Organic Synthesizer - Lasalle Scientific Inc.

Transcription

www.eyelaworld.com
Every member of Tokyo Rikakikai Co. Ltd.
endeavors to supply the products according
to our quality policy "Devoting our whole
energies to offer the stable quality and realize
customer satisfacfion". EYELA is the registered
trademark of Tokyo Rikakikai Co. Ltd., which
is a coined word from "EYE" and "LA"
laboratory and signifies our commitment to
the future science.
Products Catalogue
TOKYO RIKAKIKAI CO., LTD.
Nihonbashi Hon-cho Bldg.,
3-3-4, Hon-cho Nihonbashi, Chuo-ku,
Tokyo, 103-0023 Japan
TEL: +81-3-5201-6462
FAX: +81-3-3245-1225
E-mail: [email protected]
Safety Caution
Please read "Instruction Manual" carefully befgore using
the product for your continued safety.
08-09
A synopsis of EYELA's
chronological milestones
1955
1962
Tokyo RikaKikai CO. Ltd. founded
1986
Launch of Vacuum Stirrer
made with Teflon®
1990
Vacuum Stirrer TBO
1994
1965
Launch of 1st Rotary Evaporator
N-1 series
N-1 series
1967
1981
1984
2000
Proteomics Research Center
established in Tsukuba Japan
Beijing China Office established
Fermentation Bath developed
Participate at ACHEMA show
in Europe
Separate corporate R&D
laboratories established in
Saitama
2002
Shanghai China factory
begins production
2004
Shanghai Sales Office opened
Singapore Liaison Office opened
2004
Singapore Office opened
2005
USA Sales Office opened in
Irvine CA
2007
USA Sales Office moved to
Sunnyvale CA
Miyagi Japan factory begins
production
Miyagi factory
2
Combinatorial Chemistry products
developed
P/L Committee installed
Factory and Technical Production
Division in Saitama Japan
M-100
1979
EYELA's cell culture device
installed on board Endeavor
Space Shuttle
1995
2001
1973
Corporate Bioresearch Center
founded
2
Evaporator, Vacuum Unit
Rotary Vacuum Evaporator N-1001 Series
P.4
Rotary Vacuum Evaporator N-1001S/V/T
P.5
Automatic Rotary Vacuum Evaportator NE-1000 • 1101
P.7
Automatic Rotary Vacuum Evaportator NE-2001
P.8
Examples of System Configuration
P.9
Component Parts
P.11
Spare Parts
P.13
10L Rotary Vacuum Evaportator NE-3000 • 3000D
P.15
Large Scale Rotary Vacuum Evaportator N-21 • 51 • 101
P.16
Thin Film Vacuum Evaportator MF-10A • 10B • 10C
P.17
Centrifugal Evaporator CVE series
P.18
Vacuum Controller for Evaporators NVC-2100 • 2100L
P.19
Aspirator A-1000S
P.20
Solvent Recovery Unit DPE-1120 • 1220 • 2120
P.21
Diaphragm Vacuum Pump DTC series
P.22
Small-sized Oil Rotary Vacuum Pump GLD series
P.23
Pressured Gas Blowing Concentrator MGS-2200
P.24
2
2
Rotary Vacuum Evaporator N-1001S/V/T
Quality design
with broad versatility
N-1001S, S-W, S-WB
1L Diagonal type
1L
Product name
Rotary Vacuum Evaporator
N-1001S
Model
214429
Cat. No
216969
Rate of evaporaton
Max. 20mL/min (Water)
Ultimate vacuum
<399.9Pa/mbar (3Torr)
Induction motor 25W
Diagonal
Condenser
Cat. No.(115V) Cat. No.(230V)
Condensing surface
216949
216948
Sample flask
Bath, Cold Trap
N-1001V-W
N-1001V with SB-1000
216979
216978
Receiving flask
N-1001T-W
N-1001T with SB-1000
217009
217008
Vacuum seal
N-1001S-WD N-1001V with OSB-2000
216959
216958
Stand base
N-1001V-WD N-1001V with OSB-2000
216989
216988
Jack up height
• Unique counterbalanced sliding jack with newly integrated lock
system allows easy single-hand management of the evaporating
flak height.
• The N-1001 series can elevate up to 10 1/4" (260mm), allowing
for safe and effortless evaporating flask attachment and detachment.
Water bath SB-1000 and Oil bath OSB-2000
0.11m
Pear-shaped flask 1L 29/32 or 24/40
Round flask with ball joint 35/20, 1L
Teflon+Teflon coated Viton
T shape 400 x 320mm
110mm+150mm (slide jack+extension slide)
5~35˚C
Heighest H (mm)
790H
AC 115V AC 230V AC 115V
AC 230V
50/60Hz
Stirrer, Shaker
Stirrer, Shaker
SB-1000(W series)
1180H
AC 230V AC 115V
Low Temperature
circulator
Low Temperature
circulator
670W x 320D x 530H 495W x 320D x 920H 670W x 320D x 930H
• The wide surface area (0.11m2) of the condeser provides excellent
cooling while effectively recovering solvent.
• Chemical resistant Teflon seals (optional) allow for the recovery
of low boiling point organic solvents.
Cold finger
ø91 x 230mmH
Dimensions (mm)
Supply Voltage
• The water bath features an integrated overheat protector and
thermal fuse with PTFE coating, providing greater durability and
protection against corrosion.
Vertical
2
Ambient temperature
• The quiet motor head operates between 20 and 180rpm.
216998
20~180rpm
Motor
Model N-1001S-W
N-1001S-W N-1001S with SB-1000
216999
Oven, Incubator
Oven, Incubator
N-1001S-W
214428
Body only without bath
Rotation speed
N-1001S-W
N-1001T
N-1001V
216968
Type
applications requiring temperatures up to 180˚C and 7L maximum
bath volume capacity, allowing for usage of evaporating flasks as
small as 50ml and as large as 2000ml.
OSB-2000(WD series)
Specifications
Cat. No
SB-1000
188789
OSB-2000
188788
211739
211738
Temperature setting
Digital
Digital
Temp. control range
RT+5-90˚C
RT+5-180˚C
Heating capacity
1kW
1kW
Temp. accuracy (˚C)
±1.5
±1.5/3.0 (water/oil)
Bath material
Bath dimensions (mm)
Overall dimensions
SUS304 (PTFE-coating)
AI (PTFE-coating)
ø230 x 100H 3L
ø240 x 138H 6L
N-1001V
N-1001T
N-1001V-WD
260W x 260D x 240H 278W x 296D x 254H
Over heat protector, Fuse
Safety features
Max.1kV
Input power
Suply voltage
N-1001S
Freeze Dryer
Freeze Dryer
Smooth Operating Variable Height Jack
http://www.eyela.co.jp
Organic Synthesizer
Organic Synthesizer
Specifications
Model
4
Features
• A compact rotary evaportator for highly efficient and gentle evaporation of
solvents.
• High performance and low cost.
• Unique weight balance slide jack realizes smooth lift-up and lift-down
with a one-touch lock.
• Interchangeable glassware with existing model.
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
• Economic and durable Rotary Evaporator with a flexible modular
design. Accommodates an intergrated vacuum controller, solvent
recovery system, and vacuum pump. Easily adapted to meet more
demanding needs.
• Three glasware configurations:
Diagonal (S), used for standard applications;
Vertical (V), used in space-constrained and elevated boiling point
applications;
Dewar (T) configuration, designed for low boiling point applications.
• Two water bath options: the SB-1000 is designed for standard
applications and accommodates up to a 3L volume, with a 50ml
to 1000ml evaporating flask range. The OSB-2000 is used in
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Rotary Vacuum Evaporator N-1001 Series
115V
230V
115V
50/60Hz
230V
5
2
2
Evaporator,
Vacuum Unit
Smooth up and down
by slide jack
Manual extension slide
for bulb trap
Rotary Vacuum Evaporator NE-1001/1101
panel/Display
*Glassware
Bath, Cold Trap
Bath,Cold Trap
UG Vertical downward
cooling type
No heater element in the bath.
*Optional accessories/related products
Low Temperature Circulator
Vacuum rate
P.61
Aspirator
Starts ramp control programmed for each solvent
(Auto mode self-detection).
Conducts ramp control programmed for each
solvent (Auto mode self-setting).
P.20
Cat. No.
182650
Cat. No.
182660
Cat. No.
182670
Cat. No.
182680
procedure example of Auto mode
1
Time
Auto vapor temp.
Auto pressure
4
900
*Data (evaporation capacity)
Teflon Seal
P.13
Vacuum Pump
P.22, 23
P.14
Jack
P.14
Bath
P.5
Evaporation speed (mL/min H2O)
Glassware
25
700
7
35
25
20
400
180rpm
120rpm
75rpm
30rpm
10
5
10
20
30
40
50
Conditions:Temp. of cooling water is set 10~20˚C lower than boiling point of
sample (water). RT 25~27˚C, Sample flask is 1L (sample is 500mL).
SG Standard
VG Vertical
CG Vertical integrated
UG
RG
TG
20
500
300
15
0
30
5
2
600
t: Bath temp. and sample (water)
boiling temp. difference
Pressure
30
P.21
types of glassware options
glass assemblies available
800
Solvent Recovery Unit
*6
Freeze Dryer
Freeze Dryer
P.19
182640
Set the rotation speed, bath temperature and vapor temperature and start
operation. *Simultaneous measurement of the vapor temperature and
pressure start. *After starting the decrease of pressure, the initial boiling
point is detected automatically. *Appropriate pressure slope control
automatically starts. *Measure vapor temperature during slope control.
*Detect the point where measured vapor temperature and set temperature
cross. *Automatic setting of fixed pressure value control. *Detect automatic
stop point (temperature). *When automatic stop point is detected, pressure
control stops. Measurement will continue.
*Six
Hysteresis value set manually or automatically
Pressure setting programmed for each solvent
(Auto mode self-setting)
Vacuum Controller
Cat. No.
Stirrer, Shaker
Stirrer, Shaker
(Chiller)
*Vacuum ramp program control function
(Combined with optional Vacuum Controller NVC-2100)
*Operation
182630
Low Temperature
circulator
Low Temperature
circulator
A Vacuum controller (Option) can be connected
to the rotary evaporator.
Cat. No.
Automatic Rotary Vacuum Evaporator
NE-1001
NE-1101
188990
188919
188918
without glassware
5-240 rpm
5-160 rpm
Max. 23mL/min (water)
1kW
RT+5˚C-90˚C
RT+5˚C-180˚C
±1˚C (water)
±5˚C (oil)
-20˚C-150˚C
0-933hPa (0-700Torr/mmHg. 0-933mbar)
Concentration timer 1min-9hr 59min. Ramp time 1min-59min
Temp.: PID control, Pressure: Microprocceser ON/OFF
Rotation : Speed feedback control
Auto mode
Auto 1: single solvent. Auto 2: mixtured solvent
Normal operation (flask roating)
Manual mode
Fixed & ramp control(continuous, concentration time stop, vapor temp. stop)
Lifting mechanism
Motorized lift, 160mm
Glassware
Select from SG. VG. CG. TG. RG. UG type
Bath inner dimensions
ø250 x 110Hmm, Volume: Approx 5L, SUS304L
Connection size (mm)
Nozzle for pressure control: OD10, Leak nozzle: OD10
Ambient temperature
5-35˚C
Dimensions (mm) & weight
565W*465D*535H/20kg
Input power
1.4kVA
Supply voltage
AC 100V
AC 115V
AC 230V
Procuct name
Model
Cat. No.
Type
Rotation speed
Rate of evaportation
Bath heating capacity
Bath temp. rang
Accuracy
Vapor temp. setting range
Pressure setting range
Timer setting range
Control
Bath,Cold Trap
SG Standard
inclined type
VG Vertical type for high
boiling point substance
CG Vertical integrated type for
high boiling point substance
TG Trap type for low
boiling point substance
RG Reflux
vertical type
OSB-2000 Operation panel
Adapter to prevent
reverse flow to the
sample flask.
for NE-1001, 1101
Oven, Incubator
Oven, Incubator
*Operation
Organic Synthesizer
Organic Synthesizer
SB-1000 Operation panel
Evaporator,
Vacuum Unit
Features
• Auto-vacuum function controls the unit based on the automatically detected
boilling point and enhances solvent recovery rate significantly.
• Built-in vacuum and vapor temperature controllers available as standard.
• The sample flask can be moved up & down by motor-lift.
• Rotation speed, vapor temperature and vacuum pressure are controlled by
microprocessor and digitally displayed.
• Two operation modes are available; Auto mode which starts and stops
concentration operation automatically, and Manual mode which operates
under the preset conditions.
• 6 kinds of glassware are available that suits best for experiment requirement.
• NE-1101 is equipped with a bath for heat range from 20˚C to 180˚C by using
water and oil.
• The heating bath can be separated from the control base for bath cleaning.
Specifications
1L
6
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
NE-1001 • 1101
3
15
6
8
10
200
5
100
0
0
Time (min)
7
2
2
5L
Rotary Vacuum Evaporator; Examples of System Configuration
System 1
N-1001S-W
CCA-1111
A-1000S
216948
219950
210530
Product
Rotory evaporator
Low temperature circulator
Diapharagm Vacuum pump
Model
Cat. No.
