Rock Pile Phase II Environmental Investigation Report
Transcription
Rock Pile Phase II Environmental Investigation Report
PHASE II ENVIRONMENTAL INVESTIGATION REPORT Beech Grove Rock Pile Site Bellefontaine Street and Garstang Street Beech Grove, Indiana Schneider Job No. 6892.002 Beech Grove Redevelopment Commission 806 Main Street Beech Grove, Indiana 46107 Date: March 28, 2008 Historic Fort Harrison 8901 Otis Avenue Indianapolis, IN 46216-1037 ! " # $# %& ' () * () ) +( ) March 28, 2008 # , ' ! " $# %& )() -" . . /01 1" . ! $# %& Mr. Terry Dilk Beech Grove Redevelopment Commission 806 Main Street Beech Grove, Indiana 46107 2 3( Re: ( /% 24 1" ( 5 6 $ # %& ( 1 5 "7 1" - '. 4 $# %& ( ) Phase II Environmental Investigation Beech Grove Rock Pile Site Bellefontaine Street and Garstang Street Beech Grove, Indiana Schneider Project No. 6892.002 Dear Mr. Dilk: In accordance with our proposal dated January 4, 2008, The Schneider (( 8 1" 8 9 3 -" $# %&) Corporation (Schneider) recently conducted Phase II environmental sampling activities at the Rock Pile Site located southwest of the intersection of Bellefontaine Street and Garstang Street in Beech Grove, Indiana (see Attachment A for a site vicinity map). The scope of the Phase II sampling .( ! : 1" !6 $# !. activities was designed to investigate potential groundwater and soil impacts to the subject site associated with recognized environmental conditions (RECs) identified at the site during the completion of a Phase I Environmental Site 5 ! 2 $%5 -" )( purpose of this letter report is to present the findings of our recent Phase II site sampling activities. ! !""!! &; 6 * 1" ( % $, %() Assessment (ESA) for the property (ESA report dated February 11, 2008). The 7 Background Site Information The subject property, referred to as the Rock Pile Site, is approximately seven (7) acres in size and is undeveloped with no building structures, though several large piles of crushed rocks are currently present at the site. The following two recognized environmental conditions (i.e., evidence of a past, existing, or a material threat of a future release of hazardous substances or petroleum products) were identified at the site during the performance of the Phase I Environmental Site Assessment (ESA) for the site: ) • Limited environmental investigation activities were conducted at the study site in 1992 and 1993 on behalf of former prospective purchasers of the site. Hydrocarbon contaminated fill material was identified in 1992 during the completion of geotechnical soil borings at the site. Sampling of the fill material identified the presence of several polynuclear aromatic hydrocarbons (referred to as PAHs or by the synonym, PNAs). Subsequent site investigation work conducted in 1993 reportedly confirmed the presence of PAHs in darkly stained shallow fill material present at the site. Up to 1,000 cubic yards of PAH contaminated fill material was estimated to be present at the study site. • Three (3) Leaking Underground Storage Tank (LUST) sites that have reported soil and groundwater impacts and are actively undergoing investigation and/or remediation are located within 1/16th mile of the study site. Due to their close proximity to the study site, it is possible that the groundwater quality of the study site has been adversely impacted by these sites. Scope of Phase II Investigation The scope of the Phase II environmental sampling activities conducted at the study site consisted of the following: • Fourteen (14) soil borings were completed across the study site utilizing a Geoprobe drilling rig. Each of the borings was completed to the depth of the uppermost groundwater encountered. Ten (10) of the borings were located around the perimeter of the study site, while the remaining four (4) borings were located on the central/eastern portion of the study site (see Attachment B for a sample location map). One (1) soil sample was collected from each of the fourteen (14) soil boring locations at varying depth intervals. The depth interval sampled from each soil boring was determined through the use of a photo ionization detector (PID), in that the soil depth interval from each boring resulting in the highest PID total hydrocarbon reading was sampled. • Seven (7) samples of the uppermost groundwater at the site were collected from seven (7) of the fourteen (14) soil borings that were completed as a part of the soil sampling activities described above (at GP-2, GP-4, GP-6, GP-8, GP10, GP-11, and GP-12) (see Attachment B for sample locations). The groundwater samples were collected unfiltered with small diameter bailers from temporary 1 inch diameter PVC wells that were inserted into the seven (7) soil boring locations. • Borings from eleven (11) additional locations were completed across the site to a depth of five (5) feet below the ground surface to visually inspect the site for the presence of darkly stained shallow fill material that was described in previous site environmental studies. No samples were collected for laboratory analysis from locations where dark soils were not encountered; these locations are also illustrated on the sample location figure provided in Attachment B. • Each of the fourteen (14) soil samples and seven (7) groundwater samples collected at the site were submitted under chain-of-custody documentation to an analytical laboratory (Pace Analytical Services, Inc. of Indianapolis) for the analysis of volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), polychlorinated biphenyls (PCBs), and RCRA 8 heavy metals. The sampling activities described above were conducted at the study site on January 24th, 25th, and 26th, 2008. Results of these sampling activities are discussed below. Analytical Results The analytical results from the Phase II sampling activities are summarized in Tables 1 and 2 that are provided in Attachment C. As shown in Table 1, heavy metal compounds were detected in each of the fourteen (14) site soil samples collected. In four (4) of the site soil sample locations, one (1) or more organic compounds (i.e., VOCs, SVOCs, and/or PCB compounds) was also detected (from locations GP-9, GP-10, GP-13, and GP-23). These four (4) soil samples were all collected from the eastern portion of the study site. It is noted, however, that we suspect the lone VOC detection in soil sample GP-13 of acetone, a common laboratory agent used for cleaning instruments, to be a laboratory artifact rather than indicative of site conditions. The sample location figure in Attachment B graphically illustrates the estimated extent of the area with organic impacts in site soils. As shown in Table 2, heavy metal compounds were detected in each of the seven (7) site groundwater samples. One (1) organic compound, PCB-1254, was also detected in one (1) of the groundwater samples (GP-10). The complete analytical laboratory reports for the soil and groundwater analyses are provided as Attachment D. For comparative purposes, the tables in Attachment C also include Default Closure Levels from the Indiana Department of Environmental Management (IDEM) Risk Integrated System of Closure (RISC) Technical Guide for each of the compounds detected in the site samples. A sample detection that exceeds one (1) or both of the associated RISC Default Closure Levels is emphasized with a bold type box in the Attachment C tables. As shown in Table 1, five (5) compounds detected in site soils exceeded an associated RISC level (arsenic, chromium, lead, PCB-1254, and benzo(a)pyrene). Arsenic detections in site soils resulted in an exceedance of the associated RISC Default Closure Levels for residential and/or industrial site uses in thirteen (13) of the fourteen (14) soil sample locations. However, the levels of arsenic detected in site soils, which range from 2.8 milligrams per kilogram (mg/kg) to 9 mg/kg, appear to be in line with typical background levels of arsenic in soil. Lead detections in site soils resulted in an exceedance of the associated RISC Default Closure Levels in five (5) of the fourteen (14) soil sample locations (GP-9, GP-10, GP-12, GP-13, and GP-23). These five (5) soil sample locations are generally located on the eastern portion of the study site. The chromium detections in site soils that exceeded an associated RISC Default Closure Level occurred at GP-9 and GP-10; the PCB-1254 detection exceedance occurred at GP-9; and the benzo(a)pyrene exceedances occurred at GP-9, GP-10, and GP-23. As shown in Table 2, detections of heavy metal compounds in site groundwater resulted in an exceedance of an associated RISC Default Closure Level in each of the seven (7) site groundwater sample locations. The one detection of PCB-1254 at GP-10 also exceeded the associated RISC Default Closure Levels. Summary and Conclusions Phase II environmental sampling activities were conducted at the Rock Pile Site located in Beech Grove, Indiana on January 24th, 25th, and 26th, 2008 to investigate potential site impacts to soil and groundwater associated with recognized environmental conditions previously identified at the site during the completion of a Phase I ESA for the property. Based on the results of the sampling activities, it appears that impacts to site soils are generally limited to the eastern portion of the study site. These impacts appear likely to be associated with fill materials present on this portion of the study site. Five (5) compounds (arsenic, chromium, lead, PCB-1254, and benzo(a)pyrene) were detected in site soils at concentrations above one or both of the associated IDEM RISC Default Closure Levels, though the arsenic soil concentrations appear to be in line with typical soil background concentrations. Impacts to the uppermost site groundwater appear to be limited to heavy metal compounds and one organic compound, PCB-1254. Concentrations of arsenic, barium, cadmium, chromium, lead, selenium, and PCB-1254 from groundwater sampling locations across the study site were found to exceed one or both of the associated RISC Default Closure Levels. Due to the absence of any detectible levels of VOCs or SVOCs in site groundwater samples, it appears that the study site groundwater has not been adversely impacted by the nearby Leaking Underground Storage Tank (LUST) sites that were identified in the Phase I ESA report. It has been a pleasure to be of service to you and the Beech Grove Redevelopment Commission on this project. Please feel free to call us at (317) 826-7292 or (317) 826-7285 respectively, if you have any questions or would like to further discuss the findings of our Phase II investigation activities. Sincerely, Douglas Petroff Environmental Project Manager W. Calvin Kelly Director – Environmental Services and Brownfields Redevelopment Attachment A Site Vicinity Map """# #%&# % ! #$ ' () * +, . , / $0 !# ! Attachment B Soil and Groundwater Sample Locations Map LEGEND GP-21 GP-3 GP-2 GP-X Soil and groundwater sample location GP-Y Soil sample location GP-Z Visual inspection only GP-22 Estimated extent of organic compound impacts in soil GP-4 GP-1 GP-24 GP-19 GP-11 GP-23 GP-5 GP-10 GP-18 GP-13 GP-12 GP-6 GP-7 GP-20 GP-16 GP-17 GP-14 GP-9 GP-25 GP-15 The Schneider Corporation Historic Fort Harrison 8901 Otis Avenue Indianapolis, IN 46216 www.schneidercorp.com 866.973.7100 GP-8 Soil Boring Locations with Estimated Extent of Soil Impacts Former Rock Pile Site Beech Grove, Indiana Schneider Project Number 6892.002 Attachment C Sample Result Summary Tables TABLE I SUMMARY OF SOIL DETECTIONS Former Rock Pile Site Bellefontaine Street and Garstang Street Beech Grove, Indiana Constituent Arsenic Barium Chromium Lead Selenium Default RISC Level (mg/Kg) * PCB-1254 * Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Fluoranthene Indeno(1,2,3-cd)pyrene Phenanthrene Pyrene Acetone Naphthalene Soil (mg/Kg) Residential Industrial GP-1 (12-14) GP-2 (6-8) GP-3 (6-8) GP-4 (2-4) GP-5 (6-8) GP-6 (2-4) GP-7 (6-8) GP-8 (12-14) GP-9 (6-8) GP-10 (2-4) GP-11 (6-8) GP-12 (2-4) GP-13 (2-4) GP-23 (5-7) 3.9 1,600 38 81 5.2 5.8 10,000 120 230 53 4.8 33.6 7.7 5.8 ND 5.8 54 9.4 8.3 ND 5.5 50.2 9.7 7.6 ND 6.7 52.3 10.6 37.5 2.1 6.8 50.6 13.6 10.7 2.2 9 78.9 16.5 11.2 ND 2.8 59.6 14.9 8.2 ND 4 20.6 9.2 6.2 2.5 5.1 315 97.6 1,160 ND 9 382 149 1,480 3.8 4.5 49 9 7.5 ND 6.7 78.7 17.1 96.7 2.4 5.9 53 15.5 81.8 ND 7.7 52.6 19.8 101 2.1 1.8 18 51 5 0.5 5 -39 25 880 3.1 13 570 28 0.7 5.3 180 51 15 1.5 15 -39 25 880 3.1 170 570 370 170 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 12.7 0.43 0.954 2.09 1.94 2.52 1.3 1.29 2.15 4.4 1.17 1.92 3.63 ND 0.209 1.79 ND ND 0.544 0.567 0.843 0.38 ND 0.595 1.09 ND 0.636 0.942 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.115 ND ND ND 0.4 1.02 0.777 0.942 0.44 0.482 1.05 1.69 0.407 0.976 1.31 ND ND Notes: ND = Not Detected Boxed value exceeds default residential RISC level Samples Collected January 24, 2008 *PCB and Chromium RISC Level values presented in this table are for Total PCBs and Chromium VI Dashes (--) indicates a Default RISC Level is not available for this constituent TABLE 2 SUMMARY OF GROUNDWATER DETECTIONS Former Rock Pile Site Bellefontaine Street and Garstang Street Beech Grove, Indiana Constituent Arsenic Barium Cadmium Chromium Lead Selenium PCB-1254 Default RISC Level (mg/L) * * Groundwater (mg/L) Residential Industrial GP-2 GP-4 GP-6 GP-8 GP-10 GP-11 GP-12 0.01 2 0.005 0.1 0.015 0.05 0.01 20 0.051 0.31 0.042 0.51 0.16 1.24 0.0132 0.371 0.213 0.0497 0.078 0.86 0.005 0.249 0.114 0.0314 0.0821 0.976 0.0066 0.258 0.112 0.0312 0.519 3.26 0.0295 0.802 0.699 0.161 0.64 8.46 0.0515 1.79 9.6 0.215 0.141 1.08 0.0073 0.269 0.168 0.06 0.166 2.11 0.0101 0.343 0.82 0.0411 0.0005 0.0014 ND ND ND ND 0.0035 ND ND Notes: ND = Not Detected NA = Not Available Boxed value exceeds default residential RISC level Samples Collected January 25 and 26, 2008 All samples were collected unfiltered *PCB and Chromium RISC Level values presented in this table are for Total PCBs and Chromium VI Attachment D Analytical Laboratory Data Reports Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 LIMS USE: FR - DOUG PETROFF LIMS OBJECT ID: 5011474 February 11, 2008 Mr. Doug Petroff The Schneider Corporation 8901 Otis Ave Indianapolis, IN 46216 RE: Project: Beech Grove 6892.002 Pace Project No.: 5011474 Dear Mr. Petroff: Enclosed are the analytical results for sample(s) received by the laboratory on January 25, 2008. