CHAPTER 9. AGITATION AND MIXING
Transcription
CHAPTER 9. AGITATION AND MIXING
CHAPTER 9. AGITATION AND MIXING ABRAHAM ROGELIO MARTIN GARCIA PRESENTATION OUTLINE -Definitions -Purposes of agitation -Devices to produce agitation -Power consumption of agitators -Blending and Mixing -Suspension of solid particles -Dispersion Operations -Agitator selection and Scale up Copyright ©2003 A. R. Martin DEFINITIONS • Agitation: It refers to the induced motion of a “homogenous” material in a specified way • Mixing: It is the random distribution, into and through one another, of two or more initially separate phases PURPOSES OF AGITATION • Suspending solid particles • Blending miscible liquids • Dispersing a gas through the liquid • Dispersing a second liquid to form an emulsion or suspension • Promoting heat transfer Copyright ©2003 A. R. Martin 1 DEVICES TO PRODUCE AGITATION IMPELLERS • Propellers (high-speed, low viscosity) • Turbines (Moderate viscosity) • High-efficiency impellers Three-blade marine propeller Straight-blade turbine Disk turbine Pitched-blade turbine Concave-blade CD-6 impeller Source: McCabe et al. 2001 Copyright ©2003 A. R. Martin DESIGN OF TURBINES Da Dt 1 3 S1 E Dt 1 3 S2 H Dt 1 S3 W Da 1 5 J Dt 1 12 S5 L Da 1 4 S6 S4 Source: McCabe et al. 2001 Copyright ©2003 A. R. Martin 2 POWER CONSUMPTION OF AGITATORS It is a function of the volumetric flow rate and the kinetic energy Values of NQ NQ q Impeller K >SDa n1 k tan E SDaW @ q v nDa3 NQ Ek P P q (Flow number) nDa3 U Vt 2 U 2 q Ek 2 © P Un 3 Da5 2 D 2S 2 2 0.5 Four-blade 45q turbine (W/Da)=1/6 0.87 Disk turbine 1.3 HE-3 high-efficiency impeller 0.47 DSnDa 2 § D 2S 2 Un 3 Da5 ¨¨ Marine propellers (square pitch) · N Q ¸¸ ¹ NQ Np P Un 3 Da5 (Power number) Copyright ©2003 A. R. Martin Np \ Re, Fr, S1 , S 2 ,..., S n Source: McCabe et al. 2001 Copyright ©2003 A. R. Martin 3 P N p n 3 Da5 U For Re 10 P K L n 2 Da3 P For Re ! 10000 P K T n 3 Da5 U Source: McCabe et al. 2001 Copyright ©2003 A. R. Martin BLENDING AND MIXING Source: McCabe et al. 2001 Copyright ©2003 A. R. Martin 4 Source: McCabe et al. 2001 Copyright ©2003 A. R. Martin SUSPENSION OF SOLID PARTICLES nc Da0.85 § 'U · ¸¸ © U ¹ 0.45 SQ 0.1 D p0.2 ¨¨ g B 0.13 Shape factor S a Dt/ E S Impeller type Dt/D Six-blade turbine Da/W=5 Np=6.2 2 3 4 4 4 4 4.1 7.5 11.5 Two-blade paddle Da/W=4 Np=2.5 2 3 4 4 4 4 4.8 8 12.5 Three-blade propeller Np=0.5 3 4 4 4 4 2.5 6.5 8.5 9.5 Copyright ©2003 A. R. Martin 5 DISPERSION OPERATIONS DS Da § U C n 2 Da3 · ¸¸ © V ¹ 0.6 0.0581 5.4\ ¨¨ Source: McCabe et al. 2001 Copyright ©2003 A. R. Martin AGITATOR SELECTION AND SCALE UP AGITATOR SELECTION • Depends on the viscosity of the liquid • For specific time of mixing, the best mixer is the one that mixes in the required time with the smallest amount of power SCALE UP • Maintaining constant power per unit volume and geometric similarity 2 n2 n1 § Da1 · 3 ¨¨ ¸¸ © Da 2 ¹ Copyright ©2003 A. R. Martin 6