N-1001S-W
CCA-1111
DTC-21
216948
219950
188870
Enhances the recovery efficieney and
traps the exhaust gas
189070
5-160 rpm
Max. 43mL/min (water)
2.2kW
RT+5˚C-90˚C
±1˚C (flask rotating. water)
-20˚C-150˚C
0-933hPa (0-700Torr/mmHg. 0-933mbar)
1min-9hr 59min
Temp.: P.I.D control, Pressure: Microprocceser ON-OFF, Rotation: Speed feed back control
Auto mode 2. Manual mode 7
Motorized lift, 160mm
Selfdiagnosis (watchdog, overheat, heater fault, motor fault, bath temp. sensor, vapor temp. sensor,
pressure sensor, power failure) Independent overheat protector, Leakage/over-current braker
Over-shoot, Bath temp. Pressure, Vapor temp., Motor, Setting error
Bath(±10˚C), vapor temp.(±10˚C), Pressure(±100h Pa)
Control signal output for diaphragm pump (ON-OFF output) *optional diaphragm pump control unit is necessary.
For rotation: Stepping motor. For motorrized jack: Reversible motor
Vertical triple spiral glass pipe, Cooling area 0.25m2
Sample flask: Round flask 5L, Receiving flask 3L
Teflon, Viton seal
ø280 x 144Hmm, Volume: 8.5L, Material: SUS304L
Nozzle for pressure control: OD10, Leak nozzle: OD10
5-35˚C
625(805) W x 465(530) D x 1020(1180) H/ 29kg
AC220V, 11.8A, 2.6kVA 50/60Hz
AC200V, 13A, 2.6kVA 50/60Hz
System 3
Suitable for low boiling point solvents
using -45˚C cold trap
System Code SYS09092
System 4
Freeze Dryer
Freeze Dryer
Cat. No.
Stirrer, Shaker
Stirrer, Shaker
Alarm function (alarm display)
Compensation function
External output
Motor
Condenser
Flasks
Vacuum seal
Bath inner dimensions
Connection size (mm)
Ambient temperature
Dimensions (mm) & Weigh
Power source
Model
Low Temperature
circulator
Low Temperature
circulator
Safety features
Signal from the evaporator directs
diaphragm pump ON-OFF (option).
NE-2001
189078
System 2
Bath,Cold Trap
Bath,Cold Trap
Product name
Model
Cat. No.
Rotation speed
Rate of Evaportation
Bath heating capacity
Bath temp. range
Bath temp. accuracy
Vapor temp. setting range
Timer setting range
Control
Control mode
Lifting mechanism
Oven, Incubator
Oven, Incubator
Rotary evaporator
Aspirator
NE-2001
Diaphragm vacuum pump is used in place
of aspirator
Organic Synthesizer
Organic Synthesizer
Product
Specifications
8
Enhances the recovery efficieney by
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Features
• 5 liter large scale sample flask and built-in vacuum controller.
• Microprocessor control of the rotation speed, bath temperature, vapor
temperature and vacuum pressure.
• Two operation modes available: Auto-mode which incorporates automatic
concentration start and stop. Manual mode which allows desired condition
setting.
• Equipped with smooth up/down auto-jack. When Auto-stop functions or
alarm is detected, main unit stops operation automatically and auto-jack
lifts up the main unit.
The heating bath can be separated from
the control base for cleaning
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
NE-2001
Product
Rotary evaporator
Diaphragm vacuum pump
Solvent recovery unit
Model
Cat. No.
N-1001S-W
CCA-1111
DIVAC 1.2L
DPE-1220A
216948
219950
170660
216660
Product
Rotary evaporator
Water bath
Vacuum control unit
Cooler
Diaphragm vacuum pump
Model
Cat. No.
N-1001T
SB-350
NVC-2100
ECS-50SS
DTC-21
194780
180180
216630
113440
188870
9
2
2
Enhances the recovery efficency by controlling the
proper vacuum rate for each sample
System 5
Traps exhaust air and
conducts vacuum control.
System 6
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Component Parts of EYELA Evaporators
N-1001S
11
15 57
14
58
1
51
54
53
4
13
10
12
7
8
9
N-1001V
14
Organic Synthesizer
Organic Synthesizer
58
6
21
25
23
N-1001T
57
20
28
15
58
14
Oven, Incubator
Oven, Incubator
55
55
25
Product
Rotary Evaporator
Vacuum Controller
Diaphragm Vacuum Pump
Model
Cat. No.
N-1001S-W
CCA-1111
NVC-2100
DIVAC 1.2L
216948
219950
216630
170660
Product
Rotary Evaporator
Model
N-1001S-W
CCA-1111
DPE-1220C
DTC-21
Cat. No.
23
56
8
1
1
12
54
53
51
7
18
13
10
12
7
9
9
6
6
Low Temperature
circulator
Low Temperature
circulator
NE-1001S*1101S
NE-1001V*1101V
21
58
14
25
15
11
57
14
20
1
24
2
58
57
1
15
3
4
12
2
12
3
23
18
6
8
5
19
9
6
10
17
9
16
7
8
22
7
58
21
Product
Rotary Evaporator
Model
Cat. No.
N-1001S-W
CCA-1111
DPE-1120
DIVAC 1.2L
216948
219950
216660
170660
25
14
25
28
57
1
15
24
2
12
23
10
12
23
13
8
2
3
18
5
5
6
6
10
9
9
22
22
16
1
13
19
3
18
58
14
26
27
Freeze Dryer
Freeze Dryer
NE-1001T*1101T
NE-1001C*1101C
Stirrer, Shaker
Stirrer, Shaker
13
10
5
13
16
10
Bath,Cold Trap
Bath,Cold Trap
Enhances the recovery efficiency and traps the exhaust
air. Also shuts out the smelled components.
56
53
18
13
System 7
54
51
10
8
19
19
216948
219950
216680
188870
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
EYELA Original parts will fully enhance and maintain the performance
of EYELA evaporators. All the parts are manufactured following strict
EYELA quality standards. It is highly recommended to use only these
genuine original parts for EYELA products.
Parts name and cat. No. are referred in the tables.
7
16
8
7
11
2
2
NE-1001R*1101R
58
21
20
36
24
57
15
29
8
13
30
12
23
31
33
10
6
9
17
34
16
7
42
41
41
25
14
27
25
8
13
15
23
29
39
57
30
12
31
32
10
33
9
6
37
34
16
7
NE-2001
50
24
41
13
49
12
43
44
45
32
48
33
47
22
34
16
46
*Standard type
Length(mm)
*272
272
*178
178
*Trap Bulb
TSJ
29/38
24/40
29/38
24/40
Cat. No.
142500
142510
142520
142530
Capacity
Cat. No.
116600
116610
116620
116630
200mL
TSJ
29 x 29
29 x 24
29 x 19
29 x 15
24 x 24
24 x 19
24 x 15
29 x 29
29 x 24
29 x 19
29 x 15
24 x 24
24 x 19
24 x 15
29 x 29
29 x 24
29 x 19
29 x 15
24 x 24
24 x 19
24 x 15
29 x 29
29 x 24
29 x 19
24 x 24
24 x 19
100mL
* Included in standard setup.
*Thick type
Length(mm)
272
272
178
178
*Transparent joint type
STJ
29/38
24/40
29/38
24/40
Cat. No.
142500
142510
142520
14250
Length(mm)
272
272
178
178
TSJ
29/38
24/40
29/38
24/40
300mL
*Sample flask
(pear shaped)
Spec. 29/38
Capacity
50mL
100mL
250mL
500mL
*1L
2L
Cat. No.
216720
216710
216720
216730
216740
216750
Spec. 24/40
Capacity
50mL
100mL
250mL
500mL
1L
2L
Cat. No.
216800
216810
216820
216830
216840
216850
500mL
*Test Tube Adapter
* Included in standard setup.
*Receiver flask
Standard type (Ball joint S35/20)
Capacity
Cat. No.
100mL
116300
200mL
116310
300mL
116320
500mL
116330
*1L
116340
*2L
116350
Test tube joint
15/25
15/25
Joint
29/38
24/40
Cat. No.
116550
143870
Spec.
15/25(6 pcs/set)
Cat. No.
Test tube
201450
*Adapter for different diameters
*Above-mentioned are standard
equipments of Rotary Evaporator.
*Receiver flask with drain cock
(Ball joint 35/20)
Capacity
Cat. No.
500mL
116370
1L
116380
For Rotary
Joint
For Rotary Joint
*Jacket type receiver flask
(Ball joint 35/20)
Capacity
1L
Cat. No.
116700
116710
156700
116720
116730
156710
116740
116750
116760
156680
116770
116780
156690
116790
116800
116810
156650
116820
116830
156660
116840
116850
116860
156610
156630
156640
For Safety
Cap
For Safety Cap
Spec.
29*24
29*19
29*15
24*29
24*19
24*15
29*24
29*19
29*15
Cat. No.
116870
116880
116890
116900
116910
116920
116930
116940
116950
Cat. No.
116390
*Film coating type flask
*Cooling Hose set
Model
Y-FJ-100
Tube ID
9.0mm
15.0mm
Cat. No.
116390
Cat. No.(2m) Cat. No.(5m)
112700
174420
143340
174460
Freeze Dryer
Freeze Dryer
23
*Rotary joint (vapor duct)
Stirrer, Shaker
Stirrer, Shaker
25
Part No.
142650
187840
187850
142500
187860
142540
187890
116190
142610
116340
202790
187780
142710
142700
142690
178900
187830
185170
142520
911160
187790
142620
185180
187910
185210
185240
187800
185220
187920
185200
185250
142840
142990
913690
143010
185150
143030
185160
187810
143160
142930
142860
142940
143000
143940
142950
142820
116360
143020
142980
142880
116540
192600
192610
192620
195060
142691
202770
Low Temperature
circulator
Low Temperature
circulator
22
Quantity
2
1
1
1
1
2
1
1
2sets
1
1
1
1
1
3sets
2sets
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
12
4
Bath,Cold Trap
Bath,Cold Trap
38
58
40
Description
N. NE type
NE type
NE type
272mm 29/38
NE type
29
29
1000mL 29/32
N·NE·S·V·C·T·R·U
1000mL S35/20
S35 (SUS)
Double spiral coil
N·NE type
N·NE type
N·NE type
N·NE type
NE type PTFE tube
S·R type
178mm S29/38
V·T type
Double spiral coil
N·NE type
NE·V·T·R type
N·NE type
C·U type
N·NE-1001·1101·2001
Vertical double spiral coil with adaptor
C·U type
Cold finger
NE·R·U type
NE·R·U type
29/38
NE·R·U·2001 type
NE·R·U·2001 type
NE·R·U·2001 type
NE·R type
NE·R type
NE·U type
Descending condenser
NE·U type
NE·U type
45
NE·U type
NE-2001 type
NE-2001 type
NE-2001 type
5000mL
3000mL S35/20
NE-2001 type
NE-2001 type
Vertical triple spiral
19/40 PTFE tube
N-1001 type 29
N-1001 type
N-1001V·T type
N-1001V·T type
N·NE type
N·NE type
Oven, Incubator
Oven, Incubator
NE-1001U*1101U
Parts name
Sleev pin
Rotation stopper
Screw for removing flask
Rotary joint
Cutting screw
Joint clip (Plastic)
Joint clip (metalic)
Pear-shaped sample flask
Vacuum seal
Receiving flask
Ball joint clamp
Diagonal Condenser
Ring spring
Cap screw
Nozzle sets (white)
Cooling nozzle sets (light blue)
Capillary tube for vapor sensor
Vapor sensor
Rotary joint
Adaptor (trap monifold)
Vertical condenser
Suction nozzle
Vapor sensor
Setting screw
Support for condenser
Condenser holder
Condenser
Condensor support
Condensor (Vertical trap)
Teflon packing
Seal defenser
Joint adapter
Soft packing
Cap screw for sample flask
Rubber packing
Adaptor (built in rotary joint)
Stop valve
Adaptor (Joint trap)
Condenser
Ball join clamp
Expansion chamber
Joint clip
Connecting tube
Teflon packing
Vacuum seal
Seal defenser
Sample flask
Receiving flask
Ball join clamp
Adaptor
Condenser
Capillary
Rotary joint ring
Flask remover
Support poll for condenser
Knob bolt
Nozzle packing
Viton O-ring for nozzle set
Organic Synthesizer
Organic Synthesizer
32
No.
1
2
3
4
5
6
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
53
54
55
56
57
58
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
14
25
35
12
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Spare Parts for rotary evaporators
*Vacuum Hose
Spec.
ID6*OD15mm
ID12*OD30mm
Cat. No.
119170
119210
Q'ty
5m
5m
13
2
2
*Separable flask
Separable sample flask
Spec.
ID*H(mm)
50mL
50*60
100mL
50*100
200mL
50*110
300mL
50*125
500mL
75*152
1L
75*185
Cat. No.
116400
116410
116420
116430
116440
116450
Capacity(mL)
500*300
500, 1000
Product
Teflon seal
Cat. No.
143880
Q'ty
1
• A new vacuum sealing system is made using the mechanical-seal to ensure
a long lifespan.
• Easy to attach one-touch clamp for the evaporator flask enables one-person
operation.
• The lifting mechanism of the bath is motorized, so raising and descending
of the bath is easy and smooth.
• Inner bath heat (RT+10˚C to 180˚C), rotation speed, and vapor temperature
are digitally displayed.
• The trolley for easy mobility is equipped as standard.
• A variety of safety features such as leakage current breaker, empty heating
protector, heater malfunction alarm are incorporated.
*Cooling Hose set
Tube ID
9.0mm
15.0mm
Cat. No.(2m) Cat. No.(5m)
112700
174420
143340
174460
10L Explosion proof model N-3000D
N-3000
Cat. No.
116500
116510
Separable seal packing
Dia(mm)
Capacity(mL)
50
500*300
75
500, 1000
Specifications
Applicable model
N-1001S, V, T
N-1001S
N-1001V, T
*Glass stopper
Cat. No.
