Flow measurement in liquid metals using Lo- rentz
Transcription
Flow measurement in liquid metals using Lo- rentz
Flow measurement in liquid metals using Lorentz force velocimetry: laboratory experiments and numerical simulations Dissertation zur Erlangung des akademischen Grades Doktoringenieur (Dr.-Ing.) vorgelegt der Fakultät für Maschinenbau der Technischen Universität Ilmenau von Frau Dipl.-Ing. Dandan Jian geboren am 13.08.1978 in LiaoNing/China Acknowledgements I would like to express my immense pleasure to thank my supervisor Dr. Christian Karcher for the guidance and supporting throughout the research during the past years. He was always ready to discuss my work, but let me free to pursue my own goals in my own way. It has been a great pleasure to have him as a mentor. Thanks for his valuable suggestions, constructive criticism, and his great patience during the correction phase of this dissertation. His continued support led my future self-development to the right path. Also I would like to remark upon his recognition, trust, and career advancement to me. I would also like to express my sincere gratitude to Prof. Peter Ehrhard, not only for taking his enthusiasm for my work, but also for organizing a very interesting scientific talk on my studies in his institute. Moreover I appreciated the many discussions with him, in which he was always full of ideas. Furthermore, it is a pleasure to thank Prof. Klaus Zimmermann for his kind willingness to referee this thesis and to take part in the examination committee. Thank him also for providing constructive suggestions for presentation of research results. Last but not the least, I would like to express my sincere gratitude to Prof. Andre Thess, director of the institute of Thermodynamics and Fluid Mechanics, for giving me the opportunity to start research in the topic Time-of-Flight Lorentz Force Velocimetry and for expanding my horizon in science and business. The support provided by Dr. Christian Resagk is also acknowledged for his moral aid, his motivation and technical advice over the past years. I benefited immensely from the collaboration with Jörg Schumacher and Steffen Badtke. It is in my opinion a rare privilege to discuss ones ideas at the time they are being formed with someone able of grasping them in full and providing feedback. With both I could discuss all my work in depth and they contributed numerous useful ideas. Furthermore I gratefully acknowledge the discussions with my students Alexander Schäfer, Sebastian Schädel that contributed to the research reported in this thesis. Also, I thank them for their assistance in the laboratory experiments. Finally, special thanks goes to my husband Jörg Schumacher for understanding and encouragement, my sister Weiwei Jian, who has always stand by me and my parents, who are proud of me and I express my deepest thank for their unlimited patience. The author gratefully acknowledges the financial support from the Deutsche Forschungsgemeinschaft (DFG) in the framework of the Research Training Group “Lorentz Force Velocimetry and Lorentz Force Eddy Current Testing” (grant GRK 1567) as well as by Bundesministerium für Bildung und Forschung (BMBF) within the ForMaT2 program. Ilmenau, Nov. 2012 Dandan Jian Abstract Non-contact flow measurement in hot and aggressive metallic melts is a big challenge in metallurgic processes including continuous casting of steel and production of secondary aluminum, among others. Due to aggressiveness of metal melt, only non-contact measurement methods can be applied. Lorentz Force Velocimetry (LFV) is an electromagnetic measurement technique to meet these challenges. LFV is based on the principle of magnetofluiddynamics (MFD). A respective flow meter which exploits these principles consists of a magnet system with an attached force sensor that records the accelerating force produces by the flow. This electromagnetically induced force is proportional to the flow rate or the local velocity in the vicinity of the magnet system. A drawback of LFV is that the measured force depends on both the electrical conductivity of the fluid and the strength of the externally applied magnetic field. Therefore, an elegant method to circumvent this deficit is the so-called Time-ofFlight technique. During this technique two identical Lorentz force flow meters are arranged one behind the other separated by certain distance. Time-of-Flight Lorentz Force Velocimetry (ToF LFV) senses the passage of the triggered vortices at LFV 1 and measuring the time that the vortices need to travel to LFV 2. In this case the flow rate may be purely determined by cross-correlating the force signals provided by the two flow meters. The objective of the present investigation is to demonstrate experimentally that ToF LFV could be a promising tool for measuring the local velocities and flow rates in liquid metal flows. This thesis presents a series of experiments; first of all, the flow rate measurements in the turbulent liquid metal flow were performed on experimental facility EFCO (Electromagnetic Flow Control Channel). Furthermore, a special measuring device termed Meniscus Velocity Sensor (MVS) relying on ToF LFV technique has been designed to record local surface velocities in metallic melts. The method has been successfully tested using both solid body movement and liquid metal Ga68%In20%Sn12% on annulus channel LiMeSCo (Liquid Metal Surface Velocity Correlation Measurement). In more detail, test measurements under industry-relevant conditions using both metallic melts Sn32%Pb52%Bi at about 210°C and steel at about 1700°C were to be reported. Finally, to each experiment we present results of numerical simulations in order to get a deeper insight in the physical principles of the magnetofluiddynamics. Zusammenfassung Die Durchflussmessung von heißen und aggressiven Metallschmelzen ist eine große Herausforderung bei metallurgischen Prozessen, Beispiele hierfür sind das Stranggießen von Stahl und Produktion von Sekundär-Aluminium. Aufgrund der Aggressivität von Metallschmelzen kommen vorrangig berührungslose Messmethoden in Betracht. Die Lorentzkraft-Anemometrie (LKA) ist ein vielversprechendes Messverfahren, um diesen Herausforderungen gerecht zu werden. Das Verfahren beruht auf den physikalischen Prinzipien der Magnetofluiddynamik (MFD). Die für diese Arbeit genutzte und auf den MFD Prinzipien basierende Strömungsmesser, sogenannte Lorentzkraft-Anemometer bestehen aus einem Magnetsystem und einem Kraftsensor. Der Sensor misst die durch die Bewegung der elektrisch leitfähigen Metallschmelze durch das Magnetfeld induzierte elektromagnetische Lorentzkraft. Diese ist proportional zum Durchfluss oder der lokalen Geschwindigkeit in der Nähe des Magnetsystems. Ein Nachteil der Messanordnung besteht darin, dass die Lorentzkraft abhängig von der elektrischen Leitfähigkeit des Fluides und der Stärke des von außen angelegten Magnetfeldes ist. Eine Methode, dieses Defizit zu umgehen, ist die sogenannte Time-of-Flight Technik (ToF-LKA). Hierbei sind zwei Anemometer hintereinander mit einem bestimmten Abstand angeordnet. Diese detektieren den Durchgang einer Struktur oder einer Störung in der Strömung und misst die Zeit, die die Wirbel zum Durchlaufen des Abstandes benötigen. Aus dieser Laufzeit kann auf die Strömungsgeschwindigkeit geschlossen werden. Die Laufzeit wird durch die Bildung der Kreuzkorrelation der Kraftsignale der beiden Anemometer bestimmt. Das Ziel der vorliegenden Arbeit ist es, experimentell nachzuweisen, dass die ToF-LKA ein vielversprechender Ansatz zur berührungsfreien der Strömungsmessung in Metallschmelzen ist. Diese Arbeit stellt eine Reihe von experimentellen Untersuchungen vor. Zu Beginn wird die Durchflussmessung in einer turbulenten FlüssigmetallKanalströmung durchgeführt. Im Weiteren werden die Untersuchungen auf Flüssigmetallströmung an der Oberfläche ausgeweitet. Hier ist die lokale Geschwindigkeitsmessung an der Oberfläche von Interesse. In diesem Experiment wird das niedrigschmelzende Flüssigmetall GaInSn verwendet. Basierend auf diesen Messungen wird ein spezielles Messgerät entwickelt, um lokale Oberflächengeschwindigkeiten in heißen Metallschmelzen zu erfassen. Mit diesem Sensor werden, Testmessungen unter industrienahen Bedingungen mit der Metallschmelze (SnPbBi) bei ca. 210°C und mit geschmolzenem Stahl bei ca. 1700°C durchgeführt. Zu jedem Experiment wird das Ergebnis numerischer Simulationen präsentiert, um ein besseres Verständnis der Magnetofluiddynamik herzustellen. List of abbreviations LFF LFV LKA ToF LFV EFCO LiMeSCo MVS EMP CCS MFD SEN CFD FVM LES RANS DNS WALE GaInSn UDV US Lorentz force flow meter Lorentz Force Velocimetry Lorentzkraft-Anemometrie Time-of-Flight Lorentz Force Velocimetry Electromagnetic Flow Control Channel Liquid Metal Surface velocity Correlation measurements Meniscus Velocity Sensor Electromagentic pump Continuous Casting of Steel Magnetofluiddynamics Submerged Entry Nozzle Computational Fluid Dynamics Finite Volume Method Large Eddy Simulation Reynolds Averaged Navier-Stokes Direct Numerical Simulation Wall-Adapting Local Eddy Viscosity Galinstan-gallium, indium and tin Ultrasonic Doppler Velocimetry Ultrasound Nomenclatures B B0 b E j FL fL U UA V Vvortex Re Recrit Red Rem Rec Ha N MaM Cf x Magnetic field [T] Imposed magnetic field [T] Induced magnetic field [T] Electric field [V/m] Electric potential [V] Electric current density [A/m2] Lorentz force [N] Body force / Lorentz force density [N/m3] Averaged velocity [m/s] Alfven velocity [m/s] Flow velocity [m/s] Vortex velocity [m/s] Reynolds number Critical Reynolds number Reynolds number of duct flow Magnetic Reynolds number Cylinder Reynolds number Hartmann number Interaction parameter Magnetic Mach number Drag force coefficient Cf y Lift force coefficient C jy Coefficient of eddy current density µ0 υ ρ m M σ dH L0 L H S h A H D a β f Q Magnetic field constant [H/m] Kinematic viscosity [m2/s] Density [kg/m3] Magnetic dipole moment [A/m2] Magnetic diffusivity [m2/s] Electrical conductivity s / m Hydraulic diameter of duct flow [m] Characteristic length of free surface flow [m] Characteristic length [m] Thickness of Hartmann layers [mm] Thickness of Shercliff layers [mm] Deformation of the free surface [mm] Edge length of the cubic magnet [mm] Height [mm] Distance [mm] Diameter of the submerged cylinder [mm] Blockage ratio of the cylinder Angle of the submerged cylinder [°] Rotation frequency of the pump [Hz] Volumetric flow rate [m3/s] Contents Acknowledgements....................................................................................................................... I Abstract ......................................................................................................................................... II Zusammenfassung...................................................................................................................... III List of abbreviations .................................................................................................................. IV Nomenclatures ............................................................................................................................ V 1 Introduction......................................................................................................................... 1 1.1 A qualitative overview ................................................................................................. 1 1.2 Problem and motivation .............................................................................................. 3 1.3 State of the art in the flow rate and local velocity measurement ................................ 6 1.4 Lorentz Force Velocimetry and Time-of-Flight Lorentz Force Velocimetry .............. 10 1.5 Objective and scope ................................................................................................. 13 2 Governing equations of magnetofluiddynamics ........................................................... 15 2.1 A brief review of electrodynamics ............................................................................. 15 2.2 A brief review of fluid mechanics .............................................................................. 18 2.3 Dimensionless parameters ....................................................................................... 19 2.4 Dimensionless equations.......................................................................................... 23 3 Electromagnetic flow rate measurement in turbulent liquid metal duct flow ............ 25 3.1 Introduction ............................................................................................................... 25 3.2 Using Lorentz Force Velocimetry ............................................................................. 26 3.2.1 Experimental results .................................................................................. 26 3.2.2 Numerical simulations ............................................................................... 27 3.3 Using Time-of-Flight Lorentz Force Velocimetry ...................................................... 31 3.3.1 Experimental results .................................................................................. 32 3.3.2 Numerical simulations ............................................................................... 37 4 Electromagnetic free surface velocity measurement in annulus flow ........................ 44 4.1 Introduction ............................................................................................................... 44 4.2 Metallic body experiments ........................................................................................ 45 4.2.1 Experimental results .................................................................................. 45 4.2.2 Numerical simulations ............................................................................... 55 4.3 Liquid metal free surface experiments ..................................................................... 57 4.3.1 Experimental results .................................................................................. 57 4.3.2 Numerical simulations ............................................................................... 61 5 Application of ToF LFV to free surface velocity measurement in metallic melt ........ 72 5.1 Introduction ............................................................................................................... 72 5.2 State of the art of surface velocity sensor for melt flow ............................................ 74 5.3 A sensor for high-temperature surface velocity measurement................................. 77 5.4 Preliminary test measurement under industry-relevant condition ............................ 84 5.4.1 Open channel flow measurement using SnPbBi at 210°C ........................ 84 5.4.2 Open channel flow measurement using steel at 1700°C .......................... 87 5.5 Sub-summary ........................................................................................................... 91 6 Conclusion and outlook .................................................................................................. 93 List of figures.............................................................................................................................. VI Bibliography ............................................................................................................................. XIII Appendix .................................................................................................................................. XXII A1 Physical properties of liquid metals ................................................................................ XXII A2 Experimental matrix for open channel flow measurements ........................................ XXIII A3 Strain gauge force sensor ...............................................................................................XXIV A4 Error estimation of experiments .....................................................................................XXVI 1 1 Introduction 1.1 A qualitative overview Non-contact flow control and flow measurement in hot and aggressive metal melts are big challenges in metallurgic processes including continuous casting of steel [1] [55] and production of secondary aluminum [2] [56] [71], among others. Another example is the production of float glass [3]. During this process, flow control in the tin bath, upon which the glass is solidifying, is crucial for the quality of the final product. In most cases, non-invasive control methods are favorable since at high temperatures metal melts are chemically very aggressive. Electromagnetic methods are promising tools since metal melts are both non-magnetic and excellent electrical conductors. One of these electromagnetic methods is Lorentz Force Velocimetry (LFV) [4] [5] [6] [7] [77]. LFV is a noncontact electromagnetic measurement technique and suitable for velocity and flow rate measurement in high temperature metallurgical processes. This measurement technique exploits the principles of magnetofluiddynamics (MFD) [8] [9], as it is sketched in Fig.1. When an electrically conducting fluid like a metal melt crosses the field lines of a primary magnetic field B0 produced by an external magnet system, eddy currents j are generated within the melt. The eddy currents mainly flow in the direction that is perpendicular to both the magnetic field and the melt velocity. The eddy currents induce their own magnetic field, the so-called secondary magnet field b that adds to the applied primary one. Physically speaking, the magnetic field lines are slightly bent by the flow, see Fig. 1. The interactions of the eddy currents with the magnetic field give rise to the generation of Lorentz forces FL within the melt. The Lorentz force is proportional to both velocity or flow rate and electrical conductivity of the melt. The force tends to brake the flow. A well-known industrial application of these effects is the electromagnetic brake (EMBR) [10] [75] used during continuous casting of steel. LFV is based on measuring the counterforce of this braking Lorentz force which acts on the magnet system in the streamwise direction. This force is called Kelvin force. In a physical sense, this force results from the flow-induced secondary magnetic field that pulls at the magnet system. A respective flow sensor that operates according to this principle is called Lorentz force flow meter (LFF). It basically consists of a magnet system and an attached force sensor. 2 Fig. 1: Principle of Lorentz Force Velocimetry. It is based on measuring the Kelvin force that pulls at an externally arranged magnet system. The Kelvin force is the counteracting force to the Lorentz force that is generated in the melt due to the movement of the electrically conducting melt through the magnetic field. However, in metallurgic processes, the conductivity is often unknown or hard to evaluate as it strongly depends on both temperature and composition of the liquid metal alloy. To overcome this problem a modification of LFV has been elaborated, namely, Time-of-Flight Lorentz Force Velocimetry (ToF LFV) [26] [27]. Using this technique, two Lorentz force flow meters are arranged in a row and separated by a defined distance D. This Time-of-Flight technique can be employed for the flow measurement by purely cross-correlating the two force signals recorded by the two flow meters, see Fig. 2. Therefore, the measurement becomes independent of any fluid properties and magnetic field parameters. Fig. 2: Principle of Time-of-Flight Lorentz Force Velocimetry. Two Lorentz force flow meters are arranged one behind the other. This flow measurement technique is based on just cross-correlating the force signals recorded by the two flow meters. The method is independent of melt properties and magnetic field parameters. The main goal of this thesis is to check experimentally the potential of LFV and ToF LFV for flow measurement in metallurgical application. However, industrial 3 scale experiments with hot metallic melts are expensive and difficult to perform. To eliminate this problem at first we propose small-scale model experiments using the low-melting liquid metal GaInSn. This model melt is ideally suited for laboratory experiments as it is liquid at room temperature and non-toxic. Here we employ LFV and ToF LFV for flow rate measurement in turbulent channel flow carried out in a closed liquid metal loop. As a flow driving device we use a frequency controlled electromagnetic pump. Both Vives probe [15] [60] [61] and Ultrasonic Doppler Velocimetry (UDV) are utilized [17] [62] [63] [64] as reference flow measurement techniques. Moreover, using ToF LFV we perform measurements of local velocities in liquid metal free-surface flow. The respective test facility consists of an annulus gap filled with liquid metal GaInSn and put into a controlled rotation by an electrical motor. Finally, the model experiments result in the development of a prototype of an electromagnetic surface velocity sensor based on ToF LFV and capable of measuring locally freesurface velocities in high-temperature metallic melts. This prototype has been tested in free-surface open channel flows of both PbBiSn at 210°C and steel at 1700°C. The prototype is shown to detect motion of liquid metal flow from a few cm s-1 up to 0.65 m s-1. All the experimental investigations are supported by accompanying theoretical studies that are based on numerical simulations using commercial codes. 1.2 Problem and motivation A considerable part (about 80%) of the aluminum demand in the world is satisfied through secondary aluminum production [2] [56]. For the secondary production of aluminum, materials containing aluminum such as scrap, machining turnings, and dross are prepared, smelted and refined. A sketch of the production line is shown in Fig. 3. Rotary drum and melt furnaces are used to melt down aluminum scrap and materials containing aluminum. Typical melting temperatures are around 700 to 750 °C. After tagging, the primary melt, driven by gravity, is transferred via open-channel flow into converters for further treatment like refining, mixing, and alloying with silicium (Si) or other metals such as copper (Cu), magnesium (Mg), manganese (Mn) and zinc (Zn). The final aluminum alloy is also transferred in open channels -the so-called launders- to the casting machine where it is subsequently cast into bars or directly processed in molten form in the foundry. Nowadays, the production process is controlled only by weighing the scrap at the beginning and the final product by the end of the process. Until now, however, no in-situ mass flux or flow rate measurement technique is available for high-temperature liquid metal melt. 4 Fig. 3: Secondary aluminum production process. The aluminium melt flux is indicated by blue arrows. Scrap is melted in furnaces. The primary melt is delivered to converters within which the final melt is prepared. The figure is taken from Ref. [71] (in German). The information about the scrap performance as well as the amount of the alloying elements to be put into the converter cannot be evaluated exactly. The goal of the present study is to demonstrate of the feasibility of the non-contact electromagnetic measurement techniques of LFV and ToF LFV to measure the flow rate in such channel flows. In an aluminium recycling plant LFFs may be installed at the launders to register the flow rate during the transfer of the melt from the furnaces to the converter and further to the tundish and the casting machine. The second technical application which we deal with is to measure the molten steel flow in continuous casting of steel production. Demand for high-quality steel product is continuously increasing. In continuous casting process [1] [55], the molten steel is poured in to the mold through the submerged entry nozzle (SEN) which is set in the center plane of the mold, see Fig. 4. As thermal insulator mold powder is put on the free surface (meniscus), serving as lubricator to the mold wall and an adsorbent of impurities. Argon gas is injected into the nozzle to prevent clogging. Controlling the meniscus molten steel flow in the mold is one of the keys to achieve good quality of the slab, because the impurities are sometimes trapped from the free surface. The molten steel flow in the mold is classified into two patterns. One is a double roll flow pattern and the other is a single roll flow pattern, see the right picture in Fig. 4. 