NEW - J-KEM Scientific

Transcription

J-KEM
®
Scientific, Inc.
Instruments for Science from Scientists
Temperature
Control
Reaction
Automation
Custom
Robotics
J-KEM Scientific 2009
Product Highlights
Digital Temperature Controllers
W in
E
N 2009
Precision Temperature Controllers for Research
• Regulate volumes from 100 µL to 22 L
High Power & High Safety Controllers
• Reactors up to 100 L
• USB standard on all
200-Series temperature
and vacuum controllers
Economy Temperature Controllers
• Free Windows control &
Digital Vacuum Regulator
data logging software
• Digital Control of Vacuum Pressure from 760 to 0.1 torr
• 0.1o C Regulation
< 1o C Over-shoot
• Regulate Vacuum to 0.1 torr with DVR-1000
Parallel Synthesis & Lab Automation Equipment
Syringe Pumps
Parallel Reaction Systems
• Delivery rates
from 1 µL/min
to 375 mL/min
• Single & Multiposition pumps
• PC & stand
alone operation
• Deliver any
volume from
any syringe
• Solution phase & solid
phase reaction systems
• PC control of:
- Reagent delivery
- Temperature
- Pressure
• Custom designs
Reaction Block Systems
• KEM-Lab Personal Reaction Blocks
• Heat, cool,
& reflux
• Multiple vial
sizes
• Custom
designs
• Multiple Temperature Zones
Custom Robotic Workstations
Robotic Solutions
•
•
•
•
Custom hardware and software
Weighing • Dissolution • Reformatting
Solid & Solution phase Synthesis
Cherry picking • Solid phase extraction
User Programmable
• All robots include the original source code
NEW - Endeavour Robots
priced from $6000
Capping/Uncapping
Station
Index
Adapters, Thermocouple
Automation Equipment
Robotics
Fluid Delivery
Reactors
Chiller, Circulating
Evaporators
KEM-Vap
Microtiter Plate
Reaction Block
Custom
Fraction Collector
Gas Heater
Glass Microtiter Plate
Heating Mantles
Hand-Held Meters
KEM-Lab Reactors
KEM-Prep Reactor
KEM-Vap Evaporator
Monitors
Temperature
Vacuum
Water Flow
Nitrogen Gas Heater
Oil baths, Instatherm
Over-Head Stirrer
Parallel Synthesis Reactors
Solution Phase
Solid Phase
39
2-9
10-15
14-15, 25
24
27
23, 27
18
27
9
29
23
40
29
23
17
27
28
30
28
29
40
25
15-23
26
Personal Reaction Station
Pressure Regulator, Digital
Reaction Blocks
Single Temperature Zone
Multi-Temperature Zone
Custom
Shaker
Reaction Controller
Robotics
Instruments
Accessories
Do-It-Yourself
Safety Equipment
Lab Safety Controller
Water Flow Monitor
Digital Temperature Monitor
Temperature Controllers
Shakers
Benchtop, Reaction Block
KEM-Lab
Robotic
Solid Phase Extraction Station
Solid Phase Synthesis Reactor
Solvent Evaporator
Stirrer, Miniature Overhead
Syringe Pump
Single and Multi-Channel
Custom
Do-It-Yourself
16
31
18
22
20-21
19
14
2-7
8-9
7
28
28
28
35
19
23
8
8
26
27
25
10-13
11-14
11
Research Controllers
Multi-Channel
Safety
High Power
Oil Bath Controller
Economy
Custom
Monitors
Safety Limit Controller
Power Controller
Thermocouples & Accessories
Temperature Monitor
Thermocouples
Single Element
Dual Element
Glass Coated
Teflon Coated
Hypodermic Needle Probe
Thin Wire
Cords and Accessories
Trinity Power Controller
USB Network Extenders
Vacuum Regulator, Digital
Monitors
Precision
Variac, Solid State
Water Flow Monitor
Who We Are
32-37
34
35
35
36
36
25
28
28
29
38-39
28
38-39
35
38
38-39
39
39
38
29
37
30
30
31
29
28
41
Heating Profile of J-KEM’s
200-Series Temperature Controllers
Temperature Control
J-KEM’s patented
power control
computer makes
this the only
controller that
can heat volumes
under 100 µL with
the safety of
0.1o C regulation.
Actual heating
data is shown at
right.
Model 210 controller shown with power control computer
Ordering Information
J-KEM
®
Phone:
J-KEM Scientific, Inc.
6970 Olive Blvd.
Saint Louis, MO 63130
USA
Scientific, Inc.
(314) 863-5536
(800) 827-4849
FAX:
(314) 863-6070
Email:
[email protected]
On-line Catalog: http://www.jkem.com
The J-KEM® Guarantee
All J-KEM products are guaranteed to
be the highest quality and most accurate
instruments available. Any J-KEM product
not meeting your expectations can be
returned within 30 days for a full refund.
Robert C. Elliott / President
Custom Laboratory Robotics
Eclipse
Workstation
With four robot styles and multiple software options, J-KEM is
uniquely positioned to offer custom robotic solutions for virtually any
lab automation need.
J-KEM’s technology makes lab automation as
Simple as 1, 2, 3.
1
Key Features: • Fast • Positional accuracy
• Affordable • Multiple Z-probes
Phoenix
Workstation
Key Features: • Large deck size • Multiple Z-probes
• Generates > 100 lb. of force in the Z- direction.
Voyager
Workstation
Four Robotic Platforms to Choose From
With four different robotic platforms, J-KEM can select the one that
most efficiently automates your unique application. Each platform has
its own set of advantages including speed, positional accuracy, power,
and price that make it the preferred system for different applications.
2
Custom Solutions
J-KEM offers complete hardware and software solutions for almost any
lab automation task. Every workstation is customized with the features
and software needed to run your specific application.
Workstations for:
• Weighing • Dissolution • Synthesis • Sorting
• Crystallization • Cherry picking • SPE
• SPS • Spectroscopy
Key Features: • Fast • Optimized for microvial
weighing and cherry picking applications
Endeavour
Workstation
Key Features: • Fast • Positional accuracy
• Most affordable workstation available
Page 2
J-KEM Scientific
3
Do-It-Yourself Robotics
New in 2009
J-KEM offers each of its robotic systems with
custom programming, professional installation, and user training. For
most researchers, this is the service they both need and expect. For
those research teams who prefer to do it themselves, J-KEM now offers
each of its robotic systems as a fully configured and tested workstation,
but with no pre-installed software. With complete systems starting
under $6,000, this is a highly affordable way to introduce robotics to
your workflow. Software options are available to support your custom
development.