116540*
142590
142600
Product name
Model
Cat. No.
Rotation speed
Spec.
19/40 Teflon tube 565mm
510mm 19/40
297mm 19/40
Q'ty
1
Cat. No.
116970
N-3000D
Q'ty
1
*Operation
panel
*Bumping protector (safety cap) (PAT.)
Simply attach to rotary joint. Innovative bumping prevention is attained by focusing on the principle of bumping. Teflon-made caps can be used for all sorts of solvents. Please use suitable adaptor for different diameter (this cap is only for rotary
joint 29).
C-2 (Rocket type)
C-3 (Filter type)
The valve equipped to the top of Cap closes before bumping occurs as a
result of a difference in pressure between cooler side and sample flask
side, and opens when pressure difference is eliminated.
Applying the steam to the hemisphere part makes inside the flask wellconvected and prevents the bumping as a handy way. Suitable for the
substance with relatively weak bumping force.
Glass filter (G3) mitigates the sudden change in pressure and prevents the
bumping. This is also effective in preventing the spread of powder droplets
when drying crystal samples etc.
Cat.No.
116010
Cat.No.
Functional diameter 20.2*0.5mm
rotary joint (mm)
External dim. (mm) OD 23 x 35length
116020
Functional diameter 20.2*0.5mm
rotary joint (mm)
External dim. (mm) OD23*24length
Cat.No.
116030
Rotary Joint
applicable ID
OD
20.2*0.5mm
OD23*27L
Independent overheat
protector (N-3000)
N-3000
*One
N-3000D
touch clamp
A type Top panel 150 x 150mm up-down height 70~250mm
B type Top panel 200 x 200mm up-down height 90~320mm
Type
A
B
Moldel
EJ-A
EJ-B
Cat. No.
116120
116130
*Mechanical
valve
Freeze Dryer
Freeze Dryer
*EYELA Jack
*Drain
Stirrer, Shaker
Stirrer, Shaker
C-1 (Standard type)
Low Temperature
circulator
Low Temperature
circulator
Cat. No.
116960
10L Rotary Vacuum Evaporator
N-3000
N-3000D
221128
221138
from 10 to 130rpm
Depends on steam energy.
Rate of evaporation
Max.3.5L/h (for water)
cooling/operation conditions
Ultimate vacuum pressure
<133.3Pa (1Torr)
Temperature range
RT+10-180˚C
RT+10˚C-80˚C
Temp. accuracy
±1˚C (for water). ±3˚C (for oil)
Bath temp. control
P. I. D. microprocessor control
Thermal
empty
heating
protector, Independent overheat protector,
Safety function
ELCB, Motor-fuse, Overflow duct, Up/down limiter for the bath
Display
Bath temp., Sample flask rotation speed. Digital display.
Bath lifting mechanism
Motorized auto-lifting system
Manual
Stationary (1-760mmHg/1-1013hPa).
Automatic (Vapor temp, sensor, option).
Vacuum control function
NA
Program control (Programmed for each 10
typical solvents), Step control
For temp. control, 3.5kW
Heat exchanger
Heater
Induction motor 60W
Air motor 250W
Driving motor
Condenser
Vertical triple spiral tube, 0.5m2
Sample flask
Round shaped flask 10L
Receiving flask
Round shaped flask, 5L, with drain valve
Vacuum seal
Mechanical seal
Diameter 360*200H, 20L, material: SUS304
Connection size
Vacuum nozzle: OD 16mm, Cooling nozzle: OD 16mm
145mm
145mm (manual)
Bath height adjustment
Ambient temperature
5-35˚C
Overall Dimensions (mm) & weight
930W x 450D x 1890H/96kg
930W x 472D x 1890H/93kg
Input power
AC 220V, 1ø, 3.8kVA
Bath,Cold Trap
Bath,Cold Trap
*Three-way Cock
Cat. No.
116520
116530
Oven, Incubator
Oven, Incubator
*Glass Capillary
• Explosion-poof type that uses an air motor that will not create heating
electricity in its driving parts. This model is suitable for the concentration
and recovery of solvents with low boiling points.
• The bath can be moved up and down by just turning the handle.
• A drain valve is fixed to the receiving flask, enabling collection of the condensed
liquid under reduced pressure.
Organic Synthesizer
Organic Synthesizer
Cat. No.
116460
116470
116480
116490
Separable clamp
Dia(mm)
50
75
10L Standard type N-3000
*Teflon Seal
ID*H(mm)
50*82
50*82
75*82
75*82
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Separable cover
Spec.
29/38
24/40
29/38
24/40
* is standard equipment of Rotary Evaporator
14
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
10L Rotary Vacuum Evaporator N-3000 • N-3000D
seal
*Normal
mode
*Auto
mode
*Program (ramp) program mode
15
2
2
Thin film Vacuum Evaporator MF-10A • 10B • 10C
N-21
*Data
Bath,Cold Trap
• Continous sample injection is possible. Recovery of eluted solvents
from drain pipe during operation is possible.
• Equipped with vacuum gauge.
• Effective recovery and prevention of secondary vaporization are
realized by the cone type cooler for condenser and the sub-cooler
on top of receiver flask.
• Sample flask can be detached easily by screw frange.
• Vacuum control is possible with optional vacuum controller
NVC-2100.
Rotation
Vacuum
Vapor temp.
Hot water circulation
2000
1500
Evaporated volume
Condensed volume
1000
1000
500
500
0
60
Condenser
Sample flask
Receiver flask
Vacuum seal
Bath diameter (mm) & capacity
Weight
Power source
90
*Thin Film Evaporation
Large Scale Rotary Vacuum Evaporator
N-21NS
N-21
N-51
N-101
195580
117130
117140
117150
20~120rpm, steppless
20~120rpm
10~80rpm, stepples
less 133.3Pa (1 Torr)
RT+5~80˚C
±1~2˚C (When sample flask is rotating)
Digital setting. digital display
Overheat protector, Leakage protector.
Overflow tube, Water supply pipe, Float type overheat protector. Heater cut alarm. Leakage protector,
Empty heating protector, Sensor cut etc
Drainage resistive sheet panel. Overload protector, Non-contact zero cross output
Electrical auto jack
Electro-hydraulic auto jack
Temp. control: 2kW Aux.1kW+3kW Temp.control: 3kW Aux.2.5kW+3.5kW
Temp. control:4kW Aux.3kW+5kW
1~6kW. 4 step
induction motor
400W
7L/min. Motor output 10/15W(50/60Kz)
—
Vertical 4 spiral. cone type
Vertical 4 spiral
cooling area: 2.0m2
cooling area: 2.7m2
cooling area: 1.0m2
20L
50L
100L
20L
10L
20L
50L
10L
Teflon seal
Ø430*250H 36.2L
Ø560*300H 73.9L
Ø700*350H 134.7L
Ø450*280H 40L
220kg
280kg
330kg
200kg
3Ø 220V 6.8kVA
3Ø 220V 6.8kVA
3Ø 220V 9.8kVA
3Ø 220V 12.8kVA
While not operating
• Forms a uniform thin film on the evaporation area by centrifugal action and stirring effect, enabling to concentrate the
foaming solvents or high-viscous solvents.
• Needs short time for heating so that the sample can be concentrated without being too much degraded by heat.
• Can increase the rotation speed of propellers in order to raise the concentration ratio.
• Can remove the liquid by opening/closing the cock of receiver flask and concentrates the sample continuously.
Freeze Dryer
Freeze Dryer
Bath jack function
Heater
Motor
Circulation pump (shower)
80
Stirrer, Shaker
Stirrer, Shaker
Safety functions
70
Jacket temp. (˚C)
Specifications
Product Name
Model
Cat.No.
Rotation speed range
Ultimate vacuum
Temp. control range
Temp. control accuracy
Bath temp. setting & display
1200rpm
30mmHg
30˚C
Use HS-1
Low Temperature
circulator
Low Temperature
circulator
Features
• Full line of large capacity evaporators 20L, 50L and 100L.
• Large volume samples can be condensed, evaporated, dried and
recovered at low temperature quickly.
• Sample flask can be easily attached by using flask base.
• Many safety features are incorporated such as leakage protector,
over current protector, bath overheat protector, overflow tube,
drainage resistive sheet panel.
• Accurate temperature control enables easy bath temperature
setting and confirmation. Temperature controller adopts digital
temperature setting and display.
Evaporated volume (mL/h)
Water evaporation rate (MF-10A)
Thin film vacuum evaporator
MF-10B (With liquid sensor)
MF-10C (High temp)
117450
117450
140-1200rpm (50/60Hz) steplessly variable
1140mL/hr (water) circulating hot water 70˚C, vacuum 4.0kPa (30Torr)
Capactity of vacuum pump 133.3 Pa (1Torr)
RT +5-180˚C
*
Volume setting and digital dispaly
Rotation speed setting & display
Timer function
ON-OFF timer, solenoid valve
Feed liquid control
Vacuum seal
sensor PT-100Ω
Motor
DC brushless motor 60W
Rotation axis seal
Vacuum seal
Evaporation tube
Stainless steel (SUS304)
Jacket type, evaporation surface 0.04m2
Condenser
Vertical double spiral tube, condenser surface 0.3m2
Receiving flask
Concentration side 1L volume, Evaporation side 1L volume
Heating source
Mantle heater 800W
Hot water circulator (option)
Material
Borosilicate glass, teflon, stainless steel SUS304
Connection size
Cooling nozzle, hot water nozzle OD 12mm, suction nozzle, sample nozzle OD8mm
Sample injection
Solenoid valve, timer, needle valve Automatic control by liqid level sensor Solenoid valve, timer, needle valve
5~35˚C
Ambient temperature
Overall dimensions (mm) & weight
625W x 400D x 1416H, 40kg
Input voltage
100V
MF-10A
117440
Bath,Cold Trap
Product name
Model
Cat. No.
Rotation speed
Rate of evaporation
Ultimate vacuum
Temp. setting range
MF-10C
Oven, Incubator
Oven, Incubator
MF-10A
Organic Synthesizer
Organic Synthesizer
Specifications
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Features
• Designed for the concentration or purification of thermally sensitive materials
or of viscous materials or of high boiling point materials.
• The double-walled evaporator jacket is made of borosilicate glass and this
makes it possible to visually observe the evaporation process.
• Vacuum distillation shortens the time needed for the feed liquid to pass and
increases the efficiency of heat transfer.
• With model MF-10B, the amount of sample feeding is controllable by a level
sensor, enabling concentration while controlling the liquid level in the
evaporation tube.
• Model MF-10C is equipped with a mantle heater and a stainless steel
evaporation tube. It is suitable for high temperatures and the temperature can
be set up to 180˚C.
N-21NS
16
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Large Scale Rotary Vacuum Evaporator N-21 • 51 • 101
While operating
distillate
filling sample
filling sample
filling sample
circulating the
hot water
circulating the
hot water
auxiliary ring
At start of operation
circulating the
hot water
concentrated liquid
Just after starting operation
During operation
17
2
2
CVE series
Vacuum controller with excellent control functions. Connecting this unit to
Evaporator improves significantly the recovery rate of general solvents such
as dichloromethane, benzene, or trichloroethylene etc.
Compact-type for 1.5mL microtube suitable for concentration and
drying after ethanol precipitation.
CVE-2000
CVE-3100
CVE-200D
CVE-1000
Cat. No.187430
Diaphragm Vacuum Pump built-in type suitable for solvent removal.
CVE-2000
Suitable for low-temperature concentration of biochemical substance.
CVE-200D
R-200A
Cat. No.117748
Suitable for TFA, DMF, and DMSO and for concentrating synthetic
sample of combinatorial chemistry and removing the solvents.
R-2000A
Specifications
Cat. No.188820
R-2000B
R-200E
R-3100C
R-3100D
R-3100E
R-3100F
Acceptable container
Number of tubes
O.D. 10.8mm (1.5mL) Microtube
24 pieces
O.D. 10 to 13mm test tube (Length 80 to 100mm)
16 pieces
16 pieces
16 pieces
96 pieces
48 pieces
O.D. 16.5 to 18mm test tube (Length 90 to 120mm)
36 pieces
36 pieces
Deep well plates
2 pieces
Swing rotor (96 holes)
96 pieces
48 pieces
48 pieces
Liquid phase mathod centrifugal tube
48 pieces
50mL vial
10 pieces
Deep well plates Swing rotor (96 holes)
2 pieces
CVE-1000
CVE-2000
CVE-200D
CVE-3100
Corrosion-resistance of chamber
Rotor material
Vacuum pump
Water
Alcohol
Acid Organic solvent
(surface treatment)
*
*
*
*
Option
Aluminum(*)
*
*
*
*
Built-in
Aluminum (Alumite)
*
*
*
*
Option
Aluminum(anticorrosion treatment)
*
*
*
*
Option
SUS (Teflon)
Lid material
Acryl
PVC
Acryl
Glass+PVC
*Capacity and Temperature range of CVE series
Model
CVE-1000
CVE-2000
CVE-200D
CVE-3100
*
No. of tubes to be handled
Test tube (Max.dia)
Microtube
**
12
16
24
36
96
48
96
Temperature control range (˚C)
50
RT+5˚C
0
100
15˚C
*Option
Teflon solenoid valve, Vapor temp. sensor
To set 15˚C*RT requires Recirculating chiller.