5 Fig. 4: Meniscus flow in Continuous Casting of Steel (left). Double and single roll flow pattern (right). The figure is taken from Ref. [55]. In the double roll flow pattern, the molten steel flows from the nozzle to the narrow side of the mold. Then, some flows upward and some flow downward. At the meniscus the molten steel moves from the narrow side of the mold to the nozzle. In general, the double roll flow pattern appears when the molten steel throughput is high or the mold width is narrow. In this case, mold powder is trapped by the strong meniscus flow or meniscus level fluctuations generating surface defects. On the other hand, when the molten steel throughput is low or the mold width is wide, the molten steel occurs with ascending argon gas near the nozzle and the molten steel moves from the nozzle to the narrow side of the mold at the meniscus. It is called a single roll flow pattern. When the flow pattern is a single roll structure, molten steel flows from the nozzle does not reach the narrow side of the mold and the temperature fall down at the mold corner of the meniscus. Then, the slab corner might be cracked or the impurity carried into the molten steel, which leads to the surface defects. In order to decrease the defects on the slab and control the molten steel flow, various techniques imposing of magnetic field system have been developed. In the present thesis we report on the design of a non-contact electromagnetic meniscus velocity sensor based on ToF LFV that allows detecting both the magnitude and direction of the flow near the free surface. Thus, the sensor may register the flow pattern in the entire mold. In Fig. 4 we show schematically such a sensor as it is place in some distance above the melt surface. 6 1.3 State of the art in the flow rate and local velocity measurement Precise and reliable velocity measurement is required during casting in metallurgy process [1] [2]. A number of flow measurements methods in electrically conducting fluids have been developed over the past decades. These methods can be divided into (integral) flow rate measurement methods and (local) velocity measurements. Flow rate measurement Flow rate measurements in liquid metals are required in various technological processes ranging from the cooling of nuclear reactors to the dosing and casting of molten metals. A variety of electromagnetic flow meters have been developed starting from the late 1940s and described by Shercliff [23]. Commercially available electromagnetic flow meters typically use a pair of electrodes in direct contact to the liquid to measure the potential difference induced by the electrically conducting fluid moving through a static magnetic field. This approach is now well developed and works reliably for common liquids like water etc., but not so for liquid metals. Major problem in molten metals, especially at higher temperatures, is that electrodes are not resistant against the chemically aggressive liquid metals. Alternatively, the liquid metal flow can be determined in a contactless way by eddy-current flow meters, which determine the flow rate by sensing the flowinduced perturbation in an applied magnetic field. The magnetic fly wheel is such a flow meter which was invented by Shercliff [23] and employed by Bucenieks [11] [57] [58]. It consists of permanent magnets, which are mounted on an axle and placed close to a tube carrying the liquid metal flow; see the left picture in Fig. 5. The disk rotating rate is proportional to the flow rate. Fig. 5: Magnetic fly wheel (left). Single-magnet rotary flow meter (right). The figure is taken from Ref. [11] and [12]. Priede [12] [59] suggested an alternative design of such a flow meter, which uses just a single magnet mounted on the axle and which can freely rotate 7 around and the axis perpendicular to the direction of the magnetization, see the right picture in Fig. 5. In contrast to fly wheel, which is driven by the electromagnetic force acting on separate magnets, the single magnet is set into rotation only by the electromagnetically induced torque. This driving torque is due to the eddy currents induced by the flow across the magnetic field. As the magnet starts to rotate, additional eddy currents are induced, which break the rotation. An equilibrium rotation rate is attained when the braking torque balances the driving one, and this rate depends only on the flow velocity and the flow meter arrangement, whereas it is independent of the electromagnetic torque itself as well as the electrical conductivity of the melt. The rotation rate of the magnet was measured by an inductive magnetic proximity sensor. The main problem with this type of flow meters is the weak magnetic field perturbation which may be caused not only by the flow. Recently a new flow rate measurement method was developed which show that the flow-induced phase shift of alternating magnetic field (AC) [13] is more reliable for flow rate measurements. The phase disturbance is found to be more robust than that of the amplitude perturbation used in conventional eddy-current flow meters. The flow rate is determined by applying a weak AC magnetic field to a liquid metal flow and measuring the flow-induced phase disturbance in the external electromagnetic field, see Fig. 6. This flow meter employs the fact that the flow of a conducting liquid disturbs not only the amplitude but also the phase distribution of an applied AC magnetic field. The asymmetry of the phase distribution caused by the fluid motion can be used to determine the velocity. However, similar to standard eddy-current flow meters, phase-shift sensor is still sensitive to the electrical conductivity, thus, to the temperature of the liquid. Fig. 6: Contactless electromagnetic phase-shift flow meter for liquid metals. The figure is taken from Ref. [13]. 8 Local velocity measurement Information about local velocity in conducting fluids was obtained by various types of local probes. For instance, hot-wire and hot-film sensors by Hill and Sleicher [83] in mercury and by Platnieks and Uhlmann [84] in sodium. Permanent magnet probes were developed by Ricou and Vives [60] and Von Weissenfluh [85]. However, the described technology above reveals considerable limitations. For instance, it is intrusive but not absolutely contactless. Moreover, the short lifetime of the sensor probe limits the application potential of this method [14]. The principle of the Vives probe measurement [15] [60] [61] is governed by Ohm’s law. The probe is immersed in the molten metal at the location where the velocity is to be measured. The permanent magnet creates a magnetic field and the movement of electrically conducting liquid through this field generates an electric field, which is measured by the four electrodes lying on alongside the magnet, see the left picture in Fig. 7. The potential difference between diagonally placed sensing electrodes, which is measured by a nano-voltmeter, is proportional to the flow velocity. Vives Probe is not to be applied in high-temperature metallic melt because of his limitations of Curie temperature (570 K neodymiumiron-boron magnets to 1120 K Alnico magnets). Fig. 7: Design of Vives Probe (left) and Potential Probe (right). The figure (right) is taken from Ref. [54]. The technical principle of the potential probe [16] [51] [52] [53] [54] is governed also by the Ohm´s law in moving fluids. The probe consists of four copper wire electrodes insulated by a varnish except the sensitive tips which are in direct contact with the liquid metal. The probe provides the electric potential differences between the measuring electrodes in spanwise and streamwise directions see the right picture in Fig. 7. In recent years, ultrasound technique has drawn much attention as a nonintrusive and non-invasive measurement method due to its attractive advantages over the conventional techniques. The principle of the Ultrasound 9 Doppler Velocimetry (UDV) [17] [62] [63] [64] method is to use the pulsed echo signal of ultrasound wave and to detect the same signal reflected by the moving particles suspended in the fluid flow. The delay time between emission of ultrasound pulse and reception of the corresponding echo signal provides the distance of the particle, while the corresponding Doppler shift provides its velocity, see Fig. 8. The limitations of the application UDV in liquid metal flow are such as multiply reflection at the wall. Another problem is the wetting of the sensor by the liquid metal for achieving a sufficient acoustic coupling and the allocation of suitable tracer particles. Fig. 8: The US transducer is submerged at an angle of 60° into the liquid metal duct EFCO (left). Multiple reflections of US wave may result in imaginary velocity values outside the region of the liquid flow (right). The right figure is taken from Ref. [17]. The typical problem for UDV applications is multiple reflections of the Ultrasonic wave. As shown the right picture in Fig. 8, the US beam is reflected by the opposite channel wall in point B and transforms this interface in the transmitter. Consequently, a particle contained in the liquid moving along the dashed line may backscatter Doppler energy more than once in the direction of the transducer (at points A and C). The depth associated with the reflection at point C is located outside the flow region. Imaginary velocity component are added to the real velocity profile. The velocity measurement near the wall is affected by this phenomenon. Therefore, it is common to obtain a non-zero velocity at the far wall. 10 1.4 Lorentz Force Velocimetry and Time-of-Flight Lorentz Force Velocimetry Recently, we suggested a new electromagnetic non-contact technique, termed Lorentz Force Velocimetry (LFV), for measuring local surface velocity and flow rates in electrically conducting fluids, as well as in high-temperature metallic melts. LFV is based on the principles of magnetofluiddynamics [8] [9]. A Lorentz force flow meter measures the electromagnetically induced force acting on a magnet system that produces the magnetic field with which the flow field interacts. Hence, such a LFV basically consists of a magnet system -preferably built up by an arrangement of permanent magnets- and an attached force sensor. The force recorded by the force sensor is proportional to the product of the electrical conductivity of the fluid σ, the square of the typical applied magnetic field strength B0, and the flow rate Q or the typical flow velocity U. The scaling law between force F and flow rate Q is given by the relations FL QB 02L or FL VB 02L3 , (1), (2) where L denotes a characteristic electromagnetic interaction length. See chapter 2.1 for the theoretical derivation of these equations. An enlarged view of the magnetic field within the Lorentz force flow meter is shown in Fig. 9. Fig. 9: Principle of Lorentz Force Velocimetry for the measurement of flow rate (left) and local surface velocities (right). The difference between flow rate and local velocity measurement using LFV techniques depends on the variety of alignment of the magnet system. In case for measuring the flow rate we use big-size magnet systems of which the magnetic field penetrates the entire cross-section of the flow, see left picture in Fig. 9. In this case we have a relatively large characteristic length L. On the other hand, for local velocity measurement we may use small-size cubic permanent magnets of which the magnetic field penetrates only a small flow volume adjacent to the surface, see the right picture in Fig. 9. This case corresponds to a relatively small value of L. 11 However, in the latter case we expect that another characteristic length enters into the problem: the height H, at which the magnet is arranged above the surface, as it mainly influences the magnitude of B0, see right picture in Fig. 9. To analyze this dependence in some more detail, we consider a cubic small permanent magnet with edge length A and dipole moment m. The magnet is located at distance H above a semi-infinite fluid moving with uniform velocity u parallel to its free surface. 3 H m B The magnetic field, which we refer to as the primary field B0, is of the order at the surface of the fluid. The order of magnitude of the induced 3 H m u B u j 0 0 0 0 eddy currents is given by . The eddy currents are con centrated below the surface, and interact with the primary field to produce a Lorentz force density of the order fL jB 0 02 um 2H6 . Since the force acts on a volume H3, the total Lorentz force is FL f LH3 and we have FL 02 um 2 . H3 (3) From this formula we can draw the following conclusions [5]: (i) F is proportional to the product of velocity and electrical conductivity. (ii) F increases with the second power of the magnetization. (iii) F decreases with third power of distance. A drawback of LFV is that the measured force depends on various other quantities like electrical conductivity, geometry parameters L, H and magnetic parameters, see Eqs. (1)-(3) listed above. Therefore, intense calibration of Lorentz force flow meters is necessary to find the device constants under various flow conditions, magnetic properties and geometry parameters. An elegant method to circumvent this deficit is the so-called Time-of-Flight LFV [26] [27]. ToF LFV rely on the fundamental measurements of time and distance and do not require calibrating for individual applications. This feature contrasts strongly with another commercial electromagnetic flow meters which have to be individually calibrated for the specific pipe size in use. Here, we just measure the flow by using two LFFs that are arranged one behind the other and that sense the passage of the any vortex structures that are transported by the flow. In more detail, ToF LFV measures the flow by sensing the passage of the triggered vortices at LFV 1 and measuring the time that the vortices need to travel to LFV 2 with the typical velocity Vvortex. In Fig. 10 we have sketched such an arrangement for the case of flow rate measurement (left picture) and the case of local surface velocity measurement (right picture). 12 Fig. 10: Principle of Time-of-Flight Lorentz Force Velocimetry for the measurement of flow rate (left) and local surface velocities (right). The transit time of a tagging signal flowing through the two flow meters is determined by cross-correlating the voltage data provided by the two force sensors. With the separation distance D between the LFVs and the measured transit time at hand, the vortex Velocity Vvortex, correlating with the typical flow velocity V, can easily be calculated by Equations (4) and (5). Vvortex D , (4) V k 2 Vvortex , (5) Q k1 A Vvortex . (6) The flow rate can be determined by Equations (4) and (6). Here, k1 and k2 are calibration constants and A denotes cross-section of the flow. Mathematically, the transit time is obtained by evaluation the cross-correlation function R12() [73] using the raw voltage signals U1(t) and U2(t) provide by the two force sensors. The cross-correlation function is defined by the Equation (7) R12 ( ) 1 T U1t U2 ( t ) dt . T 0 (7) Cross-correlation techniques [28] [66] [67] [68] are based on measuring the transit time of tagging signals (turbulence, clumps of particles, etc.) in the flow between two axially separated sensors. Such techniques are well known from the use of hot-wire anemometry for the measurement of two-point velocity correlations [29]. Cross correlation is more directly used where measurements are the knowledge of time delays required, such as velocity measurement of steel [82]. 13 1.5 Objective and scope The thesis aims to summarize the fundamental as well as application-oriented research on global and local flow measurement in model experiments applying LFV, see Fig. 11 for an overview. In a first series of global flow rate measurements, employing the closed-loop test facility EFCO (Electromagnetic Flow Control channel) and utilizing both LFV and ToF LFV, we determine the volumetric flow rate Q by evaluating equations (4) and (6) and using magnet systems of which the magnetic field penetrates the entire cross-section of the flow. Vortex structures are triggered by submerging a cylinder in the flow. Flow control may be managed by adjusting the power of the respective flow-driving unit represented by an electromagnetic pump (EMP). The experimental set-up is shown in the left picture in Fig. 11. In a second series of local velocity measurements, exploiting the test facility LiMeSCo (Liquid Metal Surface velocity Correlation measurements), we apply as well the ToF LFV to determine free surface velocities. Here, we evaluate equations (4) and (5) and use small-size cubic permanent magnets of which the magnetic field penetrates only a small flow volume adjacent to the surface. To check the potential of the method, in a first step, we apply the technique to solid metal bodies that are put into controlled rotation. In this case, the calibration constant k2 is equal to unity, cf. Eq. (5). In a second step, we conduct freesurface liquid metal experiments using low-melting eutectic alloy GaInSn. Vortex structures are generated intrinsically as the used magnets themselves act as a magnetic obstacle [39] [70]. In this case, we expect that the calibration constants k2 will considerably deviate from unity. Local control shall be achieved by coupling the force measurements with electromagnetic actuators that manipulate the local flow field in a favorable manner. The experimental set-up is shown in the middle picture of Fig. 11. Moreover, a special prototype of a respective measuring device, called Meniscus Velocity Sensor (MVS), has been developed to measure local free-surface velocity in high-temperature metallic melts. In Fig. 11 the prototype is shown in the right picture. To check the functionality of the ToF LFV, in a first step we measure surface velocities during rotation of metallic substances. We observe that small fluctuations in the signals that are due to the natural inhomogeneity of the solid body can be used to determine surface velocities. In a second step we apply the technique to liquid metal free-surface flow. Here we use the liquid metal GaInSn as model liquid. In this case we observe that the crosscorrelations between the signals are much rarer and much weaker than in the solid-body cases. In more detail, we present test measurements under industryrelevant conditions using both SnPbBi at about 210°C and molten steel at about 1700°C. These experiments were conducted at Key Laboratories on EPM at North Eastern University. The evaluation of the data shows that our prototype of MVS works well in producing signals of which surface velocity can be determined. Nevertheless, there is still a big gap between the research development and the industrial application in real production process [81]. 14 Fig. 11: Sketches of the experimental facility EFCO (left) for flow rate measurements, LiMeSCo for surface velocity measurement (middle), and MVS for measurement of surface velocity in high-temperature metallic melt (right). The main goal of the present study is to demonstrate experimentally that ToF LFV is suited for the non-contact measurement of both flow rates and local surface velocities in liquid metal flow. In order to support the experimental observations, at the end of each chapter, the predictions of corresponding numerical simulations using commercial codes and simplifying assumptions were presented. This thesis is organized as follows. The principle of LFV and ToF LFV are introduced in details in chapter 1.4. In chapter 2, we will provide the theory of fundamental magnetofluiddynamics. The test facility EFCO and the results of respective flow rate measurements are described in chapter 3. In chapter 4 we are concerned with free-surface liquid metal measurement on test facility LiMeSCo and discuss the results of local velocity experiments. Studies concerning the electromagnetic surface velocity measurement for high-temperature metallic melt are reported in chapter 5. Main conclusions and perspectives are drawn in chapter 6. It should be mentioned that due to the significance to metallurgic application most of the results shown in this thesis have been pre-published in peer-review scientific journals. These articles are given in Refs. [27] [30] [31] [32] [33] [78] [79]. Therefore, some parts of these papers have been taken into this thesis. 15 2 Governing equations of magnetofluiddynamics In this chapter we would like to present the theoretical background of this thesis. Magnetofluiddynamics (MFD) is a science that covers phenomena and interactions resulting from the coupling of the velocity field u of on electrically conducting fluid and a magnetic field B. Hence, we have to consider the governing equations of both fluid mechanics and electrodynamics, i.e. the Navier-Stokes equations [42] and the Maxwell equations [46], respectively. The aim of this chapter is to provide the reader with the physical and mathematical information that serves to explain the experimental findings and that represents the basis of the numerical simulations shown in sub-chapters 3.2.2, 3.3.2, 4.2.2 and 4.3.2. The governing equations of MFD are well known since the pioneering works of the Danish physicist Julius Hartmann on experiments in liquid metal channel flow affected by a uniform magnetic field [47] [48] and of former Swedish Nobel Prize winner Hannes Alfven [43] on the existence of electromagnetichydrodynamic waves (later on referred to as Alfven waves, cf. chapter 2.4). More recently, a number of famous textbooks on this subject have been published including the standard books of Shercliff [23] [44], Roberts [49], Moreau [8], Davidson [24], and Asai [45], among others. Therefore, in this chapter we only give a brief review of the fundamental MFD relations that are already well documented in the literature listed above. Our focus shall be to point out the application of these relations towards LFV. 2.1 A brief review of electrodynamics In the following we consider the general equations of the electrodynamics of continuous conducting media under the assumption that electrical displacement currents generated by a time-dependent electrical field are much smaller than any current related to the flux of electrical charge carriers. Moreover, we assume that all fluid velocities are small compared to the speed of light. Both assumptions are well met in the present case of liquid metal flow. Within these assumptions the Maxwell equations can be written in the following form. Btj 0 . 0 B B E , , (8) (9) (10) Here, Eq. (8) represents Faraday’s law. It denotes that due to a time-dependent magnetic field B, a vortical electrical field E is induced. This law is also referred to as the induction law. Furthermore, Eq. (9) describes Ampere’s law. It denotes that an electrical current density j generates a vortical magnetic field. In Eq. (9) µ0 is the magnetic field constant given by µ0 = 4 x 10-7 H/m. Finally, Eq. (10) is 16 the so-called Gauss’ law. It states that the magnetic field is divergence-free, i.e. that any magnetic flux entering a volume is equal to the flux exiting the volume. Taking the divergence of Eq. (9) it easily follows that the electrical current density is also a solenoidal field, i.e. . 0 j (11) This set of Maxwell equations is accompanied by a constitutive law –called Ohm’s law– that expresses the capability of an electrically conducting substance to transport electric charge. Under the assumptions that the material is isotropic and that the transport is dominated by conduction rather than convection, Ohm’s law writes as follows. j E U B . (12) Here, denotes the electrical conductivity of the material. Physically Eq. (12) reveals that in a conductor an electrical current density -the so-called eddy current density- is driven by an electrical field E and/or is induced due to the movement of the conductor through a magnetic field whenever the vectors u and B are non-parallel. Concerning LFV where we face liquid metal channel flow or free-surface flow affected by superimposed spatially localized magnet fields, from Eqs. (11), (12) we can conclude that in bulk flow regions within which the imposed magnetic field is present, eddy currents are mainly generated by the u x B term. On the other hand, in the vicinity of non-conducting rigid walls, where velocity is significantly reduced, or in regions within which the magnetic field is absent, the electrical field E is the dominant driving mechanism for electrical currents. It ensures that the current path lines are closed. As we shall see later on, the eddy current distribution in the melt mainly controls the distribution of the induced electromagnetic forces, cf. Eq. (15). Unfortunately, in our test experiments on LFV we cannot measure j. Therefore, to get a better understanding in the physical principles we also perform simulation to determine j numerically. Using some elementary rules of vector calculus, Eqs. (8)-(12) can be combined to yield the following magnetic field transport equation, also known as the induction equation, which is an expression relating magnetic field B to velocity u. B t 1 2 (U ) B B (B ) U 0 Advection of Stretching of Time dependence of magnetic field magnetic field Diffusion of magnetic field (13) magnetic field Magnetic field transport equation describes the change in the magnetic field due to the fluid flow. Here, the left hand side represents the total rate of change of B due to the effects of time-dependence of the field (first term) and its advection by the flow field (second term). Moreover, the first term on the right denotes the diffusion of B within the conducting material while the second term describes the generation of B in a shear flow. In Eq. (13), the pre-factor 1/( 0 ) = M is the material property called magnetic diffusivity. As all diffusion coefficients, its dimension is given in [m2/s]. A typical value for liquid metals -that shall exclu- 17 sively be considered in this thesis- is M = 1 m2/s. Hence, in liquid metal MFD the magnetic fields are typically highly diffusive. As a physical consequence, the magnitude of any magnetic field perturbation induced by the flow remains small as it is rapidly diffused. That means that the usually strong imposed magnetic field is only weakly influenced by the flow. In this case the coupling of the u field to the B field remains also small. We will see later on that this weak coupling is due the small values of the magnetic Reynolds number. Please note that in Eq. (13) B denotes the total magnetic flux density. For the application of this equation to LFV it is instructive to split the magnetic field in the primary externally applied static magnetic field, B0 say, and in the secondary field, b say, that is induced by flow due to the generation of eddy currents. Thus we write B x , y , z; t B0 x , y , z b x , y , z; t . (14) Finally we finish this sub-chapter by introducing another very important constitutive relation that expresses a fundamental effect of MFD being the physical basis of the LFV measuring technique investigated in this thesis: The movement of an electrical conductor (liquid metal flow) through a magnetic field generates a force density within the conductor. This force density, resulting from the interaction of the induced eddy current density j and the magnetic field B, is called Lorentz force density fL and can be calculated using the relation fL j B . (15) As seen from Eq. (15) this body force is acting in the direction which is perpendicular to both j and B. If we plug in Ohm’s law, i.e. Eq. (12) into the above formula we can draw three important conclusions for the application of this interaction to LFV: (i) The magnitude of the Lorentz force density is scaling according to the relation . 