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Donna Spyker [email protected] Project Manager Illinois/NELAC Certification Number: 100418 Indiana Certification Number: C-49-06 Kansas Certification Number: E-10247 Kentucky Certification Number: 0042 Ohio VAP: CL0065 Pennsylvania: 68-00791 West Virginia Certification Number: 330 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE SUMMARY Project: Beech Grove 6892.002 Pace Project No.: 5011474 Lab ID Sample ID Matrix Date Collected Date Received 5011474001 GP-1 (12-14) Solid 01/24/08 09:00 01/25/08 13:24 5011474002 GP-2(6-8) Solid 01/24/08 09:30 01/25/08 13:24 5011474003 GP-3(6-8) Solid 01/24/08 10:00 01/25/08 13:24 5011474004 GP-4(2-4) Solid 01/24/08 10:20 01/25/08 13:24 5011474005 GP-5(6-8) Solid 01/24/08 10:45 01/25/08 13:24 5011474006 GP-6(2-4) Solid 01/24/08 11:00 01/25/08 13:24 5011474007 GP-7(6-8) Solid 01/24/08 11:30 01/25/08 13:24 5011474008 GP-8(12-14) Solid 01/24/08 13:00 01/25/08 13:24 5011474009 GP-9(6-8) Solid 01/24/08 13:30 01/25/08 13:24 5011474010 GP-10(2-4) Solid 01/24/08 14:00 01/25/08 13:24 5011474011 GP-11(6-8) Solid 01/24/08 14:30 01/25/08 13:24 5011474012 GP-12(2-4) Solid 01/24/08 15:30 01/25/08 13:24 5011474013 GP-13(2-4) Solid 01/24/08 16:00 01/25/08 13:24 5011474014 GP-23(5-7) Solid 01/24/08 17:30 01/25/08 13:24 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE ANALYTE COUNT Project: Beech Grove 6892.002 Pace Project No.: 5011474 Lab ID 5011474001 5011474002 5011474003 5011474004 5011474005 5011474006 5011474007 Sample ID GP-1 (12-14) GP-2(6-8) GP-3(6-8) GP-4(2-4) GP-5(6-8) GP-6(2-4) GP-7(6-8) Method Analysts Analytes Reported ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE ANALYTE COUNT Project: Beech Grove 6892.002 Pace Project No.: 5011474 Lab ID 5011474008 5011474009 5011474010 5011474011 5011474012 5011474013 Sample ID GP-8(12-14) GP-9(6-8) GP-10(2-4) GP-11(6-8) GP-12(2-4) GP-13(2-4) Method Analysts Analytes Reported EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE ANALYTE COUNT Project: Beech Grove 6892.002 Pace Project No.: 5011474 Lab ID Sample ID Method EPA 7471 5011474014 GP-23(5-7) Analysts LLB Analytes Reported 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 ASTM D2974-87 ILP 1 EPA 6010 FRW 7 EPA 7471 LLB 1 EPA 8082 SAQ 8 EPA 8260 ALA 73 EPA 8270 KES 66 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-1 (12-14) Lab ID: 5011474001 Collected: 01/24/08 09:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 70 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 39.7 39.7 39.7 39.7 39.7 39.7 39.7 28-137 1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 02/01/08 13:49 02/01/08 13:49 02/01/08 13:49 02/01/08 13:49 02/01/08 13:49 02/01/08 13:49 02/01/08 13:49 02/01/08 13:49 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 08:52 02/01/08 08:52 02/01/08 08:52 02/01/08 08:52 02/01/08 08:52 02/01/08 08:52 02/01/08 08:52 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 4.8 33.6 ND 7.7 5.8 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.1 2.1 2.1 2.1 2.1 2.1 2.1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.38 1 01/28/08 00:00 01/29/08 16:47 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 375 375 375 375 375 375 375 375 749 375 375 749 749 375 375 375 375 375 375 375 375 375 749 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 6 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-1 (12-14) Lab ID: 5011474001 Collected: 01/24/08 09:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 79 83 87 77 79 85 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 375 375 375 375 375 1820 1820 375 375 375 375 375 375 375 375 375 375 375 375 375 375 749 375 1820 1820 1820 375 375 1820 375 375 1820 341 375 375 375 375 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 01/31/08 02:35 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 7 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-1 (12-14) Lab ID: 5011474001 Collected: 01/24/08 09:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 88.6 88.6 88.6 4.4 4.4 4.4 4.4 4.4 4.4 22.1 4.4 4.4 4.4 8.9 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 88.6 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 8.9 4.4 4.4 88.6 88.6 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 8 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-1 (12-14) Lab ID: 5011474001 Collected: 01/24/08 09:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 98 98 101 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.4 4.4 17.7 22.1 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 88.6 4.4 8.9 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 01/29/08 14:12 0.10 1 02/01/08 11:29 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 11.9 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-2(6-8) Lab ID: 5011474002 Collected: 01/24/08 09:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 79 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 39.4 39.4 39.4 39.4 39.4 39.4 39.4 28-137 1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 02/01/08 13:58 02/01/08 13:58 02/01/08 13:58 02/01/08 13:58 02/01/08 13:58 02/01/08 13:58 02/01/08 13:58 02/01/08 13:58 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 09:20 02/01/08 09:20 02/01/08 09:20 02/01/08 09:20 02/01/08 09:20 02/01/08 09:20 02/01/08 09:20 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 5.8 54.0 ND 9.4 8.3 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.2 2.2 2.2 2.2 2.2 2.2 2.2 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.39 1 01/28/08 00:00 01/29/08 16:51 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 372 372 372 372 372 372 372 372 743 372 372 743 743 372 372 372 372 372 372 372 372 372 743 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 10 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-2(6-8) Lab ID: 5011474002 Collected: 01/24/08 09:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 83 86 87 82 83 88 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 372 372 372 372 372 1800 1800 372 372 372 372 372 372 372 372 372 372 372 372 372 372 743 372 1800 1800 1800 372 372 1800 372 372 1800 338 372 372 372 372 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 01/31/08 02:14 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 11 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-2(6-8) Lab ID: 5011474002 Collected: 01/24/08 09:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 84.5 84.5 84.5 4.2 4.2 4.2 4.2 4.2 4.2 21.1 4.2 4.2 4.2 8.5 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 84.5 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 8.5 4.2 4.2 84.5 84.5 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 12 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-2(6-8) Lab ID: 5011474002 Collected: 01/24/08 09:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 105 97 102 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.2 4.2 16.9 21.1 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 84.5 4.2 8.5 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 01/29/08 14:51 0.10 1 02/01/08 11:29 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 11.2 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-3(6-8) Lab ID: 5011474003 Collected: 01/24/08 10:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 78 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 40.6 40.6 40.6 40.6 40.6 40.6 40.6 28-137 1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 02/01/08 14:06 02/01/08 14:06 02/01/08 14:06 02/01/08 14:06 02/01/08 14:06 02/01/08 14:06 02/01/08 14:06 02/01/08 14:06 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 09:26 02/01/08 09:26 02/01/08 09:26 02/01/08 09:26 02/01/08 09:26 02/01/08 09:26 02/01/08 09:26 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 5.5 50.2 ND 9.7 7.6 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.1 2.1 2.1 2.1 2.1 2.1 2.1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.37 1 01/28/08 00:00 01/29/08 16:53 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 382 382 382 382 382 382 382 382 765 382 382 765 765 382 382 382 382 382 382 382 382 382 765 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 14 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-3(6-8) Lab ID: 5011474003 Collected: 01/24/08 10:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 75 76 80 75 76 82 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 382 382 382 382 382 1850 1850 382 382 382 382 382 382 382 382 382 382 382 382 382 382 765 382 1850 1850 1850 382 382 1850 382 382 1850 348 382 382 382 382 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 01/31/08 02:56 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 15 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-3(6-8) Lab ID: 5011474003 Collected: 01/24/08 10:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 84.6 84.6 84.6 4.2 4.2 4.2 4.2 4.2 4.2 21.1 4.2 4.2 4.2 8.5 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 84.6 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 8.5 4.2 4.2 84.6 84.6 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 16 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-3(6-8) Lab ID: 5011474003 Collected: 01/24/08 10:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 99 100 103 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.2 4.2 16.9 21.1 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 84.6 4.2 8.5 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 01/29/08 15:30 0.10 1 02/01/08 11:34 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 13.7 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 17 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-4(2-4) Lab ID: 5011474004 Collected: 01/24/08 10:20 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 22 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 207 207 207 207 207 207 207 28-137 5 5 5 5 5 5 5 5 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 14:37 02/06/08 14:37 02/06/08 14:37 02/06/08 14:37 02/06/08 14:37 02/06/08 14:37 02/06/08 14:37 02/06/08 14:37 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 09:31 02/01/08 09:31 02/01/08 09:31 02/01/08 09:31 02/01/08 09:31 02/01/08 09:31 02/01/08 09:31 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 1d S4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 6.7 52.3 ND 10.6 37.5 2.1 ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.2 2.2 2.2 2.2 2.2 2.2 2.2 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.39 1 01/28/08 00:00 01/29/08 16:54 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 3890 3890 3890 3890 3890 3890 3890 3890 7770 3890 3890 7770 7770 3890 3890 3890 3890 3890 3890 3890 3890 3890 7770 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 18 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-4(2-4) Lab ID: 5011474004 Collected: 01/24/08 10:20 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 48 44 46 43 45 41 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 3890 3890 3890 3890 3890 18800 18800 3890 3890 3890 3890 3890 3890 3890 3890 3890 3890 3890 3890 3890 3890 7770 3890 18800 18800 18800 3890 3890 18800 3890 3890 18800 3530 3890 3890 3890 3890 50-117 56-118 55-118 41-124 35-117 34-122 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 01/31/08 04:19 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 2d S4 S4 S4 Page 19 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-4(2-4) Lab ID: 5011474004 Collected: 01/24/08 10:20 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 90.1 90.1 90.1 4.5 4.5 4.5 4.5 4.5 4.5 22.5 4.5 4.5 4.5 9.0 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 90.1 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 9.0 4.5 4.5 90.1 90.1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 20 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-4(2-4) Lab ID: 5011474004 Collected: 01/24/08 10:20 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 100 99 100 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.5 4.5 18.0 22.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 90.1 4.5 9.0 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 01/29/08 16:09 0.10 1 02/01/08 11:35 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 15.4 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 21 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-5(6-8) Lab ID: 5011474005 Collected: 01/24/08 10:45 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 61 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 40.3 40.3 40.3 40.3 40.3 40.3 40.3 28-137 1 1 1 1 1 1 1 1 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 14:45 02/06/08 14:45 02/06/08 14:45 02/06/08 14:45 02/06/08 14:45 02/06/08 14:45 02/06/08 14:45 02/06/08 14:45 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 09:49 02/01/08 09:49 02/01/08 09:49 02/01/08 09:49 02/01/08 09:49 02/01/08 09:49 02/01/08 09:49 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 6.8 50.6 ND 13.6 10.7 2.2 ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.1 2.1 2.1 2.1 2.1 2.1 2.1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.40 1 01/28/08 00:00 01/29/08 16:55 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 380 380 380 380 380 380 380 380 760 380 380 760 760 380 380 380 380 380 380 380 380 380 760 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 22 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-5(6-8) Lab ID: 5011474005 Collected: 01/24/08 10:45 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 72 77 78 74 75 79 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 380 380 380 380 380 1840 1840 380 380 380 380 380 380 380 380 380 380 380 380 380 380 760 380 1840 1840 1840 380 380 1840 380 380 1840 345 380 380 380 380 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 01/31/08 03:17 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 23 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-5(6-8) Lab ID: 5011474005 Collected: 01/24/08 10:45 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 98.4 98.4 98.4 4.9 4.9 4.9 4.9 4.9 4.9 24.6 4.9 4.9 4.9 9.8 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 98.4 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 9.8 4.9 4.9 98.4 98.4 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 24 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-5(6-8) Lab ID: 5011474005 Collected: 01/24/08 10:45 