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Eclipse Robotic Workstations
The Eclipse workstation uses modular
X- and Y-axis rails combined with a
wide selection of automated tools such
as grippers, multi-position needles, and
custom probes. The open design of
the Eclipse provides easy access to the
entire workstation deck.
Value:
From $20,000
Affordability:
The affordable price of the
Eclipse (starting under $20,000)
creates new opportunities for
lab automation. For example, a
weighing station with bar code
scanner and 0.01 mg resolution
balance costs about $28,000.
Features:
• Speed: 400 mm/sec
• Positional Accuracy: ±0.02mm
• Z-Axis Force: 10 pounds
Test Tube
Weighing Station
Examples of Eclipse Workstations
• Bar code scanner
• Excel output
Plate Washer with
Heated Reaction Station
• Analytical balance
See the Eclipse
in action at:
www.jkem.com/robotics
• Multi-step synthesis program run
in micro titer plate cells
• Plate gripper
• Temperature controlled reactor
Solid Phase
Extraction Station
• 24 Columns developed in parallel
• Controls flow rate in all columns
• Solvent level in each column is optically monitored to stop
solvent flow when the solvent front reaches the top of the packing.
Derivatization Station
Spectroscopy Robot
• Automated spectroscopic
analysis of 200 samples
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
• Reagent addition to septum vials
• Heated reactor with mixing
• Reaction mixture sampled at user set
times to GC vials
www.jkem.com
[email protected]
Page 3
Advantages of J-KEM Robotics
Custom Design
While others start from an existing
design, then try to make your application
fit their instrument, every J-KEM
workstation is designed from scratch
to implement your automation task
efficiently and with an eye towards future
expandability. J-KEM’s experience in
lab automation, including temperature
control, reactor design, fluid delivery,
solid and solution phase synthesis is
invaluable when optimizing the design of
custom robotics.
Polymer Compounding Robot
Modules: 4-Temperaure zone reaction block,
balance, bar code reader, heated & cooled reagent block, cooled 4-position sonicator, precision
syringe pump with 16 reagent ports, 6-zone temperature controller, and needle wash station.
Custom Software
You Own the Solution
J-KEM believes that you should not only own the instrument, but you
should own the technology that created the instrument. That’s why
we are the only company that releases the original source code with
every robot. This gives you the power to change every aspect of the
robot’s operation as your automation needs change.
Custom software is written for every workstation to provide an
intuitive user interface. The procedure’s setup, the way data is read
into and out of the program, and the exact sequence of program steps
are all customized to make the operation of your robot both efficient
and user friendly.
Personal Service
J-KEM is committed to personal service, offering any support that’s
needed to assure the successful integration and productivity of our
automation solutions. With one phone call, you can talk to the
engineer who designed your robot, the engineer who installed it, and
the software engineer who wrote the program.
Value
J-KEM’s custom robotics are often half the price of other companies’
“one-size-fits-all” alternative. While many of the modules on a
workstation are standard J-KEM products, we also use the best
available instruments like balances, bar code readers, and pumps to
assemble the final workstation in the most affordable and efficient
manner.
It’s not really enough to own the code if it’s not easy to use.
Written in VB.Net, the robotic
software contains intuitive,
high level functions that make
understanding or modifying
your code easy. Consider the
example to the right that weighs
every vial in a 96 vial rack.
Page 4
For Vial = 1 to 96
Rack.MoveToCell(XY, Vial)
Gripper.PickUpVial()
Balance.Tare()
Balance.MoveToCell(XY, 1)
MyWeight = Balance.Weight()
PutVialBack(Vial)
Next
J-KEM Scientific
Toll-free: (800) 827-4849
Why is it important to own the original source code?
Without the source code, you’re stuck with the robot you have
rather than the robot you need as your automation needs change.
For example, suppose the robot’s original task was weighing and
dissolving samples to specific concentrations, but now you need it to
add reagents to 4 mL septum vials in a temperature controlled reactor
with mixing. In most cases you’d need to purchase a new robot.
Even for small changes, if you don’t own the original source code,
then you’re 100% dependent on the company who does. J-KEM
offers ongoing software support for all of our customers. But still,
to own the tools that place you in control of your own workstation is
invaluable.
Fax: (314) 863-6070
www.jkem.com
[email protected]
Phoenix Robotic Workstations
Phoenix workstations
have three distinctive characteristics:
1. Large deck size that allows
access to multiple racks and
modules such as shakers,
balances, and filter stations.
2. Multiple Z-probe tools. This
robot has simultaneous access
to three 2.5 mL disposable tip
probes, three 200 µL disposable
tip probes, a septum penetrating
needle, a vial gripper, three
stainless steel cannula, and a
pressure plate to filter samples
using positive pressure.
3. The Z-axis can develop over
100 pounds or force, enough to
penetrate any septum or seal any
reactor.
Sample Dilution and Filtration Station
Examples of Phoenix Workstations
Cherry Picking and Sample Reformatting Workstation
Robot Modules
• Deck fits five Gilson racks
of any style
• Disposable pipette tip probe
• Syringe pump with 8-port
selectable valve
Workstation Procedure
In this application, samples arrive in a variety of formats,
including 4 mL, 8 mL, and 20 mL vials, three different
size test tubes, 24, 48, and 96 well titer plates. This
workstation reformats samples from the various tubes to
a single 96 well plate. From the master plate, a cherry
picked plate is made based on the input from an Excel
table.
Enzyme Specific Activity Workstation
Samples are transferred,
by weight, to 400 mL
beakers where they are
diluted 1200-fold. After
mixing, diluted samples
are dispensed to sample
vials for analysis.
Robot Modules
• 60-position high power magnetic stirrer
• Syringe pump with 8-port selectable valve
• Gripper for vial transport
• Cannula for large volume dispenses (> 100 mL)
and analytical needle for microliter dispenses
Sample Dissolution and Daughter Plate Preparation
Robot Modules
• Syringe pump with 8-port
selectable valve
• Bar code station
• Gripper for vial transport
• Septum penetrating needle
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
Dissolves solid samples to a standard concentration,
then adds additional liquid reagents. After mixing,
transfers aliquots to HPLC vials with septum caps
and to a titer plate cell. The identity of all vials
are tracked by bar code, and the volume of reagents
dispensed is verified by weight.
www.jkem.com
[email protected]
Page 5
Voyager Robotic Workstations
The Voyager workstation is optimized for
weighing and sorting glass or plastic vials in 96
position tube racks. The Voyager integrates a
Mettler balance with 10 µg resolution, an Opticon
2D bar code scanner, and high speed X, Y, & Z
drives. Combining world-class hardware with
intuitive software makes the Voyager the finest
workstation for tube handling available.