*Applicable pumps
Model
CVE-1000
CVE-2000
CVE-200D
CVE-3100
0.6L
*
DIVAC
1.2L
DTC
2.2L
-21
*
MDIC
-41
GLD
-051
GCD
-051X
*
*
*
*
(Built-in)
*
*
*
*
*
*
*
*
Centrifugal evaporator CVE-2000
Rotor R-2000A
Cooling trap UT-1000
System for processing Combinatorial chemical sample
Rotor R-3100C
Vacuum control unit NCV-2100
Cold trap UT-2000
Diaphragm vacuum pump DIVAC1.2L
Wagon SST-1
System for processing multiple water content samples
Rotor R200D
Codl trap UT-1000
Diaghragm vacuum pump DIVAC 1.2L
Wagon SST-1
Model
Solenoid CV-1
valve
CV-2
Vapor Temperature
sensor
Capillary for
vapor sensor
Cat.No.
196910
196920
185170
185180
Specifications
Hose nozzle OD 10mm
for NVC-2100
Hose nozzle OD 13mm
for N-1001S series
for N-1001V. 1001T series
187830
for N-1001S series
*NORMAL
(fixed-point control) mode
*PROGRAM
(ramp control) mode
Freeze Dryer
Freeze Dryer
*A wide variety of system configuration is available by combining various related products.
System for processing small amount of sample
Mounting plate for evaporator
This is necessary to attach to Evaporator.
N-NVC3 (for N-1001 model) Cat. No.189310
*Data
Recovery rate (By program mode)
Hexane
Trichloroethane
Ethyl acetate
Banzene
Toluene
Evaporation time
9min 27sec
9min 5sec
11min 50sec
10min 43sec
13min 42sec
Stirrer, Shaker
Stirrer, Shaker
For CVE-3100 R-3100A
R-3100B
Model
Low Temperature
circulator
Low Temperature
circulator
Rotor type
For CVE-2000 R-2000A
R-2000B
R-2000C
R-2000D
For CVE-200D R-200A
R-200B
R-200C
R-200D
*Characteristics of CVE series
* Strong. * Usable, * Not usable
R-200E
Vacuum Controller for Evaporators
NVC-2100
NVC-2100L
216639 216638 216637 216649 216648 216647
0 to 1066hPa/mbar, 1 to 800mmHg
0 to 1013hPa/mbar, 1 to 760mmHg
Auto detect. auto set
—
Programmed for each typical solvent
0 to atmospheric pressure hPa/mbar,
0 to atmospheric pressure mmHg
Hysteresis Constant value control
Auto (2%) or 1 to 20mmhPa/mbar (1 to 15mmHg)
setting range Pressure ramp control
Auto(2%) or 1 to 20%
Time setting range
Ramp control time: 1 to 999min. Step: 0 to 999min
Pressure control mode
Constant-point, Auto, Ramp, Step program
Display
Display of measured set pressure value, temp. (option) at the same time
Automatic vacuum release at the end of control
Auto leak function
(manual release at the end of control is selectable)
Except for auto mode, it is possible to hold at a
Holding funcion
selected vacuum rate in ramp control.
Tubing material
PPS, PP, Teflon
10mm
22mm
Nozzle diameter
Option
Standard (included)
Teflon solenoid valve
AC outlet
*
Diaphragm pump output
AC115V AC220V AC230V AC115V AC220V AC230V
Power source
50/60Hz 100VA
50/60Hz 300VA
Procuct name
Model
Cat. No.
Pressure measurement range
Normal control
Pressure Auto control
setting
Program control
range
Step program control
R-200D
Bath,Cold Trap
Bath,Cold Trap
CVE-3100
Oven, Incubator
Oven, Incubator
*Optional accessories (Rotors)
NVC-2100
Cat. No.188810
Organic Synthesizer
Organic Synthesizer
Features
• Most appropriate vacuum value of the 10 typical regulated solvents (such
as siethyl ether. hexane, dichloromethane, acetone, benzene, toluene...) are
stored in memory and the unit is automatically adjusted for most proper
vacuum value of the selected solvent.
• 2 kind of digital displays: numerical display of pressure and graphic display
to show the ongoing control status.
• Set pressure value can be changed anytime. Regardless of the operation
status (run/stop), pressure value can be set at desired value while checking
the concentration situation.
• Adjusting the vapor temperature to the room temperature at start of operation
enables to prevent the bumping of sample solvent and to select the proper
vacuum rate automatically.
• NVC-2100L is suitable for large-sized Evaporator/Vacuum unit.
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Features
• Suitable for DNA, RNA synthesis, elution of concentrated solvent.
• Compact size of 180W x 199D x 176Hmm. Rotor which can accommodate
12 pcs 1.5mL micro tubes is equipped as standard.
• The unit is used under room temperature and is suitable for samples sensible
to heat.
• CVE-2000 is equipped with vacuum pump which gives high vacuum of 4000Pa.
CVE-1000
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Vacuum Controller for Evaporators NVC-2100 • 2100L
Centrifugal Evaporator
Recovery amount
496.0g
495.2g
493.0g
497.3g
498.9g
Recovery rate
99.20%
99.04%
98.60%
99.46%
99.78%
*AUTO
(automatic control) mode
*STEP
PROGRAM mode
Condition: Water bath temp. 40˚C, Cooling water temp.: 5˚C.:
Recovery rate is calcurated by volume in the receiving flask when 500g
of sample is placed in 1L sample flask.
18
19
2
2
Solvent Recovery Unit DPE-1120 • 1220 • 2120
DPE-1120 All-in-one unit to conduct self-control.
DPE-1220 Selectable configuration and upgrade are possible.
DPE-2120 Controls 2 evaporators with large displacement capacity.
Cooling coil CCS (SUS304)
Cat. No.119060
Power source
Ultimate vacuum (using tap water)
Tap water temp.
10˚C
20˚C
920
1290
2370
mmHg
6.9
9.7
17.8
DPE-1220C
DPE-2120C
*System example with DPE-1220 BASE
Specifications
4
3
6
5
1
DPE-1220 BASE
Product name
* DPE-1220 Base
* Vacuum controller
* Solenoid valve for Vacuum controller
* Condenser+receiving flask (Exhaust gas trap)
* Waste Iiquid trap (without bottle)
* Exhaust gas absorber
Cat. NO.
216620
216630
196910
200750
171630
197000
*Combination
*Metal
AS-2•3 (Metal)*AT-1B (Teflon) Aspirator
aspirator and Teflon aspirator
Model
Cat. No
Displacement
Ultimate vacuum
AS-2
AS-3
AT-1B
Safety functions
Tap diameter
Connection to tap
Suction dia. & Length
AS-2
119100
AT-1B
119130
6L/min
13L/min
5˚C
1.33kPa (10mmHg)
10˚C
2.0kPa (15mmHg)
10˚C
1.6kPa (12mmHg)
15˚C
3.33kPa (25mmHg)
15˚C
2.66kPa (20mmHg)
Check valve
ID 10mm x OD 14mm
ID 10mm x OD 14mm
adapter
R1/4 with screw
R 1/4 with screw
OD 9mm. 155mm
OD 9mm. 72mm
component system
(for 1 or 2 Evaporators)
Built-in Condenser and receiving flask without vacuum control type DPE-1220A
*Colsed
refresh system of Diaphragm Pump and Solenoid Valve (DPE-1120, 2120)
Exhaust
Vacuum Line
Exhaust Line
DPE model
Solenoid Valve (CV-1)
AS-3
119110
Rotary Evaporator
DPE-1220C
Absorber cartridge
Rotary Exaporator
Condenser
*All-in-one
unit, Full System
(for one Evaporator)
Exhaust
Rotary Evaporator
DPE-1220B
216679
216677
*
Freeze Dryer
Freeze Dryer
• AS-2 type can be directly hooked-up to the tap water.
• AS-2 and AS-3 suction air flow is Max. 13L/min. and can reach ultimate
vacuum in short time.
• AT-1B is Teflon made and strong against chemical corrosion.
DPE-1220C
DPE-1120
DPE-2120
216689
216659
216699
* 115V
216687
216657
216697
* 230V
*
*
*
Vacuum Controller
*
*
*
Condenser+receiving flask (500ml)
*
*
*
*
Waste liquid trap
*
*
*
*
Exhaust gas absorbing cartridge
*
*
*
*
Collecting flask
0~1065hPa/mbar
Pressure measuring range
Normal control: 0 to 1013hPa(mbar), 1 to 760mmHg
Program control: 0 to 933hPa(mbar), 1 to 700mmHg
Normal control: Auto (2%) or 1 to 20hPa (mbar)1 to 15mmHg
Hysteresis setting range
Program control: Auto (2%) or 1 to 20%
4 modes of normal, auto, ramp and combination program
Control mode
LCD digital display (mode, pressure reading, pressure setting,
Display (graphic)
temperature (option))
Automatic On-Off interlocking with set pressure, self cleaning action
Pump control
160 x 350 x 610 160 x 350 x 700 198 (200) x 380 x 485 (555), 810 when pump base is set
Overall dimensions (mm)
Product name
Model
Cat. No.
2
Stirrer, Shaker
Stirrer, Shaker
Vapor pressure
5˚C
Pa
DPE-1220B
Low Temperature
circulator
Low Temperature
circulator
Vacuum regulator with gage
VG-1000V Cat. No.212380
DPE-1220A
Bath,Cold Trap
Bath,Cold Trap
Vacuum regulator with nozzle
VG-1000 Cat. No.210550
Aspirator
A-1000S
210539
210538
210537
Pressurized circulation system by water pump
16/19L/min 50/60Hz (at 6˚C water temp.)
30Pa/7mmHg(5˚C)-4266Pa/32mmHg(30˚C)
Check valve, thermal protector
Induction motor150W
Metal aspirator x 2 (Nickel coated brass)
255W x 361D x 216H 10L
Polypropylene
O.D.9mm x 2, two independent built-in source
ø13mm
ø17.5mm
5~35˚C
255 (260.5)W x 361D x 406H
6.7kg
280VA
280VA
280VA
AC 115V
AC 220V
AC 240V
50/60Hz
Oven, Incubator
Oven, Incubator
Optional accessories
Product name
Model
Cat. No
Exhaust system
Displacement
Ultimate vacuum
Safety functions
Motor
Aspirator element
Bath material
Suction nozzle
Drain nozzle
Overflow nozzle
Ambient temperature
Weight
Input power
Organic Synthesizer
Organic Synthesizer
Specifications
A-1000S
20
Features
• Vacuum controller, Condenser, Waste liquid collecting trap (bottle), Recovery
flask and Exhaust gas absorber cartridge are compactly integrated in one
unit.
• Complicated pressure setting is not necessary. Normal control allows to
change the set pressure value anytime. Auto-control starts the control
corresponding with the vapor temperature (vapor sensor is option). Program
control memorizes the proper vacuum rate of 10 versions of typical regulated
solvents.
• Excellent corrosion resistance is achieved by using solenoid valve of Teflon
diaphragm and sensor which is anti-corrosive to organic solvents.
DPE-1120
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Features
• Highly recommended for use in an area lacking water service or where it
is difficult to obtain constant water pressure.
• Transparent lid cover makes it possible to check the water condition in
the bath. Bath structure is made to be removed and cleaned easily.
• Precisely processed metal aspirators are equipped so that the displacement
is stable.
• Since the unit circulates the water in the aspirator at constant pressure
by pump, it assures constant suction.
• Highly chemical resistive Teflon aspirator is also available as option.
Cooling coil CCU (copper)
Cat. No.119050
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Aspirator A-1000S
Closed System is introduced: a function of collecting vapor by circulating in Condenser when remained vapor
in Diaphragm pump and tubing are automatically released. This improves the durability of pump, sensor,
and solendoid valve as well as comtributes to protection of tubing and longer life for absorber.
DPE-1120
21
2
2
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Small-sized Oil Rotary Vacuum Pump
DTC series
GLD series
High ultimate vacuum, suitable for Vacuum Oven and Freeze Dryer.
DTC-21
DTC-60
Features
• Dry type pump which does not require oil change.
• Small, light weight, compact size which requires minimal installation space.
GLD-201A/BN
Specifications
GLD-166N
189130
165/200L/min
400W
400W
550W
Thermal protector, Reflux prevention valve, Oil filter
500~800mL
1100mL
1000mL
Hose end OD 22mm
1200mL
GLD-201BN
200560
200/240L/min
550W
1100mL
7 to 40˚C
150(165.5) x 394(399) x 246.7 170 x 466(475) x 256.7 170 x 479(488) x 256.5 170 x 514.5(523.5) x 256.7 170 x 507(516) x 256.5
13.9kg
24.7kg
26.0kg
28.3kg
28.0kg
for pump
Applicable pump
Oil Model
GLD series
SMR-100
Capacity
500mL2
4L
18L
Cat. No.
118700
118710
118720
*Oil
mist Trap OMS, OMT, OMI
OMS: Trap oil mist
OMT: Trap in vacuum pump
OMI: Pipe connect type
OMC: Anti-corrosie, frange type
OMC
Model name
OMS-051
OMS-100
OMT-050A
OMT-100A
OMT-200A
OMC-050
*Vacuum
Cat. No.
118610
118620
118630
118640
118650
118680
hose (ID6. 9. 12. 18mm. 5m)
Vacuum hose adapter
Length
5m
5m
5m
5m
Cat. No.
119170
119190
119210
119230
*Vacuum
hose adapter
Type
Adapter A
Adapter B
Adapter C
Adapter D
Adapter E
Adapter F
Diameter
OD 22*OD 17mm
OD 17*OD 13mm
OD 17*OD 10mm
OD 22*OD 13mm
OD 13*OD 10mm
OD 22*OD 10mm
Freeze Dryer
Freeze Dryer
Vacuum hose 1. D. x 0. D.
