 in both reservoir and petroleum engineering. He received his B.S. and M.S. degrees in Mechanical Engineering from the University of Lagos, Lagos, Nigeria, in 1986 and 1988, respectively. Olugbenga then received his Ph.D. degree in Computational Stress Analysis from Imperial College, University of London, London, U.K., in 1992. Dr. Joseph (Joe) Ansah is a Petroleum Engineer Specialist with the Southern Area Reservoir Management Department at Saudi Aramco, where he is involved in the development and management of the fields in the Khurais Complex. Previously, he worked k d for f Halliburton H llib t and WellDynamics in the areas of smart well completions, hydraulic fracturing and conformance technology, underbalanced drilling technology, well testing and reservoir simulation. Prior to that, Joe worked for Pennzoil E&P Company conducting property evaluation and field development in Houston and Midland, Texas. He received his M.S. degree from the Gubkin Russian State University of Oil and Gas, Moscow, Russia, and his Ph.D. from Texas A&M University, College Station, Texas, both in Petroleum Engineering. Joe has authored and coauthored over 18 technical papers in several industry journals and holds one U.S. patent. He also served on the Society of Petroleum Engineers (SPE) Editorial Review Committee from 2003 to 2009. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 33 Borehole Casing Sources for Electromagnetic Imaging of Deep Formations Authors: Dr. Alberto F. Marsala, Dr. Andrew D. Hibbs and Prof. Frank Morrison ABSTRACT INTRODUCTION The borehole to surface electromagnetic (BSEM) method and cross-well electromagnetic (EM) method have been shown to produce adequate subsurface electric current to image fluid distribution at reservoir depth. These methods have proven to be an efficient way to transmit EM signals deep into the reservoir, but their field deployment is potentially expensive and logistically challenging. This is because several days of logging conveyance inside a borehole is required to implement them. The ability to efficiently transmit EM signals inside the reservoir without a wellbore intervention would have a tremendous potential impact in terms of cost reduction and deployment opportunity for reservoir fluid mapping and monitoring, thanks to EM technologies already in the field. For BSEM, a current electrode is placed inside the wellbore at reservoir depth and a counter electrode is located adjacent to the wellhead at the surface. The reservoir fluids are then imaged through measurements of 1,000 EM receivers deployed at the surface. An innovative approach described in this work is to use a borehole casing as a way to introduce an electric current into the earth at a considerable depth. This new way to increase the current flowing in the subsurface at large offsets from the well is to combine a casing with one or more remote surface electrodes located at a radial distance of approximately the casing depth. Contrary to common expectations, a conducting casing is actually an advantage when used in conjunction with an electric source. Further, we analyze the performance of two specific variants of a casing combined with remote electrodes, showing the capability to detect small electrical features at a depth of 2 km out to greater than 2 km from the well. One of these source configurations has the considerable advantage of not requiring any well intervention for downhole operation. The model projections are compared to pilot surveys conducted in Saudi Arabia and at two sites in the USA with well depths of up to 2,100 m. Finally, we project the capability to detect small volumes of bypassed oil and establish the location of the oil-water boundary at significant depth and offset from a vertical well. Maximizing the recovery factor by means of detailed mapping of hydrocarbon accumulations in the reservoirs is a key requirement for oil producing companies. This mapping is currently done by interpolation of accurate measurements of fluid saturation at the wells’ locations, but a knowledge gap exists in the inter-well volumes, where typically the only direct measurements available are density-based (seismic and gravity) data. These technologies are not always effective in discriminating and quantifying the fluids inside the reservoirs (especially when the difference in fluid densities is small, such as between oil and water). Consequently, when high electrical resistivity contrasts exist, as they do between hydrocarbons and water, electromagnetic (EM) based technologies have the potential to map the distribution of the fluids, and if repeated in time, to monitor their movement during the life of the field, hundreds of meters or kilometers away from the wellbores. The objective of an EM survey is to obtain resistivity and induced polarization (IP) (or chargeability) maps of the reservoir, from which it is possible to calculate the saturating fluids distribution. The specificity of the borehole to surface electromagnetic (BSEM) method, compared to cross-well EM surveys, is such that a BSEM survey requires only one surveyed well to obtain an areal map of fluid distribution within a reservoir target layer kilometers away from the transmitting wellhead — up to 4 km, as demonstrated in Saudi Arabian pilot projects1, 2. A cross-well EM survey, on the other hand, allows higher resolution results, but it is limited to cross sections between two or more wells that are close enough for EM propagation — about 1 km in open holes and less in cased holes3. The BSEM method in its time and frequency domain is an evolution of the controlled source EM method, a surface-tosurface EM technique. The BSEM technology was first employed in the former Soviet Union at the end of the last millennium and has been extensively improved in the recent years in China, where it obtained positive results; a commercial protocol was subsequently developed and introduced by the Bureau of Geophysical Prospecting (BGP)4-6. Successful BSEM pilot studies have been reported by Saudi Aramco as producing resistivity and IP images of oil-water contact (OWC) at reservoir depth. In BSEM surveys, an electric current 34 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY is injected into the earth via a source electrode using the configuration shown in Fig. 1. A downhole source electrode is deployed sequentially at two or more depths inside the borehole via a wireline, and the transmitted electrical circuit is completed by a counter electrode located adjacent to the top of the well. Part of the electric current flows from the downhole electrode to the counter electrode through the casing, and the rest flows within the earth, where it generates surface EM fields that are characteristic of the electrical properties of the subsurface around the well. The acquisition grid at the surface is composed of an array of about 1,000 electric field sensors deployed up to 4 km around the EM transmitting wellhead. After data processing, the resulting maps reveal oil- and water-bearing zones in the investigated reservoir layers. Operating the downhole BSEM source electrode at two depths and subtracting the respective datasets in post-processing is equivalent to deploying a single downhole dipole with separation equal to the linear distance between the two downhole depths. Simulations for a 50 m dipole in an uncased well show detectable change in both the surface electric fields and the magnetic fields that occur at the earth’s surface up to 5 km in cases where a resistive fluid is injected at a depth of 2,500 m7. In a cased well, the concern is that the very high conductivity of the steel pipe will act as an electrical short circuit between the upper and lower electrodes of the BSEM source, resulting in negligible current flow in the surrounding earth. A pilot test of BSEM technology in a well with standard steel casing completion and production tubing, however, showed that this is not the case2. A primary signal level of 100 μV/m was reported Fig. 1. Conventional BSEM source configuration comprising an electrode at depth within a borehole and a counter electrode at the earth’s surface, adjacent to the borehole. The electric current within the ground is indicated by the lines and arrows (the current paths are only shown on one side, but they flow with approximately azimuthal symmetry all around the borehole). at 1 km from the wellhead8. This field level was approximately 100,000 times greater than the achievable measurement noise floor, opening the door to detecting those very small field changes arising from fluid movement in the reservoir. Next, we present the first calculations of the subsurface current and the surface electric field produced by one or more borehole electrodes operating from a cased well. We then project the subsurface currents and the surface electric fields for a conventional BSEM configuration and two new source configurations, described herein for the first time. The two new sources are designed specifically to exploit the capability of a casing to inject current into a subsurface formation. STATEMENT OF THEORY AND DEFINITIONS Basic Properties of the Three Basic Borehole Casing Source Configurations The two new borehole source configurations are illustrated in Figs. 2a and 2b. In Fig. 2a, a downhole electrode is deployed at depth in the well in the same way as for a BSEM survey, but instead of using a single electrode at the top of the well, the surface electrode is implemented as a suite of four to 12 electrodes distributed in a partial or full circle of 1 km to 1.5 km radius, approximately centered on the wellhead. Electric current flows down into the earth from this suite of electrodes, intercepting the casing along its entire length. Once it reaches the casing, the current predominantly flows down the casing to the downhole electrode — although in general some current intercepts the casing below the downhole electrode and flow upwards. For convenience, we term the source configuration in Fig. 2a a deep casing source (DCS). The initial motivation for using the DCS was to increase current flow in deep offset regions from the casing, which would extend the lateral detection range. The second new borehole source configuration is similar to that of the DCS except that instead of current flowing down the casing to an electrode at depth, current flows up the casing and is returned by a simple electrode connection to the top of the casing, as illustrated in Fig. 2b. This configuration is termed a top casing source (TCS) with the significant benefit that all required equipment is deployed at the ground surface instead of downhole. In the event the suite of surface electrodes is deployed in a complete circle, the DCS and TCS are similar to a circular electric dipole9 except that they use a borehole casing energized at depth as the central electrode and no attempt is made to equalize the currents in each surface electrode. It should be noted that the currents and fields produced at any location by a conventional BSEM source are simply the difference of those produced by the DCS and TCS, i.e., IBSEM = IDCS- ITCS. A simple way to capture the behavior of a casing source is to note that at any point along a casing in contact with the earth, the current divides into a component flowing in the SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 35 Fig. 2. The two borehole source configurations for depth to surface EM surveys: (a) with downhole electrodes, and (b) with the electrical connection at the top of the casing. Arrows show the direction of current flow in the casing at the same instant of the transmitted current waveform. m depth. Above a value of Lc = 900, the injected current is relatively independent of the value of Lc. Figure 3 therefore illustrates a beneficial property of using a casing source in an EM survey: the current injected into the formation can be relatively independent of the formation resistivity. For example, if the formation resistivity for the entire half of the subsurface varies over the range from 25 Ω-m to 30 Ω-m, i.e., 20%, the Iinj in the example of Fig. 3 varies by only 3.6%. The variation of injected current along casings connected in all three source configurations is illustrated in Fig. 4 for an earth model of a conventional producing oil field. The model comprises a low resistivity (2 Ω-m) surface layer to 1,300 m depth, a layer of moderate resistivity (12 Ω-m) from 1,300 m to 1,500 m, a reservoir layer of thickness 15 m and resistivity 1 Ω-m, and a base layer of resistivity 5 Ω-m to a depth of 4,000 m. The change in Iinj when crossing between each layer is immediately apparent. Importantly, despite the fact that the contact to the casing is made at opposite ends, the current injected into the reservoir for the TCS is 60% of that produced by the DCS. The effect of adding an annulus of thickness 15 m and resistivity of 8 Ω into the reservoir layer of the model used to generate Fig. 4 is shown in Fig. 5. The center of the annulus is at a distance of 500 m from the casing, and the data is plotted as a percentage change to the current injected at reservoir depth compared to the 50 m wide case. An annulus represents an extreme example of an anomaly because it intersects the radial current in all directions. We see that there is less than 1% change in the current in the reservoir layer up to an annulus of width, 200 m for the DCS and 400 m for the TCS. This is an important result because it shows that for many geologic features of interest, the profile of the injected current along the casing is not significantly affected by the resistivity structure of the earth, and can be calculated for the earth model alone in the absence of a target body. Detection of Subsurface Features via their Resistivity Contrast earth and a component flowing along the casing. For an infinitely long vertical casing in a uniform earth, the current flowing along the casing varies exponentially with the distance of characteristic length Lc, given by Lc = √(Sc ρf) where Sc is the casing conductance and ρf is the formation resistivity10. For example, for a 20 cm diameter casing in earth of resistivity 20 Ω-m, Lc = 910 m. The current injected into the formation, Iinj, is the spatial differential of the current flow along the casing, i.e., The purpose of using a casing source is to extend the depth of (1) The casing dimensions and resistivity are generally stable and well-defined, and so the primary parameter that affects Lc is the formation resistivity. For example, the variation of casing current and injected current as a function of Lc is shown in Fig. 3 at a depth of 1,500 m for a casing extending to a 1,600 36 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Fig. 3. Current flowing along a casing (Icas) and injected into a uniform earth at a depth of 1,500 m (Iinj) as a function of casing conductance length. Casing length is 1,600 m. Fig. 4. Variation of injected current (mA) with depth (m) for the TCS, DCS and BSEM sources. The subsurface model comprises four layers: 0 m to 1,300 m with resistivity of 2 ȉ -m; 1,300 m to 1,500 m with resisitivity of 12 ȉ -m; 1,500 m to 1,515 m with resisitivity of 1 ȉ -m; 1,515 m to 4,000 m with resistivity of 5 ȉ -m; and with casing to a depth of 1,600 m: (a) Injection current profile over all four layers, and (b) Injected current in the reservoir layer (1,500 m to 1,515 m). Fig. 6. Predicted TCS signals for a 100 m x 100 m wide region with center at 537 m indicative of a nonproducing zone in an earth model of the Marcellus shale: (a) Contour plot of the surface E-field signal per unit current produced by the anomaly for a TCS, and (b) Profile of the field in the x-direction (Ex) along the x-axis for the TCS compared with profiles for a DCS, BSEM and conventional surface EM source at the same casing location. Fig. 5. Change in injected current into the reservoir (%) vs. the width (m) of an annular resistive anomaly in the reservoir. The anomaly is centered at 500 m offset from the casing. Reservoir resistivity is 1 ȉ -m and the anomaly resistivity is 8 ȉ -m. EM investigation to the depth of typical hydrocarbon reservoirs. A particular application is to image resistivity anomalies characteristic of hydrocarbon deposits. In Fig. 6, we calculate the surface electric field signal produced by a 100 m wide x 100 m long target in an earth model representative of the Marcellus shale formation for a surface source electrode at x = 0, y = 500 m. The target is taken to be the difference between a mature shale region containing producible hydrocarbons that is characterized by a resistivity of 35 Ω-m and an immature hydrocarbon region of resistivity 10 Ω-m11. The depth to the top of the shale is 1,890 m and the reservoir formation is 60 m thick. The contour plot shows that the surface field produced by the conducting anomaly is well aligned with the physical location of the anomaly. The field differences projected in Fig. 6 are approximately 10 times higher than the minimum detectable signal for advanced electric field sensors. For example, a sensor noise level of 10-11 V/m can be achieved with less than 1 hour of recorded signal averaging. The field profile in Fig. 6b shows that both the TCS and DCS provide a dramatically improved capability to detect and image hydrocarbon resistivity features at reservoir depth compared to surface EM methods. As previously discussed, BSEM is equivalent to the difference of the TCS and DCS, and so in this example it gives a much reduced signal. As a final study, we calculate the resistivity change due to the motion of an OWC in a 2,000 m deep reservoir, which is characteristic of the geology in a Saudi Arabian super giant oil field. We define two regions; an oil region with water saturation, Sw = 13% and resistivity 55 Ω-m, extending outwards as an annular region from the well, which is bounded by an outer water region with Sw = 50% and resistivity 4 Ω-m. The reservoir SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 37 is 26 m thick. To make the signal differences easier to view, Fig. 7 shows the surface field change for an oil to water boundary at three different distances from the well relative to the value at 500 m. Importantly, the TCS produces a signal change within a factor of approximately 25% of the DCS source. Again, these fields are detectable using presently available technology. For a time-lapse measurement, considerable signal averaging is possible, and the TCS opens the door to long-term monitoring without the cost of opening the well and providing a wireline. DESCRIPTION AND APPLICATION OF EQUIPMENT AND PROCESSES PRESENTATION OF DATA AND RESULTS Figure 9 shows a comparison of the calculated and measured surface electric field along a 2 km line from a well in a producing oil field in Montana. The two values of subsurface electrical resistivity as bounded by available well resistivity logs are shown. The agreement between the predicted and measured surface electric field is good, considering that other wells and shallow connecting pipes were also present at the site. The peak in the surface field at approximately 1,500 m from the wellhead is caused by the receiver line passing very close to one of the surface source electrodes, which were deployed on Pilot Tests of EM Borehole Casing Sources Two successful pilot tests of a BSEM source were conducted by Saudi Aramco and the BGP, and results have been reported1, 8. In 2013, three successful tests of the TCS were conducted in North America: at a mature oil field, at a CO2 sequestration site and at a geothermal test well. Figure 8 shows an example of the electrical connection to the wellhead. A TCS is clearly very easy to configure and has the obvious advantage that the well does not need to be opened. It is also clearly suitable for long-term monitoring and permanent installation. Fig. 8. Photograph of a TCS connection to a wellhead for a pilot survey conducted in 2013. Fig. 7. Change in surface E-field for three positions of the boundary between oil and water relative to the field for the same boundary at 500 m from a well in a 2,000 m deep reservoir: (a) DCS, and (b) TCS. 38 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Fig. 9. Comparison of the measured and calculated surface electric field produced by a TCS as a function of radial distance from the wellhead. The source has a partial ring of surface electrodes at a radius of 2 km. a 1.5 km radius circle. The electric field at 1,800 m is 50 μV/m; approximately 10 times the value per unit currently measured at the same distance in Saudi Arabia for a BSEM source. Overall, Fig. 9 demonstrates that the TCS can be used successfully in conditions relevant for hydrocarbon reservoir monitoring. CONCLUSIONS Cross-well EM and BSEM are efficient ways to transmit EM signals underground; they allow deep selective investigation of reservoir layers, as demonstrated in recent surveys in Saudi Arabia. Nevertheless, the costs and logistics linked to prolonged downhole deployment of electrodes in the borehole could limit their fast deployment potential. The innovative idea is to use wellbore casings as “guided wave antennas” to induce EM signals from the surface, going deep into the reservoir. The EM transmission occurs, connecting an electrode at the wellhead and a counter electrode buried in the ground kilometers away. The EM signals, transmitted through the reservoir, are then recorded at the surface by arrays of hundreds of receivers. The borehole casing provides a distributed path to inject electrical current into the earth’s subsurface down to the reservoirs. Two new casing sources are described that produce considerably larger signals than a conventional surface EM measurement and the recently introduced BSEM method. One of these sources, the TCS, has the further significant advantage that it requires no downhole equipment of any kind. Importantly, the current injected into the subsurface by a casing varies as the differential of the current flow along the casing, leading to beneficial results, in that the current injected at depth from a TCS can be almost as large for a DCS and larger than for the BSEM source. Through data processing, the outcomes of those methods are resistivity, chargeability and fluid distribution maps of the investigated reservoir. The goal is to map and monitor fluid distribution in the interwell volumes, supporting production optimization and recovery increase from the hydrocarbon fields. A pilot field test was recently concluded, demonstrating the intrinsic safety of this EM transmitting method: At the wellhead, we measured a harmless mere 0.36 V (relative to the ground) on the casing connected to the source when transmitting EM signals with the high power source (20A, 800 V) required to energize a reservoir 4,000 m deep. Numerical modeling of this innovative EM transmission method validates its feasibility and potential to be deployed extensively in the field, even in time-lapse applications. Furthermore, an important issue for permanent monitoring is the longevity of the system components in contact with the earth. For a system that relies on injecting current, a particular concern is degradation of the current injection electrodes. The TCS has a particular advantage in this regard because only a simple metalto-metal connection is made at the top of the casing, compared to the need to provide electrical coupling within the fluid environ- ment inside the wellbore for all other downhole-based sources. These developments considerably enhance the application of EM methods to reservoir imaging. Both the TCS and DCS sources have the capability to detect fluid movements in an OWC using an array of electric and magnetic field sensors deployed at the surface. Because the TCS does not affect oil production, it could be considered for continuous operation, and used to provide permanent real-time monitoring in producing fields. When extensively field proven, this EM methodology will have a tremendous potential impact in terms of cost reduction and the potential to be deployed broadly for fluid distribution mapping and monitoring in hydrocarbon fields. ACKNOWLEDGMENTS The authors would like to thank the management of Saudi Aramco, GroundMetrics and Berkeley Geophysics Associates for their support and permission to publish this article. This article was presented at the SPE Annual Technical Conference and Exhibition, Amsterdam, The Netherlands, October 27-29, 2014. REFERENCES 1. Marsala, A.F., Al-Buali, M., Ali, Z.A., Ma, S.M., He, Z., Biyan, T., et al.: “First Borehole to Surface Electromagnetic Survey in KSA: Reservoir Mapping and Monitoring at a New Scale,” SPE paper 146348, presented at the SPE Annual Technical Conference and Exhibition, Denver, Colorado, October 30 - November 2, 2011. 