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 99 96 99 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.9 4.9 19.7 24.6 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 4.9 98.4 4.9 9.8 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 01/29/08 16:48 0.10 1 02/01/08 11:35 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 13.2 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 25 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-6(2-4) Lab ID: 5011474006 Collected: 01/24/08 11:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 57 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 42.0 42.0 42.0 42.0 42.0 42.0 42.0 28-137 1 1 1 1 1 1 1 1 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 14:53 02/06/08 14:53 02/06/08 14:53 02/06/08 14:53 02/06/08 14:53 02/06/08 14:53 02/06/08 14:53 02/06/08 14:53 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 09:54 02/01/08 09:54 02/01/08 09:54 02/01/08 09:54 02/01/08 09:54 02/01/08 09:54 02/01/08 09:54 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 9.0 78.9 ND 16.5 11.2 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.2 2.2 2.2 2.2 2.2 2.2 2.2 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.39 1 01/28/08 00:00 01/29/08 16:57 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 396 396 396 396 396 396 396 396 792 396 396 792 792 396 396 396 396 396 396 396 396 396 792 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 26 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-6(2-4) Lab ID: 5011474006 Collected: 01/24/08 11:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 71 72 72 69 70 76 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 396 396 396 396 396 1920 1920 396 396 396 396 396 396 396 396 396 396 396 396 396 396 792 396 1920 1920 1920 396 396 1920 396 396 1920 360 396 396 396 396 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 01/30/08 21:22 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 27 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-6(2-4) Lab ID: 5011474006 Collected: 01/24/08 11:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 87.0 87.0 87.0 4.4 4.4 4.4 4.4 4.4 4.4 21.8 4.4 4.4 4.4 8.7 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 87.0 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 8.7 4.4 4.4 87.0 87.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 28 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-6(2-4) Lab ID: 5011474006 Collected: 01/24/08 11:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 97 100 102 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.4 4.4 17.4 21.8 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 87.0 4.4 8.7 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 01/29/08 17:27 0.10 1 02/01/08 11:35 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 16.6 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 29 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-7(6-8) Lab ID: 5011474007 Collected: 01/24/08 11:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 69 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 43.6 43.6 43.6 43.6 43.6 43.6 43.6 28-137 1 1 1 1 1 1 1 1 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 15:01 02/06/08 15:01 02/06/08 15:01 02/06/08 15:01 02/06/08 15:01 02/06/08 15:01 02/06/08 15:01 02/06/08 15:01 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:00 02/01/08 10:00 02/01/08 10:00 02/01/08 10:00 02/01/08 10:00 02/01/08 10:00 02/01/08 10:00 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 2.8 59.6 ND 14.9 8.2 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.3 2.3 2.3 2.3 2.3 2.3 2.3 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.43 1 01/28/08 00:00 01/29/08 16:58 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 410 410 410 410 410 410 410 410 820 410 410 820 820 410 410 410 410 410 410 410 410 410 820 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 30 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-7(6-8) Lab ID: 5011474007 Collected: 01/24/08 11:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 74 76 76 70 73 77 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 410 410 410 410 410 1990 1990 410 410 410 410 410 410 410 410 410 410 410 410 410 410 820 410 1990 1990 1990 410 410 1990 410 410 1990 373 410 410 410 410 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 01/30/08 22:46 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 31 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-7(6-8) Lab ID: 5011474007 Collected: 01/24/08 11:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 103 103 103 5.2 5.2 5.2 5.2 5.2 5.2 25.8 5.2 5.2 5.2 10.3 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 103 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 10.3 5.2 5.2 103 103 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 32 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-7(6-8) Lab ID: 5011474007 Collected: 01/24/08 11:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 101 96 99 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 5.2 5.2 20.7 25.8 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 103 5.2 10.3 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 01/29/08 18:07 0.10 1 02/01/08 11:36 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 19.8 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 33 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-8(12-14) Lab ID: 5011474008 Collected: 01/24/08 13:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 63 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 38.5 38.5 38.5 38.5 38.5 38.5 38.5 28-137 1 1 1 1 1 1 1 1 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 15:09 02/06/08 15:09 02/06/08 15:09 02/06/08 15:09 02/06/08 15:09 02/06/08 15:09 02/06/08 15:09 02/06/08 15:09 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:06 02/01/08 10:06 02/01/08 10:06 02/01/08 10:06 02/01/08 10:06 02/01/08 10:06 02/01/08 10:06 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 4.0 20.6 ND 9.2 6.2 2.5 ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.1 2.1 2.1 2.1 2.1 2.1 2.1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.35 1 01/28/08 00:00 01/29/08 17:00 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 363 363 363 363 363 363 363 363 726 363 363 726 726 363 363 363 363 363 363 363 363 363 726 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 34 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-8(12-14) Lab ID: 5011474008 Collected: 01/24/08 13:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 78 79 76 74 78 77 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 363 363 363 363 363 1760 1760 363 363 363 363 363 363 363 363 363 363 363 363 363 363 726 363 1760 1760 1760 363 363 1760 363 363 1760 330 363 363 363 363 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 01/30/08 21:02 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 35 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-8(12-14) Lab ID: 5011474008 Collected: 01/24/08 13:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 77.5 77.5 77.5 3.9 3.9 3.9 3.9 3.9 3.9 19.4 3.9 3.9 3.9 7.7 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 77.5 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 7.7 3.9 3.9 77.5 77.5 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 36 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-8(12-14) Lab ID: 5011474008 Collected: 01/24/08 13:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 98 99 100 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 3.9 3.9 15.5 19.4 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 3.9 77.5 3.9 7.7 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 01/29/08 18:46 0.10 1 02/01/08 11:36 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 9.1 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 37 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-9(6-8) Lab ID: 5011474009 Collected: 01/24/08 13:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND 12700 ND 0 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 3900 3900 3900 3900 3900 3900 3900 28-137 100 100 100 100 100 100 100 100 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 16:44 02/06/08 16:44 02/06/08 16:44 02/06/08 16:44 02/06/08 16:44 02/06/08 16:44 02/06/08 16:44 02/06/08 16:44 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:11 02/01/08 10:11 02/01/08 10:11 02/01/08 10:11 02/01/08 10:11 02/01/08 10:11 02/01/08 10:11 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 S4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 5.1 315 ND 97.6 1160 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.1 2.1 2.1 2.1 2.1 2.1 2.1 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.38 1 01/28/08 00:00 01/29/08 17:01 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND 430 954 2090 1940 2520 1300 1290 ND ND ND ND ND ND ND ND ND ND ND 2150 ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 367 367 367 367 367 367 367 367 735 367 367 735 735 367 367 367 367 367 367 367 367 367 735 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 38 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-9(6-8) Lab ID: 5011474009 Collected: 01/24/08 13:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND 4400 ND ND ND ND ND 1170 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1920 ND 3630 ND ND 71 72 75 71 72 80 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 367 367 367 367 367 1780 1780 367 367 367 367 367 367 367 367 367 367 367 367 367 367 735 367 1780 1780 1780 367 367 1780 367 367 1780 334 367 367 367 367 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 01/31/08 00:29 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 39 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-9(6-8) Lab ID: 5011474009 Collected: 01/24/08 13:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 84.7 84.7 84.7 4.2 4.2 4.2 4.2 4.2 4.2 21.2 4.2 4.2 4.2 8.5 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 84.7 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 8.5 4.2 4.2 84.7 84.7 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 40 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-9(6-8) Lab ID: 5011474009 Collected: 01/24/08 13:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND 209 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 97 100 95 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.2 4.2 16.9 21.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 84.7 4.2 8.5 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 01/29/08 19:25 0.10 1 02/01/08 11:37 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 10.2 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 41 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-10(2-4) Lab ID: 5011474010 Collected: 01/24/08 14:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND 1790 ND 0 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 803 803 803 803 803 803 803 20-130 20 20 20 20 20 20 20 20 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/08/08 15:30 02/08/08 15:30 02/08/08 15:30 02/08/08 15:30 02/08/08 15:30 02/08/08 15:30 02/08/08 15:30 02/08/08 15:30 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:17 02/01/08 10:17 02/01/08 10:17 02/01/08 10:17 02/01/08 10:17 02/01/08 10:17 02/01/08 10:17 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 S4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 9.0 382 ND 149 1480 3.8 ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.2 2.2 2.2 2.2 2.2 2.2 2.2 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.38 1 01/28/08 00:00 01/29/08 17:02 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND 544 567 843 380 ND ND ND ND ND ND ND ND ND ND ND ND 595 ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 379 379 379 379 379 379 379 379 757 379 379 757 757 379 379 379 379 379 379 379 379 379 757 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 42 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-10(2-4) Lab ID: 5011474010 Collected: 01/24/08 14:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND 1090 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 636 ND 942 ND ND 71 75 77 69 67 72 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 379 379 379 379 379 1840 1840 379 379 379 379 379 379 379 379 379 379 379 379 379 379 757 379 1840 1840 1840 379 379 1840 379 379 1840 344 379 379 379 379 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 01/31/08 00:09 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 43 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-10(2-4) Lab ID: 5011474010 Collected: 01/24/08 14:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 95.9 95.9 95.9 4.8 4.8 4.8 4.8 4.8 4.8 24.0 4.8 4.8 4.8 9.6 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 95.9 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 9.6 4.8 4.8 95.9 95.9 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 44 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-10(2-4) Lab ID: 5011474010 Collected: 01/24/08 14:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 98 99 94 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.8 4.8 19.2 24.0 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 95.9 4.8 9.6 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 01/29/08 20:04 0.10 1 02/01/08 11:37 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 12.8 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 45 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-11(6-8) Lab ID: 5011474011 Collected: 01/24/08 14:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 61 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 42.5 42.5 42.5 42.5 42.5 42.5 42.5 28-137 1 1 1 1 1 1 1 1 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 15:37 02/06/08 15:37 02/06/08 15:37 02/06/08 15:37 02/06/08 15:37 02/06/08 15:37 02/06/08 15:37 02/06/08 15:37 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:23 02/01/08 10:23 02/01/08 10:23 02/01/08 10:23 02/01/08 10:23 02/01/08 10:23 02/01/08 10:23 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 4.5 49.0 ND 9.0 7.5 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.3 2.3 2.3 2.3 2.3 2.3 2.3 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.40 1 01/28/08 00:00 01/29/08 17:04 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 401 401 401 401 401 401 401 401 801 401 401 801 801 401 401 401 401 401 401 401 401 401 801 