2 B U fL (16) Here, U is a characteristic velocity of the flow. (ii) In the bulk region the Lorentz force density is pointing in the negative flow direction. Hence, the induced Lorentz forces tend to brake the flow as we have e fL eu . (17) where e denotes the respective unit vector. (iii) In regions adjacent to non-conducting walls or a free surface, the eddy currents have to change their direction in order to form closed loops. By that, also the Lorentz force changes its direction. In these regions we ex- 18 pect a strong component pointing into the normal direction of the wall or the surface as well as a weak component pointing into the positive flow direction, i.e. pushing the flow. LFV is based on measuring the counter force to the Lorentz forces generated in the liquid metal. This force -the so-called Kelvin force- acts on the magnet system that produces the primary magnetic field superimposed to the flow. As obvious from Eq. (16), upon measuring this force we are able to get information about the flow velocity U and/or the volumetric flow rate Q = UA. Moreover, the measured quantity, i.e. the force, is directly proportional to the unknown quantity to be determined, i.e. U and/or Q. From a point of view of measurement technology, this is an ideal constellation. Furthermore, Eq. (16) reveals, that the magnitude of the measured force is proportional to the electrical conductivity of the melt and the square of the magnetic field strength. 2.2 A brief review of fluid mechanics The flow field u of a Newtonian simple and isothermal fluid is governed by the Navier-Stokes equations. These equations comprise balances of both mass and momentum. In case of an incompressible fluid with constant density these equations write as follows. U 0, (18) U t (19) Unsteady acceleration 1 1 2 (U ) U P U (jB ) friction Convective Viscous force acceleration Pr esseure gradient Density of Lorentz force Here ρ is the fluid density, denotes its kinematic viscosity, and p is fluid pressure, respectively. Eq. (18) is the so-called continuity equation that expresses the physical fact that the flow field is divergence-free. The physical meanings of the various terms within the momentum balance, i.e. Eq. (19), are explicitly described. In contrast to ordinary fluid mechanics, in the case of MFD, we have to take into account the Lorentz force density which presents the Lorentz force per unit volume as an additional source term on the right hand side of the momentum balance. During LFV, where strong magnetic fields are of interest, we expect that the generated electromagnetic forces are relatively strong. Hence, LFV is characterized by strong coupling of the u field to the B field. This means that the electromagnetic forces are able to significantly modify or change the flow structure. In the next sub-chapter we shall see that the strength of this coupling can be quantified using the dimensionless groups of Hartmann number and interaction parameter that measure the magnitude of the electromagnetic force in units of the viscous friction force (2nd term on the right of Eq. (19)) and the inertia force, respectively. The latter force on the left of Eq. (19) is denoted by its synonym, i.e. convective acceleration. 19 As we have already mentioned before, both the magnitude and the direction of the induced electromagnetic force are controlled by the eddy current distribution. Using the arguments (i)-(iii) listed in the sub-chapter 2.1 we conclude that applying LFV we may expect the following modification to an ordinary flow profile: (i) The bulk velocity will be significantly reduced due to the braking action of strong electromagnetic forces. (ii) In turn, due to continuity, cf. Eq. (18), the velocity in the wall regions must significantly increase. (iii) This formation of boundary layers near the walls is supported by the electromagnetic force acting in these regions as they tend both to push fluid towards the wall and to accelerate the flow. A more detailed study of these effects is given by Müller & Bühler [25]. 2.3 Dimensionless parameters Based on the governing MFD equations derived above we can deduce the dimensionless parameters that control LFV and reflect all the physical phenomena described so far. Formally, these parameters can be set up by evaluating and comparing the order of magnitudes of the various terms occurring in the governing equations. In a first step, we introduce characteristic scales for length, velocity, time, pressure, and magnetic flux density. We choose x, y, z L, (u, v, w ) U, t L / U, p U2 , (B x , B y , B z ) B0 . (20)-(24) By that the scales for the electrical current density and the electrical field are also fixed. We obtain j UBo , E UB0 . (25), (26) We now introduce these scales into the induction equation (13) governing the magnetic field and the Navier-Stokes equation (19) governing the flow field. Physically, Rem is the ratio of the time scales of diffusion of the magnetic field d L2o due to the fluid motion across the magnetic field lines and the time scales of advection of the magnetic field a L U . This parameter is defined by .M / L U L U 0 eM R (27) 20 Having in mind that the total magnetic field consists of a primary and a secondary field, cf. Eq. (14), we also can write . B0 / b eM R (28) This definition shows that the magnetic Reynolds number can be interpreted as the ratio of the strengths of the magnetic field induced by the flow and the externally applied magnetic field. In liquid metal applications, including LFV, ReM is small due to the high magnetic diffusivity (M 1 m2/s) and limitations in both U and L. Typically we have ReM 10-2. Therefore, upon calculating the Lorentz force density according to Eq. (15) it is physically justified to neglect the contribution of the induced field. In this case -referred to as the quasi-static approximation- the governing MFD equations can be considerable simplified, see next sub-chapter 2.4. This is in contrast to geophysical and astrophysical MFD phenomena where the typical length scales and therefore the respective magnetic Reynolds numbers are extremely high [50]. In this case there exists a very strong coupling of the B field to the u field. We now turn to the Navier-Stokes equation (19) and take the ratio of the inertia force and the friction force. This ratio defines the Reynolds number Re given by . / L U e R (29) Physically, the Reynolds number characterizes different flow regimes, i.e. laminar or turbulent flow. When its value is less than a certain threshold, i.e. Re < Recrit, the flow is laminar characterized by smooth and steady fluid motion due to the relative dominance of momentum diffusion. On the other hand, when Re ˃ Recrit, the flow is called turbulent flow and is dominated by advection of momentum which tends to trigger random eddies, vortices, and other flow instabilities. In the present case of liquid metal flow applied to LFV, we are mostly in the turbulent regime. In our laboratory experiments we will typically have Re 1.6 x 104. Here, the large Re values are due to the small kinematic viscosity of liquid metals, typically being of the order 10-7 m2/s. Large Reynolds numbers indicate that friction forces are only significant in thin layers adjacent to rigid walls. Within this so-called boundary layer the flow velocity has to drop from the value in the inviscid bulk to zero right at the wall. In turbulent flow the typical thickness of such a boundary layer is of the order /L Re-1/5. .M / rM P Upon taking the ratio of the parameters ReM and Re we obtain the magnetic Prandtl number PrM. We find (30) Hence, the magnetic Prandtl number represents the ratio of two diffusion coefficient of the melt, i.e. the kinematic viscosity being responsible for diffusion of momentum and the magnetic diffusivity. Using the typical values for and M of a liquid metal, we obtain PrM 10-7. This indicates that the diffusive length and time scales in liquid metals differ extremely. Up to now in numerical simulations it is not possible to simultaneously resolve both diffusive fields in a physical 21 way. In liquid metal flow we can elegantly circumvent this problem by applying the quasi-static approximation within which the induced magnetic field must not be calculated. We consider again the Navier-Stokes equation (19) and take the ratio of two typical time scales. The first one, t say, is set by the friction force and is given by t (L3/(U))1/2. The second one, t say, is related to and the electromagnetic force and can be written as t (L/(UB02)1/2. The ratio of these time scales defines the Hartmann number Ha. We obtain . L B0 a H (31) More physically, Ha2 denotes the relative strength of the electromagnetic force and the viscous force. In our experiments with liquid metals we typically have Ha2 104. This relatively high value indicates that the electromagnetic forces clearly dominate viscous friction. This is clearly the case in the inviscid bulk region of the flow. However, as stated before, near solid walls friction becomes important. Hence, adjacent to walls we expect thin electromagnetic boundary layers within which there is a balance of both forces. Such layers are referred to as Hartmann layers of thickness H at walls perpendicular to the applied magnet field and Shercliff layers of thickness S at walls parallel to the applied magnetic field. The respective scaling of these layers is given by the relations H/L Ha-1 and S/L Ha-1/2. Finally, within Eq. (19) we take the ratio of the electromagnetic force and the inertia force. By that we obtain the electromagnetic interaction parameter N, sometimes also called the Stuart number. This parameter is defined as . L 20 U B 2 e a HR N (32) In our experiments we shall typically have N 1, i.e. both forces are of the same order of magnitude. Physically this means that the induced electromagnetic forces are strong enough to re-shape the flow structure significantly. We expect that this flow shaping effect is more pronounced while the flow Reynolds number is decreased. In this thesis we investigate experimentally and numerically turbulent liquid metal channel flow and turbulent liquid metal free-surface flow affected by strong localized magnet fields that are produced by the magnet systems of various Lorentz force flow meters. According to the relative values of the MFD parameters defined above we expect the following configurations. (i) The case of channel flow: in regions in front of the magnetic field we shall have a turbulent hydrodynamic flow profile characterized by an almost constant velocity in the bulk and thin viscous boundary layers near the walls. Upon entering the magnetic field this flow profile will be signifi- 22 cantly re-shaped due to the high Hartmann number and an interaction parameter of order unity. Due to the braking Lorentz forces the bulk velocity will be considerable reduced. Fluid is pushed towards the walls. Here we expect jet-like flow structures. Upon exiting the magnet field the re-shaped remains nearly unchanged due to the high-Reynolds number. (ii) The case of free-surface flow: the flow will tend to by-pass the region within which the magnetic field is present. This is the so-called magnetic obstacle effect that have been intensively studied both experimentally and numerically, see [38] [39] for reference. Hence the surface flow velocity underneath the magnet will be considerably reduced. In turn, jetlike flow is expected aside of the magnet. Again, due to the high Reynolds number the electromagnetic wake that is formed by the magnet will persist far in the downstream direction. Moreover, we will expect to detect large deformations of the free surface and the formation of surface waves due to the high Hartmann number and an interaction parameter of order unity. In the following table we summarize the main dimensionless parameters discussed above. Parameter Symbol Definition Physical Significance Typical Values of experiments Magnetic Reynolds Rem number Interaction N Parameter d a UL advection of B0 diffusion of B0 10-2 Ha 2 Re B02 L U Lorentz force inertia 1 Hartmann number B0 L Lorentz force viscous force inertia viscous force Ha 12 UL Reynolds Re number u Magmetic viscous diffusion Re m Prandtl Prm magnetic diffusion M Re number Table 1: Essential dimensionless parameters in MFD. 102 1.6 x 104 10-7 23 2.4 Dimensionless equations By using the scalings given in Eqs. (20)-(26) we can transform the governing equations into a dimensionless form. In the following we would like to give two representations. The first one refers to the full MFD case characterized by a small but infinite magnetic Reynolds number. In this case the full magnetic induction equation is considered. The second representation refers to the quasistatic approximation. Here, upon taking the limit ReM << 1, the induced magnet field must not be calculated. Instead, a Poisson equation for the scalar electric potential has to be considered. Both representations of the sets of equations are implemented in the commercial program package FLUENT which will be used later on for conducting the numerical simulations. The set of the full MFD equations is given by the following relations. U 0, B 0, (18) (10) U 1 2 Ha B B , U U p U t Re Re Re M B 1 (U ) B (B ) U 2B . t ReM 2 (33) (34) Here we have used Ampere’s law (cf. Eq. (9)) to eliminate the electric current density in the Lorentz force term, i.e. the last term in Eq. (33). Interestingly, in this term the parameter group Ha2/(ReReM) appears. Using the definitions of we can rewrite this group to obtain Ha, Re, and ReM 2 2 2 2 2 2 Ha Re ReM N ReM B0 0 U UA U MaM , where UA = B0(µ0)-1/2 is the Alfven velocity representing the propagation velocity of electromagnetichydrodynamic waves and MaM U UA is the so-called magnetic Mach number. In liquid metal MFD we typically find that MaM is much less than unity. Physically this means that the magnetic field lines are very stiff and can only slightly be bent by the flow. The problem of the above representation is that we have to equip Eq. (34) with proper boundary condition for the induced magnetic field b, cf. Eq. (14). The physically correct one would be the far-field condition b 0 as x . This means that the induced magnetic field vanishes far away from the location where it is created, i.e. far away from the fluid region within which the superimposed primary magnetic field is present. However, in numerical simulations the computational domain must be kept infinite. Therefore, in the used program package Fluent a default boundary condition is implemented that sets the tangential components of b to zero at the fluid boundaries. By that only the fluid domain has to be considered. Less problematic are the boundary conditions for the velocity field u. Along with velocity inlet and a pressure outlet condition we choose the no-slip condition at rigid walls and the stress-free condition at the free surface. 24 Within the quasi-static approximation the governing MFD equations read as U 0, (18) U 1 2 U U p U N U B 0 B o , t Re (35) 2 U B 0 (36) Here B0 denotes a given primary magnetic field distribution normalized by a characteristic value B0. Moreover, we have introduced the electric potential as within the quasi-static approximation the electric field is curl-free and can be represented by the gradient of a scalar, i.e. E = -. The electric potential is governed by a Poisson equation, cf. Eq. (36). Physically, this equation expresses that the electric current density field is divergence-free, cf. Eq. (11). Here, the gradient of the electromotive force u B0 acts as a source term. Hence, a strongly vortical applied magnetic field or a flow with a high vorticity is needed to feed the potential. During LFV both conditions are met. In this representation, along with the same hydrodynamic boundary condition as above, now we have to formulate boundary condition for . In case of an electrically non-conducting wall or a free-surface the electric current cannot penetrate into the wall or cross the surface. Hence normal derivative of is zero. At the inlet and the outlet can be set to be zero. As it can be seen from Eqs. (35)-(36), by applying the quasi-static approximation we have derived a considerable simplification compared to the full MFD case. Instead of solving the unknown vector field b we just have solve the scalar field determined by a Poisson equation. Moreover, we have got rid of the extremely different diffusive length and time scales set by and . Finally, without any restrictions the computational domain is given by the fluid region as physically correct electromagnetic boundary condition can be applied at all fluid boundaries. 25 3 Electromagnetic flow rate measurement in turbulent liquid metal duct flow 3.1 Introduction Electromagnetic flow rate measurements are carried out in the test facility EFCO. The experimental set-up is shown in Fig. 12. The facility consists of a closed channel with rectangular cross-section of height × width = 80 × 10mm2 corresponding to a hydraulic diameters of dH = 18mm. Each Lorentz force flow meter consists of two block-type permanent magnets of height × width × thickness = 100 × 30 × 20mm3 that produce a magnetic induction about 300mT at their inner surfaces corresponding a Hartmann number of 140. The magnets are connected by an iron yoke that guides the magnetic flux density. A force sensor is mounted on the yoke to record the force that the fluid exerts on the magnet. Fluid flow is driven by a frequency-controlled electromagnetic pump (EMP) based on rotating permanent magnets. Moreover, the facility is equipped with a Vives probe to measure the local velocity in the mid plane of the channel and an Ultrasonic Doppler Velocimetry to measure velocity profile across the height of the channel. The low-melting liquid metal GaInSn was applied as working medium. Its temperature is measured by a submerged thermocouple and regulated at 20°C by a water-cooled heat exchanger. Fig. 12: Set-up of test facility EFCO for non-contact flow rate measurement in turbulent liquid metal flow using single LFV. 26 3.2 Using Lorentz Force Velocimetry 3.2.1 Experimental results In this chapter a summary of the experimental results of non-contact flow rate measurements using single Lorentz Force Velocimetry was provided. The channel is equipped with a single LFV consisting of two permanent magnets that generate a localized spanwise magnetic field. Attached to the magnetic system is a force sensor that records the Kelvin force acting in the streamwise direction. In Fig. 13, the measured Lorentz force is plotted as a function of the volumetric flow rate. We observe that at low and moderate flow rates there is a linear relation between the measured force and the flow rate. This finding corresponds exactly to the scaling law according to Eq. (1-2). However, at higher flow rate values, we find a deviation from the linear behaviour: upon increasing volumetric flow rate Q, there is only a slight increase of the corresponding Lorentz force. We attribute this experimental result mainly to fact that in this regime, saturation of the EPM may take place. Fig. 13: Lorentz force FL as a function of volumetric flow rate Q. Fig. 14 shows results of UDV measurements at rotation frequency of EMP at 25Hz corresponding to a Reynolds number of 1.6 ×104. Here, the streamwise velocity is plotted versus the depth of the channel. When the EPM operates in the counterclockwise mode, we detect a purely hydrodynamic turbulent flow profile characterized by a nearly constant bulk velocity and sharp gradients near the top and bottom of the channel. On the other hand, in the case of clockwise EPM operation mode, a typical M-shaped MFD profile is registered. Here, the bulk velocity is reduced due to the braking Lorentz forces. However, according to the principle of mass flux conservation, fluid is pushed aside. Within this socalled side layers (at top and bottom of the channel) the induced electric eddy currents turn to loop back. The generated Lorentz forces basically act in the 27 side layers supporting the pushing. This is a well-known finding is MFD flow with electrically insulating side walls. Fig. 14: Velocity profiles at the mid plane of the channel measured by UDV. Counterclockwise mode: turbulent hydrodynamic profile. Clockwise mode: M-shaped MFD profile. The reason why we do not find the velocity going to zero at the bottom of channel wall are considered to be occurrence of multiple reflections of ultrasonic beam on the channel walls. The detail explanation about this effect was described in chapter 1.2. 3.2.2 Numerical simulations To support the experimental findings we perform numerical simulations using the commercial code ANSYS/FLUENT. We consider turbulent liquid metal channel flow affected by a localized constant magnetic field that is pointing in the spanwise direction (positive z-direction), see Fig.15. The geometry of the channel for the numerical simulation is identical to the experimental set-up. Here, we simultaneously solve the Navier-Stokes equations and the magnetic induction equations. These equations are fully coupled via the Lorentz force term in the Navier-Stokes equations (19) and the effects of advection-stretching of magnetic field lines by the flow in the induction equation (13). As appropriate hydrodynamic boundary conditions we use no-slip conditions at rigid channel walls, a turbulent purely hydrodynamic flow profile as an inlet condition, and a zero-pressure as outlet condition. Furthermore, as electrodynamic boundary conditions, we choose electrically insulating channel walls, as well as perfectly 28 conducting interfaces at the entrance and exit planes of the magnetic field. It is to be noticed, at these planes the tangential component of the induced magnetic field is set to be zero. Fig. 15: Numerical simulation for Re = 1.54 x 106 and Ha = 140. Top graph: geometry of the channel wall. Bottom graph: velocity profiles in entrance, inside, and at the exit of the magnet field. We observe that the initially hydrodynamic profile is reshaped under the influence of the localized magnetic field. In accordance with the measurements we find a considerable reduction of the bulk velocity and the pushing of fluid into the side layers, see Fig.15. At the walls perpendicular to the magnetic field, socalled Hartmann layers [25] [65] are formed, the thickness Ha of which scaling according to the relation Ha/dH Ha-1. (37) In the Hartmann layers the velocity sharply increases from zero at the wall to the almost constant value in the core. As we shall see later on, in these layers strong eddy currents are induced that are flowing in the opposite direction than in the core in order to form closed loops. Hence, the Lorentz forces act as a flow driving mechanism contributing to the creation of such thin Hartmann layers. The transversal electric current of maximal intensity is generated in the central area of the gap between the magnetic poles due to the interaction of the horizontal component of magnetic field with the streamwise component of the flow velocity. So far as the electrical current must close outside the region of magnetic field, it changes its direction from spanwise to streamwise near the side walls. By virtue of this effect, the streamwise component of the braking Lorentz force is higher in the mid plane of the magnet gap compared to the value in the 29 vicinity of the sidewalls. It is characterized by low values of velocity in the central part of the channel and two strong maxima near the sidewalls. Such kind of velocity profile is usually referred to as an M-shaped profile. [25] The flow profile deformations described above can physically be understood by analyzing the flow paths of the induced electric eddy currents. The results are shown in Fig. 16. Here, the magnitude of eddy current density is plotted in the xy plane at position z = 0, i.e. at mid plane of the channel. The flow comes from positive x-direction. The region, within which the localized magnetic field is present, is marked by red lines. The magnetic field points out of the paper plane. Fig. 16: Induced eddy currents in the region of the localized magnetic magnetic field. We observe that inside the magnetic field region strong eddy current are flowing in the negative y-direction. However, in the side layer the eddy currents turn their direction. Here, the currents basically flow in the streamwise direction (xdirection) and loop back outside the magnetic field region. Hence, also the Lorentz forces shall change direction, acting basically in the y-direction. The simulations results correspond well to the experimental investigation using UDV, see Fig.14. A three-dimensional picture of the eddy currents paths at half-height of the channel is shown in Fig. 17. As stated before, we observe that near the Hartmann walls which are perpendicular to the magnetic field, strong eddy currents are flowing in the positive y-direction. The interaction of these currents with the magnetic field causes the formation of thin Hartmann layers while fluid is accelerated by the generated Lorentz forces. 