SZ-100 - Apel Laser
Transcription
SZ-100 - Apel Laser
Nanoparticle Analyzer 6= VHULHV In du st r y's Wi d est Ra n ge a n d Hi gh est P reci si on Mea su rem ent In st r u m ent for Na no -p a r t i cl e Ch a ra cter i zat i on “n a n o pa r t i c a S Z -10 0” A highly advanced analyzer solves the mysteries of the nano-world. A single device analyzes the three parameters that characterize nanoparticles: particle size, zeta potential, and molecular weight. Newly developed to satisfy the need for devices to simply and accurately evaluate the size and dispersion stability of nanoparticles, the key to nanotechnology advancement: SZ -100 Series Nanoparticle Analyzer Nanotechnology research and development is a continuously evolving effort to control substances at the atomic and molecular level in order to achieve new and better materials and products. The miniaturization of components – that is, control at the nanolevel – is necessary to achieve faster, higher-performance devices and functions and to reduce energy consumption. Nanotechnology has come to play a key role in wide-ranging fields that affect our daily lives, including food, cosmetics, and the life sciences. Clear and simple multi-parameter analysis of nanoparticles! Three analyzers in a single compact body deliver high-sensitivity, high-accuracy analysis of each measurement parameter. Particle Size Measurement Range 0.3 nm to 8 μm 7KH6=6HULHVPHDVXUHVSDUWLFOHVL]HDQGSDUWLFOHGLVWULEXWLRQZLGWKE\G\QDPLFOLJKW VFDWWHULQJ'/6 $QDO\VLVDFURVVDZLGHUDQJHRIVDPSOHFRQFHQWUDWLRQV0HDVXUHPHQWRIVDPSOHVUDQJLQJ IURPORZSSPRUGHUFRQFHQWUDWLRQVWRKLJKFRQFHQWUDWLRQVDPSOHVLQGRXEOHGLJLWSHUFHQW DJHVLVSRVVLEOH$FFHSWVFRPPHUFLDOO\DYDLODEOHVDPSOLQJFHOOV$QDO\VLVRIVPDOOYROXPH VDPSOHVLVDOVRSRVVLEOH Zeta Potential Measurement –200 to +200 mV $QDO\VLVRIVDPSOHYROXPHVDVVPDOODVѥ/XVLQJ+25,%$GHYHORSHGPLFURHOHFWURSKRUHVLVFHOOV8VHWKHYDOXHRI]HWDSRWHQWLDOWRSUHGLFWDQGFRQWUROGLVSHUVLRQVWDELOLW\ +LJK]HWDSRWHQWLDOPDJQLWXGHVLQGLFDWHDVWDEOHGLVSHUVLRQXVHIXOIRUIRUPXODWLRQZRUN Molecular weight 1 10 3 to 2 10 7 Da $EVROXWHPROHFXODUZHLJKW0ZDQGWKHVHFRQGYLULDOFRHIILFLHQW$ DUHREWDLQHGE\SHUIRUPLQJVWDWLFOLJKWVFDWWHULQJ PHDVXUHPHQWDVDIXQFWLRQRIVDPSOHFRQFHQWUDWLRQDQGSUHSDULQJ'HE\HSORWV The SZ-100 Series applies sophisticated intelligence and learning capability to rapidly determine nanoparticle properties! ● 6LQFHWKH6=6HULHVDQDO\]HUFRYHUVDZLGHVDPSOHFRQFHQWUDWLRQPHDVXUHPHQWUDQJHVDPSOHGLOXWLRQDQGRWKHUSUHSURFHVVLQJLVQHDUO\HOLPLQDWHG 7KHXVHRIDGXDORSWLFDOV\VWHPHQDEOHVPHDVXUHPHQWRIKLJKFRQFHQWUDWLRQVDPSOHVVXFKDVVOXUU\DQGLQNSLJPHQWVDVZHOODVORZFRQFHQWUDWLRQSURWHLQVDQGSRO\PHUV ● $VLQJOHGHYLFHDQDO\]HVWKHWKUHHSDUDPHWHUVWKDWFKDUDFWHUL]HQDQRSDUWLFOHVSDUWLFOHVL]H]HWDSRWHQWLDODQGPROHFXODUZHLJKW ● +25,%$GHYHORSHGGLVSRVDEOHFHOOVIRU]HWDSRWHQWLDOPHDVXUHPHQWSUHYHQWVDPSOHFRQWDPLQDWLRQ 