See the Voyager in action at:
www.jkem.com/robotics
Features:
Intuitive Software
Voyager’s software includes applications for weighing, scanning, sorting, and cherry picking
tubes. Support for data input and output from a variety of file formats, including Excel, .CVS,
and .TXT files is standard. Custom input/output file formats to access corporate data bases
or to interface with other laboratory instruments is available. The Z-arm automatically adjusts
to different tube heights and even supports different tube sizes in the same run. Various liquid
dispensing options are available for microliter to milliliter aspirate and dispense operations.
• Weighs up to 220 vials per hour
• 0.00001 g (10 µg) balance
• 2D bar code scanner decodes 2D
and all 1D bar code symbologies
• Gripper customized to individual vials
• Reads and writes to any data base
• Liquid dispensing/transfer options
Applications:
• Tube identification and weighing
• Tube sorting and re-arraying
• Cherry picking
Voyager-12 Workstation
The Voyager-12 has positions for 12 tube racks and 2 additional receiving racks for re-arraying or cherry picking.
Includes a Mettler balance with 10 µg resolution and 2D bar code scanner.
Specifications:
Dimensions:
Speed, X & Y-axis:
Positional accuracy:
Tube Heights:
Communications:
Power:
30” x 26” x 20” (DxWxH)
120mm/sec
0.02mm
0.5 to 2.5 inches
Requires 1 USB port
120 watts
$19,950
Voyager-24 Workstation
The Voyager-24 has positions for 24 tube racks plus 2 additional receiving racks for re-arraying or cherry picking.
Includes a Mettler balance with 10 µg resolution and 2D bar code scanner.
Specifications:
Dimensions:
Speed, X & Y-axis:
Positional accuracy:
Tube Heights:
Communications:
Power:
30” x 38” x 20” (DxWxH)
120mm/sec
0.02mm
0.5 to 2.5 inches
Requires 1 USB port
120 watts
Optional Features
The Voyager workstation
can be equipped with custom
grippers to
transport a
variety of
tube styles,
including
centrifuge
tubes.
Page 6
J-KEM Scientific
$21,600
Microtube above
balance pod
• Stainless steel or Teflon cannula for the addition of
liquid reagents
• Spectroscopic probes
• Mixing
• Heated reaction stations
• Custom user modules
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Endeavour Robotic Workstations
Starting
under $6000
The Endeavour is J-KEM’s
most compact and affordable
system, an ideal choice when
either bench space or budgets
are limited. The Endeavour
is also a great starting point
for researchers who want to develop their own automation instruments. In one
compact enclosure, the Endeavour includes all the needed electronics, drivers,
and power supplies. Combined with J-KEM’s software, the Endeavour can
be programmed to run complex motion control programs, even 3-axis arc
interpolations, in a matter of hours. The Endeavour is servo motor controlled
to provide rapid and precise motions with positional accuracies of 0.02mm.
Software Support
Two software packages are available for the Endeavour robot. Endeavour.dll
exposes high level functions, like those shown in the example below, that handle
all of the low-level tasks associated with serial communications and motor control.
Endeavour.dll exposes functions for every motion parameter including acceleration,
positioning, homing an axis, and I/O support. Endeavour.dll is included at no charge
with all orders. J-KEM also offers its AutoKem software written in Microsoft’s Visual Studio
2008.Net in the Visual Basic language. AutoKem provides the user with a feature rich
application having classes for racks, balances, syringe pumps, bar code readers, and many other
instruments so they can be added to an application with only a few lines of code. The original
source code for AutoKem is
provided to further support
Examples of Robot Commands from Endeavour.dll
custom programming.
Command
Description
HOME(X)
Home the X axis.
MOVE(Y,127.40)
Move on the Y axis to position 127.40 mm.
MOVE(X,100.0,
Y,235.0,
Z,25.5) Perform a simultaneous 3-axis
J-KEM
move to the specified coordinates.
manufactures
OUTPUT(12,ON)
Turn
user
I/O
output
12 on.
custom
INPUT(7)
Returns 0 if the input is low, 1 if high.
modules
Two Axis Endeavour
for the Z
plate of the
Endeavour
Endeavour-22020
Catalog #
Price
robot.
Two Axis Endeavour Robot Provides 200mm of addressable space on both the
EN22020
$5,995.00
·
·
·
·
Grippers
Needles
Syringes
Disposable
tips
X- and Y-axes. Y-axis supports 9 pounds. Dim: 320 x 405 x 320 mm (W x D x H).
Two Axis Endeavour Robot Provides 400mm of addressable space on both the
X- and Y-axes. Y-axis supports 9 pounds. Dim: 520 x 605 x 320 mm (W x D x H).
Three Axis Endeavour Robot Provides 200mm of addressable space on both the
X- and Y-axes and 100mm of stroke length in the Z-dimension.
Z axis supports up to 4.5 pound loads. Dimensions: 330 x 405 x 420 mm (W x D x H).
Three Axis Endeavour Robot Provides 400mm of addressable space on both the
X- and Y-axes and 100mm of stroke length in the Z-dimension.
Z axis supports up to 4.5 pound loads. Dimensions: 530 x 605 x 420 mm (W x D x H).
Endeavour Software
Endeavour.dll Software support for the Endeavour robot.
AutoKem Software Source code in VB.Net 2008 for the Endeavour robot.
Call J-KEM for complete function list.
EN24040
7,995.00
EN32020
7,640.00
EN34040
9,340.00
Catalog #
Price
AutoKem
N. C.
$795.00
Specifications for all Endeavor Robots
Call for drill guides and additional specifications.
Speed:
1-300 mm/sec
Positional Accuracy: 0.02 mm
I/O:
16 general purpose optically isolated logic level inputs
and 16 open collector optically isolated outputs (100 mA). +24 V & Gnd.
Communications:
USB and RS232
Power:
110 - 240 Vac input; 200 watts
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 7
Robotic Workstation Accessories
Robotic Shaker
Specially designed for robotic applications, this low profile shaker is less than 5”
tall. The key feature of the RS2000 is its ability to home to an absolute X- and
Y-coordinate when stopped with accuracies better than 0.1mm in both the X and
Y dimensions. Homing to a known coordinate allows the robot to reliably access
modules attached to the shaker’s mounting plate. Triple eccentric drives provide
vigorous mixing of loads up to 60 pounds.
Specifications:
Catalog #
Price
RS2000
$5,840.00
Dimensions:
Rotational speeds:
Maximum load:
Shaking motion:
Orbital radius:
Communications:
12.25” x 20” x 4.75” (WxDxH)
40 - 525 rpm
60 pounds
Orbital or linear
0.4” Can be customized
USB, RS232, RS485, binary, manual
Solid Phase Extraction Station
The KEE-100 automates 24-positions of solid
phase extraction. The KEE-100 works by
regulating the solvent flow rate and optically
monitoring the position of the solvent front
above the top of the column packing in each
column individually. When the solvent front
reaches the top of the packing, a Teflon valve
closes preventing the packing from going
dry. Individual control of solvent flow rate
and position ensure reproducible results. SPE
columns can be developed either by vacuum or
positive pressure.