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 46 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-11(6-8) Lab ID: 5011474011 Collected: 01/24/08 14:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 68 71 69 71 71 73 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 401 401 401 401 401 1940 1940 401 401 401 401 401 401 401 401 401 401 401 401 401 401 801 401 1940 1940 1940 401 401 1940 401 401 1940 364 401 401 401 401 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 01/30/08 20:41 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 47 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-11(6-8) Lab ID: 5011474011 Collected: 01/24/08 14:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 90.4 90.4 90.4 4.5 4.5 4.5 4.5 4.5 4.5 22.6 4.5 4.5 4.5 9.0 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 90.4 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 9.0 4.5 4.5 90.4 90.4 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 48 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-11(6-8) Lab ID: 5011474011 Collected: 01/24/08 14:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 98 98 97 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.5 4.5 18.1 22.6 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 90.4 4.5 9.0 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 01/29/08 20:43 0.10 1 02/01/08 11:37 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 17.6 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 49 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-12(2-4) Lab ID: 5011474012 Collected: 01/24/08 15:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 0 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 199 199 199 199 199 199 199 28-137 5 5 5 5 5 5 5 5 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/06/08 15:45 02/06/08 15:45 02/06/08 15:45 02/06/08 15:45 02/06/08 15:45 02/06/08 15:45 02/06/08 15:45 02/06/08 15:45 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:28 02/01/08 10:28 02/01/08 10:28 02/01/08 10:28 02/01/08 10:28 02/01/08 10:28 02/01/08 10:28 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 3d S4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 6.7 78.7 ND 17.1 96.7 2.4 ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.2 2.2 2.2 2.2 2.2 2.2 2.2 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.37 1 01/28/08 00:00 01/29/08 17:08 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 3750 3750 3750 3750 3750 3750 3750 3750 7500 3750 3750 7500 7500 3750 3750 3750 3750 3750 3750 3750 3750 3750 7500 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 50 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-12(2-4) Lab ID: 5011474012 Collected: 01/24/08 15:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 76 83 83 79 77 77 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 3750 3750 3750 3750 3750 18200 18200 3750 3750 3750 3750 3750 3750 3750 3750 3750 3750 3750 3750 3750 3750 7500 3750 18200 18200 18200 3750 3750 18200 3750 3750 18200 3410 3750 3750 3750 3750 50-117 56-118 55-118 41-124 35-117 34-122 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 01/31/08 01:53 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 4d Page 51 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-12(2-4) Lab ID: 5011474012 Collected: 01/24/08 15:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 89.7 89.7 89.7 4.5 4.5 4.5 4.5 4.5 4.5 22.4 4.5 4.5 4.5 9.0 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 89.7 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 9.0 4.5 4.5 89.7 89.7 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 52 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-12(2-4) Lab ID: 5011474012 Collected: 01/24/08 15:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 98 97 96 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.5 4.5 17.9 22.4 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 4.5 89.7 4.5 9.0 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 01/29/08 21:22 0.10 1 02/01/08 11:37 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 12.0 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 53 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-13(2-4) Lab ID: 5011474013 Collected: 01/24/08 16:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 65 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 41.7 41.7 41.7 41.7 41.7 41.7 41.7 28-137 1 1 1 1 1 1 1 1 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/07/08 13:25 02/07/08 13:25 02/07/08 13:25 02/07/08 13:25 02/07/08 13:25 02/07/08 13:25 02/07/08 13:25 02/07/08 13:25 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:34 02/01/08 10:34 02/01/08 10:34 02/01/08 10:34 02/01/08 10:34 02/01/08 10:34 02/01/08 10:34 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 5.9 53.0 ND 15.5 81.8 ND ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.2 2.2 2.2 2.2 2.2 2.2 2.2 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.40 1 01/28/08 00:00 01/29/08 16:23 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 393 393 393 393 393 393 393 393 786 393 393 786 786 393 393 393 393 393 393 393 393 393 786 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 54 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-13(2-4) Lab ID: 5011474013 Collected: 01/24/08 16:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 69 70 73 68 69 72 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 393 393 393 393 393 1900 1900 393 393 393 393 393 393 393 393 393 393 393 393 393 393 786 393 1900 1900 1900 393 393 1900 393 393 1900 357 393 393 393 393 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 01/30/08 23:27 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 55 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-13(2-4) Lab ID: 5011474013 Collected: 01/24/08 16:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 115 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 87.7 87.7 87.7 4.4 4.4 4.4 4.4 4.4 4.4 21.9 4.4 4.4 4.4 8.8 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 87.7 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 8.8 4.4 4.4 87.7 87.7 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 56 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-13(2-4) Lab ID: 5011474013 Collected: 01/24/08 16:00 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 97 98 96 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.4 4.4 17.5 21.9 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 4.4 87.7 4.4 8.8 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 01/29/08 21:41 0.10 1 02/01/08 11:38 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 16.0 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 57 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-23(5-7) Lab ID: 5011474014 Collected: 01/24/08 17:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV SHORT LIST MICROWAVE Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3546 ND ND ND ND ND ND ND 57 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % 39.3 39.3 39.3 39.3 39.3 39.3 39.3 20-130 1 1 1 1 1 1 1 1 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/05/08 00:00 02/08/08 09:40 02/08/08 09:40 02/08/08 09:40 02/08/08 09:40 02/08/08 09:40 02/08/08 09:40 02/08/08 09:40 02/08/08 09:40 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 02/01/08 10:40 02/01/08 10:40 02/01/08 10:40 02/01/08 10:40 02/01/08 10:40 02/01/08 10:40 02/01/08 10:40 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3050 7.7 52.6 ND 19.8 101 2.1 ND mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.2 2.2 2.2 2.2 2.2 2.2 2.2 1 1 1 1 1 1 1 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 01/31/08 00:00 Analytical Method: EPA 7471 Preparation Method: EPA 7471 ND mg/kg 0.36 1 01/28/08 00:00 01/29/08 16:25 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND 400 1020 777 942 440 482 ND ND ND ND ND ND ND ND ND ND ND 1050 ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 371 371 371 371 371 371 371 371 742 371 371 742 742 371 371 371 371 371 371 371 371 371 742 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 Page 58 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-23(5-7) Lab ID: 5011474014 Collected: 01/24/08 17:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8270 MSSV SHORT LIST MICROWAVE 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ND ND ND ND ND ND ND ND ND ND 1690 ND ND ND ND ND 407 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 976 ND 1310 ND ND 66 82 77 70 77 77 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 371 371 371 371 371 1800 1800 371 371 371 371 371 371 371 371 371 371 371 371 371 371 742 371 1800 1800 1800 371 371 1800 371 371 1800 337 371 371 371 371 50-117 56-118 55-118 41-124 35-117 34-122 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 02/01/08 20:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 02/04/08 14:24 120-83-2 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Page 59 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-23(5-7) Lab ID: 5011474014 Collected: 01/24/08 17:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene n-Hexane 2-Hexanone Iodomethane Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg 91.8 91.8 91.8 4.6 4.6 4.6 4.6 4.6 4.6 23.0 4.6 4.6 4.6 9.2 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 91.8 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 9.2 4.6 4.6 91.8 91.8 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 67-64-1 107-02-8 107-13-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 110-54-3 591-78-6 74-88-4 Page 60 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove 6892.002 Pace Project No.: 5011474 Sample: GP-23(5-7) Lab ID: 5011474014 Collected: 01/24/08 17:30 Received: 01/25/08 13:24 Matrix: Solid Results reported on a "dry-weight" basis Parameters 8260 MSV 5035A VOA Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 02/11/2008 03:29 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 97 97 99 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % 4.6 4.6 18.4 23.0 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 4.6 91.8 4.6 9.2 82-130 81-120 65-117 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 01/30/08 00:55 0.10 1 02/01/08 11:39 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 2037-26-5 460-00-4 Analytical Method: ASTM D2974-87 11.0 % REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 61 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: MERP/1508 Analysis Method: EPA 7471 QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury Associated Lab Samples: METHOD BLANK: 5011474013, 5011474014 126575 Associated Lab Samples: 5011474013, 5011474014 Parameter Mercury mg/kg LABORATORY CONTROL SAMPLE: 126576 Parameter Mercury Blank Result Units ND Spike Conc. Units mg/kg MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Mercury Date: 02/11/2008 03:29 PM Units mg/kg Reporting Limit 0.33 LCS Result .5 ND LCS % Rec 0.51 126577 5011473001 Result Qualifiers % Rec Limits 101 Qualifiers 80-120 126578 MS Spike Conc. .62 MSD Spike Conc. .62 MS Result 0.72 MSD Result MS % Rec 0.66 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 110 MSD % Rec 101 % Rec Limits 75-125 Max RPD RPD 8 Qual 20 Page 62 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: MERP/1509 Analysis Method: EPA 7471 QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury Associated Lab Samples: METHOD BLANK: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012 126579 Associated Lab Samples: Parameter 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012 Blank Reporting Units Result Limit Qualifiers Mercury mg/kg LABORATORY CONTROL SAMPLE: 126580 Parameter Mercury ND mg/kg MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Mercury Date: 02/11/2008 03:29 PM Units mg/kg LCS Result Spike Conc. Units 0.33 .5 0.50 126581 5011471001 Result ND % Rec Limits LCS % Rec 101 Qualifiers 80-120 126582 MS Spike Conc. .53 MSD Spike Conc. .53 MS Result 0.53 MSD Result MS % Rec 0.53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 101 MSD % Rec 100 % Rec Limits 75-125 Max RPD RPD 1 Qual 20 Page 63 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: OEXT/5896 Analysis Method: EPA 8270 QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave Short Spike Associated Lab Samples: METHOD BLANK: 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013 126796 Associated Lab Samples: Parameter 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013 Blank Reporting Units Result Limit Qualifiers 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol(m&p Cresol) 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Dinitro-2-methylphenol 4-Bromophenylphenyl ether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenylphenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Date: 02/11/2008 03:29 PM ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 330 330 330 330 1600 330 330 330 330 330 330 1600 330 660 660 1600 1600 330 660 660 330 1600 1600 330 330 330 330 330 330 330 330 660 330 330 330 330 330 330 330 J 330 330 330 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 64 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 METHOD BLANK: 126796 Associated Lab Samples: Parameter 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013 Blank Reporting Units Result Limit Qualifiers Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % LABORATORY CONTROL SAMPLE: 126797 Parameter 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitroso-di-n-propylamine Pentachlorophenol Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) Date: 02/11/2008 03:29 PM ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 73 79 77 73 72 77 Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % Spike Conc. 3330 3330 3330 3330 3330 3330 3330 3330 3330 330 330 330 330 330 330 330 330 330 330 330 330 330 1600 300 330 330 34-122 56-118 35-117 50-117 41-124 55-118 LCS Result 2750 2730 2640 2880 2870 2640 2310 2830 2850 % Rec Limits LCS % Rec 82 82 79 86 86 79 69 85 85 79 82 81 78 81 82 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 54-124 56-111 61-115 42-122 57-113 52-128 24-132 54-117 51-119 34-122 56-118 35-117 50-117 41-124 55-118 Page 65 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitroso-di-n-propylamine Pentachlorophenol Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 126809 5011538002 Result ND ND ND ND ND ND ND ND 563 126810 MS Spike Conc. 4370 4370 4370 4370 4370 4370 4370 4370 4370 