6 x 15mm
9 x 21mm
12 x 30mm
18 x 42mm
Vacuum hose
Applicable pump
GLD-051
GLD-101N
GLD-051
GLD-101N
GLD-136CN, 201A/B
GCD-051X
Stirrer, Shaker
Stirrer, Shaker
OMT
200W
GLD-136N
200540
135/162L/min
6.7 x 10-2Pa
Low Temperature
circulator
Low Temperature
circulator
22
Diaphragm Vacuum Pump DTC series
Product name
DTC-21
DTC-41
DTC-60
Model
188870
188880
188030
Cat. No.
100V
200V
100V
200V
100V
200V
Input voltage
20/24L/min
40/46L/min
60/70L/min
Displacement
1.0kPa (13 Torr)
Ultimate Vacuum
1255/1555 rpm
1370/1620 rpm
1400/1630 rpm
Ratation speed (50/60Hz)
50W
100W
200W
Motor Output
Thermal protector
Safety functions
Teflon
Exhaust part material
PP. Teflon
OD 14mm hose end
Suction nozzle diameter
OD 10mm hose end
OD 14mm hose end
Exhaust nozzle diameter
OD 10mm hose end
0-40˚C
Ambient temperature
Overall dimensions (WxDxH mm) 118(142)Wx272(288.5)Dx202H 133(115)Wx320(336.5)Dx217H 150(158)Wx340Dx242H
18kg
10.3kg
7.3kg
Weight
2.2/2.3A 220/230VA 3.6/3.7A 360/370VA
1.3A 130VA
Power source
GLD-101N
189080
100/120L/min
Bath,Cold Trap
Bath,Cold Trap
DTC-21 with Rotary Evaporator N-1001
*Oil
Oil Rotary Vacuum Pump
GLD-051
190840
50/60L/min
Oven, Incubator
Oven, Incubator
Designed to comply with drainage regulations.
Gas contact part is made from Teflon. Suitable for
discharging solvents and reducing pressure.
DTC-41
Procuct name
Model
Cat. No.
Displacement (50/60Hz)
Ultimate vacuum
Motor Output
Safety function
Oil to be used (SMR type)
Suction tube dia.
Ambient temperature
Overall dimensions (W x D x Hmm)
Weight
Organic Synthesizer
Organic Synthesizer
Specifications
GLD-136CN
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Features
• Features include reverse flow prevention mechanism, gas ballast valve, forced
oil feeding system, over current protection circuit, and forced cooling system.
• Large window makes it easy to confirm oil condition.
• Dismounting or exchange of oil filter is easy and it also prevents troubles
from filter contamination.
• Low noise level and small vibration is achieved.
23
2
Evaporator,
Vacuum Unit
Pressured Gas Blowing Concentrator MGS-2200
Evaporator,
Vacuum Unit
Features
• This equipment is designed to apply to preparative samples in chromatography,
or mass spectrometry analysis.
• High heat-conductance characteristic of Aluminum block implement prompt
and uniform heating and temperature control.
• Sample oxidization is prevented by blowing inert gas.
• The unit can work with a large number of samples simultaneously.
• The amount of air flow is adjustable.
Organic Synthesizer
Bath,Cold Trap
Low Temperature
circulator
*Individual
P.26
Application examples:
• The analysis of agricultural chemicals and environment.
• The examination of food, beverages and drugs.
Personal Organic Synthesizer Process Station PPS-3510
P.29
P.30
Specifications
Personal Organic Synthesizer Process Station PPV4030 • 4060
P.31
Personal Organic Synthesizer Zodiac CCX-1100 • 1110 • 1300 • 1310
P.33
Personal Organic Synthesizer Zodiac CCX-3200
P.34
Compact Stirrer CPS-1000
P.35
Pressured Gas Blowing Concentrator
MGS-2200
Refer product composition
RT +5˚C~200˚C
±0.1˚C~0.2˚C
P. I. D control
Sheet key input, Digital display
Revising temp. display, Auto start/stop, Two-step program, Auto-tuning
Alarm functions (min./max. temp. warning power failure. Temp. regulation
Safty features
disorder, Sensor, Watch-dog). Fuse, Independent overheat protector (1 fixed)
Heater 235W, Pt100Ω
Heating method. temp. sensor
one
Number of aluminum block
90W x 125D x 70H (mm)
Dimensions of aluminum block
Refer Aluminum block table
Adaptatable Aluminum block
170W x 135D x 22H (mm) SUS304
Mani-fold
Inner diameter 1.6mm x 180mm Iength SUS304
Blowing nozzel
0.2µm dispo type
Filter
Airfow regulated valve, nozzel diameter 9mm
Conection diameter
5~35˚C
Ambient temperature
240 (260)W x 310D*600H. 7.5kg
External Dimensions (mm) & Weight
3A, 300VA•AC100V 50/60Hz
Power source
Oven, Incubator
*Operation
panel
Product compostition
gas blowing system (PAT.P)
Model
Stirrer, Shaker
A
B
C
D
MGS-2200 E
F
G
H
I
Freeze Dryer
Model
MGB-0548
MGB-1540
MGB-1240
MGB-1524
MGB-1624
MGB-1822
MGB-2116
MGB-2412
MGB-2512
24
Cat. No.
209430
209440
209450
209460
209470
209480
209490
209500
209510
Model
S-048
S-040
S-024
S-022
S-016
S-012
Mani-fold
Aluminum block
number of needle
Model
Applicable container Holes
MGB-0548 8mm microtube, 0.5 48
48
MGB-1540 11mm microtube, 1
40
40
MGB-1240 12mm test tube
40
24
24
MGB-1624 16.5mm test tube
24
22
22
16
16
12
12
12
Micro tubes and micro-plates with 96holes and flat bottoms are available.
*Aluminum
Gas Blowing Unit (Manifold)
block
Applicable container (out diameter) number of holes
8mm Micro-tube 0.5mL
48
11mm Micro-tube 1.5mL
40
12mm test tube
15mm test tube
24
16.5mm test tube
22
18mm test tube
16
21mm test tube
24mm test tube
22
25mm test tube
Cat. No.
207570
207580
207590
207600
207610
207620
207630
207640
207650
Organic Synthesizer
Personal Organic Synthesizer Process Station PPS-1510 • 2510
Product name
Model
Cat. No.
Temperature cotrol range
Temp. accuracy
Temp. control
Temp. setting & display
Function
MGS-2200
3
Model
S-048
S-040
S-024
S-022
S-016
S-012
Applicable container (out diameter)
8mm Microtube 0.5mL
11mm Micro-tube1.5mL
12mm test tube
15mm test tube, 16.5mm test tube
18mm test tube
21mm test tube
24mm.25mm test tube
number of nozzle
48
Cat. No.
206680
40
206690
24
22
16
22
206700
206710
206720
206730
Process Station Optional Accessories
P.36
Process Station System Examples
P.38
Parts for Personal Organic Synthesizers
P.39
Process Reactor React Master DDS-1000 • 1400
Parts for DDS-1000 • 1400
P.42
P.43
3
3
Organic Synthesizer
Teflon cap
PPS-15TC
Teflon cap
PPS-25TC
Aluminum block
PPS-15A
Aluminum block
PPS-25A
Cooling cartridge
PPS-15LT
Double chamber PPS-15W
Cooling cartridge
PPS-25LT
Temp. control & stirring
PPS-CTRL
Temp. control & stirring
PPS-CTRL
Variable synthesis scale. Improved work efficiency
Manual reagent injection
Gas purging
Bath,Cold Trap
Temperature controller and stirring unit are integrated and common to all
models.
By changing such parts as Teflon cap and aluminum block, synthesis scale
can be changed.
Standard Accessories
Teflon caps
Aluminum block
Double chamber
Cooling cartridge
Temp. & Stirring control uni
Septum sealing( x 5), Three-way cock( x 2), Piping set
Test tube( x 10), Stirrer( x 5)
Cold insulation hose set (Silicone ø9 x 2m, 2pcs)
Fuse( x 1), Eathing adapter( x 1)
* 5 different temperatures can be set for each heating block.
* When conducting temperature control or reflux at room temperature or lower, the unit needs to be connected to low temperature circulator.
The gas piping tube is made Teflon shutter for preventing
of Teflon.
dew
Aluminum block
Powerful stirring and reaction
Observation window
Freeze Dryer
Freeze Dryer
Variable synthesis scale
The dew preventive cooling cartridge
does not need complicated connections
of the cold water circulation hoses.
Cross shaped stirring bar
Duble chamber
Duble chamber
The temperature can be controlled independently
Teflon made drip water receiving tray.
Independent overheat protector (-10 to 150˚C)
Stirrer, Shaker
Stirrer, Shaker
Functions
Performance
Standard system
Personal Organic Synthesizer (Process Station)
PPS-1510
PPS-2510
198579
198578
198589
198588
1 to 5 pieces
1mL to 4mL (Variable)
Ferromagnetic stirrer
-10˚C to 50˚C (5*individual control)
±0.5˚C
Approximately 250 to 1600rpm at Approximately 250 to 1300rpm at
Range of stirring speed
4mL volume of water
30mL volume of water
Temperature setting, display
Membrane key pad input. digital display
Setting of stirring speed
Volume input, digital display
Gas substitution
By reducing pressure and replacing air with inert condition
The cooling water-cooled aluminium reflux head provides efficient
Reflux
condensing and refluxing
Sample injection
Pipette, syringe,dropping funnel under inert condition
Reaction observation
Through the slit of the aluminium block
Double chamber, Fuse, Dew tray, Individual overheat protectors (5),
Safety features
Thermo protector for empty heating
Materials iof sample contacting parts
Borosilicate glass (DURAN), teflon, perfluoro
Connection of cooling water
OD 10.5mm hose end
Size of reaction tubes (mm)
ø15*150 (with rim)
ø30*200H (with rim)
Size of the magnetic stirring bars
ø10*5Hmm (cross bar)
ø20*7Hmm (cross bar)
Ground joint
TS 15/25
Ambient temperature
5˚C to 35˚C
465(W)*310(D)*415(H)
465(W)*310(D)*465(H)
Weight
21kg
23kg
AC115V
AC220V
AC115V
AC220V
Power source
600VA
Teflon caps
PPS-15TC Cat.No.195189
Aluminium block
PPS-15A Cat.No.193849
Double chamber
PPS-15W Cat.No.212669
Cooling cartridge
PPS-15LT Cat.No.212679
PPS-CTRL
PPS-CTRL
PPS-CTRL
PPS-CTRL
Temp & Stirring control unit
Cat.No.191769 Cat.No.191768 Cat.No.191769 Cat.No.191768
Low Temperature
circulator
Low Temperature
circulator
Individual temperature range setting from -10˚C to 150˚C for each controller.
Product name
Model
Cat. No
Available number of reaction vessel
Synthesis scale
Stirring system
Temperature control range
Accuracy of temperature control
Specifications
Bath,Cold Trap
Cooling cartridge
Specifications
PPS 2510+CCA-1111
26
Oven, Incubator
Oven, Incubator
Operation of the temperature controller
Components(PPS-2510)
Organic Synthesizer
Organic Synthesizer
PPS-2510
Features
• Available number of reaction vessels are max. 5 tubes.
• Five heating positions enable to set 5 different temperatures. (-10˚C to
150˚C)
• Synthesis working volume is 1-4mL x 5(PPS-1510 or 10-30mL x 5 (PPS2510).
• Strong and stable vortex stirring can be executed by a powerful stirrer, making
it possible to efficiently stir highly viscous liquids.
Components(PPS-1510)
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Process Station is a 5-position organic synthesizer which is designed to improve
the efficiency of process development of new reactions and catalysis, examination
of reaction conditions and synthesis of intermediates.
Individual setting of the temperature for each position enables examining by
5 types of temperature conditions simultaneously, allowing to achieve the most
effective synthesis route.
PPS-1510 and PPS-2510 are also equipped with reflux and gas exchange
functions required for organic synthesis, in addition to temperature control and
stirring. Synthesis scale can be changed by changing the aluminium blocks.
There are such options available for post-processing, e.g. a set of operations
for liquid-liquid extraction and concentration without exchanging containers.
Components
Organic Synthesizer
Personal Organic Synthesizer Process Station PPS-1510 • 2510
The loading slot of a double chamber
accepts both right and left side insertion.
27
3
3
*Efficient, independent temperature controller
*Strong reflux
Cooling cartridge can be
inserted from either side
*Solvent reflux data
160
140
120
100
PPS-2510: Solvent volume 30mL, 500rpm, 4 hour
Cooling circulator: CA-1112(-20˚C, *CCA-1112)
100
*CCA
50
80
Diethlether
Dichloromethane
Specifications
Toluene
DMF
40
20
0
0
3
4
5
6
45
7 7.5
Time (hr)
*Powerful stirrer
50
50
60
60
120
130
With thermo-couple inlet
*Concentration time (PPS-2510)
A strong ferromagnetic stirrer is equipped for each test tube and implements strong
and smooth vortex mixing.
150
Set temperature (˚C)
Components
140
1hPa
Teflon cap
PPS-35TC
100
80
60
40
16hPa
20
0
75hPa
DMF
Solvent 30mL x 5
Set temp. 30˚C
Total evaporation 125mL
Toluene
*1. For each of the 5 heating blocks a different temperature can be set.
*2. When conducting temperature control or reflux at room temperature or lower, the unit needs to be connected to a low temperature
water circulator.
*3. To purge inert gases, the Teflon caps (included as standard) are necessary.
DCM
Cooling cartridge
PPS-25LT
Temperature control
& stirring PPS-CTRl
28
Freeze Dryer
Freeze Dryer
A reaction status (color, reaction state, stirring,
etc) can be observed form a front observation
window.