Optical
sensors
Teflon
valve
24-microcontrollers
Specifications:
Inside the
KEE-100
24 Positions
Column diameter: 1/8 to 1”
Solvent compatibility: Organic & aqueous
Flow rates: 0.05 to 4mL/min
Includes: SPE station and computer controller
KEE-100
Price:
$25,200
Multi-Position Syringe Pumps
Custom syringe pumps with 4 to 48 glass and
Teflon syringes. Syringe pump controller
(included) regulates the rate and volume of
dispense and fill cycles and automatically refills
syringes when needed. Dispenses from one or
all syringes in parallel.
Syringe sizes from 10 µL to 50 mL.
See page 10 for additional
syringe pump options
Prices
varies depending on
syringe size and features
8-Position pump:
16-Position pump:
32-Position pump:
48-Position pump:
From
From
From
From
$8,240
10,480
14,960
19,440
Custom Modules
Custom Fluid
Dispensing Options
J-KEM’s engineers
design whatever is
needed to efficiently
automate your
laboratory task
Heated and Cooled Reactors for
incubations and crystallizations
4-Position Sonicater
Florescence Probe on Z-arm
Page 8
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
Temp. Controlled Filter Station
www.jkem.com
[email protected]
Capping & Uncapping Station
J-KEM’s capping module automates the removal and replacement of caps from sample vials.
The capper removes, then replaces one cap at a time eliminating the possibility of cross
contamination. The top and bottom grippers automatically adjust to caps with diameters from
8 mm to 26 mm (2 mL to 20 mL vials) with no tooling changes, and can be adjusted for cap
diameters up to 35 mm and vial heights of 125 mm.
Thread pitch, the number of turns needed to remove
a cap, and recapping torque are all software
programmable. Available with RS232 or USB.
Capping Station Features:
Automatically adjusts for
- Cap diameter
- Vial height
- Thread pitch
Adjustable capping force
No limit on the number of turns
Price $12,750
·
·
·
The capping station mounted
to a J-KEM weighing robot
Fraction Collectors
J-KEM manufactures custom fraction collectors for any research
application, from a simple 2 axis to a sophisticated 3 axis
instrument running a custom, user specified, program.
Features:
·
·
·
·
External inputs & outputs for tube advance
Collect to a single or multiple racks
Fractions taken as a function of:
- Time
- Input voltage
- User specified parameter
Custom inputs/outputs to interface with other instruments
Custom fraction collector
holds 12 microtiter plates
The Endeavour’s affordable price makes it a perfect “intelligent fraction collector.” The Endeavour
can be programmed to collect fractions based on any input parameter and according to any pattern.
For example: 1) Place the first 40% and the last 40% of any peak in one common test tube,
but put the middle 20% in a GC vial for analysis.
2) Collect each peak to a single tube. After the fractionation process is done, go
back and transfer 1mL of each collected peak to a GC vial for analysis.
This is great stuff, but what I really need is. . . . . . .
J-KEM welcomes the opportunity to work with you on any automation project. Put our
experience in robotics, reactor design, fluidics, and custom programming to work for you.
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 9
Programmable Syringe Pumps
Model SYR-1200
Single Position
Syringe Pump
Dual Position
Syringe Pump
• Flow rates from 0.75 µL/min
to 375 mL/min
• Syringe automatically refills
to deliver any volume from
any syringe
• PC control and data logging
with KEM-Commander
software
The SYR-1200 syringe pump automates the addition of reagents at user entered rates. A programmable
distribution valve allows the system to dispense to and withdraw from up to 8 reagent bottles or reactors in any
sequence. In addition to the standard programs pre-loaded in the controller (see below), J-KEM offers custom
programming at no additional charge to automate virtually any fluid delivery task. Additionally, KEM-Commander
PC software allows the user to build sophisticated delivery programs with an intuitive drag-n-drop interface.
Ordering information
for the SYR-1200 and
accessories is on
page 13.
Standard Syringe Pump Programs
Standard programs are permanent and pre-loaded in the syringe pump controller
Program 1. Timed Addition Sequentially adds up to 16 reagents
to a single or multiple reactors at user specified rates. The syringe
automatically primes and refills with the active reagent as needed.
Example (pump fitted with a 5 mL syringe):
1) Add 12mL of reagent A at a rate of 3 mL/min
2) Add 2.5mL of reagent B at a rate of 0.025 mL/min
3) Delay 1 hour
4) Add 10mL of reagent C at a rate of 60 mL/min
Program 2. Program Loader Use KEM-Commander PC software
(included) to construct a custom syringe pump program in a drag-ndrop visual environment. Program Loader then uploads that program
to nonvolatile memory in the syringe pump controller. Once stored in
the controller, the program can be run at any time with no PC needed.
Construct programs for parallel reactions, filling titer plates, washing,
or any custom application.
Program controlled distribution valve
fills and dispenses from up to 8 ports
Glass and Teflon syringe
Delivery rates from
0.75 µL/min to 375mL/min
Up to 16 pumps can be combined
into a single system
KEM-Commander Software
Program 3. PC Control Places all functions of the syringe pump
under PC control. Useful for robotic applications or when part of a
larger automated reaction system.
KEM-Commander is
standard with every
pump and allows
the user to construct
sophisticated syringe
pump programs in
an intuitive drag-ndrop environment.
Programs can then
be run/saved/recalled
from the PC or
uploaded to the pump.
Program 4. Custom At no additional charge, the user can specify
a custom syringe pump program. This program is written by J-KEM
and stored as one of the permanent programs.
Program 5. Update Manager Allows new or updated programs,
available from J-KEM (via E-mail or web site), to be uploaded into
permanent memory.
Program 6. Concurrent Addition (SYR-2200 only) Adds two
reagents in parallel to a common reaction at two independent rates.
Program 7. Serial Dilution (SYR-2200 only) Repeatedly
dispenses two reagents in a user specified ratio.
For a comparison of the features of the SYR-1200 and the SYR-1400, see page 12.
Page 10
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
NEW
Model SYR-1400 Syringe Pump
The SYR-1400 is the most versatile syringe pump available.
The SYR-1400 is operated from a PC running J-KEM’s KEM-Pump
software. KEM-Pump implements all the programs of the SYR-1200
plus additional programs for serial and multi-reactor reagent additions.
Unlike any other syringe pump, KEM-Pump is an open source code
application that allows researchers with programming experience
to create their own applications without limitations (see blue insert
below).