2. Marsala, A.F., Lyngra, S., Widjaja, D.R., Al-Otaibi, N.M., He, Z., Guo, Z., et al.: “Fluid Distribution Inter-Well Mapping in Multiple Reservoirs by Innovative Borehole to Surface Electromagnetic: Survey Design and Field Acquisition,” IPTC paper 17045, presented at the International Petroleum Technology Conference, Beijing, China, March 26-28, 2013. 3. Marsala, A.F., Ruwaili, S.B., Ma, M.S., Al-Ali, Z.A., AlBuali, M.H., Donadille, J-M., et al.: “Crosswell Electromagnetic Tomography: From Resistivity Mapping to Interwell Fluid Distribution,” IPTC paper 12229, presented at the International Petroleum Technology Conference, Kuala Lumpur, Malaysia, December 3-5, 2008. 4. He, Z., Liu, X., Qiu, W. and Zhou, H.: “Mapping Reservoir Boundary by Using Borehole Surface TFEM Technique: Two Case Studies,” SEG-2004-0334 paper, presented at the SEG Annual Meeting, Denver, Colorado, October 10-15, 2004. 5. He, Z., Hu, W. and Dong, W.: “Petroleum Electromagnetic Prospecting Advances and Case Studies in China,” Surveys in Geophysics, Vol. 31, No. 2, March 2010, pp. 207-224. 6. He, Z., Zhao, Z., Liu, H. and Qin, J.: “TFEM for Oil SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 39 Detection: Case Studies,” The Leading Edge, Vol. 31, No. 5, May 2012, pp. 518-521. 7. Beyer, J.H., Smith, J.T. and Newman, G.: “Controlled Source Electromagnetic (CSEM) Surveys to Monitor CO2,” presentation at the West Coast Regional Carbon Sequestration Partnership Annual Business Meeting, Lodi, California, October 24-26, 2011. 8. Marsala, A.F., Hibbs, A.D., Petrov, T.R. and Pendleton, J.M.: “Six-Component Tensor of the Surface Electromagnetic Field Produced by a Borehole Source Recorded by Innovative Capacitive Sensors,” SEG Technical Program Expanded Abstracts, 2013, pp. 825-829. 9. Mogilatov, V. and Balashkov, B.: “A New Method of Geoelectrical Prospecting by Vertical Electric Soundings,” Journal of Applied Geophysics, Vol. 36, No. 1, November 1996, pp. 31-44. 10. Schenkel, C.J. and Morrison, H.F.: “Effects of Well Casing on Potential Field Measurements Using Downhole Current Sources,” Geophysical Prospecting, Vol. 38, No. 6, April 2006, pp. 663-686. 11. Schmoker, J.W. and Hester, T.C.: “Oil Generation Inferred from Formation Resistivity – Bakken Formation, Williston Basin, North Dakota,” Transactions of the 13th SPWLA Annual Logging Symposium, June 14, 1989. BIOGRAPHIES Dr. Alberto F. Marsala has more than 20 years of oil industry experience. For the last 8 years, he has been working in Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC). Alberto started his career with Eni and Agip, Agip where he participated in several upstream disciplines, including 4D seismic, reservoir characterization, petrophysics, geomechanics, drilling and construction in environmentally sensitive areas. Alberto worked on the Technology Planning and R&D committee of Eni. He was Head of Performance Improvement for the KCO joint venture (Shell, ExxonMobil, Total and others) concerned with the development of giant fields in the northern Caspian Sea. Alberto is now the Focus Area Champion for Deep Diagnostic on the Reservoir Engineering Technology team of EXPEC ARC, where he is pioneering innovative technologies for advanced mud logging, logging while drilling, and gravity and electromagnetic methods for reservoir mapping and monitoring. In 1991, Alberto received his Ph.D. degree in Nuclear Physics from the University of Milan, Milan, Italy, and in 1996, he received an M.B.A. in Quality Management from the University of Pisa, Pisa, Italy. He also holds a Specialization in Innovation Management, received in 2001. 40 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Dr. Andrew D. Hibbs is a leading scientist and industrialist in the low frequency electromagnetic sensing community. He was one of the founders of Quantum Magnetics (QM), a pioneer in aviation security technologies, which was acquired by IInVision Vi i Technologies T h l i in 1998 and later by General Electric in 2004. Prior to the acquisition of QM in 1998, Andrew founded Quantum Applied Science and Research (QUASAR) to develop bioelectric sensing systems, and he has since spun out four other companies from QUASAR covering diverse applications of EM sensing, including EEG, ion channel measurements, lightning research, and covert facilities detection and monitoring. Among other pursuits, he is currently serving as Chief Technology Officer of GroundMetrics Inc., which is pursing electromagnetic applications in subsurface imaging for resource exploration and extraction monitoring. Prof. Frank Morrison is currently a P. Malozemoff Professor Emeritus of Mineral Engineering at the University of California, Berkeley, and the President of Berkeley Geophysics Associates. During his long and distinguished career, Frank F k has h conducted research and done field and laboratory work on a wide range of topics in applied geophysics. Subjects have included numerical modeling of electrical, IP and electromagnetic (EM) methods, field studies of controlled source EM and self-potential methods for geothermal exploration, ground and marine magnetotellurics (MT) for petroleum exploration, audio frequency MT profiling for mineral and groundwater exploration, development of the theory and a full-scale prototype for a unique single coil airborne EM system, and theory and field systems for EM imaging between boreholes. He developed a new induction coil sensor for high sensitivity measurements of low amplitude magnetic fields and incorporated these sensors in the first portable magnetotelluric system. Frank was a co-founder of Electromagnetic Instruments, which successfully commercialized the new MT system. Working with Ed Nichols, he developed a controlled source audio frequency MT system designed to enable a new generation of groundwater exploration methods. This system was transferred to Geometrics and is now marketed as the Stratagem system. For his accomplishments and for his role in translating the results of many research projects into practical methods for the exploration industry, Frank was elected an Honorary Member of the Society of Exploration Geophysicists (SEG) in 1999. He has published over 70 papers in recognized geophysical journals. Frank received his Ph.D. degree in Engineering Science from the University of California, Berkeley, CA, in 1967. Laboratory Study on Polymers for Chemical Flooding in Carbonate Reservoirs Authors: Dr. Ming Han, Alhasan B. Fuseni, Badr H. Zahrani and Dr. Jinxun Wang ABSTRACT As part of the screening process for chemical enhanced oil recovery (EOR), 18 polymer samples were screened as co-injectants in a surfactant-aided waterflood scheme. Due to their higher viscosity, polymers improve waterflood sweep efficiency and reduce the permeability of the rock matrix, therefore helping to improve oil recovery. Aimed at a representative carbonate reservoir in the Middle East, the polymer screening study focused on polymer solubility and viscosity retention in high salinity brines, equivalent to the reservoir parameters. The polymers had to pass through a stringent screening process to meet the harsh conditions encountered in the reservoir: high temperatures, high salinities and the nature of the carbonate. Salinity effect was studied in a range of brines that included shallow formation water, produced water and connate water. Among the polymers studied, six were found compatible and have been shortlisted for EOR use. Based on rheological measurements and flow curves, the concentrations of the polymers were determined to achieve the target viscosity under reservoir conditions. Longterm stability and adsorption tests were conducted to ensure the continued efficiency of the polymer when exposed to reservoir conditions. Oil displacement tests with a selected polymer showed an increased oil recovery factor of 11% by polymer flooding and 18% by surfactant polymer (SP) flooding. This study demonstrates the potential application of polymers under extremely harsh reservoir conditions and their promise as good additives for chemical flooding. INTRODUCTION Water soluble polymer is one of the key components in a chemical enhanced oil recovery (EOR) process. It has been used in processes of polymer flooding alone1, 2; polymer coinjection with surfactants, such as in surfactant polymer (SP) flooding3-5 or alkaline SP flooding6-9; and as a preflush/ post-flush slug in surfactant or alkaline flooding. Usually, two kinds of polymers have been used in the field: a synthetic polymer classified as polyacrylamide and a biopolymer known as xanthan. More than 90% of polymers consumed for chemical EOR are the acrylamide type, whereas biopolymers like xanthan are used in the field to only a very limited degree1. The polymers are usually used at concentrations of 1,000 ppm to 2,000 ppm in the flood water. Recently, higher polymer concentrations were required to achieve a given viscosity under conditions of high salinity and high temperature10. Leonhardt et al. (2013)11 presented field trial results for polymer flooding with a biopolymer, schizophyllan, in a high salinity reservoir (186 g/L total dissolved solids (TDS)). Also, some new synthetic polymers have received attention in recent research and field applications, such as sulfonated polymers and sulfonic associative polymers12-15. The role of a polymer in a chemical EOR process is primarily to reduce the mobility ratio by increasing the viscosity of the water16, although other mechanisms like viscoelastic effect are involved17. It improves oil recovery beyond that achieved by waterflooding or surfactant flooding alone by increasing the contacted volume of the reservoir. In addition to increasing water viscosity, polymer reduces the permeability of the reservoir matrix. This further lowers the effective mobility of the injected fluid by increasing the residual resistance factor (achieved with permeability reduction). When the permeability is reduced, a lower polymer concentration can be used to gain equivalent mobility control. This study targeted a representative carbonate reservoir in the Middle East. The challenges were the high salinity of the reservoir brines and high reservoir temperatures. The evaluation of the polymers included tests of their compatibility with various formation brines, a rheology study, assessment of the impacts of salinity and temperature, and tests of the polymer’s long-term stability. The results of this work demonstrate the potential application of polymers under extremely harsh reservoir conditions and their promise as good additives for EOR in carbonate reservoirs. CHALLENGES OF CHEMICAL EOR IN CARBONATE RESERVOIRS Significant challenges exist in the development of chemical EOR methods for carbonate reservoirs due to the complexity of the rock mineral compositions, matrix pore structures, rock surface properties, fracture densities, aperture and orientations, as well as the different oil types18, 19. Carbonate rocks are a class of sedimentary rocks composed primarily of carbonate SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 41 minerals. The two major types are limestone, which is composed of calcite or aragonite (different crystal forms of CaCO3), and dolostone, which is composed of the mineral dolomite (CaMg(CO3)2). The nature of carbonate rocks differs from that of sandstones, which are composed of quartz (SiO2) grains cemented together with a variety of minerals. The lithology is described as a lime mud, foraminifera detrital carbonate20. The detrital carbonate presents a bimodal pore system with a pretty good permeability and porosity21. Despite its overall excellent flow characteristics, the bimodal system poses unique challenges of recovering the oil remaining in the micropores. Due to digenesis, carbonates tend to be more heterogeneous. Natural fractures are more common in carbonate rocks than in sandstones. The high density of such fractures and the resulting high permeability zones present fluid flow uncertainty. In carbonate reservoirs, Super-K zones are areas dominated by high linear flow; they can be high matrix flow zones or faults and fractures22. The flow uncertainty in the presence of fractures and high permeability zones tends to complicate the application of EOR in such reservoirs. The zones of high permeability are important conduits for the flow of oil in the early production stages of the reservoir. Subsequently, as the field matures, these same zones become the conduits for excessive water production. In an EOR project involving the injection of expensive fluids, care needs to be taken to avoid the channeling of the slug through such conduits to the producing well. Harsh reservoirs are those with high brine salinity and hardness, and with high reservoir temperatures. Most field cases of chemical flooding have been reported in moderate reservoirs. Figure 1 shows the current limitation of chemical EOR technology on a salinity and temperature plot. The high salinity and hardness of the reservoir brine degrade the chemicals’ effectiveness; polymers tend to precipitate when exposed to high concentrations of divalent cations and will partition to the oil phase at high salinities. High reservoir temperature also affects the stability of the chemicals, especially polymers. Some major reservoirs in the Middle East are in the high salinity and high temperature region. This presents significant challenges in the application of chemical EOR technologies. A majority of the big carbonate fields are developed with a peripheral water injection scheme, where water is injected on the flanks of the reservoir for pressure maintenance23-25. The objective of peripheral flooding is not only to maintain the reservoir pressure but also to sweep the oil efficiently. In spite of the carbonate’s complexity and the wide variation in rock types and permeabilities, most of the big carbonate examples have experienced semi-uniform flooding. For some major carbonate reservoirs with decent porosity and permeability, the gravity/sudation force plays an important part in the depletion process26 and the oil recovery can reach about 50% by means of a peripheral waterflood. In peripheral water injection, the well spacing is typically 0.5 km to 1 km. Such a large well spacing leads to a delayed chemical flooding incremental recovery response. The incremental response can also be reduced further as chemicals lose their effectiveness due to dispersion and adsorption. For this reason, in-fill drilling to reduce well spacing is usually required for chemical EOR implementation. EXPERIMENTAL STUDY Materials Brines. Simulated field brines were synthesized for the study based on the corresponding water analyses, including connate water, seawater (injection water) and produced water. The detailed water analyses are presented in Table 1. All the simulated brines were filtered through a 0.45 micron filter and deaerated for test use. Polymers. Several parameters have to be taken into account when screening polymers to find the best candidates for SP flooding in a Middle East carbonate reservoir. Good polymer Seawater (ppm) Produced Water (ppm) Connate Water (ppm) Sodium 18,300 19,249 59,491 Calcium 650 4,360 19,040 2,110 938 2,439 n/a n/a n/a Sulfate 4,290 1,299 350 Chloride 32,200 40,704 132,060 0 0 0 120 585 354 57,670 67,135 213,734 Ion Magnesium Potassium Carbonate Bicarbonate TDS Fig. 1. Challenge in chemical EOR for Middle East carbonate reservoirs. 42 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Table 1. Composition of field brines candidates should meet the following requirements: • Compatible with field brines. • Effective at low concentration (0.1% to 0.3%). • High viscosity (2 centipoise (cP) to 5 cP) over a wide range of salinity at 95 °C to 100 °C. • Long-term stability (<50% viscosity loss over 6 months at Polymer Type Polymer Form Active (%) PST01 HPAM Powder 86.92 PST02 Sulfonated PAM Powder 91.80 PST03 Sulfonated PAM Powder 92.16 PST04 Sulfonated PAM Powder 87.70 PST05 Biopolymer Powder 88.84 PST06 Biopolymer Powder 89.69 PST07 Biopolymer Powder 91.31 PST08 Biopolymer Powder 86.38 PST09 Modified PAM Powder 88.17 PST10 Modified PAM Powder 88.49 PST11 Associating PAM Powder 93.62 PST12 Associating PAM Powder 91.06 PST13 High Molecular Weight PAM Powder 88.04 PST14 HPAM Powder 90.54 PST15 HPAM Powder 92.37 PST16 HPAM Powder 87.45 PST17 Sulfonated PAM Powder 93.06 PST18 Sulfonated PAM Powder 93.30 Polymer 95 °C to 100 °C). • Low adsorption onto formation rock (<1 mg/g-rock). • Available in large quantities. • Easily handled in the field. A total of 18 polymer samples were tested, including polyacrylamide, sulfonated polyacrylamide and associative polyacrylamide, as well as polysaccharides like xanthan gum, scleroglucan and Welan gum. The chemicals listed in Table 2 were renamed in this article to avoid commercialism and for confidential concerns. Rheological Measurement. A MCR 301 rheometer from Anton Paar, Austria, was used for rheological measurement. The instrument enables the measuring of various viscoelastic properties, including flow curve, creep and viscoelasticity. It is equipped with concentric cylinder geometry having shear rates ranging from 0.01 s-1 to 1,000 s-1. Viscosity was also measured using DV II+Pro, a Brookfield viscometer made in the U.S., for preliminary screening. The spindle used was S18. The temperature was set at 25 °C. Polymer Concentration. The polymer concentrations were verified by carbon analysis using a total organic carbon (TOC) analyzer made by Shimadzu, Japan. Core Plugs. Natural core plugs with a 3.81 cm (1½”) diameter were selected for the coreflooding tests. The diameter and length of the plugs ranged from 3.7 cm to 3.8 cm and from 3.6 cm to 4.6 cm, respectively. The air permeability, pore volume and porosity of the core plugs were measured by routine core analysis. The dried core plug samples were evacuated and saturated with the simulated formation brine. The saturated plugs were immersed in the simulated formation brine to establish ionic equilibrium between the rock constituents and the formation brine. Brine permeability was then measured using the simulated Table 2. Polymers collected for screening Core Num. Length (cm) Diameter (cm) Porosity (fraction) Air Permeability (md) Pore Volume (cm3) Brine Permeability (md) Coreflooding Test 1 4.95 3.785 0.188 633 10.471 501 Polymer Adsorption 2 4.44 3.798 0.168 513 8.458 441 Polymer Adsorption 3 4.42 3.768 0.275 445 13.566 315 Adsorption of Surfactant and Polymer 4 4.64 3.798 0.165 428 8.664 304 Adsorption of Surfactant and Polymer 5 4.69 3.785 0.121 175 6.392 N/A Polymer Flooding 6 3.61 3.790 0.232 122 3.94 N/A SP Flooding 7 4.62 3.800 0.214 134 6.73 N/A SP Flooding Table 3. Petrophysical properties of core samples for coreflooding tests SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 43 formation brine. Table 3 lists the detailed porosity, pore volume, air permeability and brine permeability for the test samples. Seawater Produced Water Connate Water Remark PST01 C C C Declined PST02 A A A Excellent PST03 A A A Excellent PST04 A A A Excellent Polymer Coreflooding Tests. The FDES-645 coreflooding apparatus, made by Coretest System, USA, was used in this study. The schematic setup is shown in Fig. 2. Injection pressure, confining pressure, pore pressure, differential pressure and flow rate were recorded automatically during the test. The specific test procedures are described later for the experiments investigating dynamic adsorption and oil displacement. PST05 B A A Excellent PST06 B B B Good EVALUATION OF POLYMERS IN BULK SOLUTIONS PST07 C D D Declined PST08 C C D Declined PST09 A A A Excellent PST10 A C C Declined PST11 A A A Excellent PST12 D D D Declined PST13 C C C Declined PST14 A A A Excellent PST15 A A A Excellent PST16 A A A Excellent PST17 A A A Excellent PST18 A A A Excellent Compatibility with Brines Studies of the compatibility between reservoir fluids and polymers are in many cases critical to predict whether the polymer can be applied successfully. This is because the efficiency of a polymer solution will be greatly reduced if there are precipitation and insoluble particles when the solution encounters incompatible brines. Therefore, compatibility tests were conducted for all the polymers with respect to field brines. Polymer solutions with 2,000 ppm active component were prepared in different field brines. The solutions were sealed and put in an oven at 95 °C, then observed visually for evidence of precipitation. The results were recorded by compatibility codes of A: clear solution; B: slight hazy solution; C: hazy solution; and D: precipitation, Fig. 3. Table 4 illustrates the results of the compatibility studies with different field brines. Based on this study, seven out of the 18 polymers were eliminated from the candidate list. Table 4. Compatibility codes showing polymer compatibility with field brines Viscosities of Polymers in Brines The viscosity of a polymer is one of the critical parameters to evaluate its effectiveness in a given reservoir environment, especially one with high salinity and temperature. A polymer’s viscosity depends on its chemical structure (type, component and molecular weight) and its configuration (coil and rod) in brine. Figure 4 shows the viscosities of the candidate polymers in different brines (seawater, produced water and connate water). With this test, we eliminated four more polymers having low viscosity due to low molecular weights, although these polymers presented a strong potential to tolerate high salinity and high temperature environments. Fig. 2. Schematic setup for coreflooding tests. Fig. 3. Compatibility codes. 44 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Rheological Characteristics Rheological study of the deformation and flow of matter under the influence of an applied stress provides insight into the deformation/flow behavior of the material and its internal structure. The rheological properties of polymer solutions play a very important role in characterizing the polymers and determining their likely performance and effectiveness. Polymer solutions are known to exhibit non-Newtonian, shear-thinning fluid behavior. In other words, the viscosity is dependent on the shear rate. Actually, the viscosity-shear rate range. PST02, in a coil configuration, also showed shear-thinning behavior with an increasing shear rate. The Carreau model was used to cover overall performance in a full range of shear rates. In the Carreau model, the viscosity function depends on the shear rate, Eqn. 2. Fig. 4. Viscosity of the test polymers in different brines. relationship exhibits a Newtonian behavior at low shear rates and a power-law behavior at high shear rates. These properties can usually be determined in the laboratory using a rheometer. This fluid performance is critical for assessing the field application of a polymer solution because the polymer solution presents different viscosities on the surface, at the perforations and at different locations during its propagation in the reservoir. This phenomenon of differing viscosity is based on the fact that the configuration of a polymer changes with the velocity. The shear rate in the rock matrix is basically dependent on the flow velocity and rock properties, as seen in Eqn. 1. (1) where is shear rate, C is constant, ȗ is velocity, k is permeability, and is porosity. In this work, we demonstrate the characteristics of two promising polymers: a synthetic polymer (PST02) and a polysaccharide (PST06). Figure 5 shows the flow curves of PST02 and PST06 at 2,000 ppm concentration in produced water at 25 °C. PST06 is a biopolymer in a rod-like configuration, leading to a high viscosity at a low shear rate range, and significant shear-thinning behavior and low viscosity at a high shear Fig. 5. Flow curves of PST02 and PST06 solutions in produced water. (2) where 0 is zero shear viscosity, is infinite viscosity, (n-1) is slope shear thinning, and is rotational relaxation time, which is the inverse of the critical shear rate. The critical shear rate is the shear rate at which there is a transition from Newtonian to shear-thinning behavior. The rheological parameters in Table 5 were extracted from the flow curves. Figure 6 demonstrates the fit of the model with the actual data. These parameters can be used to estimate the viscosity at any shear rate, including zero-shear viscosity and infinitive viscosity. It is important to simulate the viscosity for a numerical reservoir simulator for a chemical EOR process when polymer solution propagates in the deep reservoir. The variation of the viscosity of a polymer solution, , as a function of concentration, c, can be described as: (3) Parameter PST02 PST06 h0 20.3 cP 6,230 cP h3 6.59 cP 2.06 cP x 3.16 s 11.63 s n-1 0.46 0.81 Table 5. Rheological parameters of PST02 and PST06 extracted from the flow curves Fig. 6. Simulation of flow behavior of 0.2% PST06 solution in produced water using the Carreau model matched with real data. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 45 in which s represents solvent viscosity, k1 and k2 are constants, and [] is intrinsic viscosity. The is generally referred to as zero-shear viscosity, which is determined by a flow curve. The [] and the overlap concentration can be obtained by flow curves. In a very low concentration range, [] can be determined by extrapolation of sp/c to c->0 as: (95 °C). The polymer solutions were taken from the oven periodically to measure the viscosity retention. Figure 7 shows that some polymers can withstand 6 months under the given conditions of 95 °C and an anaerobic environment, i.e., they retain sufficient viscosity. With this test, the number of potential polymers was reduced to four. Interaction with Selected Surfactants (4) The [] is related to the size (gyration radius) of a single molecule in the solution, indicating the capacity to increase the viscosity. In general, at certain conditions, the polymer molecule weight, M, can be determined by the following relationship: (5) in which k is a constant, and a is a constant between 0.5 to 1.5. The overlap concentration, C*, is an important parameter in describing a polymer solution. In polymer solution theory, polymer solutions are divided into regimes: dilute, semi-dilute and highly concentrated. The critical concentration between the dilute regime and the semi-dilute regime is called the overlap concentration. It corresponds to the solution where polymer coils begin to touch one another throughout the solution. Table 6 summarizes the values of C* and [] for two polymers in different brines. Usually, polymer concentration is selected in a semi-dilute regime. Therefore, the concentration used for PST02 should be much higher than that for PST06. In this regard, polysaccharides with a rod-like configuration in solution present advantages over synthesized polymers. This is consistent with the literature. Because some polymers were screened as co-injectants for a SP flooding scheme, the compatibility of the polymers with selected surfactants was an additional criteria for the polymers. Although polymers and surfactants are added to the water for their independent functions, some interactions may arise. Such interactions when a polymer and a surfactant are present together may lead to significant changes in the system properties, which are considered either beneficial or undesirable, depending on the prevalent conditions. Formulations of the promising polymers and surfactants were developed by changing and tuning the concentrations of the chemicals and environments to get better SP compatibility, lower interfacial tension (IFT), higher viscosity, lower adsorption and eventually higher oil recovery. Table 7 illustrates the properties of some formulations studied. This led to the elimination of polymer in formulation #8, which is obviously incompatible with a selected amphoteric surfactant. EVALUATION OF POLYMERS IN POROUS MEDIA Long-term Stability To be effective, polymer solutions must remain stable for a long time at reservoir conditions. Polymers are known to be sensitive to chemical and thermal degradations, especially in the presence of oxygen and oxidizing agents at high temperature. It is believed that the reservoir is an anaerobic environment. Therefore, the polymer solution is expected to be free of oxygen during its propagation in the reservoir. The polymer solutions were prepared by replacing oxygen using nitrogen for 2 hours before putting them in the oven at reservoir temperature Brine Fig. 7. Long-term stability of three polymer solutions in seawater in an anaerobic environment at 95 °C. PST02 PST06 C* (ppm) [h] (mL/g) C* (ppm) [h] (mL/g) Seawater 1,700 2,352 268 14,909 Produced 2,323 1,722 218 18,348 Connate 5,405 740 - - Table 6. Overlap concentration, C*, and intrinsic viscosity, [n], of PST02 and PST06 46 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Formulation Compatibility (Compatibility Code) #1 Phase Behavior (Winsor Type) IFT at 90 °C (dynes/cm) Viscosity (cP) 25 °C 95 °C 25 °C 95 °C 25 °C 95 °C Simul. Eq. A A I I 45.8 11.5 0.00606 0.0096 I I 16.9 4.84 0.00464 0.00769 #2 B B #3 B C I I 20.0 5.62 0.337 0.479 #4 B B I I 19.2 5.45 / 0.0595 #5 A B I I 21.9 5.49 / 0.0461 I I 59.6 6.7 0.0279 0.0549 #6 A B #7 A B I I 26.2 8.96 0.04520 0.0479 #8 A C I I 20.2 5.71 / 0.0215 #9 B B I I 31.5 7.75 0.00939 0.0369 I I 50.0 8.75 0.06250 0.0661 #10 A B #11 A B I I 22.5 5.29 0.03650 0.0455 #12 A B I I 131.0 15.0 0.03370 0.0667 #13 A B I I 27.6 6.66 0.00740 0.0382 Table 7. Properties of study formulations The polymer selected for further study, PST02, is a sulfonated polymer. The main objectives were to evaluate its dynamic adsorption or retention, the injectivity, and its oil recovery potential in porous media with a carbonate nature. In some cases, a selected amphoteric surfactant was used as a co-injectant to study the performance of the polymer in the presence of the surfactant, which could occur in a SP scheme. Dynamic Adsorption Two groups of dynamic adsorption tests were performed, including two tests for polymer adsorption and two tests for SP adsorption. The concentration of the polymer solution was 2,000 ppm. In the SP mixture, both surfactant and polymer concentrations were 2,000 ppm, making the total chemical concentration of 4,000 mg/L. Each injected chemical slug was 5 pore volumes (PVs) in size. The injection of the chemical slug was preceded by a seawater flooding and followed by post-seawater flooding. All tests were conducted at a constant flow rate of 0.5 cm3/min with a net confining pressure of 1,300 psi and pore pressure of 3,100 psi at 100 °C. The concentrations of the chemical collected in the effluents were analyzed to calculate the amount of chemical produced during the coreflooding test, which was then used to determine the amount of chemical adsorbed onto the rock surface. Titration and TOC methods were used for the concentration analysis. For the case of SP mixture injection, the titration and TOC analyses were performed on alternative effluent samples to determine the surfactant concentration and the total SP concentration, respectively. The amount of chemical lost in the core sample can be determined by subtracting the total chemical produced from the total chemical injected based on the mass balance. The as- sumption was that the chemical is uniformly adsorbed onto the rock surface when the amount of produced chemical is negligible at the end of post-seawater flooding. The chemical adsorption per unit rock weight was then calculated from the total amount of chemical loss during the coreflooding test and the dry weight of the core sample before it was saturated with the formation brine. The total mass of the injected chemical is the product of the total volume and the concentration of the injected chemical slug. The total mass of the produced chemical is the sum of the chemical mass in each collecting tube, which was similarly calculated as the product of volume and concentration in each tube. Two polymer injection tests were conducted. Figure 8 shows the effluent polymer concentration fraction and the ratio of the effluent polymer concentration (C) to the injected polymer concentration (Co) as a function of fluid injected. The plot starts from the beginning of the chemical slug injection and ends when effluent concentration is negligible. The dots in the figure are experimental data and the solid line is a smoothed curve. From the analyzed effluent polymer concentration and the total amount of injected polymer, the adsorptions of polymer on the rock surfaces were determined based on material balance, to be 0.121 and 0.133 mg/g-rock for the two tests, respectively. A mixture of surfactant and polymer was injected in two tests to investigate the competitive adsorption between polymer and surfactant. Figure 9 plots the effluent total chemical concentration fraction and the surfactant concentration fraction as functions of fluid injected for a test. Both concentration fractions were calculated based on the injected total chemical concentration of 4,000 ppm. The total SP adsorptions were 0.161 and 0.151 mg/g-rock for the two tests, respectively. The adsorptions of surfactant in these two tests were 0.0834 and 0.0872 mg/g-rock. The adsorptions of polymer were then SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 47 Fig. 10. Oil recovery curve of polymer flooding. Fig. 8. Profile of effluent polymer concentration. Fig. 11. Oil recovery curve of SP flooding. Fig. 9. Profiles of effluent polymer and surfactant concentrations. calculated by subtracting the surfactant adsorption from the total SP adsorption, which were determined to be 0.0776 and 0.0638 mg/g-rock for the two tests, respectively. Table 8 summarizes the results of all these four dynamic adsorption tests. Comparing the results of these two tests, it can be seen that the adsorption of polymer was evidently reduced when surfactant and polymer were co-injected. The total SP adsorption in the case of chemical co-injection was very close to the adsorption of polymer when only polymer was injected. Oil Recovery Potential Two plug samples were prepared for tertiary oil recovery tests by polymer flooding and SP flooding, respectively. Initial water saturation was established by centrifuge method using dead crude oil. The samples were then aged for four weeks before the start of the oil recovery tests. Waterflooding was conducted Test Num. Ambient Porosity (fraction) Ambient Air Perm. (md) Brine Perm. (md) Injected Chemical Total Adsorption (mg/g-rock) Surfactant Adsorption (mg/g-rock) Polymer Adsorption (mg/g-rock) 1 0.188 633 501 Polymer 0.121 N/A 0.121 2 0.168 513 441 Polymer 0.133 N/A 0.133 3 0.275 445 315 Mixture of Surfactant and Polymer 0.161 0.0834 0.0776 4 0.165 428 304 Mixture of Surfactant and Polymer 0.151 0.0872 0.0638 Table 8. Summary of dynamic adsorption results 48 It indicated that the adsorption sites of the rock surface were competitively occupied by the polymer and surfactant. WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY using seawater at the constant flow rate of 0.5 cm3/min, net confining pressure of 1,300 psi, pore pressure of 3,100 psi and a temperature of 100 °C. A chemical slug of 0.6 PV was injected when the waterflooding oil production was negligible, and then a post-waterflooding was followed. The cumulative oil recovery as a function of fluid injected for Test 5 has been plotted in Fig. 10. Waterflooding oil recovery was 61% original oil in place (OOIP). Then 0.6 PV of 3,000 ppm polymer solution was used in this test and the tertiary oil recovery reached 11% OOIP. Figure 11 presents the oil displacement coreflooding experiment results using a selected formulation composed of surfactant and polymer. Waterflooding oil recovery was about 72%, and tertiary oil recovery by surfactant and polymer was 18%. These results indicate that significant tertiary oil recovery can be achieved by the injection of a chemical slug composed of the selected SP combination. CONCLUSIONS 1. Eighteen different types of polymers were evaluated through a stringent sequential screening process to study the feasibility of polymer flooding or SP flooding for a representative Middle East carbonate reservoir. Three polymers among 18 candidates met the critical requirements of compatibility with brines, viscosity, long-term stability, and compatibility with the selected surfactant under hostile conditions. 2. A synthetic sulfonated polyacrylamide presented very low dynamic adsorption on the carbonates in the range of 0.15 mg/g-rock. When the polymer was co-injected with a selected amphoteric surfactant, the portion of the polymer adsorption was in the range of 0.06 to 0.08 mg/g-rock due to the competitive occupation of rock sites by polymer and surfactant. These phenomena indicate that the polymer can be successfully applied in carbonate reservoirs owing to the low adsorption. This allays a concern questioning if an anionic polymer could be used for carbonates with positive surface charge. 3. The oil displacement tests showed that an incremental oil recovery of 11% OOIP was achieved by polymer flooding using 3,000 ppm of the synthetic sulfonated polyacrylamide in tertiary recovery mode at reservoir conditions. For SP flooding, the incremental oil recovery reached 18% OOIP. These results indicate the great potential presented by incremental oil recovery via polymer-related chemical flooding. ACKNOWLEDGMENTS The authors would like to thank Saudi Aramco’s EXPEC Advanced Research Center for permission to publish this article. The authors are grateful to the Chemical EOR team members for their continued support and involvement in this study. This article was presented at the SPE EOR Conference at Oil and Gas West Asia, Muscat, Oman, March 31 - April 2, 2014. REFERENCES 1. 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Olarewaju, J., Ghori, S., Fuseni, A.B. and Wajid, M.: “Stochastic Simulation of Fracture Density for Permeability Field Estimation,” SPE paper 37692, presented at the Middle East Oil Show and Conference, Manama, Bahrain, March 15-18, 1997. 23. Malinowski, R.: “Water Injection, Arab-D Member, Abqaiq Field, Saudi Arabia,” SPE paper 85, presented at the SPE Middle East Regional Meeting, Dhahran, Saudi Arabia, March 27-29, 1961. 24. Rahman, M., Sunbul, M.B. and McGuire, M.D.: “Case Study: Performance of a Complex Carbonate Reservoir Under Peripheral Water Injection,” SPE paper 21370, presented at the Middle East Oil Show, Manama, Bahrain, November 16-19, 1991. 25. Kiani, M., Kazemi, H., Ozkan, E. and Wu, Y-S.: “Pilot Testing Issues of Chemical EOR in Large Fractured Carbonate Reservoirs,” SPE paper 146840, presented at the SPE Annual Technical Conference and Exhibition, Denver, Colorado, October 30 - November 2, 2011. 26. Pham, T.R. and Al-Shahri, A.M.: “Assessment of Residual Oil Saturation in a Large Carbonate Reservoir,” SPE paper 68069, presented at the SPE Middle East Oil Show, Manama, Bahrain, March 17-20, 2001. BIOGRAPHIES Dr. Ming Han works in Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC) as a Petroleum Engineering Specialist in chemical enhanced oil recovery. Before joining Saudi Aramco in 2007, he Offshore Oil Corporation worked for China National N (CNOOC), where he was Lead Engineer in Oil Field Chemistry at the CNOOC Research Center working to implement an offshore polymer flooding project. For more than 10 years of his career, Ming worked for the Research Institute of Petroleum Exploration and Development (RIPED) in China as a Research Engineer, conducting laboratory studies and field pilots in water shutoff, profile modification, polymer flooding and chemical flooding. He also served Hycal Energy Research in Canada as a Research Engineer. In 1982, Ming received his B.S. degree in Chemistry from Jilin University, Changchun, China. He received his M.S. degree from the University of Paris VI, Paris, France, and his Ph.D. degree from the University of Rouen, MontSaint-Aignan, France. Ming is a member of the Society of Petroleum Engineers (SPE) and the American Chemical Society (ACS). Alhasan B. Fuseni joined Saudi Aramco in 2006 and is a member of the Chemical Enhanced Oil Recovery (EOR) team of the Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC). Prior to joining Saudi Aramco, he worked for the King Fahd University of Petroleum and K Minerals (KFUPM) Research Institute as a Research Engineer, and for Hycal Energy Research, Calgary, Canada, as an EOR Technologist. Alhasan has taught an in-house course on core flooding applications in chemical EOR at EXPEC ARC, and he teaches the chemical EOR section of the course on EOR at Saudi Aramco’s Upstream Professional Development Center. He has authored and coauthored several papers in petroleum engineering and is currently serving as a reviewer for Elsevier’s Journal of Petroleum Science and Engineering. Alhasan received both his B.S. and M.S. degrees in Petroleum Engineering from KFUPM, Dhahran, Saudi Arabia, in 1985 and 1987, respectively. Badr H. Zahrani works in Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC) as a Senior Laboratory Technician in chemical enhanced oil recovery (EOR). He joined Saudi Aramco in 2006 as a trainee, and he went on to work as an i d then h in i 2008 2 Operator in the Safaniya Offshore Producing Department. In 2009, Badr was transferred to EXPEC ARC. His expertise is in the evaluation of EOR chemicals, and he has been involved in many research and service projects. In 2008, Badr finished his training in the Industrial Training Center (ITC) in Ras Tanura, Saudi Arabia. Badr is a member of the Society of Petroleum Engineers (SPE). Dr. Jinxun Wang works at Saudi Aramco’s Exploration and Petroleum Engineering Center – Advanced Research Center (EXPEC ARC) as a Petroleum Engineer in the chemical enhanced oil recovery focus area of the Reservoir Engineering Technology Division. Saudi Aramco, he worked with Division Before joining join Core Laboratories Canada Ltd. as a Project Engineer in their Advanced Rock Properties group. Jinxun’s experience also includes 10 years of research and teaching reservoir engineering at petroleum universities in China. Jinxun received his B.S. degree from the China University of Petroleum, his M.S. degree from the Southwest Petroleum Institute, China, and his Ph.D. degree from the Research Institute of Petroleum Exploration and Development, Beijing, China, all in Petroleum Engineering. He received a second Ph.D. degree in Chemical Engineering from the University of Calgary, Calgary, Alberta, Canada. Jinxun is a member of the Society of Petroleum Engineers (SPE) and the Society of Core Analysts (SCA). SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 51 Sweet Spot Identification and Optimum Well Planning: An Integrated Workflow to Improve the Sweep in a Sector of a Giant Carbonate Mature Oil Reservoir Authors: Dr. Ahmed H. Alhuthali, Abdullah I. Al-Sada, Abdullah A. Al-Safi and Mohammed T. Bouaouaja ABSTRACT This study illustrates a comprehensive integrated approach to identifying the potential locations for future development in one sector of a giant carbonate mature oil reservoir. The approach uses various data from several sources, including reservoir surveillance, production performance, geological interpretation and numerical simulation data, and cohesively combines them to yield an informed decision when assessing field development and management. The study area has been under peripheral waterflood for more than 50 years and is dominated by heterogeneity related to fracture corridors, a high permeability zone and reservoir zonation. These features have led to a preferential and uneven propagation of water flow, which results in unswept oil bearing spots after production using the existing well’s layout and configuration. The reservoir management team has developed an integrated workflow to address these challenges by using several reservoir engineering methods and models, including water encroachment, reservoir opportunity index (ROI), fractional flow calculation, remaining volumetric and water flow paths. The designed workflow consists of first creating derived attributes that describe these models and then filtering the sector area using those attributes to define the sweet spots. The selection and prioritization of the defined sweet spots are subsequently supported by available reservoir surveillance and production data. The scarcity of reservoir surveillance and production data in some areas of the sector motivated the reservoir management team to stretch the limits by capitalizing on logs from the gas wells penetrating the shallower oil reservoirs. The open hole logs of these wells recorded a thicker oil column than the column pre-estimated using the existing surveillance data. As a result of these efforts, a development plan has been designed to ensure reserves depletion in the identified sweet spots by drilling new wells or sidetracking existing wells. Despite the reservoir’s level of maturity, simulation forecasts indicate that the area of interest has a lot of potential to sustain a high production rate. INTRODUCTION The area of interest is located in the central part of a carbonate 52 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY oil field in Saudi Arabia. The subject reservoir has been penetrated by hundreds of wells, both vertical and horizontal, providing an excellent dataset for geologic characterization. The reservoir thickness is 350 ft of carbonate unit with an upper section dominated by grainstones and packstones, and a lower section consisting of wackestones and mudstones. Porosity and permeability increase toward the top of the unit, where the porosity range is between 22% and 28%. Permeability is excellent and can reach several Darcies in the so-called Super-K layers. The permeability is enhanced by the presence of very conductive fractures identified through different characterization tools. The area of interest is a mature area that has been producing under peripheral waterflood for many decades. The main objective of this study was to define the sweet spots in this sector and to study the possibility of further drilling opportunities in these spots. Optimization of the well’s layout followed to ensure the optimum sweep efficiency and to maximize recovery. MOTIVATION The study was motivated by the need to carefully assess the sweep efficiency between the injection line and the central producing area. The routine monitoring and surveillance data shows an excellent sweep in the bulk area; however, several facts support the existence of some delimited areas with concealed potential. This hypothesis is supported by the findings from logging the subject reservoir in a well, Well-A, that is targeting another deeper gas reservoir. Therefore, the dry oil column interpreted is higher than the pre-assumed oil column. Figure 1 illustrates the location of Well-A on a net oil column and the actual well log. An interesting result was obtained from the logs of another well, Well-B; a dead well shut-in for 9 years that was presumed to be in a swept zone based on previous surveillance results. Subsequently, a saturation log recently indicated an oil column of about 35 ft. Accordingly, the well was put onstream, flowing 2,000 stock tank barrels per day (stb/d), and it has been sustaining a stable plateau for more than one year. Fig. 1. Well-A and Well-B logs showing thicker oil column than the interpreted data in the map. (ROI), well spacing, fractures, water cut map, producing oil thickness (oil bearing thickness), cumulative water flow map and cumulative fractional flow map. Cutoff values were selected for each attribute and were integrated to define the vertical and areal continuity of the expected sweet spots. Obviously, some of these attributes may represent the same value of information, so some of them were considered as primary selection criteria and others were considered as supporting selection criteria. Once an area of interest was defined, it went through additional assessments that included examining the volumetric balances and the offset well’s performance. After encouraging results came from this assessment, the area was classified as a sweet spot with an associated opportunity for development or for additional evaluation. Finally, the development scenarios were assessed through numerical simulation for performance forecasting. Figure 2 gives an outline of the adopted methodology, which will be detailed in the following paragraphs. CHALLENGES DATA GATHERING AND PROCESSING The waterflood performance in the sector of interest is influenced by reservoir heterogeneity and the presence of a number of features in the area1, 2. Aspects like fractures and Super-K distribution are expected to have an impact on the sweep, which increases the challenge level for efficient reservoir management3. Additional challenges are related to the reservoir’s level of maturity; all the wells are cutting water, and the flow profiles recorded through the production logging tools (PLTs) show a gradual decrease in the net oil column. As would be expected in such a situation, surveillance measurements are focused on the front tracking, which adds an additional difficulty to efforts to identify the spots trapped between the fracture corridor and preferential paths or behind the general front4. Given the objectives and the study deliverables, different corporate databases and previous in-house studies were consulted to collect the following data: • Reservoir description and surveillance data, including initial well logs, production logs and reservoir saturation logs. • Most recent history matched full field reservoir simulation model and the original geological model with fracture distribution — the simulation model is a dual porosity/dual permeability model with an areal gridding of 250 m and a very detailed vertical subdivision of 45 layers5. • The well’s setup data, including operating status, orientation, deviation, and surface and subsurface locations. • Reservoir pressure, production and injection data at field and well levels. METHODOLOGY AND WORKFLOW To fulfill the objective of the project, which was to identify the sweet spots, the reservoir management team has developed a comprehensive workflow to integrate the available data, using an organized, information value-based method, under a unified platform. Numerous data from various sources were utilized to conduct the study, including data from previous studies and routine reservoir surveillance as well as from simulation models. A substantial effort has been dedicated to collecting all these data and capturing them in a format that is readable by the platform being used. A number of attributes were defined to extract the appropriate value from the different data. Some of them are basic, such as the water saturation, and others are advanced, like the water flow map. In total, 10 attributes were defined: net dry oil map, isobaric map, water saturation, reservoir opportunity index Fig. 2. Project workflow. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 53 Several queries were used to extract the relevant raw data from different sources. The raw data was then converted into a format readable by the unified platform that was used to integrate the data. • Water saturation model derived as a direct result from the calibrated 3D simulation model. • ROI computed by combining three indexes, reservoir quality index (RQI), mobile oil saturation (Som) index and pressure index7, in the following calculation: ATTRIBUTES DEFINITION AND CALCULATION This study established several reservoir engineering attributes as major elements in the sweet spot identification workflow. These attributes are directly or indirectly derived from water encroachment models, fractures networks, ROI, fractional flow calculations and numerical simulation results. The attributes can be categorized according to the originating source, Fig. 3. The following mapping and property calculation techniques were used to generate these attributes: • Isobaric map generated by the latest pressure survey data from key wells covering the area. • Net dry oil column generated by estimating the current water level in each well, and subsequently the remaining oil thickness, from production and saturation logging tools. • Water cut map generated by mapping the trend of the current water cut distribution in the area. • Oil bearing column map generated by mapping the oil producing thickness identified as the lowest oil producing level. • Fractures and a well spacing map generated from existing well data, Fig. 4, and built to identify areas to be avoided, either because they are occupied by an existing well or because they are on a fracture pathway6. Fig. 3. Attributes categorization. Fig. 4. Well spacing and fractures distribution in a part of the sector. 54 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY where P is reservoir pressure index RQI is reservoir quality index: and SOMPV is oil saturated pore volume index: SOMPV = SO × PV. • Cumulative water flow map generated by computing cumulative water flow through each grid block in the 3D simulation model, after which the 3D model is converted to a 2D model by summing up the cumulative water flow for each grid vertically; this provides useful information about the preferential water paths through the entire history. • Cumulative fractional flow map generated from the 3D simulation model by computing the phase’s flow contribution for each grid block; this map is also compared to the fractional flow calculated from the relative permeability tables for each reservoir unit. SELECTION CRITERIA Once they were generated, the above mentioned attributes were submitted to a selection process to identify reasonable cutoffs and ranges to define any favorable spot/location for future development. Some attributes, such as the isobaric map, net oil column map and oil bearing map, were used for quality checking and providing general trends of the sweep. They were used at the end of the project as extra filtering criteria to prioritize the selection of the sweet spots. As these maps generally show bottom-up sweep with good pressure maintenance all over the sector and cannot be used to identify opportunities, they are not included as the main selection criteria. For the attributes used for the main selection process, the cutoff value for each attribute was set as follows: • Unfilled spaces and fractures distribution: Based on the current spacing in the reservoir sector, a cutoff of 500 m around each existing well and 250 m around the high confidence fractures was used to identify space to be avoided. • Water saturation: A cutoff value of 50% was selected after it was correlated and cross-checked with the two other conjugate attributes; the water cut map and the cumulative fractional flow map. Through the different evaluations, it was determined that 50% water saturation will allow a reasonable oil flow, and through this analysis, that the water cut in such locations will not exceed 60%. Figure 5 illustrates the attributes of water saturation, cumulative Fig. 5. Attributes of water saturation, cumulative fractional flow map and water cut map, respectively. fractional flow map and water cut map. • ROI: An empirical selection of 25% as the cutoff ensuring the best reservoir opportunity was made, corresponding to a cutoff of 0.18, Fig. 6. • Cumulative water flow map: A cutoff of 100,000 stb/d was set to identify the zones where the cumulative water flow passing through drops below that rate so the zones can be avoided when selecting the sweet spots, Fig. 7. Although the water saturation is included in the calculation of ROI, it was kept as an independent attribute to provide an additional control for the selection process, since other parameters in the ROI, such as permeability and porosity, may have a balancing effect and dilute the water saturation effect7. It is also important to note that a redundancy appears to exist by including both the water saturation and the water flow map; nevertheless, each of the two parameters provides different information. The water flow map is an additive value — summation through all layers of all water quantities passing a particular grid block — whereas the water saturation cannot be summed to give a holistic idea about the state of saturation in a particular location. Water saturation can only be averaged and this will flatten any resultant map. attribute in Fig. 8 and defined as an area of interest (AOI). The various attribute’s AOIs were then integrated into one map to generate a master combined AOI covering the reservoir sector. This AOI presents a certain areal and vertical discontinuity, in that some areas are of infinitesimal size and so do not justify classification as a realistic opportunity. A numerical cleaning therefore was conducted to discard these zones. A total of 10 ft of continuous vertical hydrocarbon thickness and 0.25 km2 of areal connected volumes (4 grid blocks) were used as lower limits for an area to be retained as an opportunity, Fig. 9. As a DEFINING AREA OF INTEREST The previously mentioned criteria and cutoffs were applied across the study area to yield the green spots highlighted for each Fig. 7. Cumulative water flow map in a part of the sector. Fig. 6. Reservoir opportunity index distribution. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 55 for future development. Wells situated in a polygon at a distance of 1 km from the spot’s border were considered for this review. Production, surveillance and well layout data were used to build evaluation cards for each spot, summarizing the review and the engineering verdict for the offset wells, Fig. 10. Fig. 8. Retained AOI from each attribute after applying the cutoff in a part of the sector. SWEET SPOTS VOLUMETRIC EVALUATION Once the risk associated with each spot was defined, a ranking was made based on the assessed volumes. The remaining oil volume contained in each polygon spot was calculated from the simulation model prognosis. This volume was compared to the spot’s initial oil in place (OIP) to extract the current recovery factor. Table 1 presents a summary of the 40 spots’ volumetric results; the spots are classified from the highest remaining OIP. The current recovery factor reflects the state of reserves depletion in each spot. Therefore, though there are no wells in the spot’s polygon, the contained reserves may be Fig. 9. Examples of removed areas with no practical opportunity value and the retained spots. result of all of these screening methods, 40 spots were finally identified. OFFSET WELLS REVIEW To align the findings of the previous steps with an actual neighboring well’s performance, further filtering was applied to the defined 40 spots using the available well history, reservoir surveillance and production data. The spots then were given a risk factor based on an engineering judgment of these data and identified as high risk, low risk and acceptable risk Fig. 10. Example of spot 15’s evaluation card. Spot Spot Evaluation Initial Volumes (STOIP MMSTB) Reaming Volumes (STIOP MMSTB) Jan 2014 Produced Volumes (MMSTB) Current RF % Remaining Receivable Reserves (MMSTB) 1 15 Low Risk xxxx xxxx xxxx xxxx xxxx 2 17 Med Risk xxxx xxxx xxxx xxxx xxxx 3 31 Low Risk xxxx xxxx xxxx xxxx xxxx 4 16 Low Risk xxxx xxxx xxxx 13.6 xxxx 5 23 Low Risk xxxx xxxx xxxx 3.9 xxxx 37 40 Med Risk xxxx xxxx xxxx xxxx xxxx 38 35 Med Risk xxxx xxxx xxxx 43.6 xxxx 39 14 Low Risk xxxx xxxx xxxx xxxx xxxx 40 1 High Risk xxxx xxxx xxxx 45 xxxx Rank Table 1. Summary of the volumetric evaluation of different sweet spots 56 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY draining indirectly from the reservoir through the offset wells. It is worth noting that the current recovery factor, remaining oil and current saturation, though correlated, do not bring the same information value. The oil saturation is certainly an indication of the sweep status, but it is categorized by grid blocks. Looking for an average saturation — with all the associated risk of losing all the singularities — will not give the same exactitude as a recovery factor figure. SWEET SPOTS DEVELOPMENT AND WELL PLANNING The volumetric evaluation shown in Table 1 summarizes the current status of the spots and presents a basis for the development planning for these areas. The logical approach is to look to the different parameters together to decide if the spot is suitable for development through drilling new wells and sidetracking existing wells, or if it is more effective to conduct a further evaluation of the region. It was decided to discard the high risk spots from the current development, keeping them for further evaluation through reservoir surveillance or monitoring. The spots with low and medium risk were evaluated in terms of oil currently in place, i.e., whether there was a substantial amount of remaining oil; each spot was then evaluated in terms of recovery factor. The current recovery factor indicates if the offset existing wells are able to drain those reserves or if additional wells are needed to directly target those reserves. As it happens (Table 1, example spot #14), a spot containing a huge amount of OIP currently presents a high recovery factor. This indicates that there is no need to add additional wells, leaving only a sidetrack of those wells showing low performance to be considered. The process schematic is described in Fig. 11. Drilling new horizontal laterals in the retained potential areas was chosen as the main production development method, by either new drilling or reentry drilling from offset vertical wells. Later surveillance recommendations based on data from PLTs and reservoir saturation logs will be provided to better assess the discarded areas. Each of the individual spots will then receive a final specific recommendation with the specific name of the well: • New well(s) for development. Fig. 11. Procedure for designating level of development for the sweet spots. • Sidetrack of existing specific well. • Conduct production logging or saturation log in the specific well(s). Well planning is optimized by defining the trajectory of the horizontal section3. The lateral is typically placed in the best layer in the top of the reservoir, Fig. 12. SIMULATION PREDICTION AND FINAL WELL LAYOUT A total of 32 laterals were designed and nine new wells and 23 reentries from existing inactive or marginal producers are illustrated in Fig. 13. The reservoir contacts of these wells were optimized, with placement between 1,000 ft and 5,000 ft near the reservoir top, considering the current well’s spacing. To better capitalize on the designed wells, the proposed well’s production performances, production targets plateau and cumulative produced volumes were assessed through simulation prediction. The prediction confirmed the added value Fig. 12. Example of well sidetrack design. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 57 Fig. 13. Final proposed well development layout in a part of the sector. of the majority of the wells (28 out of 32) and provided a basis to include these wells in the field business plan for the upcoming years. Figure 14 illustrates the proposed development of spot #23 as an example. CONCLUSIONS This study presents a comprehensive workflow with clear logical processes to seize the advantage of available reservoir data to identify future developments in a mature area of a giant field. The data is integrated through an information valuebased method that provides relevant attributes with which to conduct the study. In this study, 10 attributes were calculated to describe reservoir characteristics in terms of saturation, reservoir quality, fluid flows, and production and surveillance data. Cutoffs are applied to the defined attributes through a well-established selection process to delineate the areas of interest. Areas compliant with the selection criteria are then Fig. 14. Spot 23 development example. 58 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY submitted to additional evaluations, which integrate the offset well’s performance and surveillance data to further distinguish the sweet spots. After a study concludes that development opportunities are not limited to in-fill drilling in the mature crestal area, but that potential spots also exist elsewhere, risk profiles are assigned to each spot based on volumetrics and the ability of the offset well to drain the reserves in the spot. A risk and reward evaluation finally leads to the design of the best scenario for developing these spots or to the need for additional evaluation requirements. These recommendations will serve to feed the field development plan for the upcoming years. ACKNOWLEDGMENTS The authors would like to thank the management of Saudi Aramco for their support and permission to publish this article. The authors also want to acknowledge the contributions of Soha Hayek, Lajos Benedek, Sikandar Gilani and Saad Mutairi for reviewing the article and Nayif Jama for assisting with the required simulation runs. This article was presented at the SPE-SAS Annual Technical Symposium and Exhibition, al-Khobar, Saudi Arabia, April 2124, 2014. REFERENCES 1. Alhuthali, A.H., Al-Awami, H.H., Soremi, A. and AlTowailib, A.I.: “Water Management in North ‘Ain Dar, Saudi Arabia,” SPE paper 93439, presented at the SPE Middle East Oil and Gas Show and Conference, Bahrain, March 12-15, 2005. 2. Alhuthali, A.H.: “Optimal Waterflood Management under Geologic Uncertainty Using Rate Control: Theory and Field Applications,” SPE paper 129511, presented at the SPE Annual Technical Conference and Exhibition, New Orleans, Louisiana, October 4-7, 2009. 3. Yuen, B.B.W., Rashid, O.M., Al-Shammari, M., Al-Ajmi, F.A., Pham, T.R., Rabah, M., et al.: “Optimizing Development Well Placements within Geological Uncertainty Utilizing Sector Models,” SPE paper 148017, presented at the SPE Reservoir Characterization and Simulation Conference and Exhibition, Abu Dhabi, UAE, October 9-11, 2011. 4. Pham, T.R., Al-Otaibi, U.F., Al-Ali, Z.A., Lawrence, P. and van Lingen, P.: “Logistic Approach in Using an Array of Reservoir Simulation and Probabilistic Models in Developing a Giant Oil Reservoir with Super-Permeability and Natural Fractures,” SPE paper 77566, presented at the SPE Annual Technical Conference and Exhibition, San Antonio, Texas, September 29 - October 2, 2002. 5. Alzankawi, O.M., Al-Houti, R.A., Ma, E., Ali, F.A., Alessandroni, M. and Alvis, M.: “Mauddud Fractured Reservoir Analysis, Greater Burgan Field: Integrated Fracture Characterization Using Static and Dynamic Data,” IPTC paper 17471, presented at the International Petroleum Technology Conference, Doha, Qatar, January 19-22, 2014. 6. Abd-Karim, M.G. and Abd-Raub, M.R.B.: “Optimizing Development Strategy and Maximizing Field Economic Recovery through Simulation Opportunity Index,” SPE paper 148103, presented at the SPE Reservoir Characterization and Simulation Conference and Exhibition, Abu Dhabi, UAE, October 9-11, 2011. 7. Stabell, F.B., Stabell, C.B. and Martinelli, G.: “Effective Assessment of Resource Plays: Handling Transition Zones,” SPE paper 167724, presented at the SPE/EAGE European Unconventional Resources Conference and Exhibition, Vienna, Austria, February 25-27, 2014. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 59 BIOGRAPHIES Dr. Ahmed H. Alhuthali is a Division Head in Saudi Aramco’s Southern Area Reservoir Management Department, overseeing the reservoir engineering and operational issues of the ‘Uthmaniyah area — the largest in the giant Ghawar field. Prior to this assignment, i t he h held h ld reservoir management and production engineering positions in different areas of Ghawar and Abqaiq fields. Ahmed has been with Saudi Aramco for 16 years. He is interested in integrated reservoir management with an emphasis on waterflooding principles, closed loop optimization, well performance and probabilistic decision analysis. Ahmed is also interested in energy economics, especially in the oil and gas sector. He received his B.S. degree in Electrical Engineering from King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia, in 1998 and an M.S. degree in Petroleum Engineering from Texas A&M University, College Station, TX, in 2003. Ahmed received his Ph.D. degree in Petroleum Engineering from Texas A&M University, College Station, TX. He also earned a business certificate from Mays Business School at Texas A&M University in May 2008. Abdullah I. Al-Sada joined Saudi Aramco in 2012 as a Reservoir Engineer working in the Southern Area Reservoir Management Department. He is currently working in the ‘Udhailiyah Reservoir Management Division involved in the reservoir engineering and operational issues of the ‘Uthmaniyah area oper — the largest in the giant Ghawar field. Abdullah’s interests include the reservoir management of mature fields and maximizing the efficiency of secondary recovery methods with respect to the asset’s heterogeneity. In 2012, he received his B.Eng. degree in Petroleum Engineering from King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia. 60 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Mohamed T. Bouaouaja joined Saudi Aramco in March 2013 as a Petroleum Engineer working in the Southern Area Reservoir Management Department. He started his career in Tunisia where he worked for the national oil company ETAP as a Reservoir Engineer, involved E i i l d in i reservoir management for both carbonate and clastic reservoirs. In 2007, Mohamed joined Schlumberger and worked in various assignments in consultancy, simulation, training and project management with an international exposure and a focus on the Arabian Gulf countries. He has published several technical reports, studies and Society of Petroleum Engineer (SPE) papers. In 2001, Mohamed received his B.S. degree in Civil Engineering Hydraulics from Ecole Nationale d’ingenieurs de Tunis (ENIT), Tunis, Tunisia. Abdullah A. Al-Safi joined Saudi Aramco in 1986 as a Petroleum Engineer. During his career, he has worked in several different production fields and in various jobs, including as a Drilling Engineer and a Production Engineer. Abdullah currently works as a Petroleum Engineer Enginee Specialist in the Southern Area Reservoir Management Department. He has coauthored several Society of Petroleum Engineers (SPE) papers. In 1986, Abdullah received his B.S. degree in Petroleum Engineering from King Saud University, Riyadh, Saudi Arabia. Innovation in Approach and Downhole Equipment Design Presents New Capabilities for Multistage Stimulation Technology Authors: Mohammed A. Al-Ghazal, Saad M. Al-Driweesh, Mustafa R. Al-Zaid and Fadel A. Al-Ghurairi ABSTRACT To date, multistage stimulation (MSS) technologies have been run in almost every type of complex hydrocarbon-bearing rock, from the much heralded shale plays in North America to the massive heterogeneous carbonate formations exhibiting a dual porosity/dual permeability system in Saudi Arabia. These technologies have also been used in offshore wells in the North Sea, Black Sea and West Africa. The main MSS market was and still is in North America, in the tight unconventional shale plays; however, in recent years, the international market (outside of North America) has been steadily catching up. One of the main leaders associated with this increase has been Saudi Aramco in its Southern Area gas fields. MSS has often been viewed as simply running a completion string followed by pumping services; however, the