30 Fig. 17: Eddy currents in the region of the localized magnetic field at half-height of the channel. Fig. 18 shows the Lorentz forces density generated within the region of the localized magnetic field at half-height of the channel. As discussed before, we observe that in the core region the Lorentz forces act as a braking force while in the Hartman layers they act as a flow driving force. Fig. 18: Lorentz force density in the region of the localized magnetic field at half-height of the channel. 31 Fig. 19: Lorentz force density in the region of the localized magnetic field at the mid plane of the channel. Finally, Fig. 19 shows the Lorentz force density within the region of the localized magnetic field at the mid plane of the channel. We observe the braking effect of the Lorentz forces within the core region of the flow. Moreover, we observe that near the top and bottom of the channel the Lorentz forces act towards the walls contributing to the formation of the M-shaped velocity profile within these side layers. The numerical results demonstrate that the main contributions to the integral Lorentz force measured by the flow meter come from the entrance and exit regions of the localized magnetic field. In this region, the strongest braking forces are induced. In the core region of the magnetic field, the braking Lorentz forces are much weaker and may completely be compensated by the accelerating forces in the Hartmann layers. 3.3 Using Time-of-Flight Lorentz Force Velocimetry In the second step we extend the experimental investigations to ToF LFV, using the same test facility EFCO. Here, two identical Lorentz force flow meters are arranged in a row and separated by a certain distance D, see Fig. 20. The measurement principle is described in chapter 1.3. In the experiments we vary the rotation frequency of EMP and the separation distance of the two flow meters. We determine the volumetric flow rate Q by using magnet systems of which the magnetic field penetrates the entire cross-section of the flow. The magnet has a flux density B of 200 mT on its surface. Vortex structures are triggered by submerging a cylinder in the flow. The measured velocity range 0 ≤ u ≤ 32 cm/s. Therefore, the corresponding ranges of Reynolds and Hartmann numbers are Re = [0, 1.6 x104] and Ha = 140, respectively. 32 3.3.1 Experimental results The present study compares the measured correlation time (transit time) with the mean convective time which the ratio of distance D between the two flow meters and the velocity V of the flow. Most of results about ToF Lorentz force flow meter in this chapter have been published in the scientific journal “Measurement Science and Technology”, see Ref. [27]. Fig. 20: Set-up of the test facility EFCO for non-contact flow rate measurement in turbulent liquid metal flow using Time-of-Flight Lorentz Force Velocimetry. Fig. 21 shows velocity profiles across the depth of the channel measured by UDV. Here, the rotating frequency of EMP is fixed at f = 25Hz. The distance between two flow meters keeps at D = 220mm. This corresponds to a mean velocity of about 32cm/s and a duct flow Reynolds number of Red = 1.64 × 104. Hence, we are in the regime of fully turbulent liquid metal channel flow. 33 Fig. 21: Velocity profiles at the mid plane of the channel measured by UDV. The green curve gives the profile when both flow meters are present. The blue curve gives the profile when LFV 2 was removed. When the second flow meter is removed, the single LFV results [32] [33] are retained, cf. blue curve. In this case, a typical M-shaped MFD profile is registered. Due to the second flow meter, the M-shape profile becomes even more pronounced, cf. green curve in Fig. 21. This indicates that a turbulent flow profile that is already shaped by MFD effects is very sensitive to the presence of a second localized magnetic field. For instance, due to the second magnetic field, the core velocity decreases by a factor of 2 while the peak velocity in the side layer increases by a factor of 3. Moreover, the side layer becomes thinner. One may expect that the profiles are symmetric with respect to the half-height of the channel at 40mm (total height of the channel 80mm). Unfortunately the used ultrasound transducer cannot resolve properly the region close to the bottom of the channel due to undesired reflections on the bottom wall. Details of the UDV measurements are given in [34]. Our experiment procedure results in evaluating the travelling speed Vvortex = D/, cf. Eq. (4), of any vortex structure that are present in the flow. To increase the rate of such vortex structures and likewise the rate of usable signals, cf. Eq. (7), a cylindrical obstacle is submerged into the flow. Such cylindrical obstacles are commonly used in vortex flow meter devices [35] [69]. The used cylinder has a diameter of a = 8mm and is submerged at an angle of = 60° to the horizontal direction. This corresponds to a submerged length of 100mm. Here the angle of 60° is experimentally pre-fixed for the UDV measurement; see the left picture in Fig. 8. Due to the restriction of experimental set-up, measurements using both 34 UDV and submerged cylinder cannot be performed simultaneously. In the present experiments the cylinder serves to trigger vortex structures that may be first registered by LFF 1 and then by LFF 2. Fig. 22: Flow velocity (in m/s) in the horizontal plane at y = 2.5mm around the cylinder submerged at an angle of = 60° into the flow. Parameters are Red = 1.6 x 104, ReC = 7.42 x 103, and the blockage ratio of the cylinder of = 0.8. To illustrate the effect of the cylinder on the flow we perform purely hydrodynamic 3D numerical simulations using the commercial CFD code ANSYS with LES turbulence modelling. A total of 3 million elements and an extra fine meshing of the cylinder region have been used. As an example, Fig. 22 shows the contours of the velocity magnitude in the cylinder wake at the position y = 2.5mm in the horizontal plane parallel to the bottom of the channel. The flow Reynolds number Red and the cylinder Reynolds number ReC, defined by Re d V dH / , Re C V a / , (38)(39) Respectively, are fixed at Red = 1.65 x 104 and ReC = 7.42 x 103. Here, dH = 18mm is the hydraulic diameter of the channel. In the present case the blockage ratio of the submerged cylinder is = 0.8 as the channel width is 10mm. Here, a fully developed turbulent flow profile is used as an inlet condition. At the outlet a fixed pressure condition is applied. We find that due to the presence of the side walls, the formation of a classical Karman vortex street [36] is suppressed. Instead, generated vortex structures travel in the near-wall jets. A parametric numerical study on this vortex shedding problem with variation of the parameters Red, , and is given in [37]. Figs. 23 and 24 illustrate our procedure to evaluate the transit time. In Fig. 23 we present the raw data of the voltages U1(t) and U2(t) delivered by the strain gauge of LFF1 and LFF 2. Here, signals are shown within a typical time period of 10s for an experimental run for which the rotation frequency of the EMP and the separation distance were fixed at f = 23Hz and D = 170mm. Each run lasts 35 320s. In Fig. 23 the red curve gives the voltage data registered by LFF 1 while the green curve refers to LFF 2. Due to the limitation of the data acquisition system is the sampling frequency in our experiments restricted to 25s-1. 60000 Original signals of LFV1 and LFV2 LFV1 LFV2 58000 56000 Voltage, µV 54000 52000 50000 48000 46000 44000 0,00 0,40 0,80 1,20 1,60 2,00 2,40 2,80 3,20 3,60 4,00 4,40 4,80 5,20 5,60 6,00 6,40 6,80 7,20 7,60 8,00 8,40 8,80 9,20 9,60 10,00 42000 Run time [s] Fig. 23: Raw voltage signals U1(t) and U2(t) delivered by the strain gauge of flow meters LFF 1 and LFF 2 over a period of 10s. Fig. 24: Auto- and cross-correlation functions calculated according to Eq. (7) from the voltage signals U1(t) and U2(t) shown in Fig. 23 above. Experimental parameters are fixed at f = 23Hz and D = 170mm. 36 Fig. 24 shows the auto- and cross-correlation functions obtained by evaluating Eq. (7) and using the voltage data given in Fig. 23. In the respective graphs, the value on the abscissa of the first peak corresponds to the desired transit time . We observe that there is a clear peak at correlation time = 0.24s, see red curve in Fig. 24. The two figures (25) and (26) below summarize the experimental findings. These graphs show the measured interrelation of the flow velocity V and the convective velocity of vortex Vvortex at the two different separation distances D = 170mm (Fig. 25) and D = 220mm (Fig. 26). The data points represent values that have been double-averaged over 20 individual time periods of 10s of each run and a total of 12 experimental runs for each pump rotating frequency. The typical standard deviation is about 10%. As expected, the diagrams indicate a linear behavior between the flow velocity V and Vvortex. Moreover, we observe that when the distance between the two LFFs is increased, the transit time for the vortex structures passing through is extended. However, we find that for each separation distance, the vortex velocity is considerably higher than the velocity of the flow, i.e. Vvortex > V. Furthermore, the slope of the curves is directly representing the calibration constant k2, cf. Eq. (5). We find the values k2 = 1.90 for D = 170mm and k2 = 0.95 for D = 220mm. Hence, the calibration constant decreases with increasing separation distance. We attribute these findings to the facts that due to the submerged cylinder nearwall jets are created that are mainly carrying the vortex structure detected by the flow meters, cf. Fig. 22, and that under the influence of the localized magnetic fields the flow profile is deformed into an M-type shape, cf. Fig. 14 and Fig. 21. At large separation distance the jets may have decayed so that calibration constant approaches unity. Fig. 25: Averaged relation between the vortex velocity Vvortex measured by ToF LFF and the velocity of the flow V measured by UDV and Vives probe. The separation distance is fixed at D = 170mm. The slope of the linear fitting curve is k2 = 1.90. 37 As mentioned before, in these test experiments, the sampling period of the data acquisition system is restricted to 40ms. This may explain the somewhat stepwise distribution of the data points shown in Fig. 26. Moreover, we observe that at larger distances, both the rate and the reproducibility of usable data decreases. We attribute this finding to the fact that any vortex structure generated by the obstacle is strongly re-shaped by the first magnetic field. Therefore, it shall hardly be re-detected by the second LFF. On the other hand, at smaller distances, the two localized magnetic field may overlap; see Fig. 51 in sub-chapter 4.2.2. Fig. 26: Averaged relation between the vortex velocity Vvortex measured by ToF LFF and the velocity of the flow V measured by UDV and Vives probe. The separation distance is fixed at D = 220mm. The slope of the linear fitting curve is k2 = 0.95. 3.3.2 Numerical simulations To support the experimental findings we perform numerical simulations using the commercial code FLUENT. We consider turbulent liquid metal channel flow affected by two localized constant magnetic fields that are pointing in the spanwise direction (positive z-direction). The geometry of the channel is identical to the experimental set-up. Here, we simultaneously solve the Navier-Stokes equations, Eq. (19) and the magnetic induction equations, Eq. (13). Fig. 27 shows the computational domain and the used mesh. A total of 3 million elements have been used. Here, within the volumes Fluid 2 and Fluid 4, a constant transverse magnetic field B0 is applied. Fluid volumes 1 and 5 represent the inlet and the outlet regions, while Fluid 3 is the volume between the two LFFs assumed to be field-free. As appropriate hydrodynamic boundary conditions we use no-slip conditions at rigid channel walls, a turbulent purely hydrodynamic flow profile as an inlet condition, and a zero-pressure outlet condition. Moreover, as electrodynamic boundary conditions, we choose electrically insulating channel walls, as well as perfectly conducting interfaces at the entrance 38 and exit planes of the magnetic field. Furthermore, at these planes the tangential component of the induced magnetic field is set to be zero. In the simulations we apply the WALE-LES turbulence model. Fig. 27: Computational domains and meshes used in the numerical simulations. Within the volumes Fluid 2 and Fluid 4 a constant spanwise magnetic field is applied. In the following we show to the graphical presentation of flow profiles in the x-yplane (at the mid plane of the channel). Fig. 28 and Fig. 29 illustrate the effect of the flow Reynolds number at a fixed value of the Hartmann number Ha =140. The Reynolds numbers are fixed at Red = 2.0×104 (Fig. 28) and Red = 3.0×104 (Fig. 29). Fig. 28: Flow velocities (in m/s) in the mid plane of the channel at Red = 2.0×104 (V = 0.4m/s) and Ha = 140. 39 The flow is from the left to the right. Black vertical lines indicate the regions within which the constant magnetic field is applied. The field points out of the plane. We observe that due to the influence of the first magnetic field, M-shaped flow profiles are formed. Therefore, MFD side layers appear at top and bottom of the channel. Fig. 29: Flow velocities (in m/s) in the mid plane of the channel at Red = 3.0×104 (V = 0.6m/s) and Ha = 140. In the region between the magnetic fields, these profiles remain unchanged. However, upon entering the second localized magnet field, the bulk flow is once more slow and more fluid is pushed into the side layers. By that, the M-shape profile becomes more pronounced. This finding corresponds well with UDV measurements, see Fig. 21. At higher Reynolds number, the braking effect is increased resulting in higher velocity gradients across the height of channel. Fig. 30 shows the effect of the Hartmann number. Here, the parameters are fixed at Red = 3.0 x 104 and Ha = 205. We observe that upon increasing the strength of the magnetic field, the MFD effects increase likewise. The difference between the bulk velocity and velocity in the side layers strongly increases and the thickness of the side layers decreases. 40 Fig. 30: Flow velocities (in m/s) in the mid plane of the channel at Red = 3.0×104 (V = 0.6m/s) and Ha = 205. Finally, Fig. 31 shows some of the calculated profiles at various positions in the streamwise direction. Parameters are fixed at Red = 4.8 x 103 (V = 0.1m/s) and Ha = 205 (B0 = 0.3T). The blue line refers to the turbulent purely hydrodynamic entrance profile. As the flow has passed LFF 1, due to the action of the Lorentz forces it has been transformed into an M-shape profile, see line 2 (green curve). As already stated above, in the field-free region between LFF 1 and LFF 2 this profile is mainly unchanged. We observe a small increase of the bulk velocity, since in this region braking Lorentz forces are absent, see line 3 (red curve). After having passed LFF 2, the profile was once more re-shaped into an M-type form and the bulk velocity has decreased again, see line 4 (black curve). Finally, at the outlet, the profile starts to transform back into a purely hydrodynamic shape. The bulk velocity increases and the side layers start to dissipate. However, the peak velocity in the side layers has increases, see line 5 (orange curve). This prediction is due to the fact that the so-called Hartmann layers rapidly breakdown. These layers are formed adjacent to the side walls of channel that are perpendicular to the magnetic field. By conservation of mass, fluid is pushed into the side layers. These numerical findings qualitatively correspond with the UDV measurements shown in Fig. 21. However, the predicted reduction of the bulk velocity and the increase of the peak velocity in the side layer due to the presence of the second magnetic field are considerably lower than observed in the experiments. We attribute these quantitative deviations to both the limited resolution of the UDV and the simplifications made in the simulations. 41 Fig. 31: Reduced velocity profiles at various positions in the streamwise direction: Line 1: inlet, Line 2: right behind LFF1, Line 3: between LFF1 and LFF2, Line 4: right behind LFF2, Line 5: outlet. The separation distance of the flow meters is D = 150mm. To get more physical insight into the formation of the M-shape velocity profile, Figs. 32 and 33 show the distribution of the induced eddy current density and the resulting distribution of the Lorentz force density in the mid plane of the channel. The flow comes from right to left. Here, LFV 1 and LFV 2 denote the regions within which the localized magnetic field is present. Parameters are fixed at Red = 1.43 x 104 (V = 0.3m/s) and Ha = 68. The separation distance of the flow meters is D = 100mm. Fig. 32: Induced eddy current density (in A/m2) in the mid plane of the channel. The applied localized magnetic fields are pointing out of the plane. 42 According to Ohm´s law, cf. Eq. (12), strong eddy currents are induced within the regions LFV 1 and LFV 2. In the bulk areas of these regions the eddy currents are mainly flowing in the positive vertical direction (positive y-direction), cf. Fig. 32 and Eq. (12). According to Eq. (15), this eddy current distribution gives rise to strong Lorentz forces pointing opposite the flow direction, cf. Fig. 33. Hence, these forces tend to brake the flow and the bulk velocities are considerably reduced. Fig. 33: Lorentz force density (in N/m3) in the mid plane of the channel. The applied localized magnetic fields are pointing out of the plane. Fig. 34 illustrates 3D M-shape velocity profile in stream- (a) and spanwise direction (b). Moreover, due to the solenoidal constraint according to Eq. (11), in the vicinity of the electrically insulation top and bottom wall, the eddy currents must turn into the flow direction. Eventually they loop back inside the liquid within the regions where the magnetic field is absent, cf. Fig. 32. Therefore, in these top and bottom regions, the Lorentz forces change their direction likewise and are mainly pointing into the top and bottom wall, see Fig. 33. This effect reinforces the formation of the M-shape profile. A parametric numerical investigation on the impact of magnetic field penetrating in spanwise direction in turbulent liquid metal duct flow is given in [41]. 43 Fig. 34: Velocity profiles in streamwise direction (a) and in spanwise direction (b). 44 4 Electromagnetic free surface velocity measurement in annulus flow 4.1 Introduction In this chapter we describe experimental results of respective measurements in the test facility LiMeSCo. To demonstrate the general feasibility of Time-ofFlight technique to sense local surface velocities employed miniaturized LFV, in a first step we measure surface velocities during solid-body rotation of metallic substances. We observe that small modulations in the signals that are due to the natural unevenness of the metallic body can be used to determine surface velocities. In a second step we apply the Time-of-Flight technique to liquid metal free-surface flow. Here we use the low-melting eutectic alloy GaInSn as a model fluid. In this case we observe that the cross-correlations between the signals are much rarer and much weaker than in the solid-body experiments. We conclude that the presence of the localized magnetic fields, produced by the permanent magnets of the miniaturized LFV, give rise to intense deformation of the free surface and the creation of surface waves. The field acts as a magnetic obstacle. We observe that the flow velocity is decreased right underneath the magnet and is accelerated in the side regions. A photograph of the experimental test facility LiMeSCo is shown in figure 35. It consists of a ring channel that is put into controlled rotation by an electrical motor. The inner and outer radii of the channel are 17.5cm and 24.5cm, respectively. At a certain height H above the channel, we arrange two small cubic magnets attached with force sensors separated by a certain distance D. Each cubic magnet is with edge length A = 20mm producing a magnetic induction of 270mT at its bottom face. Moreover, the permanent magnets are mounted on strain gauge sensors that record the Lorentz forces generated in the motion of electrically conducting liquid metal. To support these experimental findings we present results of numerical simulations in sub-chapter 4.2.2 and 4.3.2 using the commercial code MAXWELL. 45 Fig. 35: Experimental set-up of test facility LiMeSCo. 4.2 Metallic body experiments 4.2.1 Experimental results On top of the channel there are two solid aluminum sheets of thickness 1.5mm. In one sheet there is a drilling hole of 1mm in diameter. At a certain height H above the channel we arrange a small cubic permanent magnet attached with a force sensor. A blow-up is shown in the left picture in Fig. 36. To check the functionality of the measurement principle and for calibrating purposes, a thin iron wire is tightened across the channel; see the right picture in Fig. 36. Fig. 36: Single LFV with two rotating aluminum sheets, one of which with drilling hole (left); The iron wire (circled in red) is used to trigger controlled signals for counting the experimental runs (right). 46 As an example, Fig. 37 shows the force signals produced whenever the iron wire (signal 1) and the aluminum sheets (2 with hole and 3 without hole) are passing underneath the miniaturized LFV. The iron wire produces two sharp force peaks corresponding to entering (downward peaks) and exiting (upward peaks) the localized magnetic field. The iron wire signal (4) demonstrates the beginning with the 2nd rotation run of the channel. On the other hand, due to their finite extend the aluminum sheets produce more smooth signals. Here signal (2) is slightly modulated due to the presence of the small hole on the aluminium sheet. We conclude that LFV can sense both surface velocities and small perturbations caused by sudden changes of the electrical conductivity of the moving metallic bodies. Fig. 37: Voltage signals of the iron wire (1); the Aluminum sheets with hole (2) and without hole (3) and iron wire (4) as function of time. Fig. 38 summarizes the entire series of experiments. It shows the measured Lorentz forces FL [mN] as a function of the height H [mm] above the channel and the moving velocity V [cm/s]. As expected, the Lorentz force increases upon increasing velocity and by decreasing height. 