Demo software at: www.jkem.com\syringepumps
Ordering information for the SYR-1400
and accessories is on page 13.
The SYR-1400 system includes both the syringe pump and KEM-Pump software. KEM-Pump is open source, graphical software that
includes both pre-written applications and the original source code, in VB.Net, to allow users to create their own custom applications.
KEM-Pump is a bold advance in laboratory automation that provides the user unprecedented control over how the syringe pump operates.
KEM-Pump handles the low level tasks, like serial communications, then exposes high level functions for virtually any syringe pump
action, greatly simplifying the effort needed to write new applications. For example,
the code block below fully implements dispensing any volume of reagent at
a user specified rate; syringe refills are handled automatically. The list of
functions and a complete programmer’s manual is available at jkem.com.
Public Sub StartTimedAddition(ByVal Exp as RunData, Byval PumpAddress as Int32)
‘Start a timed addition experiment. Data is contained in the RunData structure
Me.mnuStart.Enabled = False
Me.mnuAbort.Enabled = True
Pump.TimedAddition(Exp, PumpAddress, False) ‘Start the experiment and return immediately
Do
Pump.DrawPump(CurrentVolume) ‘Draw a graphical representation of the pump
Me.txbAddedVolume.Text = Format(CurrentVolume, “0.000”)
While Pump.IsRunning
Me.mnuStart.Enabled = True
Me.mnuAbort.Enabled = False
Pre-written applications include:
End Sub
Timed Addition Multi-Step Timed Addition Multi-Reactor Addition Program Builder -
Adds a single reagent (any volume) to a single reactor at a user specified rate
Adds up to 16 different reagents, independent volumes and rates to a single reactor
Adds a single reagent to 1-7 different reactors at independent rates and volumes
A drag-n-drop application, for non-programmers, to build sophisticated pump programs
Custom Syringe Pump Applications
Sixteen pump system provides continuous
delivery of 8 reagents in any volume and
at independent rates. Custom Windows
software, operator and administrator
levels of program control,
and data storage.
Four Position Temperature and pH Controller
J-KEM Scientific
Pump with 4 independent temperature
controllers. Maintains the temperature
and pH in 4 independent reactions.
Custom software with data logging,
program storage and recall.
Toll-free: (800) 827-4849
16-Position with half-sized pumps
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 11
Comparing the Features of the SYR-1200 and the
SYR-1400 Syringe Pump Systems
J-KEM’s two syringe pump systems, the SYR-1200 (page 10) and the SYR-1400 (page 11) share many of the same features, but differ in
several important ways that may make one system better suited for your application. The key differences between the SYR-1200 and the
SYR-1400 are 1) the SYR-1200 has its own syringe pump controller allowing it to be used as a stand-alone instrument while the
SYR-1400 requires a PC for operation, and 2) the SYR-1400 is substantially more versatile, taking advantage of the power of a PC.
The SYR-1200
Both the SYR-1200 and
the SYR-1400 use the same
pump module. This means
that both systems provide
identical performance in
regards to flow rate range
and accuracy. It also
means that both system
use the same syringes,
distribution valves and
other accessories.
Controller
Controller
The SYR-1400 is operated from your PC.
Programs are stored and recalled, and the
experiment’s progress is displayed on the PC.
The SYR-1200 is operated from its own
computer controller which means that a PC
is not required for operation. The controller
stores and recalls the various programs and has
a keypad for user input and a screen to display
the experiment’s progress.
Standard Programs
The SYR-1400 comes with KEM-Pump
graphical control software that runs the syringe
pump module. KEM-Pump implements all of
the standard programs of the SYR-1200 plus
several others.
Standard Programs
The syringe pump controller has the most
common and useful pump applications loaded
into permanent memory (see page 10).
Custom Programs
J-KEM offers to write one custom program and
load it into permanent memory at no additional
charge.
Creating New Programs
The SYR-1200 comes with a free PC
application called KEM-Commander. With
KEM-Commander, sophisticated scriptstyle programs can be built in a drag-n-drop
environment that can then be run from the PC.
KEM-Commander programs can be thousands
of commands long. Examples of program
script commands are shown below.
Port(1)
Fill()
Rate(12.0)
Dispense(100.0)
DelayMS(500)
Withdraw(2500.0)
Home()
Page 12
The SYR-1400
Go to valve port 1
Fill the syringe
Set rate to 12 mL/min
Dispense 100 µl
Delay 500 ms
Withdraw 2.5 mL
Empty the syringe
J-KEM Scientific
Syringe
• Sizes: 10 µL to 50 mL
• Glass & Teflon wetted
parts
• Dispense resolution is
1/48,000 of the syringe
size in use
• Easily interchangeable
Valve
• With 3 to 8 program
selectable ports
• All wetted Teflon parts
Optional I/O
• Use external inputs to
start/stop flow, change
flow rate, or port
position.
• Control external valves
or other devices under
program control.
Motor
• Stall detector
Toll-free: (800) 827-4849
Fax: (314) 863-6070
Custom Programs
J-KEM offers to write one custom program
and add it to your copy of KEM-Pump at no
additional charge.
Creating New Programs
With the SYR-1400, new programs are created
by adding your code to J-KEM’s open source
syringe pump application, KEM-Pump, written
in Microsoft’s VB.Net. For researchers with
programming experience, the versatility of the
syringe pump system is limited only by your
imagination. KEM-Pump contains high level
functions that provide intuitive access to every
syringe pump feature. Using these functions,
virtually any syringe pump program can be
created in a matter of hours. For researchers
without programming experience, one of the
screens in KEM-Pump builds new syringe
pump programs by dragging commands to a
script-style command list. KEM-Pump also
has an intuitive graphical interface that displays
the status of a running experiment in real-time.
www.jkem.com
[email protected]
Syringe Pump Ordering Information
Programmable Syringe Pump, SYR-1200, with Computer Controller
Description
Single position syringe pump with stand-alone computer controller (shown on p.10).
120 Vac version
System requires the selection of one syringe and valve (below) for operation.
230Vac, CE approved
Cat #
SYR-1200
SYR-1240
Price
$2640.00
2660.00
120 Vac version
230Vac, CE approved
SYR-2200
SYR-2240
4150.00
4170.00
Programmable Syringe Pump, SYR-1400, with KEM-Pump Software
120 Vac version
Single position syringe pump with KEM-Pump software for PC control (shown on p.11).
System requires the selection of one syringe and valve (below) for operation.
230Vac, CE approved
SYR-1400
SYR-1440
$2180.00
2190.00
120 Vac version
230Vac, CE approved
SYR-2400
SYR-2440
3695.00
3710.00
SYR-DTC
$520.00
Dual position syringe pump with stand-alone computer controller (shown on p. 10).
System requires the selection of two syringes and valves (below), one for each pump.