early attempts at uncemented open hole MSS completions in Saudi Arabia were met with mixed operational success. It became clear that the standard completion approach and stimulation procedures could not be directly applied there. A new set of best practices would be required in these Middle East wells, one that included an integrated multidisciplinary approach that took a step backwards in the process — to the pre-drilling phase — and focused on well planning optimization to maximize the multistage completion technique and ultimately the well productivity. The wide range of reservoir types required engineering of the MSS completion to enable placement of a variety of matrix and fracturing stimulation techniques, further complicated by the constraints associated with operating in environments ranging from land and/or the desert to offshore areas. These completion options have included low-tier sand plugs, more sophisticated bridge and frac plugs, and high-end, open hole, uncemented liners with packers and sleeves. For Middle East wells, it is clear that “one MSS completion technique does not fit all.” This article will discuss many of these MSS solutions and highlight some of the debate over the merits of the various MSS completion designs and options — such as the preferences in isolation methods and options for connecting the wellbore to the reservoir — as deployed in the Southern Area tight gas fields of Saudi Arabia. Regardless of which MSS technology is applied, further emphasis is being placed on the integration of the completion and the stimulation treatment from the initial design of the well, to optimize reservoir contact and maximize the return on investment. Testing and field applications of newly proposed, developed and implemented MSS solutions are also presented, including an innovative packer seal technique, an engineered approach for optimal performance of fracturing sleeves, nonstandard ball increment spacing sizes, curved ball seats and a segmented body for full bore mill-out. INTRODUCTION For over a decade, multistage stimulation (MSS) has been a well-established technique in North America and is also in a period of rapid growth in many regions in the Middle East. Globally, operators have applied a multitude of MSS completion options to wells in many varying reservoirs, from conventional reservoirs, to tight gas/tight oil basins, to carbonate and clastic formations, to more unconventional shale and coalbed methane reservoirs1-12. A huge amount of information, best practices and techniques has been leveraged from the North American MSS experiences; however, as experience within the Middle East environment developed, differences among the MSS techniques and processes became clear. Certainly as a starting point, the differences logistically between the North American market and the international market are immediately evident; where tens of stages (30, 40, 50 stages and more) are deployed and fracture stimulated over the space of days in North America, stimulating the same number of stages would take weeks in many international locations. Therefore, the international stage count is significantly less and typically in open hole uncemented applications. For example, outside of North America, a maximum of 10 stages can be deployed, with an average of 4 to 5 stages, in a single lateral well. For that reason, a great deal of focus is placed on efficiency in North America, where internationally, and in the Middle East in particular, the majority of the focus is on effectiveness. For example, in Saudi Arabia, if five stages are deployed, a full five stages should be fracture stimulated to the fullest to be seen as contributing individually to their maximum potential. With that said, judging from the previously installed open hole, uncemented, lower completion systems (of which there SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 61 are approximately 80 in total) in the Saudi Arabia area, the equation of “number of stages deployed” being equal to “number of stages stimulated” is yet to be satisfactorily realized. One of the main issues is related to the difference between utilizing open hole MSS systems in a carbonate formation, where acid fracturing treatments are applied, and utilizing them in a shale formation, where proppant fracturing takes place. The concerns when using a MSS system in an acid fracturing environment are the zonal isolation between stages and ultimately the packer isolation technique selected. A typical hydraulic-set mechanical packer uses one or two seal elements that are approximately 8” to 10” in length while being deployed, and then when the packer is hydraulically set, a piston force is applied to the solid rubber element, which is forced outwards, expanding in outside diameter while contracting in overall length. That means the more the packer’s outside diameter expands, the less the contact seal length pressed to the open hole formation face becomes. This of course is assuming a perfect “gun barrel” open hole circumference where a mechanical packer can be set uniformly to the formation face. The worst case scenario is when ovality from washouts and breakouts is present. The mechanical packer attempts to conform to the open hole circumference; however, on occasions where ovality is present, the potential exists for a micro-annulus space to occur between the packer seal and the formation face, Figs. 1 and 2. Now, in standard shale/sandstone MSS applications, where proppant rather than acid is pumped, this micro-annulus leak path can easily pack off with proppant in what becomes a self-healing process, and the isolation between stages is restored, Figs. 3 and 4. Given the nature of the acid fracturing treatment in a carbonate formation, however, this leak process is not self-healing, and the phenomenon of acid working its way through the micro-annulus and dissolving away the rock around the packer seal can be very problematic. There is a clear need therefore, for an optimized packer seal technique in MSS acid fracturing applications in carbonate formations. Figs. 1 and 2. An acid fracturing case in a carbonate formation showing a slight washout at the upper side of the lateral where the acid dissolving away some of the formation around the seal causes communication between stages. Figs. 3 and 4. A proppant fracturing case in a shale/sandstone application showing a slight washout at the upper side of the lateral where packing off around the seal ensures zonal isolation is achieved. 62 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY PROPOSED MSS SOLUTION Development and qualification of a fit-for-purpose multistage swellable element was required for use in the environment of the southern gas fields in Saudi Arabia, a packer that could withstand harsh conditions in terms of bottom-hole temperatures and pressures as well as the acid fracturing application needed by the carbonate formations, Figs. 5 and 6. Previous attempts had been made to use more conventional standard swellable packers, adapted from water shutoff or inflow control device type applications. The challenge was always fulfilling the differential pressure requirements of the fracturing treatment, and the conventional method was to use standard application rubber materials and simply increase the length of the swellable elastomer. This resulted in the adoption of packer lengths of 32 ft or more to meet the high differential pressure requirements of the multistage treatments. The positive outcome was a longer seal length, and therefore, a reduced possibility of the acid dissolving the rock formation around the seal — as highlighted earlier, that is a major concern for the acid fracturing application. The negative outcome, on the other hand, was always the impact of the longer seal length of the swellable packer on deployment during the installation process. For example, with several long swellable packers being deployed in a single lower completion string, reaching target depth became a significant concern. A great deal of time and effort will be spent in determining the optimum stage lengths and open hole packer positions prior to running the MSS equipment, but when the lower completion becomes mechanically stuck and ultimately set off depth, all this effort becomes wasted and the production results are ultimately never fulfilled. The challenge of deploying MSS systems to target depth is not new in Saudi Arabia, and even with hydraulic-set mechanical packers, the initial MSS systems saw installations prematurely set several hundred feet off depth. The preferred configuration for running the MSS system involved having every fracturing sleeve placed between two open hole packers, resulting in what is known as a “balanced system,”13 where the fracturing forces are balanced between pressurized stages. The consequence of having a balanced system installation set prematurely was that the toe of the well was isolated by the lowermost open hole packer and therefore was unable to be stimulated. From that point, an open hole anchor packer would be run in an “unbalanced” multistage configuration, meaning the first toe stage was unbalanced by having a fracturing port placed below the lowermost open hole packer. Therefore, if the MSS completion system was set prematurely Figs. 5 and 6. The newly designed swellable element must achieve positive isolation in carbonate formations with acid fracturing applications (left image), as well as in sandstone/shale proppant fracturing cases (right image). off depth, then there was still the possibility of stimulating the toe section of the well, albeit if it was a very long section. The upward forces placed on the bottom of the lowermost packer, however, would be very large, as per the term unbalanced, and sliding of that packer would be likely. So the idea of deploying an open hole anchor packer became of interest, with the intent of anchoring the bottom of the completion string and resisting the movement caused by the large upward piston forces placed on that lower open hole packer. This unbalanced configuration worked well in shale type applications. Consequently, in carbonate formations, on occasion during the acid fracturing treatments of the first stage, as solution was pumped through the hydraulic frac sleeve, significant and instantaneous pressure drops were noted, and it was believed that the acid treatment had dissolved away the carbonate rock around the slips, and therefore the anchor had released, creating an immediate upward movement of the lowermost open hole packer. Once the deployment issues were rectified and completions no longer became stuck14, 15, the standard practice of running balanced configurations resumed and the open hole anchor packer become redundant. The proposed open hole solutions that followed did not require open hole anchor packers in the lower completion string. A second challenge was related to the fracturing port configuration. On occasion the integrity of the ball and ball seat interface came into question. For example, during treatments where instantaneous pressure drops of several thousand psi or more were seen in the middle of the acid fracturing process — typically this was interpreted as a mechanical failure — the cause was loss of integrity between the ball and ball seat interface. Therefore, a more robust fracturing sleeve that incorporated a newly designed ball seat was tested and qualified. Yet a coiled tubing (CT) mill-out of the ball seats in the multistage completions can be required in some cases16, 17. The results of previous CT mill-outs have been widely varied, and even if the practice of CT milling has been significantly improved in terms of bottom-hole assemblies (BHAs), mills and motors, as well as milling procedures, failures still occur. Therefore, the new, more robust ball seat was also required — from the opposite side — to be easily millable. NEWLY DEVELOPED AND FIT-FOR-PURPOSE SWELLABLE PACKERS FOR MULTISTAGE ACID FRACTURING APPLICATIONS The development that followed resulted in a multistage swellable packer (MSwP) isolation system designed to achieve open hole and cased hole isolation in many varied applications, from well construction to well completion. The swellable element is specially designed for the typically higher pressure ratings associated with a multistage fracturing job, Fig. 7. The swellable packer is engineered from a complex polymer that has properties similar to those of rubber before swelling. Fig. 7. Newly developed fit-for-purpose swell packer for multistage fracturing applications. The mechanism of the oil swell technology is to use the thermodynamic diffusion of hydrocarbons into the polymer network to cause stretching and volumetric expansion of the packer. The MSwP system, which employs bonded-to-pipe swellable packers, integrates a patented, double brass fold back shoe design to act as an anti-extrusion device, ensuring better pressure and temperature ratings and reliability. The MSwP assembly also has a built-in swelling delay mechanism that allows thermodynamic absorption to start immediately after installation. This delay, achieved without any external coatings, reduces premature swelling risks while the assembly is being run in the hole. Because of the MSwP assembly’s advanced polymer construction and its anti-extrusion device design, its differential pressure capabilities are suitable for high fracturing pressures — an indispensable criterion for a fracturing packer if isolation is required. MSWP BONDED-TO-PIPE SWELLABLE PACKERS WITH FOLD BACK SHOE TECHNOLOGY Multistage operators have expressed concern that swellable packers may not reliably seal open hole completions. To investigate this concern, benchmark testing was undertaken. The test results support the idea that industry pressure ratings may be marginal. For example, the industry length for 6,000 psi service is around 6 ft, and although it is possible to approach this pressure with conventional designs, overall performance has been suspect. A root cause analysis identified the annular extrusion gap as a limiting factor in pressure capability. The industry method to compensate is to increase the element length. While helpful, this adds cost and fails to address the root cause of the weakness. To remedy the problem, a patented, cost-effective fold back shoe technology was designed. The fold back shoes are fixed to the ends of the element. Swelling and axial pressures deploy the shoes to cover the annular extrusion gap. This feature yields industry-leading pressure performance and reliability. Figures 8 and 9 illustrate the fold back shoe technology. Several pressure tests were conducted and the test results show a linear dependence between the length of the element and the pressure rating, which will be higher for smaller open hole sizes due to less swelling. The bonded-to-pipe oil swellable packers, because of their robust rubber material coupled with the fold back shoe design, are capable of performing in the ranges of 1,600 psi/ft to 3,300 psi/ft, Fig. 10. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 63 Nonstandard Ball Increment Spacing Sizes Fig. 8. Pre-test swell packer with fold back shoes on both ends. Fig. 9. Post-test swell packer with fold back shoes deployed. Fig. 10. The graph is validated by actual full scale testing in various hole sizes. ENGINEERED APPROACH FOR OPTIMAL PERFORMANCE OF FRACTURING SLEEVES Together with the new open hole isolation packer, the development of a sliding sleeve with an incorporated ball seat design has been the main contributor to the successful application of the MSS technology. The use of incrementally increasing ball diameters — moving from toe to heel — has resulted in the possibility of deploying a high number of stages. Initially, the increment sizes typically started at ¼”, and as the demand for more stages increased, the simplest method to meet this demand was to reduce the ball increment size to ⅛”. Not satisfied with this either, the operators in North America pushed for further increases in stage count and some suppliers started deploying systems with 1/16” ball increment sizes. At issue was that the operational needs were outpacing the engineering required to fully test and qualify these modifications. A step backwards was required to properly model and test what suppliers had been proposing. It was clear that when the increment size and the overlap area between the ball and the ball seat fell below a certain value, there was a tendency for the ball to fail or become wedged in the ball seat, thereby preventing flow back of the ball. This phenomenon was made worse by larger balls; the larger the ball, the higher the risk of the ball becoming wedged in its seat. Taking an engineered approach to the ball and ball seat interface quickly determined that the larger balls needed a larger clearance between the ball and ball seat. Simply stated, a thicker metal was needed to be able to withstand the wedging effect; therefore the increment size had to be higher than the ⅛” range. For the smaller sized balls, the increment size could be reduced, and the spacing between the ball sizes could be decreased to less than ⅛” increment sizes. The ultimate achievement was to adopt nonstandard increments for the full range of ball sizes, so as to create equal forces between the ball and the ball seat’s interface for all sizes, Fig. 11. Curved Ball Seats Additionally, with this ball and ball seat interface in mind, several studies were performed to analyze the stresses acting on the ball after it contacted the ball seat area. With a conventional ball seat, the standard shape on the contact angle is a 30° profile. Testing and actual operations showed that this typically created a sharp stress point that either resulted in the ball cracking during the fracturing treatment or the ball becoming wedged in the ball seat itself, Fig. 12. The optimum design was found to be a “curved” ball seat, which resulted in a uniform stress distribution across the ball and seat interface, Fig. 13. Segmented Body for Full Bore Mill-out CT mill-out of the ball seats has always been a problematic area, prompting discussion16, 17. Even with the optimum Fig. 11. Ball seat increment calculations and finite element analysis for ball interface optimization. 64 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Fig. 12. Conventional ball seat’s high stress points potentially cause cracking or “egging” of the ball. MSWP COMPLETION SYSTEM OPERATIONAL EXECUTION Fig. 13. Curved ball seat design — uniformly distributed stresses across the ball seat reduce the chance of failure. milling BHA and procedures, failures still occur. In addition to optimizing the ball seat with a very robust design for the fracturing operation, it was noted straightaway that the ball seat design should also be easy to mill. The new ball seat has a segmented design that allows for smooth and simple milling operation. Another notable feature is that the ball seat can be milled out full bore, compared to the conventional design, which leaves a slither of metal after mill-out that can easily cause further problems with the CT operation and increases the risk of sticking or damaging the CT pipe, Fig. 14. Well-X was drilled and the pilot hole encountered good porosity development in reservoir-B, layer B1, with 40 ft true vertical depth net pay and 10% average porosity. Further analysis showed good reservoir quality but limited drainage volume. The existing vertical well was then sidetracked in the minimum stress direction with a horizontal lateral to maximize the reservoir contact, and it was equipped with a three-stage MSS completion to enhance the well productivity. The open hole MSS technology to be trial tested on this well was a 4½” MSS system with swellable packers. A 5⅞” open hole section of 2,831 ft was drilled without issue to 15,443 ft measured depth. An open hole reamer trip was run prior to running with a 4½” MSS, and one tight spot was encountered at 12,950 ft to 13,000 ft. The assembly was washed and reamed without rotation. The 4½” MSS assembly, including a liner hanger system, was smoothly deployed to total depth. A 1.700” ball was dropped to flow through the circulation valve and the valve was closed at 1,200 psi. With a closed system in place, the liner hanger was set at 2,000 psi and the running tool was released at 3,000 psi. The running tool was picked up and the liner top packer was set with 80,000 pounds (klb) of slack off. The liner top packer was tested from the annulus side to 3,000 psi for 15 minutes, Fig. 15. Fig. 14. Improved millable design, compared to the conventional design, of the ball seat. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 65 Fig. 15. Geolograph showing sequence of events. The upper completion string with a tieback seal assembly was landed in the tubing receptacle. The tubing pressure was increased to 8,800 psi. A clear indication was seen that the hydraulic frac valve had opened, Fig. 16. The newly opened, unstimulated, internal toe was expected to be very tight, and that proved to be the case as, at a relatively low circulation rate of 5 barrels per minute (BPM), a maximum bottom-hole pressure (BHP) of 15,000 psi was reached. Regardless of the lack of injectivity, the instantaneous shut-in 66 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY pressure was 600 psi lower than the first injection test, meaning that the formation had released pressure due to the previous flow back. The fact that the formation was able to release pressure from previous flow back shows that all previously injected volume had been taken by the reservoir; poroelasticity therefore was having a significant effect in the near wellbore area, limiting injection rate and volume. A decision was then made to spot acid with CT to improve injectivity. Consequently, a total of 100 bbl of 20% hydrochloric (HCl) acid inject into the formation, a decision was made to perform an acid squeeze with CT. After injection with CT at a rate of 6.5 BPM, a decision was made to perform an injection test with the fracturing equipment. The injection test showed pressure stability at the pumping rate of 20 BPM, which allowed the possibility of performing an acid fracturing treatment, Fig. 17. Subsequently, 1,900 bbl of treatment fluid, including diverting agent, 28% HCl acid and treated water were pumped. Overall, the acid injectivity in Stage 2 was very good, typically between 20 BPM and 30 BPM. Stage 1 showed poor injectivity with 1 BPM to a maximum of 8 BPM (for a very short period). This is a clear case of compartmentalization being exhibited by the swellable packers. If there had been channeling past the swellable packers, both zones should have exhibited similar injectivity behavior. CONCLUSIONS The following conclusions were noted from the performance of the new multistage fracturing completion equipment: Fig. 16. Pressure increased to 8,800 psi and dropped to 7,450 psi before holding steady. This gave a clear indication that valve had opened. was pumped and over displaced with 70 bbl of treated water. During the displacement, the pressure increased from 5,500 psi to 6,200 psi. Following the end of the first stage, the decision was to proceed with the second stage. A 3” magnesium ball was allowed to free fall in the vertical section for an hour. After an hour, pumps were started at a constant rate of 3 BPM. A clear indication was seen of the ball landing on the seat; the pressure increased from 4,100 psi to 6,100 psi, and then an immediate fall in pressure to 5,200 psi was seen, indicating that the sleeve had been opened and a new zone was available. Due to the positive opening of the sleeve and the ability to • An integrated approach, involving all departments from the operator side as well as positive communication with the service company, assisted in making the overall operation a complete success. • Thorough full-scale swellable packer testing demonstrated that the equipment exceeded the operational pressure and temperature considerations as well as the acid treatment type. • No operational lost time was recorded during the completion deployment operation as well as during the stimulation treatment. • The newly developed and installed swellable packers were successfully able to withstand and compartmentalize the fracturing pressure exerted. • The hydraulic frac sleeve was successfully opened at the first attempt, and a positive indication was recorded. An Fig. 17. Injectivity test for the newly opened Stage 2. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 67 injectivity test showed a very tight formation across the toe section. • A successful opening of the ball actuated frac sleeve was observed; this was proven by a clear pressure response when the ball landed onto the ball seat and the sleeve opened to the new formation zone. • The high fracture injection pressure response proved that a new zone was initiated, verified by BHP evaluation during the DataFRAC and main acid fracturing treatment. • The multistage completion equipment was successfully deployed to the target depth as per all the well objectives. ACKNOWLEDGMENTS The authors would like to thank the management of Saudi Aramco for their support and permission to publish this article. Also, the authors would like to recognize Saudi Aramco and the service company employees who are involved in multistage fracturing in Saudi Arabia. This article was presented at the International Petroleum Technology Conference, Kuala Lumpur, Malaysia, December 10-12, 2014. REFERENCES 1. Schmelzl, E., Schlosser, D., Alvarez, D. and Gulewicz, D.: “CTU Deployed Frac Sleeves Benchmark Horizontal Multistage Frac Isolation Performance,” SPE paper 169574, presented at the SPE Western North America and Rocky Mountain Joint Regional Meeting, Denver, Colorado, April 16-18, 2014. 2. Yalavarthi, R., Jayakumar, R., Nyaaba, C. and Rai, R.: “Impact of Completion Design on Unconventional Horizontal Well Performance,” SPE paper 168673, presented at the Unconventional Resources Technology Conference, Denver, Colorado, August 12-14, 2013. 3. Ingram, S.R., Lahman, M. and Persac, S.: “Methods Improve Stimulation Efficiency of Perforation Clusters in Completions,” Journal of Petroleum Technology, April 2014, pp. 31-36. 4. King, G.E.: “Best Practices Lead to Successful Shale Fracturing,” World Oil, Vol. 235, No. 3, March 2014, pp. 79-83. 5. Yuan, F., Blanton, E., Convey, B.A. and Palmer, C.: “Unlimited Multistage Completion System: A BallActivated System with Single Size Balls,” SPE paper 166303, presented at the SPE Annual Technical Conference and Exhibition, New Orleans, Louisiana, September 30 October 2, 2013. 6. Al-Ghazal, M.A., Al-Driweesh, S.M., Al-Ghurairi, F.A., AlSagr, A.M. and Al-Zaid, M.R.: “Assessment of Multistage 68 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Fracturing Technologies as Deployed in the Tight Gas Fields of Saudi Arabia,” IPTC paper 16440, presented at the International Petroleum Technology Conference, Beijing, China, March 26-28, 2013. 7. Al-Ghazal, M.A., Al-Ghurairi, F.A. and Al-Zaid, M.R.: “Overview of Open Hole Multistage Fracturing in the Southern Area Gas Fields: Application and Outcomes,” Saudi Aramco Ghawar Gas Production Engineering Division Internal Documentation, March 2013. 8. Al-Ghazal, M.A. and Abel, J.T.: “Stimulation Technologies in the Southern Area Gas Fields: A Step Forward in Production Enhancement,” Saudi Aramco Gas Production Engineering Division Internal Documentation, October 2012. 9. Al-Ghazal, M.A., Al-Sagr, A.M. and Al-Driweesh, S.M.: “Evaluation of Multistage Fracturing Completion Technologies as Deployed in the Southern Area Gas Fields of Saudi Arabia,” Saudi Aramco Journal of Technology, Fall 2011, pp. 34-41. 10. Al-Ghazal, M.A., Al-Driweesh, S.M. and El-Mofty, W.: “Practical Aspects of Multistage Fracturing from Geosciences and Drilling to Production: Challenges, Solutions and Performance,” SPE paper 164374, presented at the SPE Middle East Oil and Gas Show and Exhibition, Manama, Bahrain, March 10-13, 2013. 11. Rahim, Z., Al-Anazi, H.A. and Al-Kanaan, A.A.: “Improved Gas Recovery – 1: Maximizing Post-Frac Gas Flow Rates from Conventional, Tight Gas,” Oil and Gas Journal, March 2012, pp. 76. 12. Rafie, M., Said, R., Al-Hajri, M., Al-Mubarak, T., AlThiyabi, A., Nugraha, I., et al.: “The First Successful Multistage Acid Frac of an Oil Producer in Saudi Arabia,” SPE paper 172224, presented at the SPE Saudi Arabia Section Annual Technical Symposium and Exhibition, al-Khobar, Saudi Arabia, April 21-24, 2014. 13. Rahim, Z., Al-Kanaan, A.A., Johnston, B., Wilson, S., AlAnazi, H.A. and Kalnin, D.: “Success Criteria for Multistage Fracturing of Tight Gas in Saudi Arabia,” SPE paper 149064, presented at the SPE/DGS SAS Technical Symposium and Exhibition, al-Khobar, Saudi Arabia, May 15-18, 2011. 14. Wilson, S. and Johnston, B.: “Successful Deployment of Multistage Fracturing Systems in Multilayered Tight Gas Carbonate Formations in Saudi Arabia,” SPE paper 130894, presented at the SPE Deep Gas Conference and Exhibition, Manama, Bahrain, January 24-26, 2010. 15. Al-Ghazal, M.A., Al-Driweesh, S.M. and Al-Ghurairi, F.A.: “Upgrading Multistage Fracturing Strategies Drives Double Success after Success in the Unusual Saudi Gas Reserves,” SPE paper 168071, presented at the SPE Saudi Arabia Section Annual Technical Symposium and Exhibition, al-Khobar, Saudi Arabia, May 19-22, 2013. 16. Al-Ghazal, M.A., Abel, J.T., Wilson, S., Wortmann, H. and Johnston, B.B.: “Coiled Tubing Operational Guidelines in Conjunction with Multistage Fracturing Completions in the Tight Gas Fields of Saudi Arabia,” SPE paper 153235, presented at the Middle East Unconventional Gas Conference and Exhibition, Abu Dhabi, UAE, January 23-25, 2012. 17. Al-Ghazal, M.A., Abel, J.T., Al-Buali, M.H., AlRuwaished, A., Al-Sagr, A.M., Al-Driweesh, S.M., et al.: “Coiled Tubing Best Practices in Conjunction with Multistage Completions in the Tight Gas Fields of Saudi Arabia,” SPE paper 160833, presented at the SPE Saudi Arabia Section Technical Symposium and Exhibition, alKhobar, Saudi Arabia, April 8-11, 2012. BIOGRAPHIES Mohammed A. Al-Ghazal is a Production Engineer at Saudi Aramco. He is part of a team that is responsible for gas production optimization in the Southern Area gas reserves of Saudi Arabia. During Mohammed’s career with Saudi Aramco, he has led and participated in several severa upstream projects, including those addressing pressure control valve optimization, cathodic protection system performance, venturi meter calibration, new stimulation technologies, innovative wireline technology applications, upgrading of fracturing strategies, petroleum computer-based applications enhancement and safety management processes development. In 2011, Mohammed assumed the position of Gas Production HSE Advisor in addition to his production engineering duties. In early 2012, Mohammed went on assignment with the Southern Area Well Completion Operations Department, where he worked as a foreman leading a well completion site in several remote areas. As a Production Engineer, Mohammed played a critical role in the first successful application of several high-end technologies in the Kingdom’s gas reservoirs. In 2010, Mohammed received his B.S. degree with honors in Petroleum Engineering from King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia. He has also authored and coauthored several Society of Petroleum Engineers (SPE) papers and technical journal articles as well as numerous in-house technical reports. Additionally, Mohammed served as a member of the industry and student advisory board in the Petroleum Engineering Department of KFUPM from 2009 to 2011. As an active SPE member, he serves on the Production and Operations Award Committee. Recently, he won the best presentation award at the production engineering session of the 2013 SPE Young Professional Technical Symposium. Mohammed is currently pursuing an M.S. degree in Engineering at the University of Southern California, Los Angeles, CA. Saad M. Al-Driweesh is a General Supervisor in the Southern Area Production Engineering Department, where he is involved in gas production engineering, well completion, and fracturing and stimulation activities. Saad is an active member of the SSociety i t off Petroleum Engineers (SPE), where he has chaired several technical sessions in local, regional and international conferences. He is also the 2013 recipient of the SPE Production and Operations Award for the Middle East, North Africa and India region. In addition, Saad chaired the first Unconventional Gas Technical Event and Exhibition in Saudi Arabia. He has published several technical articles addressing innovations in science and technology. Saad’s main interest is in the field of production engineering, including production optimization, fracturing and stimulation, and new well completion applications. He has 26 years of experience in areas related to gas and oil production engineering. In 1988, he received his B.S. degree in Petroleum Engineering from King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia. Mustafa R. Al-Zaid is a Gas Production Engineer with Saudi Aramco’s Southern Area Production Engineering Department. He is part of a gas production optimization team, which is responsible for well completion, stimulation and fracturing activities in the Ghawar Ghaw field. Mustafa has designed and executed several critical rigless well interventions, including wireline operations and coiled tubing stimulation and cleaning in the Ghawar field. In 2010, he received his B.S. degree in Petroleum Engineering from the University of Adelaide, Adelaide, Australia. Mustafa has also successfully completed several technical courses relating reservoir management, well completion and production engineering at Saudi Aramco’s Upstream Professional Development Center, Dhahran, Saudi Arabia. Fadel A. Al-Ghurairi is a Petroleum Engineering Consultant and Technical Support Unit Supervisor working on gas fields. He has 24 years of experience in production and reservoir engineering. In the last 12 years, Fadel has specialized in stimulation and fracturing gas wells. f t i off deep d In 1988, he received his B.S. degree in Petroleum Engineering from King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 69 Deploying Global Competition by Innovation Network for Empowering Entrepreneurship, Venturing and Local Business Development: A Case Study — Desalination Using Renewable Energy Author: Dr. M. Rashid Khan The concept of open innovation (OI) became popular during the last decade. OI allowed companies to leverage global sourcing to create business value, keeping in mind that good ideas are widely distributed since not all of the smartest people in the world work for any single company. Chesbrough (2003)1 introduced the OI term to address the needs of mostly technology-focused R&D departments in large companies that were “closed” and highly secretive. It has long been recognized that opening the doors of large companies to outside input and encouraging an exchange of information will stimulate internal innovation2-6. The OI practices of large manufacturing companies, such as GE, P&G, Philips, Xerox and IBM, are widely documented7. As the goal of OI is to source the best innovations from anywhere in the world, large companies seeking to address a specific challenge and to deploy internal solutions externally deliberately introduced OI practices. Can this concept be extended to smaller entities, such as small- and medium-sized enterprises (SMEs) and entrepreneurs? Can the concept of OI be applied to encourage regional development by supporting local entrepreneurship and venturing? In a paradigm shift, Saudi Aramco Entrepreneurship (AEC) has initiated an innovation competition with multiple goals directed at addressing the needs of large organizations, SMEs and individual entrepreneurs, and identifying venture opportunity needs. The new business model, via the innovation competition, strives to create value through global participation. Large companies have successfully used innovation competitions as the primary avenue to pursue OI to fill their internal R&D voids. In the paradigm shifted model, coined “Innovation Network” (IN), innovation can be viewed from the perspective of not only large companies, but also numerous types/sizes of organizations with diverse roles and needs. In this model, OI can become relevant to entrepreneurs, startups and the organizations that support them as well as other stakeholders. Small companies can benefit in different ways from an innovation competition if it is designed effectively. This article highlights the “why” and “how” AEC with other stakeholders has used IN by launching a global competition. First, cost savings and control can be a significant benefit. When innovation competition is tightly restricted to one company, only the sponsor extracts the benefits. When organizations innovate “jointly” via IN through a global competition, a 70 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY greater value can be created at lower costs. In this model, different partners can work on different parts of the challenge and share expenses for the research and prototypes, deriving different benefits as appropriate. A significant argument for such a network model is that most entrepreneurs or SMEs do not have the needed internal technological competencies or resources. The vital strategic components of intellectual capital8, 9 for SMEs or entrepreneurs — talent, teams and technology (the 3 Ts)7, 8 — often are not fully explored because of resource limits. The new IN model may allow participants to overcome this limit by leveraging the commercial value of technologies that exist in other organizations or that had been co-developed by teaming with talented partners. Second, multidisciplinary and cross-industry collaboration around a common challenge with multiple objectives enhances creativity among the partners involved. Although a rarely used technique among SMEs, this approach can spark the search for more innovative products, services and related concepts. Third, the partnering of SMEs and/or entrepreneurial organizations with large companies may benefit from the use of “spillover technology” that is not necessarily relevant for large companies, but might be of interest to smaller ones, entrepreneurs and other vested groups. The concept of OI cannot be applied to capture the typical large company benefits — such as sharing costs and risks, faster product introduction, etc. — for entrepreneurs or SMEs. Instead, SMEs historically have engaged (or often have been forced into) innovation via a network as a consequence of major shifts in their business model, whether to seize new business opportunities and/or to boost profitability, or merely to survive. When they confront such a shift, their limited financial and human resources and their lack of technological capabilities often force them to look for different types of innovation partners. The key to success for technology development or economic development via innovation depends on (1) Identifying the strategic drivers to address the greatest needs or challenges for all, (2) Engaging stakeholders and obtaining their buy-ins, (3) Implementing or conducting an approach to the challenge in the most effective manner to derive maximum benefit for all partners and stockholders, and finally, (4) Deploying solutions by engaging partners and collaborators. Managing relationships with individual partners and organizing the overall network of diverse innovation partners is critical to success, since collaborative innovation is easier with partners of similar size and ambitions. This careful management of relations and needs is paramount and is more challenging than when an OI model is focused on one goal and a single company. A case study of innovation that addressed a regional challenge with global input and an added goal to further entrepreneurship is provided in this article, with careful consideration of all four elements listed above. To help Saudi Arabia meet its ever-growing need for potable water and to foster a culture of technology-based entrepreneurship in the Kingdom, the AEC and GE in April 2014 launched a global competition in the area of seawater desalination, with a particular focus on using renewable energy. What is the link between innovation and entrepreneurship? Why did AEC, which is focused on regional business development, get involved in such a global topic? What are the justifications for AEC’s co-sponsorship of this global innovation competition? First, the desalination topic addresses one of the greatest technical and business challenges of our time, and addressing and fulfilling a need is fundamental to entrepreneurship development. Saudi Arabia is considered to be among the poorest countries in the world in terms of natural renewable water resources, and it depends upon energy-intensive water desalination plants and its rapidly depleting groundwater reserves to meet its fast-growing water needs. The Kingdom is the world’s largest producer of desalinated water, which meets over 70% of its present drinking water needs. Over 50 cities and distribution centers in Saudi Arabia receive their water from these plants. The state-owned Saline Water Conversion Corporation (SWCC) operates 36 desalination stations, and independent power and water producers supplement these. SWCC would like to see a greater participation by the private sector, and therefore, views further development as an opportunity for entrepreneurs and local venturing. Using this initiative of global competition by IN, the AEC hopes not only to solicit innovative solutions but also to develop and deploy those solutions here in the Kingdom through collaboration between both national and global innovators. Therefore, the innovation competition was conceived with broader perspectives in mind, and the challenge was accordingly developed with partners and stakeholders to address the greatest technical need of the region, engaging SWCC, King Abdulaziz City for Science and Technology (KACST) and all key local universities. In the formulation of the competition, many avenues were explored, and many service providers were considered. Partnership with GE appeared to be the most economic and efficient way to achieve the most desirable results. The ultimate scope of the challenge developed by AEC, which served as the “main hub” of the innovation network, addressed the somewhat competing needs of all partners/stakeholders. The competition has attracted 108 proposals from global experts with multidisciplinary backgrounds with respect to geographic distribution (32 countries), organization type and experience (with combined input reflecting nearly 200 patents/peer-reviewed publications by over 100 Ph.D.s and other advanced professionals). Based on the initial assessments, many proposals address the needs of the stakeholders (SWCC, GE, Saudi Aramco, Saudi Aramco Energy Ventures (SAEV), AEC and in-Kingdom entrepreneurs). Subsequent dialogues among technology leaders in this strategic area may allow SAEV, SWCC, AEC and others to develop partnerships with global innovative companies having cutting-edge solutions for possible venturing and local deployment. Second, in Saudi Arabia, significant investment funding has been allocated to increasing potable water, creating opportunities for entrepreneurship and venturing. As the largest user of desalination processes and technology in the world, Saudi Arabia is projected to spend about $50 billion on seawater desalination technologies in the coming decade and to invest around $100 billion in solar energy. Current desalination techniques are energy intensive. To fuel desalination, Saudi Arabia is burning the equivalent of 1.5 million barrels of oil per day of precious fuels. An increase in energy efficiency and/or a reduction in energy consumption is the key to ensuring that the Kingdom receives the most value for its natural resources — value that can be used to develop the Kingdom and its people. As a result, the networkbased initiative by AEC received significant support at the outset from SWCC, the main proponent for the Kingdom’s desalination. Fig. 1. Number of patents filed worldwide related to “Osmotic Derived Membrane Process,” just one of many types of desalination methods commercially used. Source: International Desalination Report (IDS), September 2014. Fig. 2. The submissions came from 32 countries with 108 proposals, the largest number from the U.S. and the second largest input from Saudi Arabia. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 71 Third, successful entrepreneurs welcome the best concepts that address a critical need no matter where the solutions come from. As a result, the AEC charter encourages AEC to engage in activities in or outside Saudi Arabia in realizing its key objective, that of promoting entrepreneurship. According to many experts — as described in many textbooks — an entrepreneur is a person who converts an innovation into a business, no matter where the innovation originates. Khalid A. Al-Falih7, president and CEO of Saudi Aramco, routinely links entrepreneurship with innovation. Useful technology and know-how today is widely distributed and is increasing in a rapid manner, Fig. 1, and no individual organization — no matter how capable or how big — can innovate effectively on its own. Despite being the first one organized by Saudi Aramco, the global innovation competition generated a large number of quality responses, including a sizeable number from Saudi Arabia. It is clear that the Kingdom and the company can save energy and financial resources by applying creative new technologies and processes. The largest number of country-based submissions came from the U.S. (38 submissions), followed by Saudi Arabia (nine submissions), Fig. 2. The proposals received careful review by multidisciplinary teams in SWCC, GE and Saudi Aramco to identify those solutions that best address the critical needs of the region and that can be readily deployed via entrepreneurship and venturing in Saudi Arabia, in addition to fulfilling the mission of SWCC and GE. SUMMARY Entrepreneurship is always heightened by new technologies. The innovation competition generated many concepts of value for all of the parties concerned. The broader perspective of innovation so defined can be used to extract multiple benefits from larger organizations, such as SWCC, Saudi Aramco and GE, as well as from the smaller entities such as local entrepreneurs, SMEs and those engaged in local venture development. The broader perspective of the IN model should be far more effective than traditional OI. That is because the IN incorporates the perspective of regional innovation as involving many diverse players, including local research centers for fundamental, basic and applied research; business ecosystems for both established companies and startups; government institutions and entrepreneurs; and agents of technology transfer and startup incubators. Saudi Arabia is in need of cost-effective and energy-effective technologies for producing desalinated water. In the past, water production and security of supply drove technology selection. Because energy costs were low, proven, established technologies tended to be preferred over innovative solutions. This global competition, which focuses on the use of abundant renewable energy — such as solar — brings greater innovation to this critical area, and there are plans to introduce efficient new technologies in stations nearing the end of their life span, both to extend their productive life and to test new technologies. 