6LPSOHDQDO\VLVE\PHDQVRIXOWUDPLFURYROXPHGHGLFDWHGFHOOVYROXPHDVORZDVѥ/6XLWDEOHIRUDQDO\VLVRIGLOXWHVDPSOHV ● +25,%$GHYHORSHGHOHFWURGHIRU]HWDSRWHQWLDOFHOOPDGHIURPFDUERQPDWHULDOWKHPDWHULDO LVQRWFRUURGHGE\KLJKVDOWVDPSOHVVXFKDVVDOLQH SZ -100 Simply fill the sample cell and place the cell in the analyzer. Simple and Convenient Operation 01 02 03 $VSDFHVDYLQJERG\GHVLJQPDNHVWKHDQDO\]HUVXLWDEOHIRU LQVWDOODWLRQLQDQ\ODERUDWRU\HQYLURQPHQW 04 Operation MaintenanceFree Procedure [ Sampling ] [ Cell Set-Up ] [ Start Measurement ] [ Results Display ] )LOOWKHVDPSOHFHOO 3ODFHWKHFHOOLQWKHDQDO\]HU &OLFNWKH6WDUWEXWWRQ 7KHPHDVXUHPHQWUHVXOWV DUHGLVSOD\HG 1RPDLQWHQDQFHRUFOHDQLQJRI WKHDQDO\]HULVUHTXLUHG$IWHU PHDVXUHPHQWVLPSO\FOHDQRU GLVSRVHRIWKHFHOO Features of HORIBA’s Optical System Particle Size Measurement Principle 1 +LJK6HQVLWLYLW\2SWLFDO&RPSRQHQWV 7KH6=XVHVWKHWHFKQLTXHRIG\QDPLFOLJKWVFDWWHULQJWRGHWHUPLQHSDUWLFOHVL]H'\QDPLFOLJKWVFDWWHULQJLVWKH PHDVXUHPHQWRIIOXFWXDWLRQVLQVFDWWHUHGOLJKWLQWHQVLW\ZLWKWLPH7KHVHIOXFWXDWLRQVLQLQWHQVLW\DULVHGXHWRWKHUDQGRP %URZQLDQPRWLRQRIWKHQDQRSDUWLFOHV7KHUHIRUHWKHVWDWLVWLFDOEHKDYLRURIWKHVHIOXFWXDWLRQVLQVFDWWHUHGLQWHQVLW\FDQ EHUHODWHGWRWKHGLIIXVLRQRIWKHSDUWLFOHV6LQFHODUJHUSDUWLFOHVGLIIXVHPRUHVORZO\WKDQVPDOOSDUWLFOHVRQHFDQUHDGLO\ 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S+&RQWUROOHU$FFHVVRU\6SHFLILFDWLRQV 1XPEHURIWLWUDQWERWWOHV 6DPSOHIORZUDWHP/PLQ 6DPSOHYROXPHP/ S+DGMXVWPHQWUDQJH 3RZHUVXSSO\$&9+]9$ 'LPHQVLRQVDQGZHLJKW 6DPSOHFRQFHQWUDWLRQSSPS+ 0RELOLW\UDWHGѥP・FP9V 0HDVXUHPHQWUHVXOWV0RELOLW\ ѥP・FP9V =HWDSRWHQWLDO P9 6DPSOHFRQFHQWUDWLRQPRO/ $GMXVWHGWRZZLWK.&O =HWDSRWHQWLDO P9 %RG\'[:[+PPDSSUR[NJ 6WLUUHU'[:[+PPDSSUR[NJ &LUFXODWLRQSXPS'[:[+PP DSSUR[NJ S+HOHFWURGHSDUWVQXPEHU S+FDOLEUDWLRQXQLWSDUWVQXPEHU 6=60HDVXUHPHQW6SHFLILFDWLRQV SZ-100-S (particle size and molecular weight measurement only) Measurement principles Particle size measurement: Dynamic Light Scattering Molecular weight measurement: Debye plot method (static scattered light intensity) Measurement range Particle size: 0.3 nm to 8 μm Molecular weight: 1000 to 2x107 Da (Debye plot) 540 to 2x107 Da (MHS Equation)*1 Maximum sample concentration 40 wt%*2 Particle size measurement accuracy Measurement accuracy of ±2% for NIST traceable polystyrene latex 100 nm spheres (not including variation in the standard particles themselves) Measurement angles 90° and 173° (automatic or manual selection) Cells Measurement time 'DWD3URFHVVLQJ $QDO\]HU6SHFLILFDWLRQV6=6DQG6== Model Measuring unit optical system Light source: Diode pumped frequency doubled laser (532 nm, 10 mW) Detectors: Photomultiplier tubes (PMT) Laser classification Class I Operating temperature and humidity 15-35°C, RH 85% or less (no ncondensing) Holder