47 Fig. 38: Lorentz force FL vs. driving velocity V and height H. Fig. 39 shows more details about the measurements in a dimensionless representation. Here, the measured coefficient of the Lorentz force CL (Lorentz force divided by hydrodynamic pressure force) eq. (40) is plotted against the magnetic Reynolds number eq. (27) for various heights H. CL FL (1 2 V 2 A ) (40) We observe that all experiments we are within the so-called quasi-static MFD approximation characterized by Rem<< 1, i.e. the magnetic field induced by the eddy currents remain small compare to the externally applied magnetic field. As expected, the dimensionless Lorentz force CL decreases upon increasing both ReM and H. This finding reflects the fact that the Lorentz force is linearly increasing with Velocity V and decreases with height according to H-3, Eq. (3). 48 H= 0.10 cm H= 0.20 cm H= 0.32 cm H= 0.44 cm H= 0.80 cm H= 1.30 cm H= 1.90 cm H= 2.90 cm 0.025 F/1/2v2A 0.02 0.015 0.01 0.005 0 0 0.1 0.2 0.3 Re 0.4 0.5 0.6 m Fig. 39: Coefficient of Lorentz force CL as a function of magnetic Reynolds number Rem and height H. In the starting experiment, we show that using a single LFV, precise measurement of surface velocities in controlled solid body rotation is possible. Furthermore, we extend the rotary metallic bodies experiments by applying the ToF LFV to determine local velocities. A photograph of the experimental set-up is shown in Fig. 40. A thin iron wire is tightened across the channel (not shown in Fig. 40). On top of the channel there is a solid aluminum disk. At a certain height H above the channel we arrange two small cubic magnets attached with force sensors separated by a certain distance D. Here, we record the voltage signal delivered by the two LFVs as a function of time. We evaluate the time shift between the two voltage signals and recalculate the velocity V according to the relation V = D/. Fig. 40: Set-up of solid-body rotation experiments using Time-of-Flight LFV. 49 An example is given in Fig. 41. Here, large-amplitude peak signals are due to the motion of the iron wire through the two localized magnetic fields. Small peaks and signal fluctuations are due to the natural inhomogeneity of the aluminum disk. We observe that there is a clear time shift between the raw voltage signals. We detect that not only the sharp peaks produced by the iron wire but also the small fluctuations of the signals can be used to determine surface velocities. Fig. 41: Raw voltage data U1(t) (blue curve) and U2(t) (green curve) recorded by the force sensors LFV 1 and LFV 2. The velocity is fixed at V = 30cm/s. In means of standard signal processing methods, we additionally calculate the transit time using the averaged auto- and cross-correlation functions Eq. (7) denoted by Rxx and Rxy, respectively. 50 Fig. 42: Auto- and cross-correlation functions calculated according to Eq. (7) and using the raw voltage signals U1(t) and U2(t) shown in Fig. 41. On the top of the channel there is a solid aluminum sheet of thickness 1.5mm, see the left picture in Fig. 43. In a second series of experiments we replace the sheet by a ring-type aluminum plate, see the right picture in Fig. 43. At a certain height H above the aluminum plates we arrange the prototype of a Meniscus Velocity Sensor (MVS) based on the Time-of-Flight technique. A detailed description of the MVS is to be found in chapter 5.3. The two magnets are separated by the distance D = 65mm. The edge length of both cubic magnets is 20mm. For protection of the sensor against heat and dust in an assumed industrial condition, it is arranged inside a double-walled housing made of stainless steel. In the experiments we vary the rotation speed V of the channel, the separation distance D between magnets and the height of the gap between MVS sensor and the aluminum plate. Fig. 43: Set-up of the solid-body rotation experiments using an aluminum sheet (left) and an aluminum ring-type plate (right). 51 Fig. 44 represents the experimental results of the rotating sheet at V = 41.27cm/s and H = 28mm. The graph on the top of Fig. 44 shows the raw signals, i.e. the voltage recorded by the two force sensors. The graph below in Fig. 44 shows the corresponding cross-correlation functions Rxy and Ryx. We observe that there are clear peaks in the raw signals whenever the sheet passes underneath the force sensor. Moreover, we observe a clear time shift in the raw signals. 4 x 10 -1.5062 LKA1 -1.5064 Voltage, mV -1.5066 -1.5068 -1.507 -1.5072 -1.5074 0 1 2 3 4 5 6 7 8 -1721 LKA2 -1722 Voltage, mV -1723 -1724 -1725 -1726 -1727 -1728 -1729 0 1 2 3 4 Time, s 5 6 7 8 Averaged Cross Correlations for LFV1 and LFV2, T=1s 0.7 mean=0.1575 0.6 <Rxy> <Ryx> Cross-Correlation 0.5 0.4 0.3 0.2 0.1 0 -0.1 -0.2 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 Time Fig. 44: Raw signals (top) and cross-correlation function (below) for the case of a rotating aluminum sheet at V = 41.27cm/s and H = 28mm. 1 52 4 Voltage, mV -1.496 x 10 LKA1 -1.4965 -1.497 0 2 4 6 8 10 12 14 16 18 20 Voltage, mV -1610 22 LKA2 -1612 -1614 -1616 -1618 0 2 4 6 8 10 12 Time, s 14 16 18 20 Averaged Cross Correlations for LFV1 and LFV2, T=1s 0.3 <Rxy> <Ryx> 0.25 0.2 Cross-Correlation 22 mean=0.2377 0.15 0.1 0.05 0 -0.05 -0.1 -0.15 -0.2 0 0.1 0.2 0.3 0.4 Time 0.5 0.6 0.7 0.8 Fig. 45: Raw signals (top) and cross-correlation function (below) for the case of a rotating aluminum sheet at V = 27.35cm/s and H = 33mm. Fig. 45 show the corresponding results for the cases V = 27.35cm/s, H = 33mm, respectively. We observe that in these cases the peaks in both the raw signals and the cross-correlation functions are considerably weaker. We attribute this finding to the fact that a decrease in velocity and an increase in height both cause a significant decrease in the magnitude of the Lorentz force, cf. Eq.(3). Repeating the experiments for various rotation speed and height, we observe that our prototype is able to produce reliable results at relatively low heights H < 33mm and at rotation speeds within the range of a few cm/s to 65cm/s. 53 To verify the results measured using the MVS, we installed a photoelectric sensor as reference measurement. For these comparison experiments we decrease the height in a range of 5-13mm. At first, we employed a force sensor with a resolution of 0.1g (see Fig.72) and set the height of H = 10mm above the channel, thereby the edge length of the applied magnets are A = 20mm. Fig. 46 shows the results if we let the channel rotate in the counter-clockwise direction. It means that the aluminum sheet first passes underneath the LFV 1. Accordingly, Fig. 47 depicts the results if we let the channel rotate in the clockwise direction, as the aluminum sheet passes first underneath the LFV 2. In both cases the measured rotating velocity with MVS is almost the same as the measured with photoelectric sensor. However, it is remarkable that in the range of 4060cm/s the velocity is not detectable by MVS. Even though the rotating speed increases, the MVS measures always the constant velocity of 53cm/s. Fig. 46: Comparison of measured velocity using MVS with measured velocity using laser; channel rotating counter clockwise. 54 Fig. 47: Comparison of measured velocity using MVS with measured velocity using laser; channel rotating in clockwise. One possible reason for this unexpected finding might be the limited resolution of the force sensor used at that time. For further experiments we decided to employ a more sophisticated force sensor which produced by company Velomat, see Appendix 3. With the new sensor we broaden the detectable measuring capacity from a few cm/s to 65 cm/s without significant deviations from the measured reference velocity. Fig. 48: Experimental set-up for measuring the rotating speed using an aluminium sheet without housing. 55 Fig. 49: Comparison between the measured velocity using MVS with the one measured using laser by varying height above the rotating channel. Nevertheless, it can be found that by increasing the height, the sensitivity of the MVS sensor decreases. The results given in Fig. 49 show that by increasing the height from 5 to 13mm, the lowest detectable velocity will increase drastically. With the height 13mm we are not able to measure the velocities lower than 20cm/s, see the graph at the bottom right of the Fig. 49. 4.2.2 Numerical simulations For this experimental setup we perform numerical simulations using the commercial software MAXWELL. Here we solve a slightly different problem where an aluminium sheet is linearly pulled at constant speed underneath two localized magnetic fields. Magnet dimensions and arrangements correspond exactly to the experimental set-up. MAXWELL solves the three-dimensional transient induction equation in the magnetic vector potential representation. By that, we obtain the distributions of the magnetic field produced by the permanent magnets as well as the distribution of the induced eddy currents and Lorentz forces within the moving metallic sheets. Figs. 50 and 51 show the results of numerical simulations. Here, both the calculated Lorentz forces Fx [N] in the streamwise direction and induced eddy current Jz [A/m2] in spanwise direction are plotted as a function of position in streamwise direction. Moreover, the y-component (vertical direction) of the magnetic field By [mT] is added. The pulling speed is fixed at V = 30cm/s. The height is fixed at H = 2cm. 56 Fig. 50: Graphs of the y-component By of the magnetic field (red curve), the z-component jz of the induced eddy current density (blue curve), and the x-component Fx of the generated Lorentz force (purple curve). Parameters are fixed at V = 30cm/s, H = 2cm and D = 10mm. Fig. 50 refers to a separation distance of D = 10mm corresponding to the halfedge length of the cubic magnets. We observe that in this case the two magnetic field overlap. Interestingly, there are localized regions in front of the first magnet field and at the end of the second magnetic field within which the Lorentz force acts as an acceleration force on the solid body, i.e. pushing it in the streamwise direction. This is due to the fact that within these regions the eddy currents are flowing in the opposite direction to form closed loops. By that, also the Lorentz force changes its direction. 57 Fig. 51: Graphs of the y-component By of the magnetic field (red curve), the z-component jz of the induced eddy current density (blue curve), and the x-component Fx of the generated Lorentz force (purple curve). Parameters are fixed at V = 30cm/s, H = 2cm and D = 80mm. Fig. 51 shows the numerical results for a separation distance of D = 80mm and the same set of parameters as before. In this case the magnetic fields do not overlap. Moreover, within the region between the two localized magnetic fields, the Lorentz force acts in the positive streamwise direction. This indicates that the eddy currents are using the entire gap between the magnets to loop back. 4.3 Liquid metal free surface experiments 4.3.1 Experimental results Finally, we would like to present first experimental results for the case when the ring channel is filled with GaInSn. Here, we want to demonstrate that ToF LFV may also serve as a method to determine local velocities in free-surface flow. A sketch of the experimental set-up for liquid metal free-surface experiment is shown in Fig. 52. A ring channel filled with liquid metal GaInSn is put into controlled rotation. This case is closer to the metallurgic applications during continuous casting of steel and production of secondary aluminum. 58 Fig. 52: Set-up for measuring surface velocities in free-surface flow using ToF LFV. The results of flow visualization using a single permanent magnet are shown in Fig. 53. We observe that the presence of a localized magnetic field, produced by the permanent magnet, gives rise to intense deformation of the free surface and the creation of surface waves. The field acts as a magnetic obstacle which has already been Fig. 53: Visualization of liquid metal free-surface flow influenced by a localized magnet field that is produced by a small permanent magnet located above the surface. Surface deformation and surface waves are created due to the magnetic obstacle effect. predicted by numerical simulations [38] and confirmed in respective experiments [39] [70]. We observe that the flow velocity is decreased right underneath the magnet and is accelerated in the side regions. Due to the obstacle effect of the magnet on the liquid metal flow the main part of the liquid flows next to the wall boundaries. Therefore, any flow pertubation triggered by the first LFV does not reach the zone of influence of the second LFV. For this reason we equiped the first magnet with an edge length of 10mm and the second magnet with an edge length of 15mm. The experimental set-up is shown in Fig. 53. With the liquid metal in rotation and the height of the MVS kept at 5mm above the channel, we obtain the results shown in Fig. 54. The blue points are the measurable velocites. The red points represent the linear 59 fitting and the black line is the curve fitted to the blue points. Unfortunaly, very weak linear behaviour in the results has been recognised. Fig. 54: Comparison between the measured velocity using MVS and measured velocity using laser; magnet in LFV 1 with edge length 10mm and magnet in LFV 2 with edge length 15mm. Afterwards, we decided to immerse a piece of styrofoam with diameter 40mm as disturbance body in the liquid metal GaInSn, see Fig. 55, and repeat the experiment. 60 Fig. 55: Submerged styrofoam as a disturbing body in liquid metal free-surface flow measurement. With the aid of this submerged body, we can drastically increase the measurable velocities, see Fig. 56. Moreover, using the styrofoam even higher velocity up to 65cm/s were detectable. Fig. 56: Comparison of measured velocity using MVS with measured velocity using laser; magnet of LFV 1 with edge length 10mm and magnet of LFV 2 with edge length 15mm. 61 Finally, two magnets with the same edge length of 15mm are used. By that, we achieve better results, i.e. less discrepancy from the linear relationship and a wider measurement range of velocity, see Fig. 57. Fig. 57: Comparison of measured velocity using MVS with measured velocity using laser; both magnets in LFV 1 and LFV 2 are with edge length 15mm. We observe that the raw signals are very noisy and the cross-correlation is weak. Repeating the experiments for different values of H and V reveals that so far the rate of cross-correlations is clearly less than that in the solid-body experiments and that the reproducibility is modest. We attribute these findings to both the magnetic obstacle effect and the lack of design of MVS. Improvements of these deficits are a part of the future work. 4.3.2 Numerical simulations Our numerical approach consists of two steps. In a first step we calculate the applied magnetic field B0 (x, y, z) that is produced by the two small-size permanent magnets using the commercial finite-element solver MAXWELL. Basically, MAXWELL solves the Laplace equation for the magnetic scalar potential defined by 62 2 0, where B 0 0 (41)(42) As input parameters we define the geometry of the cubic-type magnets (with edge length A) and their separation distance D. Moreover, according to the data sheet provided by the manufacturer of the NdFeB permanent magnets, we specify both the magnetic remanence (Br = 1.32T) and the coercive field strength (Hc = 12kA/m). In a second step we calculate the velocity field u, the total magnetic field B = B0 + b, where b is the magnetic field induced by the flow, and the pressure field p in the flow domain using the commercial finite-volume solver FLUENT. Here, we simultaneously solve the Navier-Stokes equations (19) and the magnetic induction equations (13). As appropriate boundary conditions we apply the no-slip condition at rigid walls and a zero shear stress condition at the free surface which is assumed to be non-deformable. Fig. 58: Geometry of the problem. Two cubic-type permanent magnets of edge length A are arranged in a row separated by a certain distance D and some height H above the free surface. Numerical solutions will be given along the lines A (symmetry line in the streamwise direction), lines B (spanwise direction in front of the first magnet), and lines C (symmetry line in the spanwise direction). Moreover, we apply a constant velocity profile u = u0ex as an inlet condition and zero-pressure p = 0 as an outlet condition. All boundaries are taken to be electrically insulating. In this case the normal component of the current density is zero. ANSYS deals with this by setting the tangential component of the induced magnetic field identical to zero. Fig. 58 shows the geometry within which the equations (13) and (19) are solved. For meshing we use about 6 x 106 elements. As an appropriate turbulence model we choose the Large Eddy Simulation (LES) where the sub-scale structures are modeled by the Wall-Adapting Local Eddy Viscosity (WALE) method. 63 Applied magnetic field B0 Fig. 59 shows the magnetic field strength along line A for a fixed magnet edge length of A = 10 mm and various values of the separation distance D and height H above the free surface. Fig. 59: Magnetic field strength B0 [T] in streamwise direction. We observe that upon increasing H the magnetic field strength decreases considerably. Moreover, upon increasing the separation distance D the overlapping of the magnetic fields decreases. Results of magnetohydrodynamic simulations In the following we prefer to discuss the results using the dimensionless parameters of the problem. These are the Reynolds number Eq. (29) and the Hartmann number Eq. (31) as well as geometry parameters d, a, and h defined by the following relations d = D/L0, a = A/L0, h = H/L0. (43)-(45) Here, Bmax denotes the maximum magnetic field strength at the free surface directly underneath the magnet and L0 is the characteristic length (L0 = 0.04 m). Moreover, we use scaled values for the streamwise coordinate x, the streamwise velocity u, the Lorentz force density fL j B Eq. (15) with drag force fx 64 and lift force fz, and the eddy current density j 1 0 B Eq. (9) (spanwise component jy) according to the relations L̂ x L 0 ,Û u u0 , cfx = fx L0/(½u02), cfz = fz L0/(½u02), cjy = jy/(Bmaxu0). (46-50) The Reynolds number represents the ratio of inertia forces to viscous forces. Usually we have Re 1 indicating that the flow is turbulent. The Hartmann number represents the ration of electromagnetic forces to viscous forces. Usually we have also Ha >> 1 indicating that Lorentz force clearly dominates over friction. Please note that Ha varies with Bmax, i.e. with the height H at which the magnets are positioned above the free surface. The Lorentz forces coefficients cfx and cfz represent the electromagnetically induced drag and lift force per unit area reduced by the dynamic pressure of the flow. Physically, they indicate how strongly the flow will be reorganized under the action of the magnetic field. Streamwise velocity As an example Fig. 60 shows the reduced streamwise velocity Û at the free surface along line A for various values of the parameters Re and Ha. The geometry parameters is fixed at d = 1.25 and a = 0.25. In these graphs vertical lines indicate the location of the permanent magnets. We observe that there is a slight acceleration of the flow in front of magnet 1, i.e. Û > 1. As we shall see later on this due to the distribution of the induced eddy current density that are looping back in this region in the negative y-direction. According to the right-hand rule this gives rise to Lorentz forces acting in the position x-direction that are pushing fluid in the streamwise direction. On contrast, right underneath the magnets, the flow is strongly decelerated due to the strong braking Lorentz forces acting in the negative x-direction. According to mass conservation fluid is pushed aside in the spanwise direction surround the magnet region. This finding is wellknown as the magnetic obstacle effect. After having left the zone within which the magnetic field is present, the flow is again accelerated due to the absence of the braking Lorentz forces. Furthermore, from Fig. 60 we conclude that this obstacle effect becomes more pronounced upon increasing Hartmann number and decreasing Reynolds number. This behavior can be physically understood in terms of the electromagnetic interaction parameter N = Ha2/Re, Eq. (32) which represents the ratio of electromagnetic forces to inertia forces. In case of N > 1, Lorentz forces dominate over inertia forces. Hence, the flow profile can easily be deformed by the electromagnetic forces. On the other hand, in the case N < 1, the relatively strong inertia forces are able to prevent strong deformations of the flow profile by the Lorentz forces. 65 Fig. 60: Reduced streamwise velocity along line A for various Reynolds number and the Hartmann number. Vertical lines indicate the locations of the permanent magnets. This magnetic obstacle effect becomes more obvious when analyzing the streamwise velocity at the entire free-surface. Fig. 61 shows an example for two different Reynolds numbers. Hartmann numbers are fixed at Ha = 460 and d = 1.25, a = 0.25. As expected, for lower Reynolds number at constant Hartmann number, the magnetic obstacle is more pronounced. Moreover, Fig. 62 shows streamwise surface velocity profiles as a function of the spanwise coordinate at two different streamwise locations, i.e. along line B (left graph) and along line C (right graph), and for two different sizes of magnets. Reynolds and Hartmann numbers are fixed at Re = 21.000 and Ha = 460, and d = 1.25. As expected, we find that for larger magnets, the obstacle effect is more pronounced. Results of more parametric studies are given in Ref. [40]. 66 Fig. 61: Streamwise velocity distribution (in m/s) at the free surface. Flow direction is from left to right. Squares illustrate locations of the permanent magnets. Parameters are Re = 21.000 (top graph) and Re = 63.000 (below graph). Fig. 62: Reduced velocity in the streamwise direction as a function of the spanwise coordinate along line B (left) and line C (right) for two different sizes of magnets. Eddy current density We now would like to discuss results of our numerical simulations concerning the distribution of the induced eddy current density represented by the coeffi- 67 cient cjy = jy/(Bmaxu0). In our case the y-component, i.e. jy is the most important one as it is the dominant contribution to the braking Lorentz force. Fig. 63 shows the variation of cjy along line A for various values of the Reynolds number and the Hartmann number. Fig. 63: Distribution of the coefficient of the eddy current density along line A. Other parameters are d = 1.25 and a = 0.25. Vertical lines indicate the position of the permanent magnets. We observe that in the regions under the magnets, strong eddy current are flowing into the negative y-direction. This gives rise to strong braking Lorentz forces that contribute to the magnetic obstacle effect. Due to the solenoidal constraint, i.e. j = 0, these eddy currents must loop back in regions right in the front and right behind the magnets. By that they turn their direction as well do the induced Lorentz forces. Hence, in these regions the flow is accelerated. We expect that the magnitude of the eddy current density strongly increases upon increasing both Reynolds number and Hartmann number. However, due to the used scaling the non-dimensional coefficient cjy remains almost constant. An example of the eddy current distribution in the free-surface plane is given in Fig. 64. Here, parameters are fixed at Re = 21.000, Ha = 460, a = 0.25, and d = 1.25. We observe the formation of two eddy current loops. Underneath the permanent magnets, the currents run in the positive y-direction and loop back in field-free regions. As it can be seen, the current density induced under magnet 1 is much higher than that under magnet 2. This finding reflects the fact that the streamwise free-surface flow velocity is much smaller under magnet 2 as the flow has already been broken by magnet 1. 68 LKA 1 LKA 2 Fig. 64: Distribution of eddy current density at the free-surface. Fig. 65: Coefficient of the Lorentz force density in the streamwise direction for various Reynolds number and Hartmann number. Other parameters are fixed at a = 0.25 and d = 1.25. 