72 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Applying the newer model, global innovation has the potential to present alternatives from key experts around the world to expand the technology options for Saudi Arabian organizations, which they can then develop, leverage and deploy in the future, empowering regional entrepreneurship. Finally, the network model of innovation conducted via a global competition not only will assist the stakeholders, such as SWCC, Saudi Aramco and GE, but will also enable venture development and entrepreneurship. The contest was developed keeping localization in mind in collaboration with the key local stakeholders, such as SWCC, KACST and others. As an example of support, SWCC offered to locally facilitate the testing and deployment of those technologies with high potential, and to serve as a key stakeholder for the initiative. Desalination and renewables are among the greatest challenges for the Kingdom, as defined by KACST, following the directive of the Custodian of the Two Holy Mosques King ‘Abd Allah ibn ‘Abd Al-’Aziz Al Sa’ud. Therefore, the innovative concepts gained from the competition can be localized to create highvalue new local businesses and high value jobs in Saudi Arabia. REFERENCES 1. Chesbrough, H.: Open Innovation, Harvard Business School Press, Cambridge, MA, 2003, 227 p. 2. Tilton, J.: International Diffusion of Technology: The Case of Semiconductors, Brookings Institute, Washington, D.C., 1971, 183 p. 3. Allen, T.J.: Managing Flow of Technology, The MIT Press, Cambridge, MA, 1977, 334 p. 4. Tidd, J.: “Conjoint Innovation: Building a Bridge between Innovation and Entrepreneurship,” International Journal of Innovation Management, Vol. 18, No. 1, February 2014. 5. Rothwell, R. and Zegveld, W.: Reindustrialization and Technology, Longman, London (Harlow), 1985, 282 p. 6. Khan, M.R.: “Some Insights into Embracing an Innovation Competition to Identify Breakthrough Technologies or Processes,” Saudi Aramco Journal of Technology, Fall 2010. 7. “MIT and Saudi Aramco Augment Existing Collaboration: More Energy Research,” MOU signed by MIT and Saudi Aramco, June 18, 2012. http://mitei.mit.edu/news/mit-andsaudi-aramco-augment-existing-collaboration. 8. Khan, M.R. and Germeraad, P.: “Management of Innovation and Intellectual Capital: The Concept of Three T’s for Growth and Sustainability for an Organization and a Nation,” Les Nouvelles, March 2011, pp. 26-38. 9. Khursani, S.A., Bazuhair, O.S. and Khan, M.R.: “Strategy for the Rapid Transformation of Saudi Arabia by Leveraging Intellectual Capital and Knowledge Management,” Saudi Aramco Journal of Technology, Winter 2011. BIOGRAPHY Dr. M. Rashid Khan is Head of Intellectual Property and Innovation for Saudi Aramco Entrepreneurship, where he launched the first Global Innovation Competition for Saudi Aramco. Previously, he served as the Deputy Director of the Technology Program of Engineering Services and was a Management Progra member of the Intellectual Assets and Innovation Management Group from the onset of these programs. Rashid shaped the first Intellectual Property (IP) policy for King Abdullah University of Science and Technology (KAUST), and defined the IP strategy in executing several technology transfer agreements, while also serving as the key technical reviewer. He has extensive work experience in upstream, downstream and other diverse areas of the oil and gas industry. Rashid has served as a “Distinguished Lecturer” for the Society of Petroleum Engineers (SPE) and presented many invited lectures, including at Harvard and MIT. He served as a mentor for the MIT Energy Competition and Licensing Executive Business Competition, and taught a course on patent monetization at MIT. Rashid also taught a course on Entrepreneurship at King Fahd University of Petroleum and Minerals (KFUPM). He received Texaco’s highest technical award for creativity. Rashid also received the American Chemical Society Texaco Research Award. Additionally, he served as a Technical Advisor to the U.S. White House; was an Adjunct Professor for Vassar College, Poughkeepsie, NY; and served in the United Nations Development Program (UNDP). Rashid has around 30 patent awards and has published over 200 journal papers. He has edited or authored six books in the areas of energy, environment, innovation, IP and business development. Rashid received his M.S. in Environmental Engineering from Oregon State University, Corvallis, OR, in 1979 and his Ph.D. degree in Energy and Fuels Engineering from Pennsylvania State University, University Park, PA, in 1984. He was recognized as a “Distinguished Fellow” by the President of Licensing Executive Society. Rashid is a Certified Patent Licensing Professional. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 73 2014 SAUDI ARAMCO PATENTS GRANTED LIST CLAY ADDITIVE FOR REDUCTION OF SULFUR IN CATALYTICALLY CRACKED GASOLINE Granted Patent: U.S. 8,623,199, Grant Date: January 7, 2014 Abdennour Bourane, Omer R. Koseoglu, Musaed Al-Ghrami, Christopher Dean, Mohammed A. Siddiqui and Shakeel Ahmed Summary The patent relates to the reduction of sulfur in gasoline produced in a fluid catalytic cracking process, and more particularly, to a method and sulfur reduction additive composition for use in the fluid catalytic cracking process. HYDRATED NIOBIUM OXIDE NANOPARTICLE CONTAINING CATALYSTS FOR OLEFIN HYDRATION Granted Patent: U.S. 8,629,080, Grant Date: January 14, 2014 Abdennour Bourane, Stephan R. Vogel and Wei Xu process that includes permutable reactors and that is capable of operating at moderate temperature and pressure with reduced hydrogen consumption. DETERMINATION OF ROCK MECHANICS FROM APPLIED FORCE TO AREA MEASURES WHILE SLABBING CORE SAMPLES Granted Patent: U.S. 8,635,026, Grant Date: January 21, 2014 Mohammad Ameen Summary The patent relates to rock material characterization, and in particular, to characterization of mechanical properties of formation rock from hydrocarbon reservoirs for geological and engineering purposes, such as design and planning of well completion, well testing and formation stimulation. Summary The patent relates to a catalyst and method of preparing a catalyst for olefin hydration. More specifically, the invention relates to a catalyst and method of preparing a catalyst wherein the catalyst includes amorphous or crystalline nanoparticles of hydrated niobium oxide, niobium oxosulfate, niobium oxo-phosphate or mixtures thereof for use in the hydration of olefins. METHOD FOR PREPARING POLYPROPYLENE FILMS HAVING IMPROVED ULTRAVIOLET RADIATION STABILITY AND SERVICE LIFE Granted Patent: U.S. 8,629,204, Grant Date: January 14, 2014 Ahmed Basfar, Khondoker Ali, Milind M. Vaidya and Ahmed Bahamdan Summary The patent relates to a polyolefin resin and articles prepared from the polyolefin resin. More specifically, the invention relates to a polypropylene resin exhibiting improved ultraviolet radiation stability and articles prepared therefrom. PROCESS FOR CATALYTIC HYDROTREATING OF SOUR CRUDE OILS Granted Patent: U.S. 8,632,673, Grant Date: January 21, 2014 Stephane Kressmann, Raheel Shafi, Esam Hamad and Bashir M. Dabbousi Summary The patent relates to a pre-refining process for the desulfurization of sour crude oils using a catalytic hydrotreating 74 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY METHOD FOR REMOVING MERCURY FROM A GASEOUS OR LIQUID STREAM Granted Patent: U.S. 8,641,890, Grant Date: February 4, 2014 Feras Hamad, Ahmed A. Bahamdan, Abdulaziz Al-Mulhim, Ayman Rashwan and Bandar A. Fadhel Summary The patent relates to an apparatus and method for removing mercury or mercury containing compounds from fluids, e.g., liquids, gases and gaseous condensates. More particularly, it relates to the use of porous membranes and scrubbing solutions, which when used in tandem remove mercury from the aforementioned fluids. RECOVERY OF HEAVY OIL THROUGH THE USE OF MICROWAVE HEATING IN HORIZONTAL WELLS Granted Patent: U.S. 8,646,524, Grant Date: February 11, 2014 Khaled Al-Buraik Summary The patent relates to a method of extracting and recovering subsurface sour crude oil deposits. More specifically, the method employs microwave radiation and the permeability enhancement of reservoir rocks due to fracture by selective heating and due to the creation of critical and supercritical fluids in the subsurface area. SYSTEM AND METHOD FOR IMPROVED COORDINATION BETWEEN CONTROL AND SAFETY SYSTEMS Granted Patent: U.S. 8,649,888, Grant Date: February 11, 2014 Abdelghani A. Daraiseh and Patrick S. Flanders Summary The patent relates to regulatory control systems and safety shutdown systems, and methods for monitoring and controlling field devices used with commercial and industrial processes. In particular, it relates to systems and methods for improved coordination between control and safety systems. a subterranean hydrocarbon producing well. More specifically, the invention relates to an apparatus for the staging of cement between the casing and a wellbore. CATALYTIC PROCESS FOR DEEP OXIDATIVE DESULFURIZATION OF LIQUID TRANSPORTATION FUELS CATHODIC PROTECTION ASSESSMENT PROBE Granted Patent: U.S. 8,663,459, Grant Date: March 4, 2014 Farhan M. Al-Shahrani, Gary Martinie, Tiancun Xiao and Malcolm Green Granted Patent: U.S. 8,652,312, Grant Date: February 18, 2014 Darrell Catte Summary Summary The patent relates to an apparatus and method for use with a corrosion monitoring and/or mitigation system. More specifically, the invention relates to an apparatus and method for monitoring cathodic protection while supplying cathodic protection power to an object being protected. Yet more specifically, the invention relates to a system for determining electrolyte corrosivity and optimum site-specific cathodic protection operating levels. SULFUR STEEL-SLAG AGGREGATE CONCRETE Granted Patent: U.S. 8,652,251, Grant Date: February 18, 2014 Mohammed Al-Mehthel, Saleh Al-Idi, Mohammed Maslehuddin, Mohammed R. Ali and Mohammed S. Barry Summary The patent relates to a composition and method for disposing of sulfur by using it to produce a sulfur-based concrete. INTEGRATED HYDROTREATING AND OXIDATIVE DESULFURIZATION PROCESS The patent relates to novel catalysts, systems and processes for the reduction of the sulfur content of liquid hydrocarbon fractions of transportation fuels, including gasoline and diesel fuels, to about 10 ppm or less by an oxidative reaction. ECONOMICAL HEAVY CONCRETE WEIGHT COATING FOR SUBMARINE PIPELINES Granted Patent: U.S. 8,662,111, Grant Date: March 4, 2014 Mohammed Al-Mehthel, Bakr Hammad, Alaeddin Al-Sharif, Mohammed Maslehuddin and Mohammed Ibrahim Summary The patent relates to the field of submarine pipelines. In particular, the invention is directed to an economical heavy concrete weight coating used to keep the submarine pipeline submerged below the surface of the water. MACHINES, COMPUTER PROGRAM PRODUCTS AND COMPUTER-IMPLEMENTED METHODS PROVIDING AN INTEGRATED NODE FOR DATA ACQUISITION AND CONTROL Granted Patent: U.S. 8,658,027, Grant Date: February 25, 2014 Omer R. Koseoglu and Abdennour Bourane Granted Patent: U.S. 8,667,091, Grant Date: March 4, 2014 Soliman M. Almadi, Soliman A. Al-Walaie and Tofig A. Al-Dhubaib Summary Summary The patent relates to desulfurization of hydrocarbon streams, and in particular, to a system and process for integrated hydrotreating and oxidative desulfurization of hydrocarbon streams to produce reduced sulfur content hydrocarbon fuels. The patent relates to automated industrial processes. In particular, the invention relates to the control of and the acquisition of data from, remote and in-plant subsystems in automated industrial processes. SLIDING STAGE CEMENTING TOOL Granted Patent: U.S. 8,657,004, Grant Date: February 25, 2014 Shaohua Zhou Summary PLUGGING THIEF ZONES AND FRACTURES BY IN SITU AND IN-DEPTH CRYSTALLIZATION FOR IMPROVING WATER SWEEP EFFICIENCY OF SANDSTONE AND CARBONATE RESERVOIRS Granted Patent: U.S. 8,662,173, Grant Date: March 4, 2014 Xianmin Zhou and Yun C. Chang The patent relates to an apparatus for use while completing SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 75 Summary The patent relates to compositions and methods for treating subterranean formations. More specifically, the invention relates to compositions and methods for plugging thief zones and fractures in subterranean formations. SUPER-RESOLUTION FORMATION FLUID IMAGING Granted Patent: U.S. 8,664,586, Grant Date: March 4, 2014 Howard K. Schmidt Summary The patent relates to imaging subsurface structures, particularly hydrocarbon reservoirs and fluids therein; it relates more particularly to cross-well and borehole to surface electromagnetic (BSEM) surveying. BUOYANT PLUG FOR EMERGENCY DRAIN IN FLOATING ROOF TANK bases. More specifically, it relates to providing continuous monitoring for leaks and pressure losses in fuel pipelines, as well as providing status indications for, and control of, jet fuel supply valves, isolation valves, jet fuel pumps and other instrumentation in jet fuel piping systems. BOREHOLE TO SURFACE ELECTROMAGNETIC TRANSMITTER Granted Patent: U.S. 8,680,866, Grant Date: March 25, 2014 Alberto F. Marsala, Mohammad Al-Buali, Zhanxiang He and Tang Biyan Summary The patent relates to an electromagnetic energy source or transmitter for borehole to surface electromagnetic surveying and mapping of subsurface formations. ZERO LEAKOFF GEL Granted Patent: U.S. 8,668,105, Grant Date: March 11, 2014 Nassir S. Al-Subaiey Granted Patent: U.S. 8,684,081, Grant Date: April 1, 2014 Saleh Al-Mutairi, Ali Al-Aamri, Khalid Al-Dossary and Mubarak Al-Dhufairi Summary Summary The patent relates to floating roofs for storage tanks that contain volatile fluid, and more particularly, to an emergency drain valve for water accumulated atop a double deck roof. The patent relates to a silicate gel composition formed in situ and its method of use. More specifically, it relates to a silicate gel composition that forms in a wellbore and a method of diverting treatment fluid in a wellbore. WELL SYSTEM WITH LATERAL MAIN BORE AND STRATEGICALLY DISPOSED LATERAL BORES AND METHOD OF FORMING METHODS FOR PERFORMING A FULLY AUTOMATED WORKFLOW FOR WELL PERFORMANCE MODEL CREATION AND CALIBRATION Granted Patent: U.S. 8,672,034, Grant Date: March 18, 2014 Fahad M. Al-Ajmi and Ahmed H. Alhuthali Granted Patent: U.S. 8,688,426, Grant Date: April 1, 2014 Ahmad Al-Shammari Summary Summary The patent relates to a subterranean hydrocarbon producing well system. More specifically, the invention relates to a well system having a main bore that extends above a producing formation with lateral bores that depend from the main bore and intersect the producing formation. PIPELINE LEAK DETECTION AND LOCATION SYSTEM THROUGH PRESSURE AND CATHODIC PROTECTION SOIL Granted Patent: U.S. 8,682,600, Grant Date: March 25, 2014 Pablo D. Genta Summary The patent relates to the detection and location of fuel leakages occurring in underground jet fuel piping systems of the type employed at civil airports and military air 76 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY The patent relates to oil and gas recovery. In particular, it relates to the optimization of production and injection rates, and more specifically to systems, program product and methods that provide improved well performance modeling, building and calibration. WELLBORE PRESSURE CONTROL DEVICE Granted Patent: U.S. 8,689,892, Grant Date: April 8, 2014 Mohamed N. Noui-Mehidi Summary The patent relates to an apparatus and method for managing pressure in a wellbore. More specifically, the invention relates to the use of swirling fluids to maintain a wellbore at a desired pressure. CONVERTING HEAVY SOUR CRUDE OIL/ EMULSION TO LIGHTER CRUDE OIL USING CAVITATIONS AND FILTRATION-BASED SYSTEMS PIPELINE PIG WITH INTERNAL FLOW CAVITY Granted Patent: U.S. 8,691,083, Grant Date: April 8, 2014 M. Rashid Khan Summary Summary The patent relates to pipeline pigs used in the inspection of pipelines. The patent relates to the conversion of heavier sulfur-containing crude oil into lighter crude oil with lower sulfur content and lower molecular weight than the original crude oil. SOUR GAS AND ACID NATURAL GAS SEPARATION MEMBRANE PROCESS BY PRE-REMOVAL OF DISSOLVED ELEMENTAL SULFUR FOR PLUGGING PREVENTION Granted Patent: U.S. 8,696,791, Grant Date: April 15, 2014 Milind M. Vaidya, Jean-Pierre Ballaguet, Sebastien Duval and Anwar Khawajah Summary Granted Patent: U.S. 8,715,423, Grant Date: May 6, 2014 Ali Al-Mousa PROCESS FOR OXIDATIVE CONVERSION OF ORGANOSULFUR COMPOUNDS IN LIQUID HYDROCARBON MIXTURES Granted Patent: U.S. 8,715,489, Grant Date: May 6, 2014 Gary D. Martinie, Farhan M. Al-Shahrani and Bashir M. Dabbousi Summary The patent relates to the conversion of organosulfur compounds in liquid hydrocarbon mixtures, and more particularly, their conversion by catalytic oxidation. SLIDING STAGE CEMENTING TOOL AND METHOD The patent relates to methods for removing sulfur from gas streams prior to sending the gas streams to gas separation membranes. Granted Patent: U.S. 8,720,561, Grant Date: May 13, 2014 Shaohua Zhou SIMULTANEOUS WAVELET EXTRACTION AND DECONVOLUTION IN THE TIME DOMAIN The patent relates to an apparatus for use while completing a subterranean hydrocarbon producing well. More specifically, the invention relates to an apparatus for the staging of cement between the casing and a wellbore. Granted Patent: U.S. 8,705,315, Grant Date: April 22, 2014 Saleh Al-Dossary and Jinsong Wang Summary The patent relates to seismic data processing and more particularly, to wavelet extraction and deconvolution during seismic data processing. METHODS FOR MANAGING CONTRACT PROCUREMENT Granted Patent: U.S. 8,706,569, Grant Date: April 22, 2014 Hisham Al-Abdulqader, Ammar Al-Mubarak and Udai Al-Mulla Summary The patent relates to automated business transaction systems, in particular to contract management systems. More specifically, this patent relates to a system, program product and methods of facilitating contract procurement and contract management through an online contract procurement and management website. Summary ASPHALT COMPOSITIONS WITH SULFUR MODIFIED POLYVINYL ACETATE (PVAC) Granted Patent: U.S. 8,721,215, Grant Date: May 13, 2014 Mohammed Al-Mehthel, Saleh Al-Idi, Ibnelwaleed Hussein, Hamad Al-Abdulwahhab and Mohammed Suleiman Summary The patent relates to asphalt compositions containing asphalt and sulfur modified polyvinyl acetate polymers having improved properties relative to unmodified polyvinyl acetate polymers. WASTEWATER TREATMENT PROCESS INCLUDING IRRADIATION OF PRIMARY SOLIDS Granted Patent: U.S. 8,721,889, Grant Date: May 13, 2014 William Conner, Osama I. Fageeha and Thomas Schultz Summary The patent relates to a system and method for wastewater treatment. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 77 PRODUCTION OF SYNTHESIS GAS FROM SOLVENT DEASPHALTING PROCESS BOTTOMS IN A MEMBRANE WALL GASIFICATION REACTOR Granted Patent: U.S. 8,721,927, Grant Date: May 13, 2014 Omer R. Koseoglu Summary The patent relates to processes for the partial oxidation in a membrane wall gasification reactor of heavy bottoms, which can also contain waste materials, recovered from a solvent deasphalting unit operation to produce a high value synthesis gas. SULFUR MODIFIED ASPHALT FOR WARM MIX APPLICATIONS Granted Patent: U.S. 8,722,771, Grant Date: May 13, 2014 Milind Vidya, Anwar H. Khawajah, Rashid M. Othman and Laurand Lewandowski Summary The patent relates to an asphalt concrete mixture, an asphalt binder composition and methods of preparing the asphalt concrete mixture. WELLHEAD HIPS WITH AUTOMATIC TESTING AND SELF-DIAGNOSTICS Granted Patent: U.S. 8,725,434, Grant Date: May 13, 2014 Patrick S. Flanders Summary The patent relates to a method and an apparatus for the operation and testing of a high integrity protection system (HIPS) connected to a wellhead pipeline system. APPARATUS AND METHODS FOR ENHANCED WELL CONTROL IN SLIM COMPLETIONS Granted Patent: U.S. 8,727,016, Grant Date: May 20, 2014 Mohamed N. Noui-Mehidi and Jinjiang Xiao Summary The patent relates to well control of hydrocarbon wells. More particularly, the invention relates to well control of a slim-hole well. CLUSTER 3D PETROPHYSICAL UNCERTAINTY MODELING Granted Patent: U.S. 8,731,891, Grant Date: May 20, 2014 Roger R. Sung and Khalid S. Al-Wahabi Summary The patent relates to computerized simulation of 78 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY hydrocarbon reservoirs in the earth that have been modeled as a three-dimensional grid of cells. In particular, it relates to the determination of reservoir attributes or properties on a cell-by-cell basis for the individual cells in the reservoir model. SYSTEMS AND PROGRAM PRODUCT FOR PERFORMING A FULLY AUTOMATED WORKFLOW FOR WELL PERFORMANCE MODEL CREATION AND CALIBRATION Granted Patent: U.S. 8,731,892, Grant Date: May 20, 2014 Ahmad Al-Shammari Summary The patent relates to oil and gas recovery, in particular to the optimization of production and injection rates. More specifically, it relates to systems, program product and methods that provide improved well performance modeling, building and calibration. INDUCING FLOW BACK OF DAMAGING MUDINDUCED MATERIALS AND DEBRIS TO IMPROVE ACID STIMULATION OF LONG HORIZONTAL INJECTION WELLS IN TIGHT CARBONATE FORMATIONS Granted Patent: U.S. 8,733,443, Grant Date: May 27, 2014 Ali A. Al-Taq Summary The patent relates to a method of conditioning a long horizontal open hole water injection well in a tight formation prior to acid stimulation to improve the contact of the acid with the rock as well as the penetration of the acidic materials into the reservoir rock, and thereby enhancing the permeability of the formation and the flow rate of the injected water. DETERMINATION OF ANGLE OF INTERNAL FRICTION OF FORMATION ROCK WHILE SLABBING CORE SAMPLES Granted Patent: U.S. 8,738,294, Grant Date: May 27, 2014 Mohammed S. Ameen Summary The patent relates to rock material characterization, and in particular, to the characterization of the mechanical properties of formation rock from hydrocarbon reservoirs for geological and engineering purposes, such as design and planning of well completion, well testing and formation stimulation. INTEGRATED DESULFURIZATION AND DENITRIFICATION PROCESS INCLUDING MILD HYDROTREATING AND OXIDATION OF AROMATIC-RICH HYDROTREATED PRODUCTS AUXILIARY PRESSURE RELIEF RESERVOIR FOR CRASH BARRIER Granted Patent: U.S. 8,741,127, Grant Date: June 3, 2014 Omer R. Koseoglu, Abdennour Bourane, Farhan M. Al-Shahrani and Emad Al-Shafi Summary Summary The patent relates to integrated oxidation processes to efficiently reduce the sulfur and nitrogen content of hydrocarbons to produce fuels having reduced sulfur and nitrogen levels. INTEGRATED DESULFURIZATION AND DENITRIFICATION PROCESS INCLUDING MILD HYDROTREATING OF AROMATIC-LEAN FRACTION AND OXIDATION OF AROMATIC-RICH FRACTION Granted Patent: U.S. 8,741,128, Grant Date: June 3, 2014 Omer R. Koseoglu, Abdennour Bourane, Farhan M. Al-Shahrani and Emad Al-Shafi Summary The patent relates to integrated oxidation processes to efficiently reduce the sulfur and nitrogen content of hydrocarbons to produce fuels having reduced sulfur and nitrogen levels. METHODS OF PREPARING LIQUID BLENDS FOR BUILDING CALIBRATION CURVES FOR THE EFFECT OF CONCENTRATION ON LASER-INDUCED FLUORESCENCE INTENSITY Granted Patent: U.S. 8,742,340, Grant Date: June 3, 2014 Ezzat M. Hegazi and Abdullah H. Al-Grainees Summary The patent relates to a small volume apparatus and a trialand-error method for identifying and replicating original target liquid blends of unknown ratios by employing laserinduced fluorescence spectroscopy. STORAGE TANK FLOATING ROOF SUMP WITH EMERGENCY OVERFLOW Granted Patent: U.S. 8,746,482, Grant Date: June 10, 2014 Mohammed Ben Afeef Summary The patent relates to a drainage device for use on a floating roof of a storage tank for liquid products. Granted Patent: U.S. 8,753,034, Grant Date: June 17, 2014 Bandar Al-Qahtani The patent relates to hydraulically powered vehicle crash barrier systems, in particular vehicle crash barrier systems having an emergency mode of operation to rapidly raise the crash barrier. DISPOSAL OF SULFUR THROUGH USE AS SANDSULFUR MORTAR Granted Patent: U.S. 8,758,212, Grant Date: June 24, 2014 Mohammed Al-Mehthel, Saleh Al-Idi, Mohammed Maslehuddin, Mohammed R. Ali and Mohammed S. Barry Summary The patent relates to a composition and method for disposing of sulfur by converting waste sulfur to a useful product, namely, by producing a sulfur-based mortar. IONIC LIQUID DESULFURIZATION PROCESS INCORPORATED IN A LOW PRESSURE SEPARATOR Granted Patent: U.S. 8,758,600, Grant Date: June 24, 2014 Omer R. Koseoglu and Adnan Al-Hajji Summary The patent relates to a system and process for desulfurizing hydrocarbon fractions, and in particular, to a system and process that integrates ionic liquid extractive desulfurization with a hydroprocessing reactor. SEISMIC IMAGE FILTERING MACHINE TO GENERATE A FILTERED SEISMIC IMAGE, PROGRAM PRODUCTS AND RELATED METHODS Granted Patent: U.S. 8,762,064, Grant Date: June 24, 2014 Saleh Al-Saleh Summary The patent relates to the field of geophysical subsurface seismic imaging in geophysical seismic exploration. More specifically, this invention generally relates to machines, program products and methods to generate filtered seismic images based on seismic image data filtered by attenuating coherent noise from unfiltered seismic image data using a plurality of nonstationary convolution operators as local filters at each spatial location of an unfiltered seismic image wavefield. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 79 PERFORMANCE GRADED, SULFUR MODIFIED ASPHALT COMPOSITIONS FOR SUPER PAVE COMPLIANT PAVEMENTS Granted Patent: U.S. 8,772,380, Grant Date: July 8, 2014 Milind M. Vaidya, Anwar H. Khawajah, Rashid M. Othman and Laurand Lewandowski Summary The patent relates to an asphalt concrete mixture, an asphalt binder composition and methods of preparing the asphalt concrete mixture. SAND PRODUCTION CONTROL THROUGH THE USE OF MAGNETIC FORCES Granted Patent: U.S. 8,776,883, Grant Date: July 15, 2014 Ashraf M. Al-Tahini Summary The patent relates to a method for controlling the amount of sand produced from a wellbore. More particularly, the invention relates to a method of using magnetic forces to control the flow of loose sand particles within an underground formation to prevent the loose sand particles from damaging downhole tools. BLOCKED VALVE ISOLATION TOOL Granted Patent: U.S. 8,800,602, Grant Date: August 12, 2014 Mohammad Al-Shammary Summary The patent relates to the field of gas treatment and production facilities, and particularly to the procedures employed in a portion of a gas flow duct system for isolation and removal of a valve for inspection, repair or replacement. METHOD FOR REAL-TIME MONITORING AND TRANSMITTING HYDRAULIC FRACTURE SEISMIC EVENTS TO SURFACE USING THE PILOT HOLE OF THE TREATMENT WELL AS THE MONITORING WELL Granted Patent: U.S. 8,800,652, Grant Date: August 12, 2014 Kirk M. Bartko and Brett W. Bouldin Summary WATER SELF-SHUTOFF TUBULAR The patent relates to the field of hydraulic fracturing, monitoring and data transmission of microseismic information from a zone of interest within a reservoir. More particularly, it relates to the utilization and employment of electrically and physically isolated downhole acoustic monitoring equipment within a fracturing treatment well to detect microseismic events during fracturing operations. Granted Patent: U.S. 8,789,597, Grant Date: July 29, 2014 Mohammad Al-Shammary PARTIALLY RETRIEVABLE SAFETY VALVE Granted Patent: U.S. 8,800,668, Grant Date: August 12, 2014 Brett W. Bouldin and Stephen Smith Summary The patent relates to controlling the production of oil and gas reservoirs. More specifically, the invention relates to an apparatus and method for controlling water production with a multilayered tubular and a water sensitive composite. INTEGRATED DEASPHALTING AND OXIDATIVE REMOVAL OF HETEROATOM HYDROCARBON COMPOUNDS FROM LIQUID HYDROCARBON FEEDSTOCKS Granted Patent: U.S. 8,790,508, Grant Date: July 29, 2014 Omer R. Koseoglu and Abdennour Bourane Summary The patent relates to oxidative desulfurization, and more particularly, to a process for integrated deasphalting and oxidative removal of heteroatom-containing hydrocarbon compounds, such as organosulfur compounds, of liquid hydrocarbon feedstocks. 80 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Summary The patent relates to deep-set safety valves used in subterranean well production. More specifically, the invention relates to deep-set safety valves used in connection with submersible pumps for controlling a well. SYSTEM FOR MEASUREMENT OF MOLTEN SULFUR LEVEL IN RECEPTACLES Granted Patent: U.S. 8,801,276, Grant Date: August 12, 2014 Adel S. Al-Misfer Summary The patent relates to the measurement and control of the flow of molten sulfur that is being added to a container or receptacle, for example, to a steam jacketed tank truck for transportation or to a sulfur pit for storage. SOUR GAS AND ACID NATURAL GAS SEPARATION MEMBRANE PROCESS BY PRE-REMOVAL OF DISSOLVED ELEMENTAL SULFUR FOR PLUGGING PREVENTION Granted Patent: U.S. 8,801,832, Grant Date: August 12, 2014 Milind M. Vaidya, Jean Pierre Ballaguet, Sebastien A. Duval and Anwar H. Khawajah Summary The patent relates to a process for refining naphtha. More specifically, embodiments of the invention utilize two isomerization units and a reforming unit to create a gasoline blend having an improved octane rating as compared to the naphtha and/or to produce concentrated reformate for petrochemicals. Summary The patent relates to methods for removing sulfur from gas streams prior to sending the gas streams to gas separation membranes. CATALYTIC REFORMING PROCESS AND SYSTEM FOR PRODUCING REDUCED BENZENE GASOLINE Granted Patent: U.S. 8,801,920, Grant Date: August 12, 2014 Omer R. Koseoglu and Abdennour Bourane Summary The patent relates to the catalytic reforming apparatus and processes, particularly for producing gasoline of reduced benzene content. SUPER RESOLUTION FORMATION FLUID IMAGING DATA ACQUISITION AND PROCESSING INTEGRATED SYSTEM FOR MONITORING PERMEATE QUALITY IN WATER TREATMENT FACILITIES Granted Patent: U.S. 8,808,539, Grant Date: August 19, 2014 Nicos Isaias, Ioannis Gragopoulos and Anastasios Karabelas Summary The patent relates to a method and apparatus for monitoring permeate quality in a water treatment process. More specifically, the invention relates to a method and apparatus for monitoring the performance of individual membrane elements in a reverse osmosis or nanofiltration desalination of a water treatment plant. DEEP-READING ELECTROMAGNETIC DATA ACQUISITION METHOD Granted Patent: U.S. 8,803,077, Grant Date: August 12, 2014 Howard K. Schmidt Granted Patent: U.S. 8,812,237, Grant Date: August 19, 2014 Alberto F. Marsala, Saleh B. Al-Ruwaili, Shouxiang Ma, Michael Wilt, Steve Crary and Tarek Habashy Summary Summary The patent relates to imaging subsurface structures, particularly hydrocarbon reservoirs and fluids therein; more particularly, it relates to cross-well and borehole to surface electromagnetic (BSEM) surveying. The patent relates to the planning, acquisition, processing and interpretation of geophysical data, and more particularly, to methods for interpreting deep-reading electromagnetic data acquired during a field survey of the subsurface. MICROWAVE PROMOTED DESULFURIZATION OF CRUDE OIL AUTOMATED METHOD FOR QUALITY CONTROL AND QUALITY ASSURANCE OF SIZED BRIDGING MATERIAL Granted Patent: U.S. 8,807,214, Grant Date: August 19, 2014 M. Rashid Khan and Emad N. Al-Shafei Summary The patent relates to the processing of crude oil using microwave energy to reduce the sulfur content. PROCESS DEVELOPMENT BY PARALLEL OPERATION OF PARAFFIN ISOMERIZATION UNIT WITH REFORMER Granted Patent: U.S. 8,813,585, Grant Date: August 26, 2014 Md. Amanullah, John T. Allen and Mohammed Kilani Summary The patent relates to drill-in fluids used in oil and gas drilling, and in particular, to a laboratory method for evaluating the durability of sized bridging materials used in the formulation of drill-in fluids to eliminate or minimize formation damage. Granted Patent: U.S. 8,808,534, Grant Date: August 19, 2014 Cemal Ercan, Yuguo Wang, Mohammad Al-Dossary and Rashid M. Othman SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 81 PROCESS FOR UPGRADING HEAVY AND HIGHLY WAXY CRUDE OIL WITHOUT SUPPLY OF HYDROGEN CIRCULATION AND ROTATION TOOL Granted Patent: U.S. 8,815,081, Grant Date: August 26, 2014 Ki-Hyouk Choi Summary Summary The patent relates to a continuous process for upgrading heavy crude oil and highly waxy crude oil to produce more valuable crude oil feedstock having a higher API gravity; lower content of asphaltene, sulfur, nitrogen and metallic impurities; increased middle distillate yield; and/or a reduced pour point. APPARATUS AND METHOD FOR MULTICOMPONENT WELLBORE ELECTRIC FIELD MEASUREMENTS USING CAPACITIVE SENSORS Granted Patent: U.S. 8,816,689, Patent Date: August 26, 2014 Daniele Colombo, Timothy H. Keho, Michael A. Jervis and Brett W. Bouldin Summary Granted Patent: U.S. 8,826,992, Grant Date: September 9, 2014 Shaohua Zhou The patent relates to making up and breaking out pipe connections during drilling operations. In particular, it relates to a tool for allowing circulation of fluid through, and rotation of, a pipe string while making up or breaking out pipe connections. HYDROCRACKING PROCESS WITH FEED/ BOTTOMS TREATMENT Granted Patent: U.S. 8,828,219, Grant Date: September 9, 2014 Omer R. Koseoglu Summary The patent relates to hydrocracking processes, and in particular, to hydrocracking processes adapted to receive multiple feedstreams. SELF-CONTROLLED INFLOW CONTROL DEVICE The patent relates to an apparatus and method for evaluating oil and gas reservoir characteristics. More specifically, the invention relates to triaxial field sensors for low frequency electromagnetic fields. ELECTROCHEMICAL PROMOTION OF CATALYSIS IN HYDRODESULFURIZATION PROCESSES Granted Patent: U.S. 8,821,715, Grant Date: September 2, 2014 Ahmad D. Hammad, Esam Z. Hamad and Mohammed S. Elanany Summary The patent relates to the removal of sulfur from hydrocarbon streams, and more particularly, to a catalytic hydrodesulfurization process, which allows for the in situ control of catalyst activity and selectivity. Granted Patent: U.S. 8,833,466, Grant Date: September 16, 2014 Shaohua Zhou Summary The patent relates to well production devices, and in particular, to a self-controlled inflow control device. DRILLING, DRILL-IN AND COMPLETION FLUIDS CONTAINING NANOPARTICLES FOR USE IN OIL AND GAS FIELD APPLICATIONS AND METHODS RELATED THERETO Granted Patent: U.S. 8,835,363, Grant Date: September 16, 2014 Md. Amanullah and Ziad Al-Abdullatif Summary PROCESS FOR UPGRADING HYDROCARBON FEEDSTOCKS USING SOLID ADSORBENT AND MEMBRANE SEPARATION OF TREATED PRODUCT STREAM The patent relates to drilling, drill-in and completion fluids and related additives for use in oil and gas field applications. More specifically, the invention relates to drilling, drill-in and completion fluids that include nanoparticles and related additives. Granted Patent: U.S. 8,821,717, Grant Date: September 2, 2014 Omer R. Koseoglu VALVE ACTUATOR FAULT ANALYSIS SYSTEM Granted Patent: U.S. 8,838,413, Grant Date: September 16, 2014 Pablo D. Genta Summary The patent relates to the upgrading of hydrocarbon oil feedstock to remove undesirable sulfur and nitrogen containing compounds using solid adsorbents. 82 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Summary The patent relates to valve actuators, and more specifically, to a fault analysis system for detecting and locating actuator malfunctions, performance deviations and failures, as well as causal factors of any such malfunction, performance deviation or failure, to facilitate the determination of adequate remedial actions. INTEGRATED HYDROTREATING AND ISOMERIZATION PROCESS WITH AROMATIC SEPARATION Granted Patent: U.S. 8,852,426, Grant Date: October 7, 2014 Omer R. Koseoglu Summary The patent relates to hydrotreating processes to efficiently reduce the sulfur content of hydrocarbons. DEVICE AND METHOD FOR MEASURING ELEMENTAL SULFUR IN GAS IN GAS LINES Granted Patent: U.S. 8,852,535, Grant Date: October 7, 2014 Ihsan Al-Taie, Abdulaziz Al-Mathami and Helal Al-Mutairi Summary The patent relates to the sampling of gases, and more particularly, to a device and method for measuring the level of elemental sulfur present in a gas in a gas line. STRUCTURE INDEPENDENT ANALYSIS OF 3D SEISMIC RANDOM NOISE Granted Patent: U.S. 8,855,440, Grant Date: October 7, 2014 Saleh Al-Dossary and Yuchun Wang Summary The patent relates to the field of image processing and specifically to the suppression of image data to estimate and identify random noise in post-stacked three-dimensional seismic data containing geological structures, such as faults. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 83 At Saudi Aramco, our passion is enabling opportunity. From the depths of the earth to the frontiers of the human mind, we’re dedicated to fostering innovation, unleashing potential, and applying science to develop new solutions for the global energy challenge. As the world’s preeminent energy and chemicals company, it is our responsibility — our privilege — to maximize the opportunity available in every hydrocarbon molecule we produce. That’s how we contribute to our communities, our industry, and our world. Saudi Aramco is there, at the intersection of energy and opportunity, building a better future for all. 84 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY SUBSCRIPTION ORDER FORM To begin receiving the Saudi Aramco Journal of Technology at no charge, please complete this form. Please print clearly. 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The Saudi Aramco Journal of Technology is published by the Saudi Aramco Public Relations Department, Saudi Arabian Oil Company, Dhahran, Saudi Arabia. SAUDI ARAMCO JOURNAL OF TECHNOLOGY WINTER 2014 85 GUIDELINES FOR SUBMITTING AN ARTICLE TO THE SAUDI ARAMCO JOURNAL OF TECHNOLOGY These guidelines are designed to simplify and help standardize submissions. They need not be followed rigorously. If you have additional questions, please feel free to contact us at Public Relations. Our address and phone numbers are listed on page 85. Length Varies, but an average of 2,500-3,500 words, plus illustrations/photos and captions. Maximum length should be 5,000 words. Articles in excess will be shortened. Acknowledgments Use to thank those who helped make the article possible. Illustrations/tables/photos and explanatory text Submit these separately. Do not place in the text. Positioning in the text may be indicated with placeholders. Initial submission may include copies of originals; however, publication will require the originals. When possible, submit both electronic versions, printouts and/or slides. Color is preferable. File formats Illustration files with .EPS extensions work best. Other acceptable extensions are .TIFF, .JPEG and .PICT. What to send Send text in Microsoft Word format via email or on disc, plus one hard copy. Send illustrations/photos and captions separately but concurrently, both as email or as hard copy (more information follows under file formats). Permission(s) to reprint, if appropriate Previously published articles are acceptable but can be published only with written permission from the copyright holder. Procedure Notification of acceptance is usually within three weeks after the submission deadline. The article will be edited for style and clarity and returned to the author for review. All articles are subject to the company’s normal review. No paper can be published without a signature at the manager level or above. Format No single article need include all of the following parts. The type of article and subject covered will determine which parts to include. Working title Abstract Usually 100-150 words to summarize the main points. Author(s)/contributor(s) Please include a brief biographical statement. Submission/Acceptance Procedures Papers are submitted on a competitive basis and are evaluated by an editorial review board comprised of various department managers and subject matter experts. Following initial selection, authors whose papers have been accepted for publication will be notified by email. Papers submitted for a particular issue but not accepted for that issue will be carried forward as submissions for subsequent issues, unless the author specifically requests in writing that there be no further consideration. Papers previously published or presented may be submitted. Submit articles to: Introduction Editor Different from the abstract in that it “sets the stage” for the content of the article, rather than telling the reader what it is about. Main body May incorporate subtitles, artwork, photos, etc. The Saudi Aramco Journal of Technology C-86, Wing D, Building 9156 Dhahran 31311, Saudi Arabia Tel: +966-013-876-0498 E-mail: [email protected] Submission deadlines Conclusion/summary Assessment of results or restatement of points in introduction. Endnotes/references/bibliography Use only when essential. Use author/date citation method in the main body. Numbered footnotes or endnotes will be converted. Include complete publication information. Standard is The Associated Press Stylebook, 49th ed. and Webster’s New World College Dictionary, 5th ed. 86 WINTER 2014 SAUDI ARAMCO JOURNAL OF TECHNOLOGY Issue Paper submission deadline Release date Summer 2015 Fall 2015 Winter 2015 Spring 2016 March 1, 2015 June 1, 2015 September 1, 2015 December 1, 2015 June 30, 2015 September 30, 2015 December 31, 2015 March 31, 2016 Additional Content Available Online at: www.saudiaramco.com/jot.com First Successful Proppant Fracture for Unconventional Carbonate Source Rock in Saudi Arabia Nayef I. Al Mulhim, Ali H. Al-Saihati, Ahmed M. Al-Hakami, Moataz M. Al-Harbi and Khalid S. Al-Asiri ABSTRACT Widely recognized as the world leader in crude oil production, Saudi Aramco has only recently begun to explore for unconventional gas resources. Saudi Aramco started evaluating its unconventional reservoirs to meet the anticipated future demands for natural gas. One of the subject plays that is currently being evaluated is a carbonate source rock with nanoDarcy permeability and very low porosity. The target formation has few, if any, analogs that can be used for comparison. Knowledge of the formation characteristics, geomechanics, stimulation response and production potential has been nonexistent until recently. Well Site Energy Harvesting from High-Pressure Gas Production Dr. Jinjiang X. Xiao, Wessam A. Busfar, Rafael A. Lastra and Muhammad Adnan ABSTRACT Chokes are control valves built into the production systems so that wells can be produced at desired rates, while at the same time reservoir depletion and sweep can be optimized, and formation and well completion integrity can be protected. The use of surface chokes also allows surface flow lines and facilities to be designed more economically due to reduced pressure ratings. Substantial pressure drops can occur through well surface chokes, especially at early stages of production when the reservoir pressure is still high and lower choke settings are applied. This article investigates energy loss through wellhead chokes for gas wells, with attention to the laws of thermodynamics. Optimization and Post-Job Analysis of the First Successful Oil Field Multistage Acid Fracture Treatment in Saudi Arabia Tariq A. Al-Mubarak, Majid M. Rafie, Dr. Mohammed A. Bataweel, Rifat Said, Hussain A. Al-Ibrahim, Mohammad F. Al-Hajri, Peter I. Osode, Abdullah A. Al-Rustum and Omar Al-Dajani ABSTRACT Multistage acid fracture treatments are utilized in low permeability carbonate reservoirs (permeability <10 millidarcies (mD)) to stimulate the formation by creating highly conductive fractures in the formation and bypassing near wellbore damage. The fracture is generated at high pressures, which are required to break the rock open, while using a viscous pad. The fracture is then kept open by adding gelled or emulsified acid to create uneven etches on the surface of the fracture. Microgravity Flood Front Monitoring: Reducing Inversion Ambiguity by Use of Simulation A Priori Data Stig Lyngra, Dr. Gleb Dyatlov, Dr. Alberto F. Marsala, Antonius M. (Ton) Loermans, Dr. Yuliy A. Dashevsky, Alexandr N. Vasilevskiy, Dr. Carl M. Edwards and Dr. Daniel T. Georgi ABSTRACT Traditional areas using gravimetry methods are surface gravity for mining and oil exploration and bulk density borehole gravity logging. Large-scale reservoir saturation monitoring is a new application. Substitution of oil or gas by water leads to density changes in large reservoir volumes, which causes time-dependent gravity field changes. This article presents a time-lapse gravity data inversion problem for a complex reservoir. The customary bitmap approach requires many input parameters and results in a well-known inversion ambiguity. The same ambiguity in this work was reduced by introducing a priori information obtained by biasing the inversion with history matched reservoir simulation data. On the Cover Multiple FIB-SEM images were used to construct a 3D characterization for different rock properties in a short turnaround time. Representative 3D FIB-SEM images were used to quantify mineralogy, organic matter and porosity. The 3D volume shows organic matter in green, connected porosity in blue and disconnected porosity in red. Organic matter and porosity for shale gas samples were characterized by multi-scale imaging technology. High resolution FIB-SEM images were utilized to link between mineralogy, porosity and flow properties. AT T E N T I O N ! M O R E S A U D I A R A M C O J O U R N A L O F T E C H N O L O G Y A R T I C L E S AVA I L A B L E O N T H E I N T E R N E T. Additional articles that were submitted for publication in the Saudi Aramco Journal of Technology are being made available online. You can read them at this link on the Saudi Aramco Internet Website: www.saudiaramco.com/jot The Saudi Aramco Journal of Technology is published quarterly by the Saudi Arabian Oil Company, Dhahran, Saudi Arabia, to provide the company’s scientific and engineering communities a forum for the exchange of ideas through the presentation of technical information aimed at advancing knowledge in the hydrocarbon industry. EDITORIAL ADVISORS (CONTINUED) P R O D U C T I O N C O O R D I N AT I O N Sami A. Al-Khursani Richard E. Doughty Program Director, Technology Ammar A. Nahwi DESIGN Manager, Research and Development Center Pixel Creative Group, Houston, Texas, U.S.A. Waleed A. Mulhim Manager, EXPEC ARC Complete issues of the Journal in PDF format are available on the Internet at: http://www.saudiaramco.com (click on “publications”). SUBSCRIPTIONS Send individual subscription orders, address changes (see page 85) and related questions to: Saudi Aramco Public Relations Department JOT Distribution Box 5000 Dhahran 31311, Saudi Arabia Website: www.saudiaramco.com EDITORIAL ADVISORS CONTRIBUTIONS Relevant articles are welcome. Submission guidelines are printed on the last page. Please address all manuscript and editorial correspondence to: EDITOR William E. Bradshaw The Saudi Aramco Journal of Technology C-86, Wing D, Building 9156 Dhahran 31311, Saudi Arabia Tel: +966-013-876-0498 E-mail: [email protected] Vice President, Southern Area Oil Operations Ibraheem Assa´adan Unsolicited articles will be returned only when accompanied by a self-addressed envelope. Executive Director, Exploration President & CEO, Saudi Aramco Abdullah M. Al-Ghamdi Nasser A. Al-Nafisee General Manager, Northern Area Gas Operations Executive Director, Corporate Affairs Salahaddin H. Dardeer Essam Z. Tawfiq Zuhair A. Al-Hussain Manager, Jiddah Refinery ISSN 1319-2388. Khalid A. Al-Falih General Manager, Public Affairs © COPYRIGHT 2014 A R A M C O S E R V I C E S C O M PA N Y ALL RIGHTS RESERVED No articles, including art and illustrations, in the Saudi Aramco Journal of Technology, except those from copyrighted sources, may be reproduced or printed without the written permission of Saudi Aramco. Please submit requests for permission to reproduce items to the editor. The Saudi Aramco Journal of Technology gratefully acknowledges the assistance, contribution and cooperation of numerous operating organizations throughout the company.