temperature control temperature settings 1-90°C (up to 70°C for cells with electrodes and plastic cells) Purging Dry gas purge port tube connection is possible. Power supply AC 100-240 V, 50/60 Hz, 150 VA Navigation files turn complex parameter input into simple to use operating procedures. / Store 100 data items on a data list. / Display individual data items with a single mouse click. / Perform pH, temperature, and sample concentration trend measurement. 3DUWLFOH6L]H0HDVXUHPHQW Real-time display of the autocorrelation function / Display of median size, specific surface area, mode size, average size, standard deviation, coefficient of variation, span value, percentage size (max. of 10 items), Z average, polydispersity index, size percentage (max. of 10 items displayed) / Particle distribution graph, autocorrelation function, residual error / Refractive index, viscosity, computing range, and data recalculation after measurement 0ROHFXODU:HLJKW0HDVXUHPHQW Cuvettes Dimensions 385 (D) x 528 (W) x 273 (H) mm (excluding protrusions) Approx. 2 min. under ordinary conditions Weight 25 kg (from the start of measurement to the display of results for particle size measurement) Personal computer Windows computer with one available USB port Interface USB 2.0 (between measuring unit and PC) OS Windows® XP™ 32 bit, Vista™ 32 bit or 7™ 32/64 bit Required sample volume Minimum volume of 12 μL*3 to 1000 μL (differs depending on cell material) Usable liquids Water, ethanol, organic solvents Molecular Weight Measurement Real-time display of Debye plots / Display of molecular weight and the second virial coefficient / Recalculation of Debye plot graph display data =HWD3RWHQWLDO0HDVXUHPHQW Zeta potential, standard deviation, electrophoretic mobility, and average zeta potential at each peak / Display of zeta potential graphs, mobility graphs, recalculation of data 0DUN+RZLQN6DNXUDGD(TXDWLRQ, dHSHQGLQJRQVDPSOH 'HSHQGLQJRQVDPSOH )0LFURFHOO 2SWLRQV 21CFR Part 11 software / Zeta potential measurement organic solvent cells / pH control unit / IQ/OQ/PQ support / High power laser 532nm 100mW 6==0HDVXUHPHQW6SHFLILFDWLRQV 3DUWLFOHVL]HDQGPROHFXODUZHLJKWPHDVXUHPHQWVSHFLILFDWLRQVDUHWKHVDPHDVIRUWKH6=6 Model SZ-100-Z (with zeta potential measurement unit) Measurement principle Zeta potential measurement: Laser Doppler electrophoresis Measurement range -200 to +200 mV Size range suitable for measurement Minimum 2.0 nm, Maximum 100 μm*4 &ODVV,ODVHUSURGXFW &(FHUWLILFDWLRQ 'LPHQVLRQVPP 0 to 20 Maximum sample concentration 40 wt%*6 Cells Dedicated cell with electrodes Measurement time Approx. 2 min. under ordinary conditions Required sample volume 100 μL Carrier fluids Water Measurement conductivity range S/m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