Aluminum block
PPS-35A
Components
Reaction observation window
Stirrer, Shaker
Stirrer, Shaker
120
With Teflon shutter
Specifications
2
Time (min.)
1
PPS-3510
210359
210358
1 to 5 pcs
-10˚C to 130˚C (5 x individual control)
±0.5˚C
Approx. 250 to 1100rpm (at 60mL water volume)
Membrane key pad input, digital display
Volume imput, digital display
Vacuum and gas injection (Executed in the vessel) *3
The cooling water-cooled aluminum reflux head provides efficient
Reflux
condensing and refluxing
Sample injection
Pipette, syringe,dripping funnel-under inert condition
Through the slit of the aluminum block
Double chamber, Fuse, Dew tray, Independent over heat protectors (5),
Safety features
Empty heating protector
Materials of sample contacting part
Borosilicate glass (DURAN), Teflon, Perfluoro
End connection of cooling water
OD 10.5mm hose end
Size of reaction tubes (mm)
ø35 x 200H (with rim)
Size of the magnetic stirring bars
ø25 x 8Hmm (cross bar)
Ground joint
TS 15/25
Ambient temperature
5˚C to 35˚C
465(W) x 310(D) x 475(H)
Weight
25kg
Power source
AC115V, 600VA, 50/60Hz
AC220V, 600VA, 50/60Hz
Teflon caps
Aluminum block
Double chamber
Cooling cartridge
Temp & Stirring control unit
PPS-CTRL (191769)
PPS-CTRL (191768)
Low Temperature
circulator
Low Temperature
circulator
-20 0
Functions
Perfermance
60
The temperature can be set from -10˚C to 150˚C for each of the five heating
blocks.
Product name
Model
Cat. No
Synthesis scale
Stirring system
Temperature control accuracy
Stirring speed range
Temperature setting & display
Stirring speed setting & display
Gas substitution
Bath,Cold Trap
Bath,Cold Trap
DMF temperature (˚C)
PPS-2510: solvent 25mL x 5, 500rpm
Cooling circulator: CA-1112(max. -20˚C) Measured by Chemi-thermo monitoring
unit
Recovery rate (%)
*Solvent temperature data
Oven, Incubator
Oven, Incubator
PPS-3510
Features
• The available number of vessel is max. 5 test tubes.
• Five heating positions enable to set 5 different temperatures.
(-10˚C to 130˚C)
• The working volume of synthesis is 50-60mL x 5 positions
• Strong and stable vortex stirring can be executed by a powerful stirrer, making
it possible to efficiently stir highly viscous liquids.
Organic Synthesizer
Organic Synthesizer
Corresponding to five heating blocks, each of five blocks is independently equipped with
the temperature sensor and thermo regulator.
Each of the five blocks which are capable to control heating and cooling is able to control
the temperature range independently from -10˚C to 130˚C.
It also realized a precise temperature control (*0.5˚C). It also features smooth temperature
fall. When temperature control is stopped, high speed cooling is possible and prevents over
reaction.
Different temperature setting between neighboring blocks is possible up to max. 150˚C.
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
PPS series is developed to improved the efficiency of the synthesis process.
Designed as a system with 5 independent reactors, each with its own temperature
control, the system is time-saving and efficient. The relatively large vessel size
is developed for users that work with larger amounts of sample volume and it
is ideal for development, verification experiments, experiments for optimization
and also for large volume intermediate synthesis. Five different temperatures
can be set for five test tubes, saving time and performing efficient synthesis.
Refluxing, gas purging, heating, cooling, and stirring functions are all equipped
as standard.
Organic Synthesizer
Organic Synthesizer
Standard Accessories
Teflon caps
Aluminum block
Double chamber
Cooling cartridge
Temp. & Stirring control uni
Septum sealing ( x 5), Three-way cock ( x 2), Piping set
Test tube ( x 10), Stirrer ( x 5)
Cold insulation hose set (Silicone ø9 x 2m, 2pcs)
Fuse ( x 1), Earthing adapter ( x 1)
29
3
3
Cooling cartridge
PPS-55LT
*2
*4
5 different temperatures can be set for each heating block.
When conducting temperature control or reflux at room temperature or lower, the unit needs to be connected to a low temperature water
circulator.
Manifold (PPS-55M) is useful when executing gas flushing in block.
PPS-5510 without manifold can also be supplied.
High pressure manifold panel PPV-40HP
Cooling cartridge PPV-40LT
Standard
Aluminum
sleeve
HIP-30
Performance
Functions
PPV-4030
Specifications
*1
*3
PPS-55M Manifold
Pressure vessel
PPV-4060
Double chamber PPV-40W
HIP-60
Aluminum block temp. controller
& stirrer PPV-CTRL
Freeze Dryer
Freeze Dryer
Aluminum block PPS-55A
Components
*Components
A branched reaction vessel and 3-way
cock make it possible to ijnject reagent
in inactive condition or let it drip through
a dosing funnel, indeal for heat generating
solvents.
Components
Product name
PPV-4030
PPV-4060
Model
225638
225628
Cat. No
Avaiable number of reaction vessels
1 to 4 pcs
ø30:40mL (Volume: 42mL)
ø60:63mL (Volume: 190mL)
Synthesis scale
Stirring system
From room temperature to 200˚C (2*Each two vessels can be controlled)*4
Approx. 250 to 1300rpm (30mL of water up to 1300rpm, 60mL of water up to 1100rpm
Designed temperature of pressure-resistant vessel
Max. operation temperature 255˚C
Meembrane pad key input, digital display
Volume input, digital display
Bourdon tube pressure gauge is built in for each vessel
Pressure display
(2400kPa F.S. accuracy ±1.0% F.S, 6000kPa F.S. (option)
Gas substitution
Needle valves (2 lines for gas introduction.1 for exhaust)
For each vessel the pressure is regulated independently
Gas pressure regulation
(Pressure can be precisely regulated by needle valve).
Method of adding and taking out Before and after the reaction, the sample can be taken out after removing
sample/reagent
the pressure-connector, also reagent can be added under innert gas flowing
Temperature measuring
*
Protective pipe for temperature sensor
Relief functions: 1relief valve is working under high pressure side pressure can
be regulated (0.34Mpa to 2.41Mpa) relief valve for each vessel (optional accessory)
Safety features
*2 Function for preventing back-flow of gas: a check valve is attached to injecting
each gas into inlet with electrification prevention variabl overheat protector (2).
double chamber, tray for receiving dew fuse
End conection of cool water
External diameter: 12mm (hose end) for silicon hose (ø9*13m)
Pressure-proof vessel, pressure gage, valve, pipes: SUS316, "o"ring,
Materials of sample contacting parts
perflurro Glass vessel, Teflon vessel, Seal for relief valve-fluorocarban
Ambient temperature
5˚C to 35˚C
420(W)*390(D)*600(H)(chamber)
420(W)*390(D)*600(H)(chamber)
Weight
33kg
39kg
Power source / Input power
13A, 1300VA•AC220V 50/60Hz
High pressure manifold
PPV-40HP, Catalogue No.218540
Pressure-proof vessel
HIP-30, Catalogue No.218290
HIP-60, Catalogue No.218310
Aluminum chamber (test tube adapte)
Catalogue No.206420
Double chamber
PPV-40W Catalogue No.218590
Cooling cartrige
PPV-40LT Catalogue No.218600
Aluminium block with
PPV-CTRL Catalogue No.225648
Temperature controller and stirring
Stirrer, Shaker
Stirrer, Shaker
Prevents dew in aluminum block
The temperature can be set ranging from room temperature to 200˚C.
Two different temperatures can be set for each block.
Specifications
Components
*Dosing sample
Functions
*Teflon shutter
Low Temperature
circulator
Low Temperature
circulator
Since the reflux adapter which touches
the cooled reflux block, cools down the
top of reaction tubes, the reaction solvent
vapor can be refluxed sufficiently.
PPS-5510
212719
212718
5 positions (1-20 reactions)
0.5mL to 60mL (Variable)
-10˚C to 150˚C (5x individual temperature control (50 to 60mL up to 130˚C) *1, *2
Temperature difference between neighbouring heating blocks is up to
Individual temperature control
130˚C (when the set temperature is higher than 0˚C)
Temperature control accuracy
±0.5˚C
250-1600rpm (with 30mL of water : max. 1300rpm. with 60mL of water:
max. 1100rpm)
Membrane key pad input. digital display
Stirring speed setting 8 display
Volume input. digital display
Gas substitution
Vacuum and gas injection (Executed in the vessel) *3
Reflux
Not applicable/Reflux adapter/Cool water manifold*2
Sample injection
Pipette. syringe. dripping funnel
Reaction process observation
Double chamber, Fuse, Tray for dipping, Independent overheat protectors
Safety function
(5).Empty heating protector
Materials of sample contcting part
Borosilicate glass (DURAN)
Size of reaction vessels
ø12 to ø35 (14types)
ID 9mm, silicone hose (PPS: 55LT): OD 12mm (hose port), silicone hose
End connection for cool water
ø9 x 13m (PPS-55M)
Ambient temperature
5˚C to 35˚C
465(W)*310(D)*315(H) (Top). 800H(Pole). 22kg
AC115V 600VA 4A 50/60Hz
AC220V 600VA 2.7A 50/60Hz
Power source
Manifold
OD 75mm, Easy-to-set hose (For silicone hose ø5 x 8mm)*5
Drip-proof cover
Option
Reflux adapter
Option
Reaction vessel
Option
Test tube adapter
Option
Aluminum block
PPS-55A catalogue No.212739
Double chamber
PPS-55W catalogue No.212749
Cooling cartridge
PPS-55LT catalogue No.212759
PPS-55CTRL catalogue No.191768
Temperature & stirring control unit PPS-55CTRL catalogue No.191769
Product name
Model
Cat. No
Available No. of reaction vessels
Synthesis scale
Stirring system
Bath,Cold Trap
Bath,Cold Trap
By using test tube adapters, it is possible
to change the size and number of
reaction vessels. Synthes is reactions
within the scqale from 0.5mL to 60mL
can be implemented. Up to 20 reaction
tubes can be placed in the system.
Specifications
Performanc
*Removable reflux adapter
PPV-4030•4060
Oven, Incubator
Oven, Incubator
PPS-5510
Features
• Two built-in individual temperature controllers (from room temperature to 200˚C.
Four synthesis reactors can be controlled at two different temperatures.
• The designed maximum operation pressure is up to 20MPa, but only the
flammable gas to <1MPa.
• Individual pressure control.
Pressure gauge and two needle valves (for pressurizing and relief) are equipped
for each of four reaction vessels. The pressure of each vessel can be controlled
and measured individually.
• By removing the connection, sampling can be done before and after conducting
the reaction. Also, it is possible to add and extract sample under inert gas flow.
• Excess reaction is controlled by the cooling cartridge. This cartridge cools
down the reaction vessels quickly after completing a polymerization reaction
and prevents excess reaction. Also, if excessive heat is generated by a catalyst
reactions, etc., it can suppress the heat.
The cooling cartridge can be inserted from each side of the unit.
• By using a rare earth magnetic stirrer, highly viscous sample can be mixed well.
Organic Synthesizer
Organic Synthesizer
Features
• The number of vessels can be changed and the maximum 20 test tubes can
be mounted by using test tube adapters in the 5 positions.
• Five heating blocks enable to set 5 different temperatures. The range is from
-10˚C to 150˚C (or up to 130˚C for 50mL to 60mL).
• By connecting the cool water manifold to a Dimroth condenser, efficient reflux
experiments can be implemented.
• Strengthened gas purge function.
By using sealed tubes, Schlenk tubes, pressure resistant vessels and DeanStark Traps, degas, deoxidization and high-pressure can be used for
creating new experiment conditions.
• Highly viscous reaction liquids can be stirred with strong magnetic stirrer.
• Various types of reaction vessels can be used to expand your possibilities
of organic synthesis experimenting.
Process Station PPV-4030/4060 is able to perform pressurized reaction efficiently.
It enables to carry out evaluation for hydrogenation, carbonylation and autoclave
for pharmaceuticals, agrichemical intermediates, polymers and fine chemicals.
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Process Station PPS-5510 is a parallel synthesizer that is useful for chemical
reactions of the liquid phase.
5 different reactions can be implemented within the range from 0.5mL to 60mL.
Various sizes and types of vessels are available depending on application.
*Synthesis scale can be changed
30
Personal Organic Synthesizer Process Station PPV-4030 • 4060
Organic Synthesizer
Organic Synthesizer
*1. Notice: Do not use oxygen gas. The parts may be ageing rapidly
*2. Applicable law Labour Safety Regulation (PV<0.004)
*3. Electric parts can be converted into air purge (nitrogen purge) or pressurizing model, Please contact your dealer.
*4 When controlling temperature from room temperature, a hose is required to connect to tap water or low temperature circulator.
31
3
3
Available only for PPV-4060, By
connecting soft thermo (temperature
interface), the temperatures of
sample liquids contained in four
vessels can be monitored while
implementing the reaction and save
the record as a file.
*Changing the vessel for PPV-4060
By using ø30 aluminum sleeve and ø30 pressureresistant vessel (optional accessories), synthesis scale
can be changed from ø60 to ø30.
*In some cases the instrument may not work even though the operating condition is appropriate.
Since testing solft thermo device is available, please check the connetions and operations before
using the actual instrument.