MSD Spike Conc. 4370 4370 4370 4370 4370 4370 4370 4370 4370 MS Result 4940 5320 4620 5280 5890 5680 3470 5160 5170 MSD Result MS % Rec 3120 2930 2630 3200 3480 3380 2000J 2930 5360 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 113 122 106 121 135 130 79 118 105 53 67 62 62 55 51 MSD % Rec 71 67 60 73 80 77 46 67 110 68 75 68 67 70 68 % Rec Limits 57-121 35-125 55-120 27-130 55-114 40-133 10-135 36-130 51-121 34-122 56-118 35-117 50-117 41-124 55-118 Max RPD RPD 45 58 55 49 51 51 55 4 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Qual R1 R1 R1 R1 M0,R1 R1 R1 R1 R1 R1,S0 Page 66 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: OEXT/5909 Analysis Method: EPA 8270 QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave Short Spike Associated Lab Samples: METHOD BLANK: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005 127147 Associated Lab Samples: Parameter 5011474001, 5011474002, 5011474003, 5011474004, 5011474005 Blank Reporting Units Result Limit Qualifiers 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol(m&p Cresol) 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Dinitro-2-methylphenol 4-Bromophenylphenyl ether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenylphenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Date: 02/11/2008 03:29 PM ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 330 330 330 330 1600 330 330 330 330 330 330 1600 330 660 660 1600 1600 330 660 660 330 1600 1600 330 330 330 330 330 330 330 330 660 330 330 330 330 330 330 330 J 330 330 330 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 67 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 METHOD BLANK: 127147 Associated Lab Samples: Parameter 5011474001, 5011474002, 5011474003, 5011474004, 5011474005 Blank Reporting Units Result Limit Qualifiers Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % LABORATORY CONTROL SAMPLE: 127148 Parameter 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitroso-di-n-propylamine Pentachlorophenol Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) Date: 02/11/2008 03:29 PM ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 83 83 84 80 84 87 Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % Spike Conc. 3330 3330 3330 3330 3330 3330 3330 3330 3330 330 330 330 330 330 330 330 330 330 330 330 330 330 1600 300 330 330 34-122 56-118 35-117 50-117 41-124 55-118 LCS Result 2670 2540 2370 2710 2640 2650 2490 2600 2840 % Rec Limits LCS % Rec 80 76 71 81 79 80 75 78 85 80 79 76 74 77 82 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 54-124 56-111 61-115 42-122 57-113 52-128 24-132 54-117 51-119 34-122 56-118 35-117 50-117 41-124 55-118 Page 68 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitroso-di-n-propylamine Pentachlorophenol Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 127149 5011565001 Result ND ND ND ND ND ND ND ND ND 127150 MS Spike Conc. 3960 3960 3960 3960 3960 3960 3960 3960 3960 MSD Spike Conc. 3960 3960 3960 3960 3960 3960 3960 3960 3960 MS Result 2500 2440 2320 2650 2470 2530 2200 2470 2510 MSD Result MS % Rec 2290 2460 2240 2430 2520 2700 2130 2580 2380 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 63 62 58 67 62 64 56 62 63 64 66 68 62 64 68 MSD % Rec 58 62 56 61 63 68 54 65 60 60 63 68 64 62 60 % Rec Limits 57-121 35-125 55-120 27-130 55-114 40-133 10-135 36-130 51-121 34-122 56-118 35-117 50-117 41-124 55-118 Max RPD RPD 9 1 3 9 2 6 3 4 5 Qual 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Page 69 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: MSV/7190 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics Associated Lab Samples: METHOD BLANK: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012 127302 Associated Lab Samples: Parameter 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012 Blank Reporting Units Result Limit Qualifiers 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene Date: 02/11/2008 03:29 PM ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 100 5.0 25.0 100 100 100 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 70 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 METHOD BLANK: 127302 Associated Lab Samples: Parameter 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012 Blank Reporting Units Result Limit Qualifiers cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Hexane n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % LABORATORY CONTROL SAMPLE: 127303 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene Date: 02/11/2008 03:29 PM ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 98 100 99 Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Spike Conc. 50 50 50 50 50 50 50 50 5.0 5.0 5.0 5.0 10.0 5.0 5.0 100 5.0 5.0 20.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 100 5.0 10.0 65-117 82-130 81-120 LCS Result LCS % Rec 43.8 48.6 55.9 55.2 48.7 51.9 48.7 47.1 % Rec Limits 88 97 112 110 97 104 97 94 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 69-124 67-129 68-130 72-129 68-128 65-138 71-126 63-130 Page 71 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 LABORATORY CONTROL SAMPLE: 127303 Parameter 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Hexane n-Propylbenzene Naphthalene Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Spike Conc. 50 50 50 50 50 50 50 50 50 50 50 50 250 50 250 50 250 250 1000 1000 50 50 50 50 50 50 100 50 50 50 50 50 50 50 50 50 50 50 50 50 100 50 100 50 50 50 50 50 LCS Result 51.6 40.8 45.3 50.5 44.9 52.0 51.7 45.1 44.4 53.2 47.2 41.5 286 46.4 297 43.5 275 280 3600 1120 49.2 48.1 57.1 45.8 38.0 56.9 97.1 41.6 45.6 58.3 48.4 47.6 51.4 41.4 41.5 52.8 41.7 56.0 46.8 44.3 96.8J 43.2 111 52.5 42.9 54.0 46.7 52.2 LCS % Rec % Rec Limits 103 82 91 101 90 104 103 90 89 106 94 83 114 93 119 87 110 112 360 112 98 96 114 92 76 114 97 83 91 117 97 95 103 83 83 106 83 112 94 89 97 86 111 105 86 108 93 104 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 52-131 59-132 72-129 71-126 72-128 63-130 73-124 72-132 73-130 71-127 71-125 61-134 59-150 73-135 46-150 72-130 54-146 41-150 50-150 L0 50-150 72-129 72-127 63-144 71-128 62-124 45-144 63-171 59-130 73-125 60-140 67-127 38-141 76-132 61-114 70-131 75-132 50-179 50-150 77-131 70-133 70-130 72-128 66-139 48-121 68-132 70-130 74-136 60-131 Page 72 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 LABORATORY CONTROL SAMPLE: 127303 Parameter p-Isopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % Spike Conc. 50 50 50 50 50 50 50 50 50 50 50 200 50 150 LCS Result 37.0 46.7 44.9 37.0 43.7 49.7 50.1 41.2 39.9J 50.7 44.2 181 41.7 134 LCS % Rec % Rec Limits 74 93 90 74 87 99 100 82 80 101 88 91 83 89 101 101 100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 69-134 74-135 75-125 69-124 55-123 75-127 71-131 62-114 50-150 72-123 62-150 50-150 54-136 70-130 65-117 82-130 81-120 Page 73 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: MSV/7193 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics Associated Lab Samples: METHOD BLANK: 5011474013 127310 Associated Lab Samples: 5011474013 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Blank Result Reporting Limit ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Qualifiers 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 100 5.0 25.0 100 100 100 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 74 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 METHOD BLANK: 127310 Associated Lab Samples: 5011474013 Parameter Units Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Hexane n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % LABORATORY CONTROL SAMPLE: 127311 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene Date: 02/11/2008 03:29 PM Reporting Limit ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 98 99 99 Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Blank Result Spike Conc. 50 50 50 50 50 50 50 50 50 50 50 Qualifiers 5.0 5.0 10.0 5.0 5.0 100 5.0 5.0 20.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 100 5.0 10.0 65-117 82-130 81-120 LCS Result LCS % Rec 41.3 47.3 50.9 55.0 50.6 53.1 51.0 48.2 48.5 44.4 43.8 % Rec Limits 83 95 102 110 101 106 102 96 97 89 88 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 69-124 67-129 68-130 72-129 68-128 65-138 71-126 63-130 52-131 59-132 72-129 Page 75 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 LABORATORY CONTROL SAMPLE: 127311 Parameter 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Hexane n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Spike Conc. 50 50 50 50 50 50 50 50 50 250 50 250 50 250 250 1000 1000 50 50 50 50 50 50 100 50 50 50 50 50 50 50 50 50 50 50 50 50 100 50 100 50 50 50 50 50 50 50 50 LCS Result 51.1 46.6 52.7 53.3 44.1 44.4 52.8 45.4 42.1 292 46.1 283 43.6 265 286 3700 1150 50.1 49.0 53.8 44.6 37.3 49.4 101 41.0 46.5 38.2 49.5 42.5 52.2 39.2 39.5 54.8 41.6 50.9 47.3 43.1 93.1J 45.2 114 50.4 42.2 52.7 46.2 51.6 42.1 45.6 44.1 LCS % Rec % Rec Limits 102 93 105 107 88 89 106 91 84 117 92 113 87 106 114 370 115 100 98 108 89 75 99 101 82 93 76 99 85 104 78 79 110 83 102 95 86 93 90 114 101 84 105 92 103 84 91 88 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 71-126 72-128 63-130 73-124 72-132 73-130 71-127 71-125 61-134 59-150 73-135 46-150 72-130 54-146 41-150 50-150 L0 50-150 72-129 72-127 63-144 71-128 62-124 45-144 63-171 59-130 73-125 60-140 67-127 38-141 76-132 61-114 70-131 75-132 50-179 50-150 77-131 70-133 70-130 72-128 66-139 48-121 68-132 70-130 74-136 60-131 69-134 74-135 75-125 Page 76 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 LABORATORY CONTROL SAMPLE: 127311 Parameter tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % Spike Conc. 50 50 50 50 50 50 50 50 200 50 150 LCS Result 38.7 42.7 47.9 51.0 38.8 41.7J 50.9 42.8 173 42.4 136 LCS % Rec % Rec Limits 77 85 96 102 78 83 102 86 87 85 90 103 101 99 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 69-124 55-123 75-127 71-131 62-114 50-150 72-123 62-150 50-150 54-136 70-130 65-117 82-130 81-120 Page 77 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: MSV/7194 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics Associated Lab Samples: METHOD BLANK: 5011474014 127312 Associated Lab Samples: 5011474014 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Blank Result Reporting Limit ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Qualifiers 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 100 5.0 25.0 100 100 100 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 78 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 METHOD BLANK: 127312 Associated Lab Samples: 5011474014 Parameter Units Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Hexane n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % LABORATORY CONTROL SAMPLE: 127313 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene Date: 02/11/2008 03:29 PM Reporting Limit ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 99 97 99 Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Blank Result Spike Conc. 50 50 50 50 50 50 50 50 50 50 50 Qualifiers 5.0 5.0 10.0 5.0 5.0 100 5.0 5.0 20.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 100 5.0 10.0 65-117 82-130 81-120 LCS Result LCS % Rec 35.3 41.8 50.8 49.9 48.1 50.2 49.2 48.0 49.0 45.1 44.7 % Rec Limits 71 84 102 100 96 100 98 96 98 90 89 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 69-124 67-129 68-130 72-129 68-128 65-138 71-126 63-130 52-131 59-132 72-129 Page 79 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 LABORATORY CONTROL SAMPLE: 127313 Parameter 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Hexane n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Spike Conc. 50 50 50 50 50 50 50 50 50 250 50 250 50 250 250 1000 1000 50 50 50 50 50 50 100 50 50 50 50 50 50 50 50 50 50 50 50 50 100 50 100 50 50 50 50 50 50 50 50 LCS Result 45.4 46.4 48.9 52.2 44.6 45.8 49.6 46.0 41.8 287 47.0 268 44.2 250 282 3440 1080 48.0 47.2 51.6 40.4 31.2 52.4 99.6 34.6 45.1 42.7 46.6 48.7 50.2 38.3 33.8 51.6 41.3 44.7 46.2 43.2 90.7J 44.8 103 45.5 43.2 50.4 48.0 48.4 43.1 45.9 43.5 LCS % Rec % Rec Limits 91 93 98 104 89 92 99 92 84 115 94 107 88 100 113 344 108 96 94 103 81 62 105 100 69 90 85 93 97 100 77 68 103 83 89 92 86 91 90 103 91 86 101 96 97 86 92 87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 71-126 72-128 63-130 73-124 72-132 73-130 71-127 71-125 61-134 59-150 73-135 46-150 72-130 54-146 41-150 50-150 L0 50-150 72-129 72-127 63-144 71-128 62-124 45-144 63-171 59-130 73-125 60-140 67-127 38-141 76-132 61-114 70-131 L0 75-132 50-179 50-150 77-131 70-133 70-130 72-128 66-139 48-121 68-132 70-130 74-136 60-131 69-134 74-135 75-125 Page 80 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 LABORATORY CONTROL SAMPLE: 127313 Parameter tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % Spike Conc. 50 50 50 50 50 50 50 50 200 50 150 LCS Result 41.5 41.7 46.1 49.0 37.9 44.8J 48.0 42.3 179 48.6 134 LCS % Rec % Rec Limits 83 83 92 98 76 90 96 85 90 97 89 104 97 98 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 69-124 55-123 75-127 71-131 62-114 50-150 72-123 62-150 50-150 54-136 70-130 65-117 82-130 81-120 Page 81 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: MPRP/2495 Analysis Method: EPA 6010 QC Batch Method: EPA 3050 Analysis Description: 6010 MET Associated Lab Samples: METHOD BLANK: 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014 127478 Associated Lab Samples: Parameter 5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014 Blank Reporting Units Result Limit Qualifiers Arsenic Barium Cadmium Chromium Lead Selenium Silver mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg LABORATORY CONTROL SAMPLE: 127479 Parameter Arsenic Barium Cadmium Chromium Lead Selenium Silver ND ND ND ND ND ND ND Spike Conc. Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Arsenic Barium Cadmium Chromium Lead Selenium Silver Date: 02/11/2008 03:29 PM LCS Result 50 50 50 50 50 50 25 4.8 33.6 ND 7.7 5.8 ND ND LCS % Rec 52.9 50.1 49.7 49.4 49.8 50.5 25.3 127480 5011474001 Result Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2.0 2.0 2.0 2.0 2.0 2.0 2.0 % Rec Limits 106 100 99 99 100 101 101 Qualifiers 80-120 80-120 80-120 80-120 80-120 80-120 80-120 127481 MS Spike Conc. 55.1 55.1 55.1 55.1 55.1 55.1 27.6 MSD Spike Conc. 51.7 51.7 51.7 51.7 51.7 51.7 25.8 MS Result 54.7 93.0 45.6 58.4 53.5 48.3 26.5 MSD Result MS % Rec 50.2 86.4 42.1 53.7 49.2 44.3 24.