Apollo 300 - LOT Quantum Design
Transcription
Apollo 300 - LOT Quantum Design
CamScan Superior Electron Optics By Design Apollo 300 CamScan Apollo 300 Field Emission SEM Apollo 300, versatility without compromise; designed by microscopists Obducat CamScan has worked in partnership with its customers for more than 35 years to produce outstanding solutions for Scanning Electron Microscopists. The world class engineering and electron optical design has ensured a reliable and long service life. This coupled with one of the most versatile vacuum sample chambers available ensures the CamScan SEM range brings value for money to all users. Variable energy optics provide excellent Low kV performance A low energy electron beam suffers from increased aberrations as the electrons travel through the column. The concept of variable energy optics allows higher electron energies to be used for the electron beam in the column, and minimises degradation of the beam. Electrostatic Lens C1 Anode Gun Alignment Gun Stigmator Coils Gun Alignment 6 Position Aperture Changer Condenser Lens C2 Isolation Valve In Column Back Scattered Detector (BSTL) In Column SED (SETL) Scan Coils Stigmator Coils Final Condenser Scan Coils Dynamic Focus Coils Chamber SE Detector Through lens detectors for high resolution at short working distances (Less than 10 mm) The Apollo 300 column is designed to incorporate the Delphi* Through Lens Detector assembly This provides both Secondary and Back scattered detectors in the column. *(Gk:Delphi – the location for the Oracle used as a source of information by the Ancient Gods) - Superior Electron Optics by Design Helios software; one platform for all CamScan SEM’s The Helios software incorporates an easy to use GUI which allows the operator to choose the setup which most suits their style of operation, whether it is mouse control or keyboard shortcuts. Appearance may be changed to include preferred tool bars and multiple windows or a more simple layout with one window and pegged control panels The optional Delta pad desktop module enables the microscope to be operated in a more traditional way through manual controls. Operators quickly find the simultaneous use of both mouse and Delta pad control leads to greater efficiency. CamScan Apollo 300 Field Emission SEM Optimised Chamber The spacious CamScan chamber has gained a reputation for excellent geometry and has evolved to provide the most effective solution for the critical analytical tasks of today. The superior quality of the engineering and the position of ports make this the first choice for demanding analytical research. The euccentric stage is door mounted which allows easy sample or sub-stage exchange. Nitrogen gas backfill minimises water vapour and environmental particle contamination improving pump down time. • Large or awkward samples can be both loaded and moved around with minimal restriction • Major detector systems including EDX, WDX and EBSD are mounted on the same side of the chamber and face the tilt axis of the stage • Sixteen (16) ports are optimised for multiple detector analysis and extended research applications Standard airlock system Specialist Load-lock systems Large swing-out door for easy access Large capacity stage - Superior Electron Optics by Design One platform - multiple signal detection %,%#42/. 02/"% #, 7$8 %$8 "3$ /04)#!, 3%) %"3$ 3!$ 3!-0,% !"3/2"%$#522%.4 BSD (1) CL BSD (2) The precision eucentric stage complements the functional geometry of the large multiported sample chamber to fulfil the demands of routine and research applications. The location of the detectors for high or variable vacuum modes gives optimal sample information and workflow. WDX SEI EDX EDX Sample stage The robust sample stage is a 6 axis, true eucentric design which is capable of millions of operations without compromising accuracy and reliability. Choices of motorisation and position encoders provide ideal solutions for all applications. The stage will accept large heavy samples without effecting eucentricity or the ability to tilt through 90 degrees; allowing edge observation without having to remount the sample. Various stages may be fitted to the door to allow experiments such as heating, cooling and tensile tests to be carried out. Cathodoluminescence stage STEREO OPTICAL MICROSCOPE Delphi through lens detectors WDX VIEWING WINDOW EBSD CAMERA AIRLOCK Vacuum System • The meticulous design of the vacuum system on the CamScan Apollo 300 ensures efficient pump down and ultimate cleanliness: • Careful material selection and component design for best vacuum practice. • Nitrogen chamber venting (eliminates influx of water vapour). • Turbomolecular Pump with isolation interlock. • Foreline Trap to prevent rotary pump back streaming. • Large vacuum reservoir (enables Rotary Pump to be automatically switched off to give a quiet environment). • Optional liquid nitrogen trap. • Ion Pumps for gun and column with automatic isolation during sample exchange. • Sample Load-lock fitted as standard. • Dry backing pump options. Nanotechnology Materials Science PCB contacts York stone IC bond contact Zinc Oxide on glass Lithography grid Woven cotton sample Life Science Site Requirements Services: Electrical Supply: Single Phase: 220/240v ±10v, 50Hz, 3.5kVA Connection should be through a 16A IPP44 Industrial Socket to IEC/EN 6039-2. A 20A in line isolation switch should be included. Water: Mains Water: OR Water Re-circulator: Whole mammalian cochlea sample courtesy of Dr D.N.Furness, Keele University Nitrogen: Dry Nitrogen: Liquid Nitrogen: Environment: Temperature: Humidity: Vibration: Magnetic Field: 2Litres/min; temperature 15ºC ± 5°C Minimum pressure 2bar Heat Extraction Capacity1.5kW Minimum Pressure 3bar. 99.99% purity regulated to 5.5 bar (80psi) Not required for SEM 20°C ± 5°C 70° RH < 3μm p-p for frequencies >5HzAC < 5mG p-p (W/LaB6) < 3mG p-p (FE) Weight: Approximate total weight 900kg (Column 500kg approx.) Segment of butterfly wing The site requirements for the Scanning Electron Microscope should be selected to ensure the minimum disturbance from both mechanical vibration and stray magnetic fields. Lift motors, plant machinery, heating and ventilating plant, machine tools and electrical transport facilities (trams, railways etc.) should be as far away as can be achieved. A ground floor location is recommended to fulfil the vibration specification. Allow approximately 60 cm between rear of console and wall Water Out Water In Rotary Pump 256 cm 60 cm Fan Box: do not restrict air flow 92 cm Allow approx. 30 cm for EDS detector E.D.S. Segment of cochlea showing the inner and outer steriociliary bundles Sample courtesy of Dr. D.N.Furness, Keele University 127 cm 400kg approx weight 60 cm 500kg approx. weight 74 cm Height of Electron Gun = 180 cm All dimensions are approximate. Scale 1 : 20 CamScan Superior Electron Optics By Design Obducat CamScan Limited CamScan House, Pembroke Avenue, Waterbeach, Cambridge. CB25 9PY UK Tel: +44 (0)1223 861 066 Fax: +44 (0)1223 861 077 [email protected] www.camscan.com A member of the Obducat Group Local Distributor LOT-Oriel GmbH & Co. KG contact: www.lot-oriel.com [email protected]