CCX-1100/1110
High pressure gas introcuction
CCX-1300/1310
Pressure gauge
Pressure gauge
Relidf valve
Specifications
Inactive gas
Pressureizing
Reaction gas
Emission
Needle valve
Emission
Cooling Bath CCX-11LT
Catalogue No. 212950
-78˚C is possible when using the CCX11LT Cooling Bath
Relief valve for each vessel (option)
Relidf valve for each vessel
Performance
Connector
Relief valve can be attached to the pressure-resistant vessel if required. It releases
inner pressure at the setting value when catalyst reaction proceeds excessively or
controlling upper pressure limit of autoclave. It controls the pressure at the setting
value automatically.
Screw locked
Attaching 4 relief valves for each vessel
Depressurizing valve
Pressure gauge
4MPa
4MPa
4MPa
Relief valve 1000kPa
Check
valve
Inert gas
Check
Reaction gas
valve
Emission line
ø20 glass
vessel
Earth wire
Strong stirring
Indiviolual gas
substitution
Stirring & heating
unit
ø45 glass
vessel
Septum rubber
Relief valve
-78˚C experiment
Freeze Dryer
Freeze Dryer
Pressurizing valve
4MPa
Manual addition liquid
Protective pipe for
temperature sensor
Stirrer, Shaker
Stirrer, Shaker
Design
Pressure-resistant vessel
+
Rear
Connector
Personal Organic Synthesizer Zodiac
CCX-1100
CCX-1110
208709
208708
208809
208808
1 to 12 positions (Max. 32 pcs)
3mL to 15mL
RT+15˚C to 160˚C
Approx.50 to 900rpm (in water)
Membrane padkey input, digital display
Volume setting, analogue display
By reducing pressure and replacing air with inert gas
Possible
Pipette, syrings, dripping funnel
5˚C to 35˚C
195(W) x 280(D) x 490(H). 8kg
115V
230V
115V
230V
5.5A, 630VA
2.7A, 630VA
5.5A, 630VA
2.7A, 630VA
50/60Hz
1. Temperature controller
ITP-1000 CATALOG NO. 205050
CCX-10TC Catalogue No.198720 CCX-11TC Catalogue No.205050
2. PTFE Capes, come complete
(Simple tube without rim)
(Tube is screw locked with rim)
with glass reaction tubes (12pcs)
3. Aluminium block, comes
complete with standard stirring
CCX-11A type Catalogue No.198719
bars (12pcs)
ERC-1000H Catlogue No.198959 (115V)
4. Stirring & heating unit
ERC-1000H Catlogue No.198958 (230V)
Low Temperature
circulator
Low Temperature
circulator
Connector
Product name
Model
Cat. No
Synthesis scale (Working Volume)
Stirring system
Gas substitution
Refluxing
Sample injection
Ambient temperature
Input voltage
Input power
Bath,Cold Trap
Bath,Cold Trap
Glass vessel, which is useful for handling
sample, is supplied with pressure-resistant
vessel as standard. PTFE vessel, which can
accommodate fluorinated acid, is also
available as an optional accessory.
Oven, Incubator
Oven, Incubator
Internal vessel (Glass, PTFE)
condition (E830)
OS: Windows 95/Windows 98/Windows Me/Windows XP
PC: DOS/V and NEC PC-9821
RS-232C port is required (usb is also available).
CPU: Pentium 90MHz or higher Memory; More than 16MB (32MB is recommended).
Hard disk: More than 20MB, Screen size: 800 x 600 dots or more
Organic Synthesizer
Organic Synthesizer
*Operating
Pressure-resistant vessel with valve
(optional accessory) is useful for adding
and exhausting hydrogen gas before and
after implementing reaction experiment
while the installation space is limited.
You can carry pressure-resistant vessel
with valve easily. It cools down the vessel
effectively after autoclave.
Features
• The single powerful magnetic inductive stirring drive to stir all 12 glass
reaction tubes. With a new, extremely powerful magnetic inductive stirring
drive, it has high traction power and is mainteance-tree, since the drive
contains no mechanically moving parts. Thanks to the new "micro-step",
activation speed of less than 150rpm has been made possible.
• Electronic temperature controller with Fazzy logic control from ambient to
160˚C. With digital temperature display. new technology for fast heat-up
cycles with a chemical resistant white coated plate surface.
• Efficient Refluxing with a Integral Water Cooled Aluminum Block. (eg. DCM
b.p.+20˚C, Reflux Loss, 4 HR: 1%).
• Inert Atmosphere: Central inlet for vacuum and inert gas, combined with PTFE
caps, allows reaction under an inert atmosphere. PTFE caps with PTFE vallve
allows individual reaction to be isolated.
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Pressure-resistant vessel is easy to handle.
Designed pressure is 20MPa. Protective
pipe for temperature sensor is mounted in
the ø60 vessel.
Handy pressure-resistant vessel with valve
Zodiac CCX-1100•1110 is designed to be used by individual chemists, allows
chemists to perform 12 reactions, with a working volume of 3mL to 15mL x
12 reactions. This allows the multiple parallel synthesis, brings benefit in drug
and compound siscovery and chemical development (optimization). Provided
as standard with heating, stirring, refluxing and gas purging facilities to be
equipped. Light weight and compact size to be set anywhere required, suitable
for the personal use.
Monitoring the reaction temperature.
Chemi Thermo monitoring unit. (option)
Components
Two sizes of pressure-resistant vessels are available. Synthesis scale: 14ml
(ø30), 63mL (ø60) x 4
Organic Synthesizer
Organic Synthesizer
Personal Organic Synthesizer Zodiac CCX-1100 •1110 •1300 •1310
Product name
Model
Catalogue No.
Voltage
Quick and easy connection
Personal organic synthesizer Zodiac Glacier
CCX-1300
CCX-1310
214739
214738
214749
214748
115V
230V
115V
230V
Pressure connection
32
33
3
3
Compact Stirrer CPS-1000
Zodiac CCX-3200 is designed to control stirring of up to eight reactors (from
0.5mL to 60mL) in parallel.
Design
Components
Specifications
Product Name
Model
Cat.No
Rotation speed range
Maximum shaft torque
Maximum stir viscosity
Stirrer speed setting & display
Material of solvent contacting part
Safety features
Accessories
Performance
Stirrer shaft & Stirrer impeller
Product name
PPS-1510 • 2510 • 3510
PPS-5510
PPV-3000
PPS-1510
PPS-2510
PPS-3510
PPS-5510
PPV-3000
Stir seal (TS15)
Motor joint (With height adjustment screw)
TS24
TS29
Stir seal TBO
TS34
TS40
Application example
Compact Stirrer
CPS-1000
213290
31 to 266rpm
68.6mN • m
10000mPa • s
Volume setting, digital display
PTFE (stirring impeller). PEEK (stirring shaft)
Motor over load protection (Auto-stop function)
Motor joint, Wrench
Cat.No
218810
222730
218820
218830
218840
218850
218860
218870
218800
222740
121090
121100
121110
121120
Freeze Dryer
Freeze Dryer
Double chamber CCX-32M
Combination with the organic
synthesizer PPS
Stirrer, Shaker
Stirrer, Shaker
Aluminum block CCX-32A
Most suitable for the routine experiment process.
Easy-to use new design.
Stir shaft
Performance
Manifold CCX-32M
Personal Organic Synthesizer Zodiac
CCX-3200
212960
1 to 8 pcs (Max.32)
0.5mL to 60mL
From RT +10˚C to 280˚C (50 to 60mL: 200˚C)
100 to 1200rpm (water)
Membrane pad key, digital display
Setting by volume knob, digital display
By reducing pressure and replacing air by inert gas
No refluxing/Cooling water manifold*2
Pipette, syringe, dropping funnel
Throught the slit of the aluminum block
Double chamber, fuse, independent overheat protector
Glass (DURAN)
OD: 12mm (hose end), for silicone hose (ø9 x 13m)
OD: 7.5mm One touch hose inlet (sillcone hose ø5 x 8m)
5˚C to 35˚C
245 (W) x 275 (D) x 200 (H) (Chamber), 800H (Poll), 8kg
8.5A, 850VA•AC100V 50/60Hz
CCX-32M Catalog No.212970
optional, reactor size:ø34 (12types)
Optional
CCX-32A Catalogue No.212980
CCX-32W Catalogue No.212990
CCX-CTRL2 Catalog No.213000
Low Temperature
circulator
Low Temperature
circulator
Product name
Model
Cat. No
Available number of reaction vessels
Synthesis scale
Stirring system
Temperature setting, display
Stirring speed setting, display
Gas purging system
Refluxing
Sample injection
Safety features
Materials of sample contacting part
End connection of cooling water
Connector inlet/outlet of manifold
Ambient temperature
Input power
Manifold
Reaction vessels
Test tubes
Aluminium chamber (test tube adapt)
Double chamber
Stirring & heating unit
Bath,Cold Trap
Bath,Cold Trap
Specifications
Oven, Incubator
Oven, Incubator
CPS-1000
Organic Synthesizer
Organic Synthesizer
CCX-3200
Stir impeller
Evaporator,
Vacuum Unit
Features
• Interchangeable joint (TS 15/25) can be mounted.
• Motor overload protection function is incorporated as an over-current protection
circuit. When the circuit is over-current, motor automatically stops.
• Different shapes of impellers available depending on the synthesizers used
with the sitter.
• Rotation speed can be set to desired value. Slow-up function prevents overload
caused by sudden rotation speed increase. Rotation speed change during
operation and operation interruption by power switch are also possible.
• DC brushless motor is adopted to realize smooth and strong rotation. Rotation
speed range is 31~226 rpm and Max. torque is 68mN/m.
• The stirring wing (impeller) is made of PTFE and the stirring rod (shaft) is made
of PEEK. Both are inert specification and the experiment can be conducted
wigthout problem of the solvent chemical resistance.
Evaporator,
Vacuum Unit
It is designed for personal organic synthetic Process Station (PPS, PPV series)
and features compact size, overhanging stirrer. Because plural units can be
used in parallel, it is convenient for the polymerization reaction, the stirring of
crystal and reaction examination of a small volume sample. Compact size
design contributes to space saving in the laboratory.
Features
• No. Of positions; 1-8 positions (Max. 32 vessels). Synthesis scale; 0.5mL60mL.
• Wide temperature control range from RT+10˚C to 280˚C (200˚C for the scale
of 50-60mL).
• Gas purge function is strengthened by the use of sealing tube, Shrenk tube,
pressure vessel and Dean-Stark trap.
• Cold water manifold and Dimorth condenser realize strong and efficient
reflux experiment.
Reaction vessels can be changed (ø12~34)
Organic Synthesizer
Organic Synthesizer
Personal Organic Synthesizer Zodiac CCX-3200
Stirring and heating unit
34
35
3
3
Organic Synthesizer
Organic Synthesizer
Process Station Optional Accessories
Concentration unit (For Chemistation)
Parallel concentration of synthesized materials
Liquid-Liquid extraction unit
Without separating funnel, extraction is easily available.
Suction
Dripping
Bottom phase can be completely
drained.
When sucking upper phase,
separate the separation tube
and drain bottom phase.
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Mixing
PPS-VAP
Organic Synthesizer
Organic Synthesizer
Pippetter Separatory tube
Independent inert flow route without
contamination
Individual stop cock to adjust vapor
volume
One touch mixing by magnetic
stirrer.
Pippetter
Separation tube
Accelerate concentration and prevent
bumping
Oven, Incubator
Oven, Incubator
Individual concentration
Inert gas controller
Cat.No.
198600
201660
Parallel type organic synthesis and concentration system Chemievaporation system by PPS Synthesizer
IGR-030•035B
Back (IGR-030)
Back (IGR-035)
Perfor
Composition mance
Design
CA-1111+PC2001 1R/EK+PPS2510+PPS-VAP
It is possible to start concentration after synthesizing process.
PC2001
Freeze Dryer
Freeze Dryer
36
Product name
IDiaphragm vacuum pump Solvent recovery vacuum pump
Type
MD-1C
PC-2001
Cat.No.
198530
198590
20/23L/min
26/26L/min
Displacement(50/60Hz)
2hpa (1.5Torr)
Ultimate pressure
—
500mL round bottom flask
Suction side waset liquid trap
—
Equipped
EXhaust side cooling recierer
resistance to corrosion. Piezo
—
Pressure sensor
resi stance conversion type
Materials of gas contacting pa
PFA. FFKM, PTFE
Inlet/outlet. OD 10mm
Cooling circulating nozzel
—
OD 8•10mm
Conection nozzel
OD 10mm
290W*320D*480H 10kg
Overall dimension & Weight
165W*315D*220H 6.5kg
Stirrer, Shaker
Stirrer, Shaker
Teflon diaphragm vacuum pump
MD-1C
Low Temperature
circulator
Low Temperature
circulator
PPS-5510 Connection example
Type
PPS-VAP
PPS-VAP
Inert gas controller
IGR-030
IGR-035
186870
186880
Manual type
—
0 to 0.06Mpa
0.03Mpa (Fixation)
0.56Mpa under
Analog display. safety valve
PEEK. Teflon.PP.SUS
PP. Aluminium. Brass
Inlet:1/4 inch tube. Outlet:1/4-28 fitting
80W*235 (285)D*131H. 2kg
Bath,Cold Trap
Bath,Cold Trap
Product name
For PPS 5 parallels
Concentation unit
For PPV 4 parallels
Product name
Type
Cat.No.
Control methord
Pressure range
Input Pressure
Display & Safty function
Materials of gas contacting
Connection diameter
Overall dimension & Wgight
37
3
3
Parts for Personal Organic Synthesizers
The synthes is system that can do the different liquid phase application reserch promptly and efficiently.
*PPS-5510, CCX-3200 Parts
*Drip proof cover
• 20 positions parallel screening and reaction condition study are
possible.
• Enables catalytic reaction.
• Teflon made easy to use 2 way cock.
• After synthesis, condenstaion can be done promptly.