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 90 108 82 92 86 85 96 MSD % Rec 88 102 81 89 84 83 95 % Rec Limits 75-125 75-125 75-125 75-125 75-125 75-125 75-125 Max RPD RPD 8 7 8 8 8 9 7 Qual 20 20 20 20 20 20 20 Page 82 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: OEXT/5929 Analysis Method: EPA 8082 QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB Associated Lab Samples: METHOD BLANK: 5011474001, 5011474002, 5011474003 127494 Associated Lab Samples: Parameter 5011474001, 5011474002, 5011474003 Blank Units Result PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % LABORATORY CONTROL SAMPLE: 127495 Parameter PCB-1016 (Aroclor 1016) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) ND ND ND ND ND ND ND 100 PCB-1016 (Aroclor 1016) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) Date: 02/11/2008 03:29 PM Spike Conc. Units ug/kg ug/kg % MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Units ug/kg ug/kg % Reporting Limit 35.0 35.0 35.0 35.0 35.0 35.0 35.0 28-137 LCS Result 167 167 ND ND % Rec Limits LCS % Rec 173 172 127505 5011585002 Result Qualifiers 104 103 99 Qualifiers 50-150 50-150 28-137 127506 MS Spike Conc. 189 189 MSD Spike Conc. 189 189 MS Result 151 137 MSD Result MS % Rec 131 122 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 80 73 74 MSD % Rec 69 65 65 % Rec Limits 50-150 50-150 28-137 Max RPD RPD 14 11 Qual 20 20 20 Page 83 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: PMST/2211 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: SAMPLE DUPLICATE: 5011474001, 5011474002 127969 Parameter Units Percent Moisture SAMPLE DUPLICATE: 5011626001 Result Dup Result 2.8 % Max RPD RPD 2.9 4 Qualifiers 5 127970 Parameter Percent Moisture Date: 02/11/2008 03:29 PM Units % 5011623004 Result 14.0 Dup Result Max RPD RPD 14.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 2 Qualifiers 5 Page 84 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: PMST/2212 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: SAMPLE DUPLICATE: 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014 127974 Parameter Percent Moisture Date: 02/11/2008 03:29 PM Units % 5011474003 Result 13.7 Dup Result Max RPD RPD 11.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 14 Qualifiers 5 R2 Page 85 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: OEXT/5984 Analysis Method: EPA 8270 QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave Short Spike Associated Lab Samples: METHOD BLANK: 5011474014 128273 Associated Lab Samples: 5011474014 Parameter 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol(m&p Cresol) 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Dinitro-2-methylphenol 4-Bromophenylphenyl ether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenylphenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg Blank Result Reporting Limit ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Qualifiers 330 330 330 330 1600 330 330 330 330 330 330 1600 330 660 660 1600 1600 330 660 660 330 1600 1600 330 330 330 330 330 330 330 330 660 330 330 330 330 330 330 330 330 330 330 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 86 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 METHOD BLANK: 128273 Associated Lab Samples: 5011474014 Parameter Units Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % LABORATORY CONTROL SAMPLE: 128274 Parameter 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitroso-di-n-propylamine Pentachlorophenol Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) Date: 02/11/2008 03:29 PM Reporting Limit ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 84 82 83 75 82 90 Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % Blank Result Spike Conc. 3330 3330 3330 3330 3330 3330 3330 3330 3330 Qualifiers 330 330 330 330 330 330 330 330 330 330 330 330 330 1600 300 330 330 34-122 56-118 35-117 50-117 41-124 55-118 LCS Result 2290 2310 2190 2330 2420 2250 2090 2400 2330 % Rec Limits LCS % Rec 69 69 66 70 72 68 63 72 70 87 83 83 76 83 87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 54-124 56-111 61-115 42-122 57-113 52-128 24-132 54-117 51-119 34-122 56-118 35-117 50-117 41-124 55-118 Page 87 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitroso-di-n-propylamine Pentachlorophenol Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) Date: 02/11/2008 03:29 PM Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % % % % % % 128275 5011626001 Result ND ND ND ND ND ND ND ND ND 128276 MS Spike Conc. 3420 3420 3420 3420 3420 3420 3420 3420 3420 MSD Spike Conc. 3420 3420 3420 3420 3420 3420 3420 3420 3420 MS Result 2180 196J 823 ND 2190 1970 ND 1530 2330 MSD Result MS % Rec 2200 175J 760 ND 2340 2300 ND 1400 2560 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 64 6 24 0 64 57 0 36 66 0 75 7 67 40 87 MSD % Rec 64 5 22 0 68 67 0 32 73 0 79 5 71 38 92 % Rec Limits 57-121 35-125 55-120 27-130 55-114 40-133 10-135 36-130 51-121 34-122 56-118 35-117 50-117 41-124 55-118 Max RPD RPD 1 8 6 16 9 10 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Qual M0 M0 M0 M0 M0 S0 S0 S0 Page 88 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove 6892.002 Pace Project No.: 5011474 QC Batch: OEXT/6013 Analysis Method: EPA 8082 QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB Associated Lab Samples: METHOD BLANK: 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014 128786 Associated Lab Samples: Parameter 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014 Blank Reporting Units Result Limit Qualifiers PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg % LABORATORY CONTROL SAMPLE: 128787 Parameter PCB-1016 (Aroclor 1016) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) ND ND ND ND ND ND ND 83 ug/kg ug/kg % MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter PCB-1016 (Aroclor 1016) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) Date: 02/11/2008 03:29 PM Spike Conc. Units LCS Result 167 167 ND ND LCS % Rec 148 137 128788 5011662001 Units Result ug/kg ug/kg % 35.0 35.0 35.0 35.0 35.0 35.0 35.0 28-137 % Rec Limits 89 82 84 Qualifiers 50-150 50-150 28-137 128789 MS Spike Conc. 175 175 MSD Spike Conc. 175 175 MS Result 98.0 98.0 MSD Result MS % Rec 88.1 110 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 56 56 48 MSD % Rec 50 63 43 % Rec Limits 50-150 50-150 28-137 Max RPD RPD 11 12 Qual 20 20 20 Page 89 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALIFIERS Project: Beech Grove 6892.002 Pace Project No.: 5011474 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. ANALYTE QUALIFIERS 1d The Sample was analyzed at dilution due to its physical characteristics. SAQ 02.08.08 2d Due to the viscosity of the extract, it was run at 10x. KES 1-31-07 3d The Sample was analyzed at dilution due to its physical charachteristics. SAQ 02.08.08 4d Due to the viscosity of the extract, it was run at 10x. KES 1-31-08 J Analyte detected below reporting limit, therefore result is an estimate. L0 Analyte recovery in the laboratory control sample (LCS) was outside QC limits. M0 Matrix spike recovery was outside laboratory control limits. R1 RPD value was outside control limits. R2 RPD value was outside control limits due to matrix interference S0 Surrogate recovery outside laboratory control limits. S4 Surrogate recovery not evaluated against control limits due to sample dilution. Date: 02/11/2008 03:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 90 of 90 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 LIMS USE: FR - DOUG PETROFF LIMS OBJECT ID: 5011526 February 12, 2008 Mr. Doug Petroff The Schneider Corporation 8901 Otis Ave Indianapolis, IN 46216 RE: Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Dear Mr. Petroff: Enclosed are the analytical results for sample(s) received by the laboratory on January 28, 2008. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Donna Spyker [email protected] Project Manager Illinois/NELAC Certification Number: 100418 Indiana Certification Number: C-49-06 Kansas Certification Number: E-10247 Kentucky Certification Number: 0042 Ohio VAP: CL0065 Pennsylvania: 68-00791 West Virginia Certification Number: 330 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE SUMMARY Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Lab ID Sample ID Matrix Date Collected Date Received 5011526001 GP-11 Water 01/25/08 10:30 01/28/08 11:48 5011526002 GP-10 Water 01/25/08 11:30 01/28/08 11:48 5011526003 GP-8 Water 01/25/08 13:30 01/28/08 11:48 5011526004 GP-12 Water 01/25/08 15:30 01/28/08 11:48 5011526005 GP-2 Water 01/25/08 17:00 01/28/08 11:48 5011526006 GP-4 Water 01/26/08 12:30 01/28/08 11:48 5011526007 GP-6 Water 01/26/08 14:00 01/28/08 11:48 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE ANALYTE COUNT Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Lab ID 5011526001 5011526002 5011526003 5011526004 5011526005 5011526006 5011526007 Sample ID GP-11 GP-10 GP-8 GP-12 GP-2 GP-4 GP-6 Method Analysts Analytes Reported EPA 6010 FRW 7 EPA 7470 LLB 1 EPA 8082 SAQ 8 EPA 8260 SLB 72 EPA 8270 KES 66 EPA 6010 FRW 7 EPA 7470 LLB 1 EPA 8082 SAQ 8 EPA 8260 SLB 72 EPA 8270 KES 66 EPA 6010 FRW 7 EPA 7470 LLB 1 EPA 8082 SAQ 8 EPA 8260 SLB 72 EPA 8270 KES 66 EPA 6010 FRW 7 EPA 7470 LLB 1 EPA 8082 SAQ 8 EPA 8260 SLB 72 EPA 8270 KES 66 EPA 6010 FRW 7 EPA 7470 LLB 1 EPA 8082 SAQ 8 EPA 8260 SLB 72 EPA 8270 KES 66 EPA 6010 FRW 7 EPA 7470 LLB 1 EPA 8082 SAQ 8 EPA 8260 SLB 72 EPA 8270 KES 66 EPA 6010 FRW 7 EPA 7470 LLB 1 EPA 8082 SAQ 8 EPA 8260 SLB 72 EPA 8270 KES 66 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-11 Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Date: 02/12/2008 03:16 PM Lab ID: 5011526001 Results Units Collected: 01/25/08 10:30 Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ND ND ND ND ND ND 94 ug/L ug/L ug/L ug/L ug/L ug/L ug/L % 0.68 0.68 0.68 0.68 0.68 0.68 0.68 10-143 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/31/08 15:23 01/31/08 15:23 01/31/08 15:23 01/31/08 15:23 01/31/08 15:23 01/31/08 15:23 01/31/08 15:23 01/31/08 15:23 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 01/31/08 03:20 01/31/08 03:20 01/31/08 03:20 01/31/08 03:20 01/31/08 03:20 01/31/08 03:20 01/31/08 03:20 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3010 141 1080 7.3 269 168 60.0 ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10.0 100 5.0 10.0 10.0 10.0 50.0 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 6.0 1 01/29/08 00:00 01/30/08 15:45 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 12.2 12.2 12.2 12.2 12.2 12.2 12.2 12.2 24.4 12.2 12.2 24.4 24.4 12.2 12.2 6.1 12.2 12.2 12.2 12.2 12.2 12.2 24.4 12.2 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 120-83-2 Page 4 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-11 Parameters 8270 MSSV Semivolatile Organic Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Acetone Acrolein Acrylonitrile Date: 02/12/2008 03:16 PM Lab ID: 5011526001 Results Collected: 01/25/08 10:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 76 72 71 38 59 73 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % 12.2 12.2 12.2 12.2 61.0 61.0 12.2 12.2 12.2 6.1 12.2 12.2 6.1 12.2 24.4 12.2 12.2 12.2 12.2 12.2 24.4 6.1 61.0 61.0 61.0 12.2 12.2 61.0 12.2 12.2 61.0 12.2 12.2 12.2 12.2 12.2 40-112 31-114 10-116 10-100 13-100 26-125 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 100 100 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 01/30/08 18:51 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 10:54 67-64-1 01/31/08 10:54 107-02-8 01/31/08 10:54 107-13-1 Page 5 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-11 Parameters 8260 MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone Iodomethane Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Date: 02/12/2008 03:16 PM Lab ID: 5011526001 Results Collected: 01/25/08 10:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 25.0 10.0 5.0 5.0 5.0 25.0 4.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 591-78-6 74-88-4 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 Page 6 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-11 Parameters 8260 MSV Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Lab ID: 5011526001 Results Collected: 01/25/08 10:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 106 101 98 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 2.0 10.0 82-122 73-120 80-120 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 01/31/08 10:54 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 460-00-4 2037-26-5 Page 7 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-10 Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Date: 02/12/2008 03:16 PM Lab ID: 5011526002 Results Units Collected: 01/25/08 11:30 Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ND ND ND ND 3.5 ND 66 ug/L ug/L ug/L ug/L ug/L ug/L ug/L % 1.1 1.1 1.1 1.1 1.1 1.1 1.1 10-143 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 02/07/08 16:41 02/07/08 16:41 02/07/08 16:41 02/07/08 16:41 02/07/08 16:41 02/07/08 16:41 02/07/08 16:41 02/07/08 16:41 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 01/31/08 03:26 01/31/08 03:26 01/31/08 03:26 01/31/08 03:26 01/31/08 03:26 01/31/08 03:26 01/31/08 03:26 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3010 640 8460 51.5 1790 9600 215 ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L 50.0 500 25.0 50.0 50.0 50.0 250 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 20.0 1 01/29/08 00:00 01/30/08 15:47 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 13.7 13.7 13.7 13.7 13.7 13.7 13.7 13.7 27.4 13.7 13.7 27.4 27.4 13.7 13.7 6.8 13.7 13.7 13.7 13.7 13.7 13.7 27.4 13.7 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 120-83-2 Page 8 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-10 Parameters 8270 MSSV Semivolatile Organic Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Acetone Acrolein Acrylonitrile Date: 02/12/2008 03:16 PM Lab ID: 5011526002 Results Collected: 01/25/08 11:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 81 79 78 41 57 77 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % 13.7 13.7 13.7 13.7 68.5 68.5 13.7 13.7 13.7 6.8 13.7 13.7 6.8 13.7 27.4 13.7 13.7 13.7 13.7 13.7 27.4 6.8 68.5 68.5 68.5 13.7 13.7 68.5 13.7 13.7 68.5 13.7 13.7 13.7 13.7 13.7 40-112 31-114 10-116 10-100 13-100 26-125 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 100 100 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 01/31/08 01:11 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 11:24 67-64-1 01/31/08 11:24 107-02-8 01/31/08 11:24 107-13-1 Page 9 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-10 Parameters 8260 MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone Iodomethane Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Date: 02/12/2008 03:16 PM Lab ID: 5011526002 Results Collected: 01/25/08 11:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 25.0 10.0 5.0 5.0 5.0 25.0 4.