Dual position syringe pump with KEM-Pump software for PC control (shown on p.11).
System requires the selection of two syringes and valves (below), one for each pump.
Syringe Pump Options
Built-in digital temperature controller. Controls the temperature of an attached piece of equipment to 0.1o C.
Data logging, PC control, 120 V, 1200 watts
I/O Package. Includes 3 high current outputs (170 mA, 24 Vdc), 3 digital TTL inputs, 1 analog input (8 bits, 0-5 Vdc).
Control solenoid valves or read input sensors, all under program control. Includes internal power supply.
Programmable 120 V outlet. Turns equipment On/Off under program control. 3 amps @ 120 Vac (12 amp available)
Custom Syringe Pumps
Program controlled
distribution valve provides
32 selectable ports of
reagent or reactor access.
SYR-I/O
390.00
SYR-120V
155.00
Syringes (one needed for each syringe module)
Description
Cat #
Price
10 µL glass syringe with Teflon plunger
SPGS-10
$196.50
SPGS-25
112.50
SPGS-50
112.50
SPGS-100
102.50
SPGS-250
102.50
SPGS-500
102.50
1.0 mL glass syringe with Teflon plunger
SPGS-1000
102.50
SPGS-1250
102.50
SPGS-2500
102.50
5 mL glass syringe with Teflon plunger
SPGS-5000
102.50
SPGS-10000 102.50
SPGS-25000 157.50
SPGS-50000 196.50
Teflon Distribution Valves (one needed for each syringe module)
$132.50
3-Port distribution valve (syringe + 3 addressable ports) SPDV-3
150.00
180.00
196.50
Teflon Tubing & Fittings
System sequentially delivers 20 reagents and solvents,
or mixture of any combination of reagents. PC
software runs 1024 unattended experiments with data
logging and flushing of the reactor cell.
Heated syringe
Startup Kit.
Startup Kit.
Startup Kit.
Startup Kit.
20 feet 1/8” OD tubing, 12 nuts & ferrules
Dimensions: SYR1200 12”x3.5”x13” (HxWxD)
SYR2400 12”x7”x13” (HxWxD)
Pressure Limit: 80 psi
Microfluidic reaction system provides continuous delivery of 24 reagents and
solvents to a heated reactor. PC control automates 1000 reaction combinations
J-KEM Scientific
Toll-free: (800) 827-4849
Eight independent half-size
syringe pumps
Fax: (314) 863-6070
www.jkem.com
SP-SK1
SP-SK2
SP-SK3
SP-SK4
$120.00
380.00
92.00
290.00
Flow rates: 0.75 µL/min to 375 mL/min
Accuracy: 0.33% CV, full stroke
Precision: 0.007% full stroke
Custom pump drives 4-48 syringes in
parallel. See page 8.
[email protected]
Page 13
Reaction Controller
Automate the addition of
reagents based on:
• Time
• Temperature
• pH
• Pressure
The Reaction Controller has all the features and runs all of the programs of the
model SYR-1200 syringe pump (page 10). In addition, the Reaction Controller
has integrated thermocouple and pH inputs expanding its capabilities to add
reagents not just as a function of time, but also, temperature, and pH. Common
applications include maintaining a constant solution pH during the course of
a reaction, or adjusting the addition rate of a reagent as a function of reaction
temperature. J-KEM also offers custom programming at no additional charge
to meet the unique requirements of your application.
Custom....
Let J-KEM design a fully automated reaction system for your lab. We automate reaction setups involving
weighing, reagent delivery, temperature control, mixing, pressure control, and any other feature.
Combined with custom Windows software, J-KEM can make the perfect reaction system for your research needs.
Programmable Reaction Controller
Description
Reaction Controller with Thermocouple Input
Syringe pump with thermocouple input adds multiple reagents as a function of time and temperature. Logs all reaction
parameters to internal memory or PC. Requires the selection of one syringe and valve from page 13 for operation.
Reaction Controller with Thermocouple and pH Input
Syringe pump with thermocouple and pH inputs adds multiple reagents as a function of time, temperature and/or pH.
Logs all reaction parameters to internal memory or PC. Requires the selection of one syringe and valve from page 13.
Cat #
INF-RC-T
Price
$3460.00
INF-RC-TP
3520.00
SYR-DTC
$520.00
SYR-PSI
600.00
Options
Digital Temperature Controller Channel
Digital temperature controller built into the Reaction Controller regulates the temperature of the addition reaction.
Digital Pressure Monitor
Monitors the pressure of the addition process. Use to add reagents as a function of pressure or to stop addition if
pressure reaches a user set safe limit. Selectable pressure ranges. Contact J-KEM for pressure range options.
Examples of Custom Reactors
Catalyst Testing Station
Controls 4 independent reactions:
· Temperature (-20 to 100o C)
· Stir rate and torque
· Addition sequence and rate of
12 reagents
· PC control and data logging
Page 14
J-KEM Scientific
Titer Point Device
Automatically finds the
titer point of fatty acids.
· 0.01o C resolution
· Programmable heating
and cooling rates
· Range: -20 to 100o C
Toll-free: (800) 827-4849
Four place,
independently heated
and cooled reaction
system. PC control
with data logging.
Temperature range: -20
to 100o C
Fax: (314) 863-6070
www.jkem.com
Controller
prepares and
charges reactor
with substrate
and reagents to
sequentially run
1000 unattended
reactions
testing catalyst
longevity.
Catalyst activity
is determined by
the addition rate
of base needed
to maintain a
constant pH.
[email protected]
Something
unusual
from a scientific
instrument company
From the beginning, J-KEM has worked to be part of the research community, rather than
just a supplier to the research community. That’s why J-KEM offers substantial Academic
discounts on every item we sell, because we believe that supporting the next generation
of researcher is part of our corporate responsibility. J-KEM’s Continuous Flow Reactor
continues that commitment by supplying the high quality instruments that are needed for
research today. At the time this catalog was printed, our continuous flow reactor was still in
development, but even in development, its performance and features so significantly exceeded
those of any other flow reactor that we decided to provide a preview of what’s coming.
Continuous Flow Reactor
J-KEM’s continuous flow reactor can be configured to operate in either of two modes, reaction discovery mode or preparative synthesis
mode. In discovery mode, a homogeneous mixture of reaction materials are loaded into a sample injection loop which are then injected into
the flow reactor. The reactants flow through the reactor being pushed forward by a continuous stream of clean solvent. While the reactants
from the first injection are in the reactor, the reactants for a second injection are being measured out and mixed by a robotic workstation that
both prepares reactants for injection and acts as a fraction collector for the reaction products as they elute. Up to 128 reactions can be fully
automated without requiring operator intervention. In discovery mode, 50 - 100 mg of products
are typically produced in each experiment.