69 Drag force coefficient Cfx According to the relation fL j B the Lorentz force density is generated as the result of the interaction of the eddy current and the applied magnetic field. Fig. 65 shows the Lorentz force coefficient cfx = fx L0/(½u02) at the free-surface along line A for various Reynolds numbers and the Hartmann numbers. We observe that underneath the magnets strong braking Lorentz forces are generated. According to the equation above, this is the result of the eddy currents running in the positive y-direction and the applied magnetic field basically pointing in the negative z-direction. However, in the regions in the front and behind the magnets, the drag force coefficient becomes positive indicating accelerating Lorentz forces. As mentioned before, this finding is due to the fact that in these regions the induced eddy currents loop back, i.e. running in the negative ydirection. Moreover, we find that cfx increases upon increasing the Hartmann number. This finding reflects the fact that Ha is a non-dimensional parameter of the electromagnetically induced drag force. However, from Fig. 65 we conclude that cfx decreases with increasing Reynolds number. Mathematically, this finding is due to the scaling of the Lorentz force using the dynamic pressure being proportional to u2. Physically speaking, this finding demonstrates that in the low-Re case, flow profiles are more sensitive to deformation due to the presence of electromagnetic forces. Finally, we observe that the magnitude of cfx is much higher underneath magnet 1 than underneath magnet 2. Again, this result indicates that magnet 1 acts as an obstacle forming a wake. This reduces the velocity and although the induced Lorentz forces underneath magnet 2. Lift force coefficient and surface deformation Cfz Finally, we would like to have a look at the electromagnetically generated lift forces. This force basically results from the interaction of the induced eddy current density jy in the y-direction and the applied magnetic field in the z-direction. Although, we have assumed that the free-surface in non-deformable flow, the evaluation of this force may give some practical information about the surface deformation and the generation of surface waves that have been observed in the laboratory experiments. To this end, neglecting curvature effects, we make a simple balance of the hydrostatic and the electromagnetic pressure across the free-surface that is elevated in the vertical direction by some height h. This balance reads as gh fzL0. (51) Upon rearranging Eq. (51) we obtain for the reduced magnitude of deformation h/L0 = fz/(g). (52) Fig. 66 shows some results of this evaluation. Here, the reduced surface deformation along line A is given for various Reynolds numbers and Hartmann numbers. Other parameters are fixed at a = 0.25 and d =1.25. We observe a nonsymmetric distribution of lift force and the possible resulting surface deformation. In front of the magnets there are negative lift forces resulting in the formation of depressed area. Behind the magnets, respective positive lift forces 70 result in the formation of amplified area on the free surface. Similar deformations were observed in laboratory experiments [31]. Moreover, a strong positive lift force underneath the left-hand side and strong negative lift force underneath the right-hand side of the magnets while the force underneath the vertical symmetry line of magnets is zero. This is expected since the streamwise component of the magnetic field is likewise changing its direction being zero in the vertical symmetry line. Another expected result is that the surface deformations become more pronounced when both Reynolds number and Hartmann number are increased. Larger values of Reynolds number lead to higher eddy current densities and larger values of Hartmann number lead to stronger magnetic fields. Fig. 66: Reduced surface deformation along line A for various Reynolds number and the Hartmann number. Vertical lines indicate the location of the magnets. Both effects contribute to higher electromagnetic forces. Eventually, underneath magnet 1 the magnitudes of the lift forces are much higher than underneath magnet 2. Again, this reflects the fact that due to the obstacle effect behind 71 magnet 1 a wake is formed that reduces the streamwise velocities under magnet 2. Summary We have numerically investigated free-surface liquid metal flow influenced by two localized magnet fields that are produced by small cube-type permanent magnets that are arranged in some distance above the surface and that are arranged one behind the other separated by a certain distance in the streamwise direction. Such an arrangement serves as a model to study ToF LFV for the non-contact measurement of local surface velocities in metallurgic applications. We have analyzed the effects of the Reynolds number and the Hartmann number as well as geometric parameters on the distributions of streamwise surface velocity, induced eddy current density, and generated Lorentz force density. Our main findings main be summarized as follows. i. Magnet 1 acts like a magnetic obstacle. Due to strong braking Lorentz forces acting underneath the magnet, the streamwise velocity is reduced and fluid is pushed aside, by-passing the region in which the magnetic field is present. A wake is formed. These effects are more pronounced upon increasing Ha and decreasing Re. ii. Magnet 2 is located in the wake produced by magnet 1. Hence, streamwise velocities, eddy current densities, and Lorentz forces are reduced underneath magnet 2. 72 5 Application of ToF LFV to free surface velocity measurement in metallic melt 5.1 Introduction Global and local control of liquid metal flow is crucial for success of many metallurgic processes. 90% of the worldwide steel is produced by continuous casting. During this process, non-steady melt flow in the mould may lead to highly unwelcome slab surface defects. Both DC and AC electromagnetic fields are utilized to improve the ability of controlling the melt flow by induced Lorentz forces. Plant measurements of melt flow are important to record the electromagnetic effects. Of special interest is knowledge of both the direction and the magnitude of the flow velocity at the surface in the mold are critical for the final product quality [1]. To provide the continuous casting machine with liquid steel, scrap is melted in electric furnace. The primary melt is delivered to the tundish where it is heated by plasma torches. During the casting process, liquid steel is continuously fed from the tundish to the mould through the submerged entry nozzle (SEN). The flow rate of steel in the tundish and in the mould is controlled either using a sliding gate mechanism or a stopper rod device, which is mounted beneath the tundish. The surface of steel in both ladle and tundish is usually covered with casting powder to avoid oxidation upon contact with the atmosphere. The mould oscillates to prevent sticking of the solidifying shell at the mould. Mould walls consist of water-chilled copper plates. Hence, upon contact with the wall, liquid steel immediately solidifies due to intense heat transfer provided by the mould cooling system. When the solidified shell is thick enough to bear up against the ferrostatic pressure of the liquid steel inside the strand, it leaves the mould and is further cooled by a secondary cooling system using water sprays. Rollers keep the strand in shape until it is completely solidified. The strand is cut into specified lengths at a slitting station and further treated by rolling. This continuous casting of steel process is schematically shown in Fig. 67. 73 Fig. 67: Continuous casting of steel process. The figure is taken from Ref. [55]. The steel flows from the tundish to the mould through SEN by gravity. Hence, the SEN has an important influence on mould flow and thus on steel quality. To prevent problems such as generation of surface waves, meniscus freezing, and crack formation, steel should be delivered constantly into the mould. If the liquid steel jet leaving the SEN impinges too strongly on the narrow face of the mould, the jet may split to flow upwards along the narrow face. This may lift the level of the molten steel, changing its profile and also generating large level fluctuations near the meniscus. Mould flux may be pushed away from the narrow face, leading to surface quality problems [1]. Hence, non-contact measurement of both the magnitude and the direction of the velocity in the melt flow near the surface is advantageous for casting control. However, the surface is covered by a non-transparent layer of mould powder to prevent formation of slag. Thus, surface flow cannot be registered by optical measurement techniques. Moreover, due to aggressiveness of metal melt at high temperature, only non-contact measurement methods can be applied. The aim of the present experimental study is to investigate the feasibility of the meniscus velocity measurement based on ToF LFV for high-temperature liquid metal. In this chapter we present a series of test experiments conducted at North Eastern University (NEU) in close cooperation with Key Laboratory of Electromagnetic Processing of Materials Ministry of Education. The experiments aim to demonstrate that the MVS is also feasible to measure free-surface velocity of the melt in open channel under nearly industry-oriented conditions, i.e. hot liquid metals. In more detail, we present test measurements using SnPbBi at about 74 210°C and liquid steel at 1700°C. During these experiments the melts are transported by gravity in an open channel from an upper ladle to a lower holding container. We record the voltage of the force sensors by varying the distance of the sensors to the free-surface flow and the dimension of the used magnet systems. The evaluation of the data shows that meniscus velocity sensor (MVS) works well in producing signals in the solid body and the SnPbBi experiments. However, in the liquid steel experiments no clear cross-correlations were found. We attribute this finding to the relatively low number of individual experimental runs and the relatively short duration of each run. 5.2 State of the art of surface velocity sensor for melt flow Various methods to measure velocities in high-temperature metal melts have been developed and reported. For instance, one similar measurement method in ToF LFV is the Mass Flow Control (MFC) sensor [18] [80] which consist of two probes located close to each other behind the copper mould plates. Each probe consists of a permanent magnet and a detector, see Fig. 68. As the steel travels through each associated magnetic field, an electrical signal is induced in each detector caused by the electrical eddy currents induced by the fluid motion. The liquid steel velocities were measured by computing the time delay of the signals recorded by the two probes. The time shift of the two signals is a measure of the time taken by the flow to convect from one probe to the other. The average velocity in the region between the probes is then the distance between the probes divided by this time shift. The drawbacks of this sensor are twofold: First, flow past one probe often does not even reaches the other probe. Second, this MFC sensor should be placed in regions of steady horizontal flow, such as found near the top surface. Fig. 68: Mold Flow Control Sensor (MFC) from german company AMEPA. The figure is taken from Ref. [80]. On the other hand, simpler methods using basic fluid mechanics principles were also developed. A Karman vortex probe [19] was developed by Iguchi et al. to 75 measure the liquid steel velocities near meniscus based on the linear relationship between molten steel velocity and the shedding frequency of Karman vortex streets that is formed by the immersed cylindrical probe in the mold. The deficit of this method is as following: it is not contactless and requires a complicated signal processing process to filter the noises in the signal. Kubota et al. [20] [76] utilized a simpler technique with a rod dipped into the molten steel and the deflection angle of the rod and the torque acting on it was measured. The quantities were then transformed into surface steel velocities. A much simpler method to measure meniscus velocities using nail boards was pioneered by Dauby et al. Rietow and Thomas [21] extended this method to acquire velocity information by analysing the thicknesses of deposition layers on the nails. As molten steel flows past the nail, liquid steel builds up at the impinging point on the nail lump as it solidifies, and all kinematic energy is converted into potential energy at the stagnation point. Liquid steel level drops at the opposite side of the nail lump. After dipping the nail board into the steel liquid pool and removing it, the steel skulls that solidified on the end of each nail. This deformation of the meniscus is recorded by the shape of the solidified lump. By investigating the lump shape and lump height difference between the flowfacing side and its opposite side, the magnitude and direction of the surface steel velocity can be determined. 76 Fig. 69: Continuous casting mold showing steel flow, top-surface slag layers and location of nail-board insertion (top) and Nail-board method to measure steel surface velocity and direction (below). The figure is taken from Ref. [55]. The Swedish company MEFOS has already developed a respective VelocityMeasurement-Level-Measurement sensor. It operates also according to the principle of the LFV. The velocity is measured by measuring the force which is acting on the magnetic element. However, a fully functional prototype has not successfully produced yet [22]. 77 Fig. 70: Velocity-Measurement-Level-Measurement Sensor developed by the company MEFOS. The figure is taken from Ref. [22]. 5.3 A sensor for high-temperature surface velocity measurement Recently, we suggested an alternative and much more compact design of such a surface velocity sensor termed Meniscus Velocity Sensor (MVS). The present meniscus velocity sensor operates according to the non-contact measurement of Lorentz forces acting on magnet systems. Its working principle relies on the ToF LFV, which has been successfully tested at Ilmenau University using both solid body movement and GaInSn as a low-melting model melt. This sensor can also be used to record local surface velocities in high-temperature metal melts. The principle design of MVS prototype is shown in Fig. 71. Basically, it consists of two cubic permanent magnets of edge length A, each of which equipped with a strain gauge based force sensor and separated by a certain distance. It can be equipped with 4 different sizes of cubic permanent magnets with edge lengths of 20mm, 15mm, 12mm, and 10mm. The magnets are fixed on special holders of adjusted lengths so that the gap between the bottom face of the magnet and the bottom of the housing is constant for all magnet sizes. Power supply for the velocity sensor is provided by a 12V rechargeable car battery. The total dimensions of the MVS are 105mm x 62mm x 110mm (length x width x height). The distance between two magnets is fixed at 65mm. 78 Fig. 71: Design of Meniscus Velocity Sensor (MVS). The MVS is positioned close to the surface of the melt flow. The strain gauge measures the forces acting on the magnets and generated by the melt flow. Both force sensors are fixed at a common holding plate. To protect the MVS against heat and dust, it is embedded in a double housing of which the gap is filled with thermally insulating material “Superwool 607 HT Paper” from company D&W. Cables and wires for power supply and data transfer are guided through a pipe outside of the housing. The diameter of this pipe is 20 mm. This pipe also serves to fix the MVS at an external positioning system. Temperature of the magnet system is measured by a thermocouple. All parts of the velocity sensors are made of non-magnetic stainless steel. Force sensor The most important part of MVS is the force sensor. For force measurement, we use commercial strain gauge based force sensors produced by the company MAUL alpha, see Fig. 72. The used sensors were selected according to the necessary level of accuracy, resolution, and critical frequency. To select the suitable sensor the following considerations were taken into account: i. The quantity of the dead load (magnet and holder) and the maximum deformations in the direction of load measurement. 79 ii. The quantity of the desired resolution and sampling rate of measurement. iii. The measurement uncertainties due to the influencing effects of temperature, wind, and mechanical vibration. Fig. 72: Digital strain gauge from the precision scale MAUL alpha fixed on cube magnets. Amplifier The amplifier is an important part of signal processing devices. Here, parameters like power supply, connectivity, signal filtering, sensitivity, resolution, offset, and interface are important for proper selection. As a cost-effective solution we choose the amplifier Soemer LDU 78.1, see Fig. 73. The performance parameters are shown in Appendix 3: Fig. 73: Amplifier Soemer LDU 78.1. 80 Magnets As the generate Lorentz forces are proportional to the square of the applied magnet field, usage of strong permanents magnets is favorable. We choose NdFeB magnet showing the following properties: Material: Edge length: Remanent flux: Coercivity: NdFeB N45 20mm, 15mm, 12mm, 10mm Br = 1.33 to 1.37T Hcb => 955A/m Fig. 74: Cubic NdFeB magnet. Radiative heat transfer simulation To check the transient thermal behavior of the prototype, heat transfer simulations are performed. In steel application, the magnet temperature may not exceed 80°C when the sensor is exposed to the hot melt surface. To this aim, a simple numerical model has been built up using the commercial software ANSYS, see Fig. 75. Here, an iron cube with edge length 30mm is arranged in a single housing made of stainless steel. The wall thickness of the housing amounts 4mm. The distance between magnet and the bottom of housing is 26mm. The housing is filled with air to allow for thermal convection inside. As a thermal load we apply arranged a hot plate at a fixed temperature of 1000°C some 100mm below the bottom of the housing. Heat is delivered by thermal radiation from the hot plate to the bottom of the housing. The selected arrangement results in a view factor of 0.451. An initial temperature of 20°C is applied to all parts of the sensor. 81 Fig. 75: Model of heat transfer simulation. 82 Fig. 76: Temperature distributions of radiation exposure across the sensor are plotted after 30s (above) and after 90s (below). Fig. 76 shows some results of our transient simulations. As expected, the hot spot is located in the centre of the bottom plate of the housing. After 90s, we obtain a hot spot temperature of about 780°C. More interestingly, we observe that the temperature of magnet is only 37.1°C at the bottom face and 31.4°C at the upper face. Therefore, we conclude that our design of MVS prototype using passive double-housing cooling with insulating material in between is well suited for some minutes of measurements above molten steel surface. Measurement procedure As the entire equipment has not been intensively tested before, it has been agreed to proceed in three experimental steps by continuously increasing difficulty and temperature. These steps are: Solid body experiments at room temperature with a copper rod rolling in a controlled manner underneath the meniscus flow sensor. SnPbBi at 210°C flowing in an inclined trapezoidal open channel of dimensions L x B (top) x B (bottom) x H = 1550mm x 50mm x 40mm x 18mm underneath the meniscus flow sensor. 83 Molten steel at 1700°C flowing in an inclined ceramic channel of dimensions L x B x H = 300mm x 80mm x 20mm underneath the meniscus flow sensor. All experimental runs were conducted using a sampling frequency of 25Hz. 84 5.4 Preliminary test measurement under industryrelevant condition 5.4.1 Open channel flow measurement using SnPbBi at 210°C We now turn to the experiments aiming to measure the surface velocity in melt flow using MVS. As a first test melt we use SnPbBi at 210°C. The experimental set-up is schematically shown in Fig. 77. Photographs of the experiments are provided in Fig. 78. The flow experiments are carried out in a trapezoidal open channel of dimension L x B (top) x B (bottom) x H = 1550mm x 50mm x 40mm x 18mm. The angle of inclination is 2.277°. Before each run, a volume of 22.95l of SnPbBi (density 9.9g/cm³) was melted in a gas-fired crucible. The melt was poured into the channel by tilting the crucible, lifted by a crane, by using a handle wheel. Fig. 77: Set-up of SnPbBi experiment. Fig. 78: Picture of the set-up for open channel flow experiments with SnPbBi (left). After the run the melt was put back into the ladle (right). The main object of these experiments is to find cross-correlations between the force signals. To this aim we carried out experiments with and without a submerged copper cylinder of diameter 20mm. The idea of using the cylinder is to 85 trigger extra vortices to enhance cross-correlation signals. Snapshots of the flow without and with submerged cylinder are shown in Figs. 79. We observe that without the use of the cylinder, a smooth free-surface flow adjusts in the channel. Using the cylinder, clear vortices are created in the wake. However, the obstacle additionally contributes to dam oxides. By that the flow rate slows down, see Fig. 80. Fig. 79: Smooth flow when no cylinder was submerged in the melt; The MVS is placed above the free surface liquid metal channel flow. The gap height is 30mm. The angle of inclination is 2.277° (left), with cylinder was submerged in the melt (right). Fig. 80: Wake formation behind the submerged cylinder. In the upstream direction the cylinder causes piling up of oxides slowing down the flow rate. A total of 18 individual runs, each lasting about 200s, were performed. For a given parameter set, the experiments were repeated 3 times. An experimental procedure matrix is shown in Appendix 2. The following parameters were varied: The gap height between channel and MVS (30mm, 20mm, 10mm). The edge length of the magnets (20mm, 15mm). With and without submerged cylinder. 86 Using data of a typical run, the duration of the run and the melt volume at hand, the following rough calculations can be conducted: . Q 0,02295m3 / 164s V 0,2 m / s. A 0,02 0,04m2 V D 0,065 0,26 m / s . 0,25 These calculations serve to check the plausibility of the data obtained later on. Results and discussion A total of 18 individual runs were carried out. Each run lasts about 115-341s. Only two runs were successfully completed, i.e. cross-correlations between the force signals were detected. In both of these runs the gap height was fixed at 30mm. One successful run was with using the submerged cylinder, the other one was without. 4630 4625 4620 0 x 10 50 100 150 200 4500 4480 4460 4440 250 4 -1.532 LKA2 -1.538 50 100 Time, s 150 200 100 150 200 250 LKA2 -1.534 -1.536 -1.538 -1.54 250 0 50 100 150 200 250 Time, s LKA1 LKA1 4490 Voltage , m V 4628 4626 4624 4488 4486 4484 4482 4622 0 5 10 15 20 25 4 x 10 -1.5355 -1.537 -1.5375 -1.538 0 0 x 10 5 10 15 20 25 4 LKA2 LKA2 -1.5365 V oltage , m V Voltage, mV 50 x 10 4492 4630 -1.536 0 4 -1.537 -1.539 0 Voltage, mV LKA1 Voltage, mV Voltage, mV -1.536 4520 LKA1 Voltage, mV Voltage, mV 4635 5 10 Time, s 15 20 25 -1.536 -1.5365 -1.537 -1.5375 0 5 10 15 20 25 Time, s Fig. 81: SnPbBi_gap height 30mm without cylinder, Data-04_41_28 (left); with cylinder, Data-07_05_00 (right). Raw signals (above), magnified signals (below). Fig. 81 (above) presents the raw signals as the voltages delivered by the two force sensors are plotted against the total running time. Fig. 81 (below) shows a magnification of the raw signals taken during a consecutive time interval of 25s. Overall, the signal conditioning is poor. Signal to noise ratios are not sufficient. The signals of LFV 2 indicate that propagating waves are present, probably triggered by uncontrollable parasitic vibrations. On the other hand, the crosscorrelation function reveals that there is a delay time of 0.25s. This particular value corresponds surprisingly very well with the correlation time of 0.26s calculated beforehand. Using an estimate of the mean velocity based on total volume 87 and total running time. However, it should be noted that only in 2 of the 18 runs cross-correlating have been detected. The following observations were made: (i) Clear cross-correlations were found for 20mm magnets at gap height 30mm. (ii) There is no obvious difference between with or without the submerged cylinder. (iii) The surface velocity, obtained by evaluating the transit time out of crosscorrelation function, corresponds well with a simple calculation using the total time of the run, the melt volume, and an estimate of the flow crosssection. (iv) The submerged cylinder generates a vortex street; however, it also causes a piling up of oxides diminishing the flow rate. (v) During the experiments, the MVS heats only slightly up. We conclude that the MVS is feasible to measure surface velocities in liquid metal free-surface flow. Having a closer look on the data, we decided to choose the 15mm magnets for the final experiments in molten steel. No submerged cylinder will be used. 5.4.2 Open channel flow measurement using steel at 1700°C Finally, we would like to present results of open channel free-surface flow measurement using steel at 1700°C. A total of six runs were performed. An experimental procedure matrix is shown in Appendix 2. Before each run, a solid steel rod of 8.72kg was melted in a 45kW induction furnace. The steel was poured into the ceramic channel with dimension L x B (top) x H = 300mm x 80mm x 50mm, see Fig. 82, by lifting and tilting the furnace via handles by men. The angle of inclination of the channel is 2.06°. 