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 591-78-6 74-88-4 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 Page 10 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-10 Parameters 8260 MSV Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Lab ID: 5011526002 Results Collected: 01/25/08 11:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 106 101 96 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 2.0 10.0 82-122 73-120 80-120 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 01/31/08 11:24 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 460-00-4 2037-26-5 Page 11 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-8 Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Date: 02/12/2008 03:16 PM Lab ID: 5011526003 Results Units Collected: 01/25/08 13:30 Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ND ND ND ND ND ND 90 ug/L ug/L ug/L ug/L ug/L ug/L ug/L % 0.64 0.64 0.64 0.64 0.64 0.64 0.64 10-143 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/31/08 15:40 01/31/08 15:40 01/31/08 15:40 01/31/08 15:40 01/31/08 15:40 01/31/08 15:40 01/31/08 15:40 01/31/08 15:40 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 01/31/08 03:31 01/31/08 03:31 01/31/08 03:31 01/31/08 03:31 01/31/08 03:31 01/31/08 03:31 01/31/08 03:31 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3010 519 3260 29.5 802 699 161 ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L 50.0 500 25.0 50.0 50.0 50.0 250 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 20.0 1 01/29/08 00:00 01/30/08 15:48 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 13.5 13.5 13.5 13.5 13.5 13.5 13.5 13.5 27.0 13.5 13.5 27.0 27.0 13.5 13.5 6.8 13.5 13.5 13.5 13.5 13.5 13.5 27.0 13.5 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 120-83-2 Page 12 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-8 Parameters 8270 MSSV Semivolatile Organic Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Acetone Acrolein Acrylonitrile Date: 02/12/2008 03:16 PM Lab ID: 5011526003 Results Collected: 01/25/08 13:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 88 79 74 44 59 74 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % 13.5 13.5 13.5 13.5 67.6 67.6 13.5 13.5 13.5 6.8 13.5 13.5 6.8 13.5 27.0 13.5 13.5 13.5 13.5 13.5 27.0 6.8 67.6 67.6 67.6 13.5 13.5 67.6 13.5 13.5 67.6 13.5 13.5 13.5 13.5 13.5 40-112 31-114 10-116 10-100 13-100 26-125 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 100 100 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 01/31/08 01:32 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 11:54 67-64-1 01/31/08 11:54 107-02-8 01/31/08 11:54 107-13-1 Page 13 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-8 Parameters 8260 MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone Iodomethane Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Date: 02/12/2008 03:16 PM Lab ID: 5011526003 Results Collected: 01/25/08 13:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 25.0 10.0 5.0 5.0 5.0 25.0 4.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 591-78-6 74-88-4 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 Page 14 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-8 Parameters 8260 MSV Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Lab ID: 5011526003 Results Collected: 01/25/08 13:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 105 101 96 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 2.0 10.0 82-122 73-120 80-120 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 01/31/08 11:54 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 460-00-4 2037-26-5 Page 15 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-12 Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Date: 02/12/2008 03:16 PM Lab ID: 5011526004 Results Units Collected: 01/25/08 15:30 Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ND ND ND ND ND ND 92 ug/L ug/L ug/L ug/L ug/L ug/L ug/L % 0.60 0.60 0.60 0.60 0.60 0.60 0.60 10-143 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/31/08 15:48 01/31/08 15:48 01/31/08 15:48 01/31/08 15:48 01/31/08 15:48 01/31/08 15:48 01/31/08 15:48 01/31/08 15:48 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 01/31/08 03:37 01/31/08 03:37 01/31/08 03:37 01/31/08 03:37 01/31/08 03:37 01/31/08 03:37 01/31/08 03:37 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3010 166 2110 10.1 343 820 41.1 ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10.0 100 5.0 10.0 10.0 10.0 50.0 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 20.0 1 01/29/08 00:00 01/30/08 16:44 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 12.0 12.0 12.0 12.0 12.0 12.0 12.0 12.0 24.1 12.0 12.0 24.1 24.1 12.0 12.0 6.0 12.0 12.0 12.0 12.0 12.0 12.0 24.1 12.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 120-83-2 Page 16 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-12 Parameters 8270 MSSV Semivolatile Organic Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Acetone Acrolein Acrylonitrile Date: 02/12/2008 03:16 PM Lab ID: 5011526004 Results Collected: 01/25/08 15:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 81 77 80 38 56 77 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % 12.0 12.0 12.0 12.0 60.2 60.2 12.0 12.0 12.0 6.0 12.0 12.0 6.0 12.0 24.1 12.0 12.0 12.0 12.0 12.0 24.1 6.0 60.2 60.2 60.2 12.0 12.0 60.2 12.0 12.0 60.2 12.0 12.0 12.0 12.0 12.0 40-112 31-114 10-116 10-100 13-100 26-125 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 100 100 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 01/30/08 19:38 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 12:29 67-64-1 01/31/08 12:29 107-02-8 01/31/08 12:29 107-13-1 Page 17 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-12 Parameters 8260 MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone Iodomethane Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Date: 02/12/2008 03:16 PM Lab ID: 5011526004 Results Collected: 01/25/08 15:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 25.0 10.0 5.0 5.0 5.0 25.0 4.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 591-78-6 74-88-4 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 Page 18 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-12 Parameters 8260 MSV Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Lab ID: 5011526004 Results Collected: 01/25/08 15:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 102 99 97 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 2.0 10.0 82-122 73-120 80-120 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 01/31/08 12:29 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 460-00-4 2037-26-5 Page 19 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-2 Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Date: 02/12/2008 03:16 PM Lab ID: 5011526005 Results Units Collected: 01/25/08 17:00 Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ND ND ND ND ND ND 93 ug/L ug/L ug/L ug/L ug/L ug/L ug/L % 0.63 0.63 0.63 0.63 0.63 0.63 0.63 10-143 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/31/08 15:57 01/31/08 15:57 01/31/08 15:57 01/31/08 15:57 01/31/08 15:57 01/31/08 15:57 01/31/08 15:57 01/31/08 15:57 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 01/31/08 03:43 01/31/08 03:43 01/31/08 03:43 01/31/08 03:43 01/31/08 03:43 01/31/08 03:43 01/31/08 03:43 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3010 160 1240 13.2 371 213 49.7 ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10.0 100 5.0 10.0 10.0 10.0 50.0 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 20.0 1 01/29/08 00:00 01/30/08 16:45 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 11.8 11.8 11.8 11.8 11.8 11.8 11.8 11.8 23.5 11.8 11.8 23.5 23.5 11.8 11.8 5.9 11.8 11.8 11.8 11.8 11.8 11.8 23.5 11.8 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 120-83-2 Page 20 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-2 Parameters 8270 MSSV Semivolatile Organic Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Acetone Acrolein Acrylonitrile Date: 02/12/2008 03:16 PM Lab ID: 5011526005 Results Collected: 01/25/08 17:00 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 86 77 75 38 58 86 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % 11.8 11.8 11.8 11.8 58.8 58.8 11.8 11.8 11.8 5.9 11.8 11.8 5.9 11.8 23.5 11.8 11.8 11.8 11.8 11.8 23.5 5.9 58.8 58.8 58.8 11.8 11.8 58.8 11.8 11.8 58.8 11.8 11.8 11.8 11.8 11.8 40-112 31-114 10-116 10-100 13-100 26-125 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 100 100 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 01/30/08 19:59 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 13:33 67-64-1 01/31/08 13:33 107-02-8 01/31/08 13:33 107-13-1 Page 21 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-2 Parameters 8260 MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone Iodomethane Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Date: 02/12/2008 03:16 PM Lab ID: 5011526005 Results Collected: 01/25/08 17:00 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 25.0 10.0 5.0 5.0 5.0 25.0 4.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 591-78-6 74-88-4 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 Page 22 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-2 Parameters 8260 MSV Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Lab ID: 5011526005 Results Collected: 01/25/08 17:00 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 104 102 97 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 2.0 10.0 82-122 73-120 80-120 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 01/31/08 13:33 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 460-00-4 2037-26-5 Page 23 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-4 Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Date: 02/12/2008 03:16 PM Lab ID: 5011526006 Results Units Collected: 01/26/08 12:30 Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ND ND ND ND ND ND 97 ug/L ug/L ug/L ug/L ug/L ug/L ug/L % 0.62 0.62 0.62 0.62 0.62 0.62 0.62 10-143 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/31/08 16:05 01/31/08 16:05 01/31/08 16:05 01/31/08 16:05 01/31/08 16:05 01/31/08 16:05 01/31/08 16:05 01/31/08 16:05 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 01/31/08 03:48 01/31/08 03:48 01/31/08 03:48 01/31/08 03:48 01/31/08 03:48 01/31/08 03:48 01/31/08 03:48 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3010 78.0 860 5.0 249 114 31.4 ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10.0 100 5.0 10.0 10.0 10.0 50.0 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 6.0 1 01/29/08 00:00 01/30/08 16:47 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 14.1 14.1 14.1 14.1 14.1 14.1 14.1 14.1 28.2 14.1 14.1 28.2 28.2 14.1 14.1 7.0 14.1 14.1 14.1 14.1 14.1 14.1 28.2 14.1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 120-83-2 Page 24 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-4 Parameters 8270 MSSV Semivolatile Organic Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Acetone Acrolein Acrylonitrile Date: 02/12/2008 03:16 PM Lab ID: 5011526006 Results Collected: 01/26/08 12:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 86 77 54 43 59 80 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % 14.1 14.1 14.1 14.1 70.4 70.4 14.1 14.1 14.1 7.0 14.1 14.1 7.0 14.1 28.2 14.1 14.1 14.1 14.1 14.1 28.2 7.0 70.4 70.4 70.4 14.1 14.1 70.4 14.1 14.1 70.4 14.1 14.1 14.1 14.1 14.1 40-112 31-114 10-116 10-100 13-100 26-125 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 100 100 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 01/31/08 00:50 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 14:08 67-64-1 01/31/08 14:08 107-02-8 01/31/08 14:08 107-13-1 Page 25 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-4 Parameters 8260 MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone Iodomethane Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Date: 02/12/2008 03:16 PM Lab ID: 5011526006 Results Collected: 01/26/08 12:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 25.0 10.0 5.0 5.0 5.0 25.0 4.