Fully automated operation runs up to 128 unattended reactions
• Prepares reactant mixtures and loads the sample loop
• Controls timing of reactant injections and product collection
• Program control of flow rate and reactor temperature
J-KEM’s continuous flow reactor can also be configured to run in preparative
mode to produce gram quantities of reactants. In prep mode, the reactants
are continuously pumped into the reactor in the desired ratios by adjusting the
flow rate of the two reactant pumps. This method was used to run the reaction
shown at the left, which resulted in the preparation of 1.94 g of the aryl amine
during a 3.5 hour run.
Reactor Features
• Multiple reactor options:
- Stainless steel, Inconel, PEEK, PTFE
- Tube OD’s of 1/16” and 1/8”
- Tube ID’s from 0.02” to 0.14”
- Reactor volumes from 1 mL to 20 mL
• Flow rates from 0.01 to 5.0 mL/min
• High pressure (4000 psi) pump
• Temperature range from RT to 300o C
• Back pressure regulators from 100 to
1000 psi
• Manual or fully automated operation
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 15
MedChem
Synthesis in
a Parallel
Format
Built-in
Magnetic
Stirring
Heat, Cool, Reflux
• Add reagents
• Sample reactions
in an inert atmosphere
The Personal Reaction
Station has every
feature needed for lead
development and high
throughput applications.
The reactor provides
precise temperature
control, powerful
magnetic stirring, and an
inert atmosphere for each
reaction tube. Reactions
Remove individual reactions
are run in 50 mL glass
without disturbing the
tubes that fit inside a
atmosphere in any other tube
heated and cooled reactor
base. Six built-in
magnetic stirrers provide uniform stirring even for viscous and heterogeneous reactions. A reflux condenser
plate surrounds the midsection of each reaction tube providing for a continuous reflux with no cross
contamination or solvent loss. Reactors connect to an inert gas manifold through separate
needle valves and quick disconnect fittings, allowing individual reactors to be removed
without disturbing the atmosphere in other reactor. All reactors have Teflon septum needle
ports for adding reagents and for sampling the reactor content.
Custom reactor
with inputs for
thermocouple and
reagent addition
tube for each
reactor.
For reaction volumes from 0.5 to 8
mL, J-KEM offers a limited volume
reactor and heat transfer ring.
Provides homogeneous heating and
reflux for small volume reactions.
Description
Personal Reaction Station Includes reactor with built-in magnetic stirrers, twelve 50 mL
120 Vac version:
glass reaction tubes, six Teflon reactor plugs, septum fittings and magnetic stirring bars.
Requires Model PRS-T digital temperature/stirring controller.
230 Vac version, CE:
Digital Temperature and Stir Rate Controller for Personal Reaction Station. Controller adjusts
120 Vac version:
both the stirring rate and reaction temperature. Digital controller provides precise temperature
o
regulation (±0.1 C), temperature ramping, and J-KEM enhanced RS232 serial communications
for remote controller and data logging applications.
230 Vac version, CE:
Reduced Volume Kit Tapered glass reaction tubes for solution volumes from 0.5 to 8 mL. Reduced volume tube fits
in a heat transfer ring for homogeneous heating. Includes six glass reaction tubes and six heat transfer rings.
50 mL Glass Reaction Tubes Glass reaction tubes with Teflon lined caps. (Package of 36)
10 mL Glass Reaction Tubes Reduced volume glass reaction tubes with Teflon lined caps. (Package of 6)
Evaporator Head for Personal Reaction Station Evaporator injects streams of nitrogen gas into each reaction tube.
External Temperature Probe Insert Teflon probe into one reactor to regulate solution temperature.
Replacement Teflon Septa Septa for syringe injection port. (Package of 48)
Replacement Septum Fittings Threaded fitting secures Teflon septum into reaction head. (Package of 12)
Replacement Reactor Plug Teflon plug fits inside reaction tube forming an air tight seal. Includes cap
Replacement Inert Gas Lines Inert gas delivery lines and quick connect fittings. (Package of 6)
Teflon Stirring Bars
Teflon coated ‘star’ stirring bar optimized for PRS tubes. (Package of 6)
Reactor Specifications:
Page 16
Temperature range: -80 to 130o C
Stirring speed:
60-1000 rpm
J-KEM Scientific
Toll-free: (800) 827-4849
Cat #
PRS-120R
Price
$2385.00
PRS-230R
PRS-T-120
2395.00
684.00
PRS-T-230
PRS-RDK
694.00
230.00
KPS50-GT
PRS10-GT
PRS-VAP
PRS-RTD
PRS-SEP
PRS-SF
PRS-TP
PRS-IL
PRS-MSB
147.50
187.50
680.00
122.00
32.00
28.50
45.00
15.00
58.50
Temperature variation: ±0.5o C
Condenser efficiency: 2% loss of CH2Cl2 after 7 days at reflux
Fax: (314) 863-6070
www.jkem.com
[email protected]
KEM-Prep Parallel Reactor
·
·
Glass reactors
Inert atmosphere
Heat, Cool, Reflux
Add reagents Sample reactions in an inert atmosphere
·
·
·
Built-in condenser refluxes 24 reactions
Inert gas swept interior
KEM-Prep reactor shown with model KLS-150/T temperature controller
KEM-Prep Jr.
Classical Synthesis in a Parallel Format
The KEM-Prep and KEM-Prep Jr. reactors are ideally suited for lead
development or high throughput applications. Reactions are run in either
25 or 50 mL glass reaction tubes which fit inside the heated and cooled
reactor base. A reflux condenser plate surrounds the midsection of each
tube enabling a continuous reflux with no cross contamination or solvent
loss. Reactors are maintained in an inert atmosphere while reagents are
added through a Teflon septa port. Mixing is achieved by mounting the
reactor on J-KEM’s bench top shaker. The KEM-Prep reactor holds 24
reaction tubes while the KEM-Prep Jr. holds 6 tubes.
KEM-Prep reactor shown with
optional solvent evaporator
KEM-Prep Reactors
Description
KEM-Prep Reactor for 25 mL reaction Tubes. Includes 24-position KEM-Prep reactor, 36 glass reaction tubes, and
Teflon septum sheet. Requires a KLS temp. controller (see below). 120 V.
Available for 230 V, CE approved
KEM-Prep Reactor for 50 mL reaction Tubes. Includes 24-position KEM-Prep reactor, 36 glass reaction tubes, and
Teflon septum sheet. Requires a KLS temp. controller (see below). 120 V.