88 80 50 70 Fig. 1: Dimension of ceramic channel. Fig. 82: Dimension of the ceramic channel. The experimental set-up for open channel steel flow experiments is shown in Figs. 83. Fig. 83: Set-up for open channel steel flow experiments. 89 During the experiments we vary the gap height (10mm, 20mm). For each gap height 3 individual runs were performed. A typical run lasts about 20s. The preparation time for one individual run is about 60min. Snapshots of a typical experimental run are shown in Fig. 84. Fig. 84: Snapshots of a typical run at gap height 20mm (a) and 10mm (b). Results and discussion Fig. 85 presents the raw signals of three selected individual runs. The peaks in the raw signals are due ambient parasitic tremors that do not contribute to the evaluation of the delay time. More measurements are necessary to support the conjecture that the MVS is capable to detect surface velocities in liquid steel free-surface flow. However, also in these experiments no clear cross-correlating signals were detected. Voltage, mV -9050 LKA1 -9100 -9150 0 2 4 6 8 10 12 14 16 18 Voltage, mV -5200 20 LKA2 -5250 -5300 -5350 0 2 4 6 8 10 12 14 16 18 20 Time, s Fig. 85: Raw voltage signals u1(t) and u2(t) delivered by the two force sensors of MVS with gap height 20mm, Data-05_40_42. 90 Voltage, mV -9000 LKA1 -9050 -9100 -9150 -9200 0 2 4 6 8 10 12 14 16 Voltage, mV -5500 18 LKA2 -5600 -5700 -5800 0 2 4 6 8 10 12 14 16 18 Time, s Fig. 86: Raw voltage signals u1(t) and u2(t) delivered by the two force sensors of MVS with gap height 20mm, Data-07_07_35. Voltage, mV -9350 LKA1 -9400 -9450 -9500 0 2 4 6 8 10 12 14 16 18 20 Voltage, mV -5300 22 LKA2 -5400 -5500 -5600 0 2 4 6 8 10 12 14 16 18 20 22 Time, s Fig. 87: Raw voltage signals u1(t) and u2(t) delivered by the two force sensors of MVS with gap height 10mm, Data-07_55_00. The following observations were made: (i) The MVS heated up to a maximum temperature of 55°C by steel temperature 1700°C with measuring time 26s. We conclude that the passive cooling system was sufficient to protect the magnets from overheating. (ii) Due to short running times, limited test conditions, and limited force sensor quality, no clear cross-correlating signals were detected. 91 5.5 Sub-summary A first prototype of a Meniscus Velocity Sensor, which operates according to the Time-of-Flight Lorentz Force Velocimetry method, has been tested in both solidbody experiments and free-surface model experiments. In the solid-body experiments we use an aluminium sheet and an aluminium disk both of which rotating at controlled speed underneath the two Lorentz force flow meters. Best results were obtained for the case of the rotating sheet. Here, the quality of the force signals is good and the measured transit times correspond well with the applied rotation speed. In the case of the rotating disk we observe that usable measurement signals are obtained due to the natural unevenness of the disk. However, the quality of the signals depends strongly on the applied rotation speed and the gap height between sensor and disk. In the case of free-surface melt flow we observe that the magnetic obstacle effect restricts the determination of the local surface velocity as the applied magnetic field strongly influences both the magnitude of the velocity and the shape of the free surface. At the present time the reproducibility of these measurements is quiet moderate. Although some first results look promising, further model experiments using improved equipment and advanced signal processing method are required to demonstrate the feasibility of Time-of-Flight Lorentz force velocimetry in practical applications. All these efforts aim to improve the quality of the cross-correlation signals. To improve the existing prototype in term of suitability for plant application and extension of capability, the following tasks are to do aiming to improve the quality of the cross-correlation signals: I. Tailored magnet system (temperature-resistant, lightweight and high-field magnet systems, low Integration of magnetic field lines by small distance, strong magnetized, shielding and guiding magnetic flux in defined direction) II. Highly sophisticated force sensor (fast response time, dynamic instead of static sensor) III. Electronic signal processing (damp noise signals from mechanical vibration) IV. High-resolution electronic signal processing packages/and data acquisition systems V. Damping system for preventing mechanical vibration VI. Insulating measurement device against overheating (active: water or air cooling; passive: ceramic housing) VII. Signal strength vs. distance (explained below) 92 As a consequence, the most important factor that could be addressed during the present study is the effect of the distance between the sensors and melt flow. Upon decreasing the distance between the sensor and the liquid steel surface, clear cross-correlations are more probable. However, in this case active cooling of the sensor may be necessary. 93 6 Conclusion and outlook We experimentally and numerically study turbulent liquid metal flow in the test facility EFCO using the eutectic alloy GaInSn as a test fluid. Our model experiments demonstrate that Time-of-Flight Lorentz Force Velocimetry is a feasible non-contact tool for measuring flow rates in such flows. The present technique measures the transit time of a tagging vortex that is transported by the flow and registered by two Lorentz force flow meters that are arranged in a certain distance one behind the other. The measurement is based on just crosscorrelating the force data registered by the two flow meters. By that it becomes independent of any fluid properties and the magnetic field strength. However, the flow rate experiment show that intense calibration of the measuring device is necessary as the ratio between transit time and characteristic flow time depends strongly on the separation distance of the flow meters and, presumably, on the geometry of the obstacle which is submerged into the flow for producing detectable vortex structures. Instead of permanent magnet in LFF1, an electromagnet may be employed in the further investigations with the intention to produce controllable excitation by pulse generation. Furthermore, the meniscus velocity sensor (MVS) has been evaluated during industrial-relevant conditions. The test experiments show that ToF LFV is a potential non-invasive method to measure surface velocities in high-temperature metallic melts. The challenge in the development of MVS is to obtain a weakly noisy sampling rate due to the small and weak nature of the force signals as well as to find applicable pulse generators, which provide more clearly crosscorrelation peaks even in laminar flow. Further experimental and numerical investigations have to be performed to transfer the non-contact electromagnetic flow rate and free-surface velocity measurement technique relying on ToF LFV into industrial applications, for instance, continuous casting of steel and the production of secondary aluminium. Listoffigures Fig. 1: Principle of Lorentz Force Velocimetry. It is based on measuring the Kelvin force that pulls at an externally arranged magnet system. The Kelvin force is the counteracting force to the Lorentz force that is generated in the melt due to the movement of the electrically conducting melt through the magnetic field. .................................................................................................................... 2 Fig. 2: Principle of Time-of-Flight Lorentz Force Velocimetry. Two Lorentz force flow meters are arranged one behind the other. This flow measurement technique is based on just cross-correlating the force signals recorded by the two flow meters. The method is independent of melt properties and magnetic field parameters. ................................................................................................. 2 Fig. 3: Secondary aluminum production process. The aluminium melt flux is indicated by blue arrows. Scrap is melted in furnaces. The primary melt is delivered to converters within which the final melt is prepared. The figure is taken from Ref. [71] (in German)......................................................................... 4 Fig. 4: Meniscus flow in Continuous Casting of Steel (left). Double and single roll flow pattern (right). The figure is taken from Ref. [55]. .................................. 5 Fig. 5: Magnetic fly wheel (left). Single-magnet rotary flow meter (right). The figure is taken from Ref. [11] and [12]. ................................................................ 6 Fig. 6: Contactless electromagnetic phase-shift flow meter for liquid metals. The figure is taken from Ref. [13]. .............................................................................. 7 Fig. 7: Design of Vives Probe (left) and Potential Probe (right). The figure (right) is taken from Ref. [54]. ........................................................................................ 8 Fig. 8: The US transducer is submerged at an angle of 60° into the liquid metal duct EFCO (left). Multiple reflections of US wave may result in imaginary velocity values outside the region of the liquid flow (right). The right figure is taken from Ref. [17]. ............................................................................................ 9 Fig. 9: Principle of Lorentz Force Velocimetry for the measurement of flow rate (left) and local surface velocities (right). ............................................................ 10 VII Fig. 10: Principle of Time-of-Flight Lorentz Force Velocimetry for the measurement of flow rate (left) and local surface velocities (right). The transit time of a tagging signal flowing through the two flow meters is determined by cross-correlating the voltage data provided by the two force sensors. .............. 12 Fig. 11: Sketches of the experimental facility EFCO (left) for flow rate measurements, LiMeSCo for surface velocity measurement (middle), and MVS for measurement of surface velocity in high-temperature metallic melt (right). . 14 Fig. 12: Set-up of test facility EFCO for non-contact flow rate measurement in turbulent liquid metal flow using single LFV. ..................................................... 25 Fig. 13: Lorentz force FL as a function of volumetric flow rate Q. ...................... 26 Fig. 14: Velocity profiles at the mid plane of the channel measured by UDV. Counter-clockwise mode: turbulent hydrodynamic profile. Clockwise mode: Mshaped MFD profile. .......................................................................................... 27 Fig. 15: Numerical simulation for Re = 1.54 x 106 and Ha = 140. Top graph: geometry of the channel wall. Bottom graph: velocity profiles in entrance, inside, and at the exit of the magnet field. .................................................................... 28 Fig. 16: Induced eddy currents in the region of the localized magnetic magnetic field. .................................................................................................................. 29 Fig. 17: Eddy currents in the region of the localized magnetic field at half-height of the channel.................................................................................................... 30 Fig. 18: Lorentz force density in the region of the localized magnetic field at halfheight of the channel. ........................................................................................ 30 Fig. 19: Lorentz force density in the region of the localized magnetic field at the mid plane of the channel. .................................................................................. 31 Fig. 20: Set-up of the test facility EFCO for non-contact flow rate measurement in turbulent liquid metal flow using Time-of-Flight Lorentz Force Velocimetry. .. 32 Fig. 21: Velocity profiles at the mid plane of the channel measured by UDV. The green curve gives the profile when both flow meters are present. The blue curve gives the profile when LFV 2 was removed. ...................................................... 33 Fig. 22: Flow velocity (in m/s) in the horizontal plane at y = 2.5mm around the cylinder submerged at an angle of = 60° into the flow. Parameters are VIII Red = 1.6 x 104, ReC = 7.42 x 103, and the blockage ratio of the cylinder of = 0.8. .............................................................................................................. 34 Fig. 23: Raw voltage signals U1(t) and U2(t) delivered by the strain gauge of flow meters LFF 1 and LFF 2 over a period of 10s. .................................................. 35 Fig. 24: Auto- and cross-correlation functions calculated according to Eq. (7) from the voltage signals U1(t) and U2(t) shown in Fig. 23 above. Experimental parameters are fixed at f = 23Hz and D = 170mm. ........................................... 35 Fig. 25: Averaged relation between the vortex velocity Vvortex measured by ToF LFF and the velocity of the flow V measured by UDV and Vives probe. The separation distance is fixed at D = 170mm. The slope of the linear fitting curve is k2 = 1.90......................................................................................................... 36 Fig. 26: Averaged relation between the vortex velocity Vvortex measured by ToF LFF and the velocity of the flow V measured by UDV and Vives probe. The separation distance is fixed at D = 220mm. The slope of the linear fitting curve is k2 = 0.95......................................................................................................... 37 Fig. 27: Computational domains and meshes used in the numerical simulations. Within the volumes Fluid 2 and Fluid 4 a constant spanwise magnetic field is applied. ............................................................................................................. 38 Fig. 28: Flow velocities (in m/s) in the mid plane of the channel at Red = 2.0×104 (V = 0.4m/s) and Ha = 140. ............................................................................... 38 Fig. 29: Flow velocities (in m/s) in the mid plane of the channel at Red = 3.0×104 (V = 0.6m/s) and Ha = 140. ............................................................................... 39 Fig. 30: Flow velocities (in m/s) in the mid plane of the channel at Red = 3.0×104 (V = 0.6m/s) and Ha = 205. ............................................................................... 40 Fig. 31: Reduced velocity profiles at various positions in the streamwise direction: Line 1: inlet, Line 2: right behind LFF1, Line 3: between LFF1 and LFF2, Line 4: right behind LFF2, Line 5: outlet. The separation distance of the flow meters is D = 150mm................................................................................. 41 Fig. 32: Induced eddy current density (in A/m2) in the mid plane of the channel. The applied localized magnetic fields are pointing out of the plane. ................. 41 IX Fig. 33: Lorentz force density (in N/m3) in the mid plane of the channel. The applied localized magnetic fields are pointing out of the plane.......................... 42 Fig. 34: Velocity profiles in streamwise direction (a) and in spanwise direction (b)...................................................................................................................... 43 Fig. 35: Experimental set-up of test facility LiMeSCo. ....................................... 45 Fig. 36: Single LFV with two rotating aluminum sheets, one of which with drilling hole (left); The iron wire (circled in red) is used to trigger controlled signals for counting the experimental runs (right). .............................................................. 45 Fig. 37: Voltage signals of the iron wire (1); the Aluminum sheets with hole (2) and without hole (3) and iron wire (4) as function of time. ................................. 46 Fig. 38: Lorentz force FL vs. driving velocity V and height H. ............................ 47 Fig. 39: Coefficient of Lorentz force CL as a function of magnetic Reynolds number Rem and height H. ................................................................................ 48 Fig. 40: Set-up of solid-body rotation experiments using Time-of-Flight LFV. ... 48 Fig. 41: Raw voltage data U1(t) (blue curve) and U2(t) (green curve) recorded by the force sensors LFV 1 and LFV 2. The velocity is fixed at V = 30cm/s. .......... 49 Fig. 42: Auto- and cross-correlation functions calculated according to Eq. (7) and using the raw voltage signals U1(t) and U2(t) shown in Fig. 41. .................. 50 Fig. 43: Set-up of the solid-body rotation experiments using an aluminum sheet (left) and an aluminum ring-type plate (right)..................................................... 50 Fig. 44: Raw signals (top) and cross-correlation function (below) for the case of a rotating aluminum sheet at V = 41.27cm/s and H = 28mm. ........................... 51 Fig. 45: Raw signals (top) and cross-correlation function (below) for the case of a rotating aluminum sheet at V = 27.35cm/s and H = 33mm. ........................... 52 Fig. 46: Comparison of measured velocity using MVS with measured velocity using laser; channel rotating counter clockwise. ............................................... 53 Fig. 47: Comparison of measured velocity using MVS with measured velocity using laser; channel rotating in clockwise. ........................................................ 54 Fig. 48: Experimental set-up for measuring the rotating speed using an aluminium sheet without housing. ..................................................................... 54 X Fig. 49: Comparison between the measured velocity using MVS with the one measured using laser by varying height above the rotating channel. ................ 55 Fig. 50: Graphs of the y-component By of the magnetic field (red curve), the zcomponent jz of the induced eddy current density (blue curve), and the xcomponent Fx of the generated Lorentz force (purple curve). Parameters are fixed at V = 30cm/s, H = 2cm and D = 10mm.................................................... 56 Fig. 51: Graphs of the y-component By of the magnetic field (red curve), the zcomponent jz of the induced eddy current density (blue curve), and the xcomponent Fx of the generated Lorentz force (purple curve). Parameters are fixed at V = 30cm/s, H = 2cm and D = 80mm.................................................... 57 Fig. 52: Set-up for measuring surface velocities in free-surface flow using ToF LFV. .................................................................................................................. 58 Fig. 53: Visualization of liquid metal free-surface flow influenced by a localized magnet field that is produced by a small permanent magnet located above the surface. Surface deformation and surface waves are created due to the magnetic obstacle effect. .................................................................................. 58 Fig. 54: Comparison between the measured velocity using MVS and measured velocity using laser; magnet in LFV 1 with edge length 10mm and magnet in LFV 2 with edge length 15mm........................................................................... 59 Fig. 55: Submerged styrofoam as a disturbing body in liquid metal free-surface flow measurement. ............................................................................................ 60 Fig. 56: Comparison of measured velocity using MVS with measured velocity using laser; magnet of LFV 1 with edge length 10mm and magnet of LFV 2 with edge length 15mm. ........................................................................................... 60 Fig. 57: Comparison of measured velocity using MVS with measured velocity using laser; both magnets in LFV 1 and LFV 2 are with edge length 15mm. .... 61 Fig. 58: Geometry of the problem. Two cubic-type permanent magnets of edge length A are arranged in a row separated by a certain distance D and some height H above the free surface. Numerical solutions will be given along the lines A (symmetry line in the streamwise direction), lines B (spanwise direction in front of the first magnet), and lines C (symmetry line in the spanwise direction). .......................................................................................................... 62 XI Fig. 59: Magnetic field strength B0 [T] in streamwise direction. ......................... 63 Fig. 60: Reduced streamwise velocity along line A for various Reynolds number and the Hartmann number. Vertical lines indicate the locations of the permanent magnets. ........................................................................................................... 65 Fig. 61: Streamwise velocity distribution (in m/s) at the free surface. Flow direction is from left to right. Squares illustrate locations of the permanent magnets. Parameters are Re = 21.000 (top graph) and Re = 63.000 (below graph). ............................................................................................................... 66 Fig. 62: Reduced velocity in the streamwise direction as a function of the spanwise coordinate along line B (left) and line C (right) for two different sizes of magnets. ........................................................................................................... 66 Fig. 63: Distribution of the coefficient of the eddy current density along line A. Other parameters are d = 1.25 and a = 0.25. Vertical lines indicate the position of the permanent magnets. ............................................................................... 67 Fig. 64: Distribution of eddy current density at the free-surface. ....................... 68 Fig. 65: Coefficient of the Lorentz force density in the streamwise direction for various Reynolds number and Hartmann number. Other parameters are fixed at a = 0.25 and d = 1.25. ....................................................................................... 68 Fig. 66: Reduced surface deformation along line A for various Reynolds number and the Hartmann number. Vertical lines indicate the location of the magnets. 70 Fig. 67: Continuous casting of steel process. The figure is taken from Ref. [55].73 Fig. 68: Mold Flow Control Sensor (MFC) from german company AMEPA. The figure is taken from Ref. [80]. ............................................................................ 74 Fig. 69: Continuous casting mold showing steel flow, top-surface slag layers and location of nail-board insertion (top) and Nail-board method to measure steel surface velocity and direction (below). The figure is taken from Ref. [55]. 76 Fig. 70: Velocity-Measurement-Level-Measurement Sensor developed by the company MEFOS. The figure is taken from Ref. [22]. ....................................... 77 Fig. 71: Design of Meniscus Velocity Sensor (MVS). ........................................ 78 Fig. 72: Digital strain gauge from the precision scale MAUL alpha fixed on cube magnets. ........................................................................................................... 79 XII Fig. 73: Amplifier Soemer LDU 78.1.................................................................. 79 Fig. 74: Cubic NdFeB magnet. .......................................................................... 80 Fig. 75: Model of heat transfer simulation. ........................................................ 81 Fig. 76: Temperature distributions of radiation exposure across the sensor are plotted after 30s (above) and after 90s (below). ................................................ 82 Fig. 77: Set-up of SnPbBi experiment. .............................................................. 84 Fig. 78: Picture of the set-up for open channel flow experiments with SnPbBi (left). After the run the melt was put back into the ladle (right). ......................... 84 Fig. 79: Smooth flow when no cylinder was submerged in the melt; The MVS is placed above the free surface liquid metal channel flow. The gap height is 30mm. The angle of inclination is 2.277° (left), with cylinder was submerged in the melt (right). .................................................................................................. 85 Fig. 80: Wake formation behind the submerged cylinder. In the upstream direction the cylinder causes piling up of oxides slowing down the flow rate. ... 85 Fig. 81: SnPbBi_gap height 30mm without cylinder, Data-04_41_28 (left); with cylinder, Data-07_05_00 (right). Raw signals (above), magnified signals (below). ............................................................................................................. 86 Fig. 82: Dimension of the ceramic channel. ...................................................... 88 Fig. 83: Set-up for open channel steel flow experiments. .................................. 88 Fig. 84: Snapshots of a typical run at gap height 20mm (a) and 10mm (b). ...... 89 Fig. 85: Raw voltage signals u1(t) and u2(t) delivered by the two force sensors of MVS with gap height 20mm, Data-05_40_42. ................................................... 89 Fig. 86: Raw voltage signals u1(t) and u2(t) delivered by the two force sensors of MVS with gap height 20mm, Data-07_07_35. ................................................... 