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 591-78-6 74-88-4 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 Page 26 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-4 Parameters 8260 MSV Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Lab ID: 5011526006 Results Collected: 01/26/08 12:30 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 106 99 98 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 2.0 10.0 82-122 73-120 80-120 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 01/31/08 14:08 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 460-00-4 2037-26-5 Page 27 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-6 Parameters 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Date: 02/12/2008 03:16 PM Lab ID: 5011526007 Results Units Collected: 01/26/08 14:00 Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ND ND ND ND ND ND 89 ug/L ug/L ug/L ug/L ug/L ug/L ug/L % 0.68 0.68 0.68 0.68 0.68 0.68 0.68 10-143 1 1 1 1 1 1 1 1 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/30/08 00:00 01/31/08 16:14 01/31/08 16:14 01/31/08 16:14 01/31/08 16:14 01/31/08 16:14 01/31/08 16:14 01/31/08 16:14 01/31/08 16:14 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5 877-09-8 01/31/08 03:54 01/31/08 03:54 01/31/08 03:54 01/31/08 03:54 01/31/08 03:54 01/31/08 03:54 01/31/08 03:54 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 Analytical Method: EPA 6010 Preparation Method: EPA 3010 82.1 976 6.6 258 112 31.2 ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10.0 100 5.0 10.0 10.0 10.0 50.0 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 2.0 1 01/29/08 00:00 01/30/08 16:48 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 14.7 14.7 14.7 14.7 14.7 14.7 14.7 14.7 29.4 14.7 14.7 29.4 29.4 14.7 14.7 7.4 14.7 14.7 14.7 14.7 14.7 14.7 29.4 14.7 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 100-51-6 101-55-3 85-68-7 59-50-7 106-47-8 111-91-1 111-44-4 108-60-1 91-58-7 95-57-8 7005-72-3 218-01-9 53-70-3 132-64-9 91-94-1 120-83-2 Page 28 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-6 Parameters 8270 MSSV Semivolatile Organic Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Di-n-butylphthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Acetone Acrolein Acrylonitrile Date: 02/12/2008 03:16 PM Lab ID: 5011526007 Results Collected: 01/26/08 14:00 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 158 147 146 91 134 151 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % 14.7 14.7 14.7 14.7 73.5 73.5 14.7 14.7 14.7 7.4 14.7 14.7 7.4 14.7 29.4 14.7 14.7 14.7 14.7 14.7 29.4 7.4 73.5 73.5 73.5 14.7 14.7 73.5 14.7 14.7 73.5 14.7 14.7 14.7 14.7 14.7 40-112 31-114 10-116 10-100 13-100 26-125 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 100 100 1 1 1 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/29/08 00:00 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 01/30/08 19:22 84-66-2 105-67-9 131-11-3 84-74-2 534-52-1 51-28-5 121-14-2 606-20-2 117-84-0 117-81-7 206-44-0 86-73-7 87-68-3 118-74-1 77-47-4 67-72-1 193-39-5 78-59-1 91-57-6 95-48-7 91-20-3 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 95-95-4 88-06-2 4165-60-0 321-60-8 1718-51-0 13127-88-3 367-12-4 118-79-6 S3 S3 S3 S3 S3 Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 15:17 67-64-1 01/31/08 15:17 107-02-8 01/31/08 15:17 107-13-1 Page 29 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-6 Parameters 8260 MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone Iodomethane Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Date: 02/12/2008 03:16 PM Lab ID: 5011526007 Results Collected: 01/26/08 14:00 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 25.0 10.0 5.0 5.0 5.0 25.0 4.0 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 106-93-4 74-95-3 95-50-1 541-73-1 106-46-7 110-57-6 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 142-28-9 594-20-7 563-58-6 10061-01-5 10061-02-6 100-41-4 97-63-2 87-68-3 591-78-6 74-88-4 98-82-8 99-87-6 75-09-2 108-10-1 1634-04-4 Page 30 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 Sample: GP-6 Parameters 8260 MSV Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Lab ID: 5011526007 Results Collected: 01/26/08 14:00 Units Report Limit Received: 01/28/08 11:48 DF Prepared Matrix: Water Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 105 97 95 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 2.0 10.0 82-122 73-120 80-120 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 01/31/08 15:17 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 1868-53-7 460-00-4 2037-26-5 Page 31 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 QC Batch: OEXT/5892 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV Associated Lab Samples: METHOD BLANK: 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 126776 Associated Lab Samples: Parameter 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 Blank Reporting Units Result Limit Qualifiers 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-Methylphenol(o-Cresol) 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol(m&p Cresol) 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Dinitro-2-methylphenol 4-Bromophenylphenyl ether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenylphenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Date: 02/12/2008 03:16 PM ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10.0 10.0 10.0 10.0 50.0 10.0 10.0 10.0 10.0 10.0 10.0 50.0 10.0 20.0 20.0 50.0 50.0 10.0 20.0 20.0 10.0 50.0 50.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 20.0 10.0 10.0 5.0 5.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 32 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 METHOD BLANK: 126776 Associated Lab Samples: Parameter 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 Blank Reporting Units Result Limit Qualifiers Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % LABORATORY CONTROL SAMPLE: 126777 Parameter 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitroso-di-n-propylamine Pentachlorophenol Phenol Pyrene 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) Date: 02/12/2008 03:16 PM ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 82 75 52 81 34 89 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % % % Spike Conc. 100 100 100 100 100 100 100 100 100 10.0 10.0 10.0 5.0 10.0 20.0 10.0 10.0 10.0 10.0 10.0 5.0 10.0 50.0 10.0 10.0 10.0 26-125 31-114 13-100 40-112 10-100 10-116 LCS Result 93.1 80.5 82.6 44.8J 86.9 89.8 81.8 36.6 93.1 % Rec Limits LCS % Rec 93 81 83 45 87 90 82 37 93 89 79 57 85 36 95 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 39-129 39-105 44-115 10-80 40-116 35-129 16-133 12-120 44-126 26-125 31-114 13-100 40-112 10-100 10-116 Page 33 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 QC Batch: MPRP/2490 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: METHOD BLANK: 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 126785 Associated Lab Samples: Parameter 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 Blank Reporting Units Result Limit Qualifiers Arsenic Barium Cadmium Chromium Lead Selenium Silver ug/L ug/L ug/L ug/L ug/L ug/L ug/L LABORATORY CONTROL SAMPLE: 126786 Parameter ND ND ND ND ND ND ND Spike Conc. Units Arsenic Barium Cadmium Chromium Lead Selenium Silver ug/L ug/L ug/L ug/L ug/L ug/L ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Arsenic Barium Cadmium Chromium Lead Selenium Silver Date: 02/12/2008 03:16 PM Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10.0 100 5.0 10.0 10.0 10.0 50.0 LCS Result 1000 1000 1000 1000 1000 1000 500 993 944 962 937 958 964 501 126787 5011471008 Result 1730 9700 14.2 268 791 114 ND LCS % Rec % Rec Limits 99 94 96 94 96 96 100 Qualifiers 80-120 80-120 80-120 80-120 80-120 80-120 80-120 126788 MS Spike Conc. 1000 1000 1000 1000 1000 1000 500 MSD Spike Conc. 1000 1000 1000 1000 1000 1000 500 MS Result 2540 10500 802 1090 1580 892 462 MSD Result MS % Rec 2500 10000 812 1080 1580 882 455 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 80 78 79 82 79 78 92 MSD % Rec 77 35 80 81 79 77 90 % Rec Limits 75-125 75-125 75-125 75-125 75-125 75-125 75-125 Max RPD RPD 1 4 1 1 0 1 2 Qual 20 20 P6 20 20 20 20 20 Page 34 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 QC Batch: MERP/1511 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: METHOD BLANK: 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 126811 Associated Lab Samples: Parameter 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 Blank Reporting Units Result Limit Qualifiers Mercury ug/L LABORATORY CONTROL SAMPLE: 126812 Parameter ND Spike Conc. Units Mercury ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Mercury Date: 02/12/2008 03:16 PM Units ug/L 2.0 LCS Result 5 4.2 126813 5011471008 Result ND LCS % Rec % Rec Limits 83 Qualifiers 80-120 126814 MS Spike Conc. 50 MSD Spike Conc. 50 MS Result 41.8 MSD Result MS % Rec 39.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 83 MSD % Rec 78 % Rec Limits 75-125 Max RPD RPD 6 Qual 20 Page 35 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 QC Batch: OEXT/5911 Analysis Method: EPA 8082 QC Batch Method: EPA 3510 Analysis Description: 8082 GCS PCB Mod Associated Lab Samples: METHOD BLANK: 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 127169 Associated Lab Samples: Parameter 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 Blank Reporting Units Result Limit Qualifiers PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) ug/L ug/L ug/L ug/L ug/L ug/L ug/L % LABORATORY CONTROL SAMPLE: 127170 Parameter PCB-1016 (Aroclor 1016) PCB-1260 (Aroclor 1260) Tetrachloro-m-xylene (S) Date: 02/12/2008 03:16 PM ND ND ND ND ND ND ND 84 Units ug/L ug/L % 0.50 0.50 0.50 0.50 0.50 0.50 0.50 10-143 LCS Result Spike Conc. 5 5 % Rec Limits LCS % Rec 5.0 4.8 101 96 85 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 40-160 40-160 10-143 Page 36 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 QC Batch: MSV/7225 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Associated Lab Samples: METHOD BLANK: 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 127884 Associated Lab Samples: Parameter 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 Blank Reporting Units Result Limit Qualifiers 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Date: 02/12/2008 03:16 PM ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 25.0 5.0 25.0 5.0 25.0 100 100 100 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 37 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 METHOD BLANK: 127884 Associated Lab Samples: Parameter 5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007 Blank Reporting Units Result Limit Qualifiers Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % LABORATORY CONTROL SAMPLE: 127885 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) Date: 02/12/2008 03:16 PM ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 99 106 98 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Spike Conc. 50 50 50 50 50 50 50 50 50 50 50 50 5.0 5.0 100 5.0 5.0 10.0 5.0 4.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 100 5.0 5.0 10.0 2.0 10.0 73-120 82-122 80-120 LCS Result LCS % Rec 53.9 54.2 47.0 49.9 50.1 53.6 52.6 50.2 48.0 49.4 46.9 48.3 % Rec Limits 108 108 94 100 100 107 105 100 96 99 94 97 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 70-126 70-128 66-134 71-131 72-125 66-140 72-125 63-130 50-139 61-129 72-128 70-130 Page 38 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 LABORATORY CONTROL SAMPLE: 127885 Parameter 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Date: 02/12/2008 03:16 PM Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Spike Conc. 50 50 50 50 50 50 50 50 250 50 250 50 250 250 1000 1000 50 50 50 50 50 50 100 50 50 50 50 50 50 50 50 50 50 50 50 50 100 50 100 50 50 50 50 50 50 50 50 50 LCS Result 47.8 53.2 50.7 46.1 47.4 48.7 47.5 57.3 237 44.7 263 45.2 241 307 219 948 46.8 47.1 48.6 55.0 45.1 39.6 107 59.5 45.0 63.3 49.8 39.4 49.6 45.7 53.8 51.8 40.8 48.8J 47.0 53.1 86.1 48.8 106 49.7 51.9 48.6 50.9 48.2 48.4 47.0 40.2 40.9 LCS % Rec % Rec Limits 96 106 101 92 95 97 95 115 95 89 105 90 96 123 22 95 94 94 97 110 90 79 107 119 90 127 100 79 99 91 108 104 82 98 94 106 86 98 106 99 104 97 102 96 97 94 80 82 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 72-129 66-131 72-125 72-130 74-128 70-130 72-124 62-134 44-150 74-133 38-150 73-129 55-142 29-150 50-150 L0 50-150 75-126 72-129 67-139 70-130 63-127 43-146 52-172 65-125 74-123 61-141 68-127 42-138 77-132 60-119 72-133 76-133 50-179 70-130 70-129 71-132 70-130 74-126 68-139 50-119 70-130 74-135 56-134 70-133 75-133 75-125 69-121 55-121 Page 39 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 LABORATORY CONTROL SAMPLE: 127885 Parameter Units Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % MATRIX SPIKE SAMPLE: 127886 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Date: 02/12/2008 03:16 PM LCS % Rec LCS Result 50 50 50 50 50 50 200 50 150 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Spike Conc. 46.1 55.7 47.4 51.5J 49.6 48.6 199 39.2 143 5011524001 Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Spike Conc. % Rec Limits 92 111 95 103 99 97 100 78 95 104 105 97 MS Result 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 250 50 250 50 250 250 1000 1000 50 50 50 50.6 55.6 45.6 48.3 50.1 57.5 54.2 46.2 45.7 45.3 45.6 45.7 46.6 52.1 49.8 45.8 45.3 47.5 45.5 57.9 231 45.3 251 44.8 233 256 2040 924 47.5 46.1 47.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers 72-126 73-131 59-119 50-150 73-123 65-145 50-150 54-139 72-127 73-120 82-122 80-120 MS % Rec % Rec Limits 101 111 91 97 100 115 108 92 91 91 91 91 93 104 100 92 91 95 91 116 92 91 100 90 93 103 204 92 95 92 95 Qualifiers 54-134 63-130 59-139 64-136 67-129 59-150 68-127 39-136 41-137 34-137 36-143 64-132 52-136 62-134 67-128 33-145 47-139 63-134 46-135 51-136 54-148 43-147 60-140 46-139 56-147 27-163 50-150 M0 50-150 66-135 57-135 61-142 Page 40 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 MATRIX SPIKE SAMPLE: 127886 Parameter Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethyl methacrylate Ethylbenzene Hexachloro-1,3-butadiene Iodomethane Isopropylbenzene (Cumene) Methyl-tert-butyl ether Methylene chloride n-Butylbenzene n-Propylbenzene Naphthalene p-Isopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-d8 (S) Date: 02/12/2008 03:16 PM Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % 5011524001 Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Spike Conc. 50 50 50 100 50 50 50 50 50 50 50 50 50 50 50 50 50 100 50 100 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 200 50 150 MS Result 51.9 43.3 41.4 111 59.7 43.9 64.8 49.6 40.8 49.5 44.1 50.2 50.5 46.5 47.2J 46.5 50.7 84.1 49.2 104 50.0 50.4 48.2 47.2 47.7 48.6 46.5 38.7 41.8 45.7 57.0 44.5 46.8J 50.3 53.3 180 43.5 144 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. MS % Rec % Rec Limits 104 87 83 111 119 88 130 99 82 99 88 100 101 93 94 93 101 84 98 104 100 101 96 94 95 97 93 77 84 91 114 89 94 101 107 90 87 96 103 104 97 Qualifiers 60-135 50-127 32-148 46-173 51-130 59-135 58-153 61-133 44-135 75-133 51-121 56-139 70-136 25-175 50-150 59-143 50-155 70-130 48-139 62-147 46-119 50-156 33-153 40-136 38-143 35-151 53-133 37-136 40-127 63-137 70-134 49-121 50-150 61-131 64-146 50-150 54-140 54-140 73-120 82-122 80-120 Page 41 of 42 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALIFIERS Project: Beech Grove Site 6892.002 Pace Project No.: 5011526 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. BATCH QUALIFIERS Batch: MSSV/2236 [1] A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume. Batch: GCSV/2315 [1] A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume. ANALYTE QUALIFIERS L0 Analyte recovery in the laboratory control sample (LCS) was outside QC limits. M0 Matrix spike recovery was outside laboratory control limits. Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the spike level. Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias. P6 S3 Date: 02/12/2008 03:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 42 of 42
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