• Small overhead stirrers.
Hose
connection
Screw top
Enabing condensation polymerization while removing water.
Dean-Stark, Condensation polymerization
Dimroth
conderser
System cord
Synthesis Scale
Temp. control range
Branched
reaction tube
Drip-proof
cover
Test tube
adapter
SYS13050
7mL,12.5L, 30mL.
60mL*5 pcs
-10˚C to 150˚C
up till 130˚C: 50~60mL
Hose
connection
Screw top
Reliable full condensation of vapors from the reacion solvent, and efficient refluxing.
Dimroth
conderser
• Suitable for heat reaction study above the boiling point.
• Strong reflux experiments are made possible by using efficient Dimroth condenser.
• Reflux by water realizes polymerization experiments and greem chemistry.
Synthesis Scale
Temp. control range
Reagent injection
Branched
reaction tube
SYS13051
7mL,12.5L, 30mL.
60mL*5 pieces
-10˚C to 150˚C
up till 130˚C: 50~60mL
Teflom shutter
Drip-proof
cover
Test tube
adapter
Safety features
Part name
Test tube adapter (ø12 4 positions)
Test tube adapter (ø13)
Test tube adapter (ø13*3 positions)
Test tube adapter (ø15*3 positions)
Test tube adapter (ø16.5)
Test tube adapter (ø30) for pressure resistant vessel
Test tube adapter (ø34) for PPS-5510 only
Catalog. No
217080
212810
217090
212820
217100
212830
212840
212850
212860
212870
212880
212890
212900
218550
217110
Type
*
*
*
*
*
Catalog. No
212700
218420
218410
218430
195710
1
Type Catalog. No
*
182100
*
191840
*
200280
*
200290
*
200300
*
213110
*
213120
*
218330
*
218340
2
4
3
5
7
6
9
10
Freeze Dryer
Freeze Dryer
Teflon made shutter to protect aluminum block
from dew.
Even if a test tube breaks by any uxexpected cause and the
solvent spills, the dew receive tray made of Teflon protects the
device.
Double chamber protects the aluminum block from dew and
also prevents dispersion when the tule is damaged.
Part name
4 PTFE Magnetic stirring bar (disk shape D9*6H) used for D12.10pcs
5 PTFE Magnetic stirring bar (cross shape D10*5H) used for D13-D18.10pcs
6 PTFE Magnetic stirring bar (football shape D6*15L) used for D24.5pcs
7 PTFE Magnetic stirring bar (football shape D10*20L) used for D0 and 34,5pcs
8 PTFE Magnetic stirring bar (football shape D10*25L) used for D34.5pcs
9 Powerful magnetic stirring bar (oval shape) D24-D30,1pce
10 Powerful magnetic stirring (for viscous liquids), usde for D24-D30,1pce
11 Glass stirring bar (Thin cylinder shape, D5*12L) for high temp, used for D18-30,4pcs
12 Glass stirring bar (Thin cylinder shape, D9.5*12.7L) for high temp, used for D18-30,1pcs
By using a test tube adapter, the size and
number of reaction vessels can be changed,
to one, three or four per position.
The system can be made fit for up to 20
reaction tubes.
Septem, Stirrig bar
*Septa
Part name
1 Suba seal (silicone rubber, for GL14, 10pcs)
2 Septum (natural rubber, for 14, 10pcs)
3 septum (silicone rubber, for 14, 10pcs)
septum (natural rubber, for 15, 10pcs)
septum (silicone rubber, for 15, 10pcs)
Since the reflux adapter cools down the
top of the reaction tubes, the reaction
solvent vapor can be refluxed effectively.
Test tube adapter
*Stirring bars
Sampling or injection by dripping funnel can be done
by using a reactive container with branch and threeway cock under inert condition.
38
Type
*
*
*
*
*
*
*
*
*
*
*
*
*
*
*
Reflux adapter
Stirrer, Shaker
Stirrer, Shaker
Heating the sample, Cooling, Reflux, Stirring, Gas
purging depressurization, Sampling.
Catalog. No
217320
217330
217340
217350
217360
217370
217380
217390
217400
217410
217420
217430
Low Temperature
circulator
Low Temperature
circulator
Dimroth, Plymerization, Green chemistry
System cord
Part name
Reflux adapter (ø12*4 positions)
Reflux adapter (ø13)
Reflux adapter (ø16.5)
Reflux adapterr (ø18)
*Test tube adapter
02 Personal organic Synthesizer
Main function
Type
*
*
*
*
*
*
*
*
*
*
*
*
*Reflux adapter
Cover to prevent dew in the aluminum
block necessary when using the cooling
cartridge.
Bath,Cold Trap
Bath,Cold Trap
Removing surplus water from azeotropes,
Heating of the sample. Cooling and reflux
by condenser, Gas puging, Stirring and
depressurization Samping.
Dean-Stark
trap
Catalog. No
217610
217620
217630
217640
217650
217660
217670
217680
217690
217700
217710
217720
217730
217740
217750
Oven, Incubator
Oven, Incubator
• It is suitable for the condensation polymerization reaction.
• In condensation polymerization reactions, where a small molecule like water is
generated, it is necessary to continuously remove the small molecules like
water in order to proceed the reactions to the direction of polymerization.
• Heating while removing water is possible by the use of Dean-Stark trap. Under
reduced pressure, small quantity of water removal is possible.
Main function
Drip proof cover
Type
*
*
*
*
*
*
*
*
*
*
*
*
*
*
*
Organic Synthesizer
Organic Synthesizer
01 Personal Organic Synthesizer
Part name
Drip proof cover (ø12*4 positions)
Drip proof cover (ø13)
Drip proof cover (ø16.5)
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Features
• Condensed polymerization while removing water.
• Reliable full condensation of vapors from the reaction solvent and
efficient refluxing.
• Reaction temperature monitoring.
• Total removal of oxygen by freeze degassing.
• Water-free/oxygen-free reactions.
Organic Synthesizer
Organic Synthesizer
Process Station System Examples
8
11
12
39
3
3
Organic Synthesizer
Organic Synthesizer
*Reactor glass tube
Reactor tube, condenser, hose, 14/23•GL14 related parts
Type
*
*
*
*
*
*
*
Catalog. No
217190
212770
217290
217220
217310
217210
217300
Type
*
*
*
*
*
*
Catalog. No
217230
217240
217250
217260
217280
217270
3
4
Part name
Dimroth condenser 14/23, GL14
Liebig condenser L100 14/23, GL14
Silicone-hose (used for manifold 5m)
Cooling insulation hose set (silicone ø91m, 2pcs) CT-1S
Cooling insulation hose set (silicone hose ø92m, 2pcs) CT-2S
6
14/23 related parts
Part name
Three-way cock for dosing sample, with solid glass plug
Dan-Stark trap for PPW•CCX type
Stopper 14/23 with hexagonal plate (10pcs)
DIN-Screwthread with Cone (10pcs)
Adapter with Ground joint, upper TS 15/25 lower cone 14/23
Dropping funnel 25mL 14/23
"Keck" Conical Joint Clip type 14, TS15 metal (10pcs)
7
Bath,Cold Trap
Part name
Screw-Cap with opening for screwthread tubes GL14(10 pcs)
Screw-Cap for screwthread tubes GL14 with PTFE (10 pcs)
Plastic Hose Connection, straight (10 pcs)
Plastic Hose Connection, bent (10 pcs)
Silicone Rubber Seals, Septa (25 pcs)
Silicone Rubber Sealings with Bore
12
15
14
16
17
ST-3F
*
*
HIP-HE
*
*
*
*
*
*
206430
218480
218490
218320
206420
218500
218470
218510
218380
218370
*
218390
*
218400
*
*
*
*
*
*
*
218460
215040
215050
218520
218530
218440
218450
5
4
3
1
6
2
7
8
9
10
11
12
13
14
16
15
17
24
20
21
22
23
PPS-15TC
PPS-25TC
PPS-35TC
25
*CCX-1100/1110•1300•1310 O Parts
Part name
Cross-shaped Stirring bar ø24 for CCX-1100/1110 type (10pcs)
Powerful magnetic stirring bar (oval shape) for CCX-1100•1110
Test tube ø24 (without rim) for CCX-10TC (25 pcs)
Test tube ø24 (with rim) for CCX-11TC (25 pcs)
O-ring for CCX-10TC (nitrile rubber, 20pcs) for replacement
O-ring for CCX-10TC (perfluoro) for replacement
O-ring for CCX-11TC (nitrile rubber, 20pcs) for replacement
O-ring for CCX-11TC (perfluoro) for replacement
CCX type gas manifold
Type Catalog. No
ST-2X 191850
ST-2F 213110
CT-2S 198740
*
213130
*
198750
*
198760
*
213150
*
213140
*
214390
Reaction Vessel
(PPV-3000)
Gas Manifold
(CCX-1000•1010•1200•1210)
Stirrer, Shaker
Stirrer, Shaker
Freeze Dryer
Freeze Dryer
Catalog. No
191840
191850
212680
191920
194050
201830
195670
195690
212690
195760
195770
213070
195640
195650
213100
195780
195790
213080
195700
213090
195620
195630
213110
10
PPS-1510/2510/3510 Teflon Cap
Type
ST-1X
ST-2X
ST-3X
QK-3P
CT-1S
CT-2S
*
*
*
*
*
*
*
*
*
*
*
*
*
*
*
*
18
ST-2F
Low Temperature
circulator
Low Temperature
circulator
*PPS-1510•2510•3510 parts
13
11
19
Part name
Cross-shaped Stirring bar for ø15 (10pcs)
Three-way cock (10pcs)
Cooling insulation hose (1m*2pcs)
Cooling insulation hose (2m*2pcs)
ø15test tube (with rim) (50pcs)
Perfluoro O-ring for PPS-15TC
Screw ring for Teflon cap ø15 (5pcs)
Teflon O-ring for PPS-15TC (10pcs)
Two-way cock for Teflon cap (10pcs)
Gas piping set (PPS type teflon cap)
PPS type ø15 Cap part (without Screw cap, with O-ring)
PPS type ø30 Cap part (without Screw cap, with O-ring)
8
9
*GL14 related parts
40
5
PPV-4300•4060 Parts
Type Catalog. No
HIP-30 218290
HIP-60 218310
*
218560
*
212340
*
218570
*
218580
Bath,Cold Trap
Catalog. No
212780
212720
212790
194050
201830
2
Part name
1 ø30 Pressuer-resistant vessel (SUS316), incl. glass vessel and stirring bar
2 ø60 Pressuer-resistant vessel (SUS316), incl. glass vessel and stirring bar
3 ø20 Glass vessel for ø30 Pressure-resistant vessel height 134mm
4 ø45 Glass vessel for ø60 Pressure-resistant vessel height 120mm
5 ø20 Teflon vessel for ø30 Pressuer-resistant vessel
6 ø45 Teflon vessel for ø60 Pressuer-resistant vessel
7 Tdflon Powerful magnetic stirring bar (football-shaped, ø10*15L,1 pce) for ø20 vess
ST vess ST-2F)
8 Tdflon Powerful magnetic stirring bar (football-shaped, ø14*25L,1 pce) for ø45 vess
ST vess ST-2F)
9 Pressure gauge (SUS316, pressure range: 100/0/2400kpa)
10 Pressure gauge (SUS316, pressure range: 0/6000kpa)
11 Pressure-resistant head with valve
12 Aluminum sleeve (for ø30 pressure-resistant vessel,1pce)
13 Protective pipe for temperature sensor (SUS316, 1 pce)
14 Pressure connection (high pressure joint, SUS316)
15 Individual Relief valve (Relief pressure: 0.34-2.4MPa)
Seal kit of the relief valve (Fluorocarbon) for replacement
Seal kit of the relief valve (Ethylene propylene rubber) for replacement
16 Spiral hose for connecting to the gas injection port (outer diameter:1/16", Swagelok
one end 1/4"screw nut SUS316) x 1
Spiral hose for connecting to the vessels (outer diameter:1/16", Swagelok
both end 1/4"screw nut SUS316) x 1
17 Flexible hose for connecting to the gas exhaust port (outer diameter:1/4", Swagelok
one end 1/4"screw nut SUS316) x 1
Spring kit(2.41-5.16Mpa)
Spring kit(0.34-2.41Mpa)
O-ring of the pressure-resistant vessel (for ø30,Perfluofo) for replacement
O-ring of the pressure-resistant vessel (for ø60,Perfluofo) for replacement
Back-up ring for pressure-resistant vessel (for ø30,Teflon) 10pcs
Back-up ring for pressure-resistant vessel (for ø60,Teflon) 10pcs
Oven, Incubator
Type
*
*
*
*
*
1
*PPV-4030•4060 Parts
*Condenser, connection hose
*
Oven, Incubator
Catalog. No
217120
217130
217140
217150
212760
217160
217170
217180
218290
218320
Organic Synthesizer
Organic Synthesizer
Type
*
*
*
*
*
*
*
*
*
*
Evaporator,
Vacuum Unit
Evaporator,
Vacuum Unit
Part name
Standard reaction vessel (ø18 14/23)
tandard reaction vessel (ø24 14/23)
tandard reaction vessel (ø18 14/23, GL14)
tandard reaction vessel (ø24 14/23, GL14)
tandard reaction vessel (ø30 14/23, GL14
Standard reaction vessel (ø34 14/23, GL14)
Sealing reaction vessel (ø16)
Sealing reaction vessel (ø24)
ø30 Stainless pressure resistant vessel (HIP-30)
On head part (with pressure gauge) HIP-HEAD
41

Organic Synthesizer - Lasalle Scientific Inc.

Transcription

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