90 Fig. 87: Raw voltage signals u1(t) and u2(t) delivered by the two force sensors of MVS with gap height 10mm, Data-07_55_00. ................................................... 90 XIII Bibliography [1] M.M., Wolf: History of Continuous Casting, in Steelmaking Conf. Proc. 1992, Iron & Steel Society, Warrendale, PA: Toronto, Canada. p. 83-137. [2] K. Krone: Aluminium-Recycling (Düsseldorf: VDS), 2000. [3] F. H. Zschacke: Lehrbuch der Glastechnik / Teil 3 / Die Veredlung des Flachglases, 3. verb. Aufl., Nachdr. 1950 [4] A. Thess, E. Votyakov, B. Knaepen, O. Zikanov: “Theory of Lorentz force flow meter”, New Journal of Physics, Vol. 9(8), 299, 1-27, 2007. [5] A. Thess, E. Votyakov, Y. Kolesnikov: “Lorentz Force Velocimetry”, Phys. Rev. Lett. 96(16), 164501, 2006. [6] A. Thess, Y. Kolesnikov, Ch. Karcher patent (2005): Verfahren und Anordnung zur berührungslosen Inspektion bewegter elektrisch leitfähiger Substanzen, Patentschrift TU Ilmenau. [7] A. Thess, Y. Kolesnikov, Ch. Karcher: patent WO 2007/033982, (2007). [8] R. Moreau: Magnetofluiddynamics. Fluid mechanics and its applications. Kluwer Academic Publishers, Dordrecht (1990). [9] G.K. Batchelor: An Introduction to Fluid Dynamics. Cambridge mathematical library. Cambridge University Press. (2000). [10] K. Cukierski and B. G. Thomas: Flow Control with Local Electromagnetic Braking in Continuous Casting of Steel Slabs, Metallurgical and Materials Transactions B, 2008, Volume 39, Number 1, pp. 94107. [11] I. Bucenieks: “Modeling of rotary inductive electromagnetic flow meter for liquid metal flow control” In: Proceedings of the 5th International Symposium on Magnetic Suspension Technology, Dresden, Germany, 2005, 204-208. XIV [12] J. Priede, D. Buchenau and G. Gerbeth: „Singel-magnet rotary flow meter for liquid metals“. J. Appl. Phys. 110, 034512(2011.) [13] J. Priede, D. Buchenau and G. Gerbeth: „Contactless electromagnetic phase-shift flow meter for liquid metals“. Meas. Sci. Technol. 22(5), 055402 (2011). [14] S. Eckert, W. Witke, G. Gerbeth:“A new mechano-opitical technique to measure local velocities in opaque fluids“. Flow Meas. Instrum, 11, 71-78. (2000). [15] H. Hayashi, A. Becker and J.W. EVANS: “Toward A Probe for Velocity Measurement in Molten Metals at High Temperatures”. Metallurgical and Materials Transactions B, vol 30 (B), 1999, pp. 623-630. [16] O. Andreev, Yu. Kolesnikov, A. Thess: “Experimental study of liquid metal channel flow under the influence of a non-uniform magnetic field”. Phys. of Fluids, 19, 039902 (2007). [17] S. Eckert, G. Gerbeth: “Velocity measurements in liquid sodium by means of ultrasound Doppler velocimetry”. Experiments in Fluids, 32, 542-546. (2002). [18] B.G. Thomas, et al.: “Comparison of four methods to evaluate fluid velocities in a continuous slab casting mold”. ISIJ International (Japan), 41(10). 1262-1271. (2001). [19] M. Iguchi, et al.: “Development and calibration of a karman vortex probe for measurement of molten-steel velocities”. Metals and Materials Transactions B, Vol 30(B), p. 53-59. 1999. [20] J. Kubota, et al.: “Steel Flow Control in Continuous Caster Mold by Traveling Magnetic Field”. NKK Tech. Rev. pp. 1-9. (2001). [21] B. Rietow and B.G. Thomas: “Using Nail Board Experiments to Quantify Surface Velocity in the CC Mold”. AISTTech Steelmaking Conference Proc., (Pittsburgh, PA, May 5-8, 2008). XV [22] S.R. Higson, P. Drake, M. Lewus: Flowvis: Final report “Measurement, prediction and control of steel flows in the casting nozzle and mould”, Research Fund for Coal and Steel, 01.07.2004-30.06. (2008). [23] J. A. Shercliff: The Theory of Electromagnetic Flow Measurement; Cambridge University Press. (1962). [24] P. A. Davidson: An Introduction to Magneto hydrodynamics. Cambridge University Press. Cambridge (2001). [25] L. Bühler, U. Müller: Magnetofluiddynamics in Channels and Containers; Berlin, Springer (2001). [26] A. Vire, B. Knaepen, A. Thess: “Lorentz force velocimetry based on Time-of-Flight measurements”, Phys. Fluids 22, 125101 (2010). [27] D. Jian, Ch. Karcher: Electromagnetic flow measurements in liquid metals using Time-of-Flight Lorentz force velocimetry, Meas. Sci. Technol. 23, 074021 (14pp). (2012). [28] M. S. Beck: “Correlation in instruments: Cross correlation flowmeters”. J. Phys. E 14, 7 (1981). [29] J. B. Morton and W. H. Clark: “Measurements of two-point velocity correlations in a pipe flow using laser anemometers”, J. Phys. E 4, 809 (1971). [30] D. Jian, Ch. Karcher: Flow rate measurements in turbulent liquid metal channel flow using Time-of-Flight Lorentz force velocimetry. PAMM • Proc. Appl. Math. Mech. Submitted in December 2012. [31] D. Jian, Ch. Karcher: Non-contact measurements in liquid metal freesurface flow using Time-of-Flight Lorentz force velocimetry, 141st TMS Annual Meeting & Exhibition, Orlando, FL, USA, 11.-15. March.2012. (EPD Congress 2012). pp. 105-112. [32] D. Jian, Ch. Karcher: Electromagnetic flow rate measurement in turbulent liquid metal channel flow. PAMM Proc. Appl. Math. Mech. Volume 11, Issue 1, pp. 645–646, December 2011. XVI [33] D. Jian, Ch. Karcher: Electromagnetic flow control using Lorentz force velocimetry: experimental investigations and numerical modeling. Proceeding of 8th PAMIR International Conference, Borgo, Corsica, France, 05. - 09. Sept. 2011, pp. 665-669. [34] M. Rivero, D. Jian, C. Karcher and C. Sergio: Ultrasound Doppler Velocimetry measurements in turbulent liquid metal channel flow. 63rd Annu. Meeting of the APS Division of Fluid Dynamics. (2010). [35] J D. Siegwarth: Vortex Shedding Flow Meter Performance At High Flow Velocities (Washington, DC: US Government Printing Office). (1986). [36] H. Schlichting et. al: Boundary-Layer Theory. Berlin: Springer. (2004). [37] Y. Li: Numerische Untersuchungen zur Wirbelstrassenbildung in turbulenten Flüssigmetall-Kanalströmungen mit kleinem Aspektverhältnis Masterarbeit, Institut of Thermodynamics and Fluid Mechanics, Ilmenau University of Technology, 2012. [38] Y. Kolesnikov, A. Thess: “Experimental investigation of liquid metal flow across a non-homogeneous magnetic field”. - In: Proceedings / International Conference on Electromagnetic Processing of Materials; 6 (Dresden). pp. 41-44 (2009). [39] E. Votyakov, Y. Kolesnikov, O. Andreev, E. Zienicke, and A. Thess: “structure of the wake of a magnetic obstacle”, physical review letters, PRL 98, 144504 (2007). [40] A. Mansour: Numerische Untersuchungen zur Time-of-Flight Lorentzkraft-Anemometrie in Flüssigmetallströmungen mit freier Grenzfläche. Masterarbeit, Institut of Thermodynamics and Fluid Mechanics, Ilmenau University of Technology, 2012. [41] S. Buhl und M. Habqa: Simulation von Flüssigmetallströmungen unter lokalem Magnetfeldeinfluss. Projektseminar, Institut of Thermo- XVII dynamics and Fluid Mechanics, Ilmenau University of Technology, 2012. [42] L.D. Landau, E.M. Lifshitz: Course of theoretical physics. Vol. 6: Fluid mechanics 2nd Ed., Pergamon Press, pp. 336-343.(1987) [43] H. Alfven: Existence of electromagnetic – Hydrodynamic waves, Nature. Vol. 150, pp. 405-406. (1942) [44] J. A. Shercliff: A textbook of Magnetofluiddynamics, Pergamon, (1965). [45] S. Asai: Electromagnetic Processing of Materials: Materials Processing by Using Electric and Magnetic Functions. Fluid Mechanics and Its Applications, Vol. 99. XI, Dordrecht, Springer. (2012) [46] J.D. Jackson: Classical Electrodynamics. Wiley, New York, 3rd edition (1998) [47] J. Hartmann: Hg-dynamics I. Theory of the laminar flow of an electrically conductive liquid in a homogeneous magnetic field. Det Kgl. Danske Videnskabernes Selskab: Mathemastisk-fysiske Meddelelser, 15 (6): 1-28, (1937) [48] J. Hartmann and F. Lazarus: Hg-dynamics II. Experimental investigations on the flow of mercury in a homogeneous magnetic field. Det Kgl. Danske Videnskabernes Selskab: Mathemastisk-fysiske Meddelelser, 15 (7): 1-45, (1937) [49] P.H. Roberts: An Introduction to Magnetofluiddynamics. American Elsevier Publishing Company, Inc., New York (1967). [50] A. Galitis., O. Lielausis, E. Platacis, G. Gerbeth, F. Stefani: The Riga Dynamo Experiment, Suveys in Geophysics, Vol. 24, Issue 3, pp 247267. [51] J. Hemp: Theory of eddy currents in electromagnetic flowmeters. J. Phys D: Appl. Phys. 24, pp. 244-251. (1991). XVIII [52] M.K. Bevir: The theory of induced voltage electromagnetic flowmeters. J. Fluid Mech. 43, pp. 577-590. (1970). [53] A. Cramer, J. Pal and G. Gerbeth: Turbulence measurements in a rotating magnetic field driven flow. Phys. Fluids 24, 045105 (2012). [54] A. Cramer, K. Varshney, Th. Gundrum, G. Gerbeth: Experimental study on the sensitivity and accuracy of electrical potential local flow measurements. Flow Measurement and Instrumentation 17, pp. 1-11. (2006). [55] R. McDavid and B.G.Thomas: “Flow and thermal behavior of the top surface flux/powder layers in continuous casting molds” Metall. Mat. Trans. B, vol. 27B, pp. 672-685. (1996). [56] R. P. Pawlek: Secondary Aluminium Activities during 2006; Int. Aluminium J. 83(3). (2007). [57] I. Bucenieks: Perspectives of using rotating permanent magnets in the design of electromagnetic induction pumps. Magnetofluiddynamics, 36(2), 2000. [58] I. Bucenieks: Electromagnetic induction flowmeter on permanent magnets. Proceedings of the 8th International Pamir Conference on Fundamental and Applied MFD, 103-105, (2002). [59] J. Priede, D. Bucheau and G. Gerbeth: Force-free and contactless sensor for electromagnetic flowrate measurements. Magnetofluiddynamics, 45(3): pp. 451-458, (2009). [60] R. Ricou and C. Vives: Local velocity and mass transfer measurements in molten metals using an incorporated magnet probe. International Journal of Heat and Mass Transfer, 25: 1579-1588, (1982). [61] J.U. Knebel and L. Krebs: Calibration of a miniature permanent magnet flowmeter probe and its application to velocity measurements in liquid sodium. Experimental Thermal and Fluid Science, 8(2): 135148, (1994). XIX [62] O. Andreev, Y. Kolesnikov and A. Thess: Application of the ultrasonic velocity profile method to the mapping of liquid metal flows under the influence of a non-uniform magnetic field. Exp. Fluids, 46, pp. 7783, (2009). [63] S. Eckert, G. Gerbeth and V.I. Melnikov: Velocity measurements at high temperatures by ultrasound Doppler velocimetry using an acoustic wave guid. Exp. Fluids, 35, pp. 381-388, (2003). [64] Y. Takeda: Measurement of velocity profile of mercury flow by ultrasound Doppler shift method. Nuclear Technology, 79, pp. 120-124. (1987). [65] L. Buehler: Magnetohydrodynamic flows in arbitrary geometries in strong non-uniform magnetic fields. Fusion Technol., 27, pp. 3-24, (1995). [66] F. Boonstoppel, V. Veltman and F. Kergrouwen: The measurement of flow by cross correlation techniques, IEE Conf., Publication No. 43, (1968). [67] M. S. Beck, J. Drane, A. Plaskowski and N. Wainwright: Particle velocity and mass flow measurement in pneumatic conveyors, Powder Technology 2, 269-77, (1968). [68] P. G. Bentley and D. G. Dawson: Fluid flow measurement by transit time analysis of temperature fluctuations, Trans. Soc. Instrum. Technol. 18 183-93. [69] G. Pankanin: The vortex flowmeter: various methods of investigating phenomena. Meas. Sci. Technol. 16, (2005). [70] S. Cuevas, S. Smolentsev and M.A. Abdou: On the flow past a magnetic obstacle, Journal of Fluid Mechanics, 553, pp. 227-252, (2006). [71] Ch. Karcher, Y. Kolesnikov, H. Schreiber, A. Thess: Lorentz Force Velocimetry: Industrial Application. 2nd International Workshop on XX Measuring Techniques for Liquid Metal Flows, MTLM2007, Dresden, April 23-25. [72] J. Wernstedt: Experimentelle prozessanalyse. Berlin: Verl. Technik, 1989. [73] J. Hoffmann: Taschenbuch der Messtechnik. Fachbuchverl. Leipzig im Carl-Hanser-Verl. 2011. [74] John R. Taylor: Fehleranalyse: eine Einführung in die Untersuchung von Unsicherheiten in physikalischen Messungen. Weinheim: VCH, 1988. [75] H. Harada, T. Toh, T. Ishii, K. Kaneko and E. Takeuchi: Effect of magnetic field conditions on the electromagnetic braking efficiency. ISIJ INT, 41(10), pp. 1236-1244. (2001). [76] J. Kubota: in Mold Operation for Quality and Productivity, Cramb, Szekeres, eds. Iron & Steel Soc., 1991. [77] Y. Kolesnikov, Ch. Karcher and A. Thess: Lorentz force flow meter for liquid aluminum: Laboratory experiments and plant tests. Metall. Mater. Trans. B, 42(3), (2011). [78] D. Jian, Ch. Karcher: Non-contact local flow measurement using Lorentz force velocimetry in Time-of-Flight arrangement, Proceedings of International symposium on liquid metal processing and casting (LMPC), Nancy, France 25.-28. Sept. 2011. [79] D. Jian, Ch. Karcher, A. Thess, X. Xu, A. Deng, En. Wang: Development of Non-contact electromagnetic surface velocity sensor for molten metal using Time-of-Flight technique, Journal of Iron and Steel Research, International. Vol. 19, Supplement 1-1, pp. 509 - 513, 2012, ISSN 1006-706X. /CN 11-3678/TF. [80] K. U. Köhler, P. Andrezejewski, E. Julius, H. Haubrich: „Measurement of Steel Flow in the Mould." International Symposium on Elec- XXI tromagnetic Processing of Materials, 1994, Nagoya, Japan, pp. 344 – 349. [81] Discussions with P.A. Davison, 10.01.2012. [82] M.H. Butterfield, G.F. Bryant and J. Dowsing: A new method of strip speed measurement using random waveform correlation. Trans. Soc. Instrum. Tech. 13. 111-123 (1961). [83] J.C Hill, C.A Sleicher: Directional sensitivity of hot-fil sensors in liquid metals. Rev Sci Instrum 42, pp. 1461-1468. (1971). [84] I. Platnieks, G. Uhlmann: Hot-wire sensor for liquid sodium. J Phys E: Sci Instrum 17, pp. 862-863. (1984). [85] T. Von Weissenfluh: Probes for local velocity and temperature measurements in liquid metal flow. Int J Heat Mass Transfer 28. pp. 15631574. (1985). XXII Appendix A1Physicalpropertiesofliquidmetals Steel Liquidus temperature T [°C] 1510 Solidus temperature T [°C] 1480 7.89 Density [103 kg/m3] -6 2 0.85 Kinematic viscosity [10 m /s] 6 0.77 (liquid) Electrical conductivity σel [10 /Ωm] 0.8 (solid) Thermal conductivity λ [W/Km] 25 Surface tension σ [N/m] 1.6 Table A1: Physical properties of liquid metals. Sn60Bi40 170 138 8.25 0.19 1.05 Ga68In20Sn12 10.5 35 0.46 39 0.53 6.36 0.34 3.46 Klaus Timmel, Sven Eckert, Gunter Gerbeth, Frank Stefani and Thomas Wondrak: ISIJ International, Vol. 50 (2010), No.8, pp. 1134-1141. XXIII A2Experimentalmatrixforopenchannelflowmeasure‐ ments The Tables below (Table A2-1 and A2-2) summarize the experimental matrix for open channel flow measurement using SnPbBi at 210°C. Table A2-1: ToF LFV; edge length of magnet 20mm Run 1 2 3 4 5 6 7 8 9 10 11 12 Gap height Cylinder Data # H=30mm without 312 313 314 with 315 316 320 H=10mm with 317 318 319 without 321 322 323 04_41_28 05_18_57 05_54_45 06_36_46 07_05_00 09_03_46 07_33_09 08_01_25 08_32_32 03_52_44 04_11_37 04_37_17 TSnPbBi [°C] 215-120 205-157 204-147 212-155 205-149 213-147 220-157 213-144 217-154 209-148 208-169 209-154 Table A2-2: ToF LFV; edge length of magnet 15mm 13 H=20mm without 324 05_17_52 216 14 05_48_00 213 325 15 06_26_46 210 326 16 06_56_00 212 with 327 17 07_42_12 208 328 18 08_12_19 207 329 trun [s] 260 285 222 190 263 269 233 252 276 166 179 212 Thousing [°C] 30.5-33.5 34.6-34.8 35.5-35.2 35.3-35.5 35.7-35.9 36.6-36.5 36-36.3 35.9-36.1 36.3-36.4 27.7-28.2 29.0-29.3 30.6-30.8 164 155 172 302 341 270 31.1-31.1 31.6-31.6 31.7-31.7 31.7-31.7 31.8-31.5 31.5-31.5 The Table below (Table A2-3) summarizes the experimental matrix for open channel flow measurement using steel at 1700°C. Run Gap height[mm] 1 H=20mm 2 3 4 H=10mm 5 6 Data # 330 05_10_56 331 05_40_42 332 07_07_35 333 07_29_07 334 07_55_00 335 08_20_38 Tsteel [°C] 1667 1700 1680 1680 1670 1680 trun [s] 26,7 19,5 16,35 18,2 21 18,65 Thousing [°C] 28,9-29,1 38,1-40 35,9-42 42-50 48-54 52,3-55 XXIV A3Straingaugeforcesensor The employed force measurement systems are based on measuring the deflection of a parallel aluminum spring. The aluminum parallel spring acts as the deflection element when a force is superimposed on it [73]. The sensitive direction of the parallel spring is in streamwise direction. The deflection is measured with a strain gauge. This strain gauge is basically a thin electrical wire that changes its resistance upon changing its length. A picture of the force measurement system is shown in Fig. A3. By means of the basic relations we explain the functional principle of strain gauge sensor. The maximum load and the resolution of which the aluminum deflection element bears are shown in Table A3-1. Accordingly, the performance parameters of the used D/A converter and amplifier are shown in Table A3-2. l l0 relative change of length Hooke’s law E EE mod ulus of elasticity tensile stress Poisson’s ratio d l d l d relative change of diameter d l relative change of length l l A density of conductor Resistance law R Fig. A3: Design of a strain gauge force sensor. A cross sec tion l length of conductor R k 1 2 R k-factor: sensitivity of strain gauge XXV Nominal load Measurement priciple Nominal variable Class of accuracy Error of linearity Operate voltage Fmax Soemer Platform load cell Model 1004 Velomat PBB-8A-2N-2.00 Maul Alpha scale 16405 3N 2N 4.9N DMS full bridge DMS full bridge 0.86mV/V±0.1% C3 0.5mV/V±0.1% 0.1 ≤0.1SN Max. 10V 3V/10V 8N 5N 10V 3N+250% Temperatur compensated Resolution 0.1g Fmin 0.002N Total Error ±0.02% of load Table A3-1: Performance parameters of the used force sensor. Soemer LDU 78.1 InstruNational Instru- National ments ments NI USB 9237 NI USB-9219 Resolution 19bit 24 bit 24bit Bridge voltage UB 5V 0,125--60V 2,5-10V Channel 1 4 4 Sampling rate 25Hz(real) 100Hz 50kHz pro channel Linearity <0,002% Input signal 2,2mV/V Max. voltage range -60V/60V -10V/10V Min. voltage rage -125mV/125mV -2,5V/2,5V Accuracy by UB= +/-0,4% 4V Connection RS-422 USB USB USB Table A3-2: Performance parameters of the used D/A converter and amplifier. XXVI A4Errorestimationofexperiments During any experiments, various random and systematic errors appear. To eliminate all errors in an experiment is impossible. Hence, the experimentalist has to keep the influences of the errors as less as possible. Therefore, it is necessary to know the possible sources of errors and to calculate quantitatively the values of errors, if possible. Systematic errors include errors that occur because of incorrectly calibrated measuring instruments or the influence of the measured object on the measurement device. Such errors occur repetitively in the experimental runs. It can be captured by estimation of average and standard deviation of a large number of repeated measurements. The arithmetic average x and the standard deviation s of a measured quantity x are defined by the following relations. Arithmetic average: x 1 n xi . n i 1 (A1) Standard deviation: s n 1 ( xi x)2 . n (n 1) i 1 (A2) Random errors are in principle not controllable. Due to fluctuations of voltage in the electrical power supply, the opening and the closing of doors and windows in the experimental environment, stochastic vibrations of the building, or acoustic noise triggered by the air conditioning unit in the laboratory. Since there are many potential interferences and influence factors that cannot be exactly determined -such as humidity, temperature inside the laboratory, discontinuity in the probe, bucking the driving engine, and externally generated mechanical vibrations by walking- the random errors can only be roughly estimated. Error estimation of the measured Lorentz force FL using single LFV We start with the error estimation in the model experiment LiMeSCo where the measured force acting on a magnet due to the rotation of solid aluminum sheet. The relation between the measured Lorentz force FL and the influencing factors, i.e. the rotating speed u of the aluminum sheet, the height H between magnet and solid body, the magnitude of magnetization m and the electrical conductivity of the metallic body is given by the relation 02um2 FL . H3 (A3) See chapter 1.4 for the detailed derivation of this formula. Here we take the values for both m and from respective data sheets and suppose that the uncer- XXVII tainty in these values is negligible compared to the uncertainty in the measurement of H. Due to the positioning system used in the experiment, H can be measured with an uncertainty of 0.01 mm. Table A4 summarizes error estimation for a given constant rotation speed of the metallic body u = 32.76cm/s. Here, we list the measured quantities H and FL along with the average and the standard deviation of as well as the error in FL by varying the height H. H [mm] arithmetic average of FL [mN] standard deviation standard of FL [mN] in % deviation 1.4 398.5497 41.3585 10% 1.6 374.6205 41.5839 11% 2 335.3014 35.8837 11% 2.4 300.8547 44.4736 15% 2.8 271.4194 25.7318 9% 3 255.1280 50.2966 20% 3.4 227.0289 22.5932 10% 3.8 205.6078 18.5867 9% 4.2 188.0563 17.2553 9% 4.6 167.9492 18.1923 11% 5 142.4282 18.8820 13% 8 76.7906 13.0395 17% 10 51.1089 13.5545 27% 12 34.7239 11.7275 34% 14 24.8306 3.7032 15% 16 16.4672 8.1893 50% 19 10.2717 6.1984 60% 23 5.5654 2.2559 41% 27 3.2810 2.1739 66% 29 2.5572 1.5512 61% 31 1.8834 1.1239 60% 33 1.5669 0.9578 61% 37 1.0019 1.8128 181% Table A4-1: Error estimation of the measured FL using single LFV. From these data we can clearly conclude that an increase in H results in an increase of the standard deviation of measured FL. Error estimation of the measured velocity using ToF LFV For the Time-of-Flight method, the two important influencing quantities are the separation distance D of the two Lorentz force flow meters and the measured time shift . With these two values at hand we calculate the vortex velocity Vvortex according to the relation XXVIII Vmeasured D . (A4) See chapter 1.4 for details. The uncertainty V of the calculated velocity can be determined by propagation of uncertainty [74]: ∆D D d d 2 . ∆V V(D,) ∆D V(D,) ∆ dD dτ (A5) Here we have omitted the subscript in representing the vortex velocity. The uncertainty of the two input parameters and their standard deviation in the measured velocity for the electromagnetic free surface velocity measurement in annulus flow is shown in the following table. Input parameters Distance of magnetsystem D Transit time Typical quantities Respective uncertainty Standard deviation 7.5cm 0.2cm 2.67% 0.24s 0.01s 4.17% + Measured V =33.48cm/s 7.14% 31.25cm/s V =29.20cm/s Velocity V 6.56% Table A4-2: Error estimation of the free surface velocity measurement. First we estimate the uncertainty of the measurement of D overall to be 0.2cm. The uncertainty of the reference photoelectric sensor from the manufacturer is 0.12mm. The uncertainty of the driving unit of the channel (electrical motor) is ±0.2%. The standard deviation is less than 5% when the rotating speed of the channel smaller than 15cm/s. The deviation of the measured velocity comparing MVS sensor to reference sensor is approximately about 3%. Interestingly, the smaller the disturbing body the higher is the discrepancy from the measured velocity. We find an uncertainty of about 10% for a styrofoam diameter of 40mm and an uncertainty about 20% for a diameter of 10mm. Input parameters Typical quantities Respective uncertainty Distance of 22cm 0.5cm magnetsystem D Transit time 0.73s 0.04s Measured V+=32.60cm/s 30.14cm/s V-=27.29cm/s Velocity V Table A4-3: Error estimation of flow rate measurement. Standard deviation 2.27% 5.48% 8.16% 9.45% Erklärung (gemäß Anlage 1 der Siebten Änderung der Promotionsordnung der TU Ilmenau – Allgemeine Bestimmungen) Ich versichere, dass ich die vorliegende Arbeit ohne unzulässige Hilfe Dritter und ohne Benutzung anderer als der angegebenen Hilfsmittel angefertigt habe. Die aus anderen Quellen direkt oder indirekt übernommenen Daten und Konzepte sind unter Angabe der Quelle gekennzeichnet. Bei der Auswahl und Auswertung folgenden Materials haben mir die nachstehend aufgeführten Personen in der jeweils beschriebenen Weise entgeltlich/unentgeltlich 1) geholfen: 1. .........Numerische Untersuchungen im Rahmen von Projektseminar: Stefan Buhl, Mohsen Habqa 2. .........Numerische Untersuchungen im Rahmen von Masterarbeit: Abdallah Mansour 3. .........Numerische Untersuchungen im Rahmen von Studienarbeit: Yang Li Weitere Personen waren an der inhaltlich-materiellen Erstellung der vorliegenden Arbeit nicht beteiligt. Insbesondere habe ich hierfür nicht die entgeltliche Hilfe von Vermittlungs- bzw. Beratungsdiensten (Promotionsberater oder anderer Personen) in Anspruch genommen. Niemand hat von mir unmittelbar oder mittelbar geldwerte Leistungen für Arbeiten erhalten, die im Zusammenhang mit dem Inhalte der vorgelegten Dissertation stehen. Die Arbeit wurde bisher weder im In- noch im Ausland in gleicher oder ähnlicher Form einer Prüfungsbehörde vorgelegt. Ich bin darauf hingewiesen worden, dass die Unrichtigkeit der vorstehenden Erklärung als Täuschungsversuch bewertet wird und gemäß § 7 Abs. 10 der Promotionsordnung den Abbruch des Promotionsverfahrens zur Folge hat. (Ort, Datum) (Unterschrift) --------------------------------------------------------------------------1) Unzutreffendes bitte streichen