Available for 230 V, CE approved
KEM-Prep Jr. Reactor for 25 mL reaction Tubes. Includes 6-position KEM-Prep Jr. reactor, 12 glass reaction tubes,
and Teflon septum sheet. Requires a KLS temp. controller (see below). 120 V. Available for 230 V, CE approved
KEM-Prep Jr. Reactor for 50 mL reaction Tubes. Includes 6-position KEM-Prep Jr. reactor, 12 glass reaction tubes,
and Teflon septum sheet. Requires a KLS temp. controller (see below). 120 V. Available for 230 V, CE approved
Cat #
Price
KPS25-120R $2990.00
KPS50-120R
2990.00
KPJ25-120R
2380.00
KPJ50-120R
2380.00
Digital Temperature Controller for KEM-Prep Reactor. Temperature ramping and 0.1o C regulation. RS232 optional KLS-150
Digital Temperature Controller with 100 Hour Timer for KEM-Prep Reactor. Temperature ramping and 0.1o C
KLS-150/T
regulation. 100 Hour timer turns heating On/Off at user set time. RS232 serial port for PC control is optional.
Accessories
Evaporation Head for KEM-Prep Reactor Evaporator fits on top of reactor base and directs a jet of nitrogen gas into
each of the 24 reactors through a stainless steel needle. Needle height above solvent front is adjustable.
Evaporation Head for KEM-Prep Jr. Reactor Evaporator fits on top of reactor base and directs a jet of nitrogen gas
into each of the 6 reactors through a stainless steel needle. Needle height above solvent front is adjustable.
Replacement Teflon Septum Sheet for KEM-Prep reactor.
Replacement Teflon Septum Sheet for KEM-Prep Jr. reactor.
25 mL Glass Reaction Tubes. Package of 36 tubes with Teflon lined caps.
50 mL Glass Reaction Tubes. Package of 36 tubes with Teflon lined caps.
Shakers and Mounting Plates
Digital Bench Top Shaker for mixing KEM-Prep reactor (see p. 19). Requires KPS-MP or KPJ-MP mounting plate.
Analog Bench Top Shaker for mixing KEM-Prep reactor (see p. 19). Requires KPS-MP or KPJ-MP mounting plate.
KEM-Prep Shaker Mounting Plate. Secures the reactor to the bench top shaker platform for mixing.
KEM-Prep Jr. Shaker Mounting Plate. Secures the reactor to the bench top shaker platform for mixing.
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
$520.00
678.00
KPS-VAP
$1480.00
KPJ-VAP
680.00
KPS-SEP
KPJ-SEP
KPS25-GT
KPS50-GT
59.25
37.25
147.50
147.50
BTS-3500
BTS-1500
KPS-MP
KPJ-MP
[email protected]
$1985.00
1495.00
120.00
120.00
Page 17
Reaction Blocks
Reaction Block Index
Single temperature zone blocks
Multi-temperature zone blocks
Custom reaction blocks
Reaction block accessories
Three Styles of Reaction Blocks to choose from:
p. 18
p. 22
p. 20
p. 19
Heated
Heated & Cooled
Reflux
Built-in internal heater
for rapid and
homogeneous heating
Built-in heater and
internally milled
coolant flow path
surrounding every vial.
Cooling is provided by
a circulating chiller.
Three layer block.
Heated bottom layer,
cooled top layer, and
insulating middle layer.
Cooled top (condenser)
maintains reflux in a
capped vial. Cooling
can be added to the
heated bottom layer
(optional) to provide
heating, cooling, and
reflux in the same
block.
Reaction Block
Evaporators
Reaction blocks are an efficient way to
provide uniform heating and cooling for
multiple reactions.
·
·
·
Evaporators fit on top of the reaction
block directing jets of nitrogen gas
into each individual vial. Heating and
gently shaking the block evaporates
solvents in a fraction of the time needed
by other methods.
Temperature homogeneity of ±1o C
Efficient mixing, even for heterogeneous mixtures
Heated Reaction Blocks
Description
Heated block for 2 mL vial size (12 x 32 mm vial).
Heated block for 4 mL vial size (15 x 45 mm vial), 1 dram.
Heated block for 8 mL vial size (17 x 60 mm vial), 2 dram.
Heated block for 20 mL vial size (28 x 61 mm vial).
Cat #
RB-2
RB-4
RB-8
RB-20
96 vial positions in an 8 x 12 array
63 vial positions in a 7 x 9 array
Heated and Cooled Reaction Blocks
Heated and Cooled block for 2 mL vial size (12 x 32 mm vial).
Heated and Cooled block for 4 mL vial size (15 x 45 mm vial), 1 dram.
Heated and Cooled block for 8 mL vial size (17 x 60 mm vial), 2 dram.
Heated and Cooled block for 20 mL vial size (28 x 61 mm vial).
Price
$845.00
845.00
845.00
845.00
RBC-2 $1194.00
RBC-4
1194.00
RBC-8
1194.00
RBC-20 1194.00
Reflux Reaction Blocks
Note: The vial used with a reflux block is twice the size of the block itself. For example, the 4 mL reflux block (RBR-4) uses an 8 mL vial to provide 4 mL sample volume and 4 mL head space for condensation.
Reflux block for 2 mL vial size (15 x 45 mm vial).
Reflux block for 4 mL vial size (17 x 60 mm vial), 1 dram.
Reflux block for 8 mL vial size (21 x 70 mm vial), 2 dram.
Reflux block for 20 mL vial size (28 x 95 mm vial).
Optional cooling channels added to heated bottom layer. To order, add the suffix “-BCP”. Example: “RBR-8-BCP”
RBR-2 $1960.00
RBR-4
1960.00
RBR-8
1960.00
RBR-20 1960.00
-BCP
475.00
Evaporators for Reaction Blocks
Evaporator for 96 position blocks. Fits RB-2, RB-4, RB-8, RBC-2, RBC-4, RBC-8, RBR-2, RBR-4
Evaporator for 63 position blocks. Fits RB-20, RBC-20, RBR-8, RBR-20
RBV-96
RBV-63
$965.00
965.00
Reaction blocks for custom vial sizes or configurations are available. Contact J-KEM for information.
Page 18
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
The Complete Reaction Block System Consists of:
+
2) Bench top shaker
1) Any style reaction block
Rotary Shakers
+
+
4) Temperature controller
3) Reaction block thermocouple
J-KEM offers both a digital and analog shaker specifically designed to handle the high temperatures and
weights of our reactions blocks.
10% discount on shakers when ordered with a reaction block
Rotary Bench Top Shakers
Description
Cat #
Price
BTS-3500 $2295.00
Digital bench top shaker for reaction blocks. Digital speed control.
Continuous operation or 100 hr. timer, unbalance sensor. 120 V
Analog bench top shaker for reaction blocks. Rotational speed set via BTS-1500 1635.00
front panel dial. Continuous operation or 1 hr. timer. 120 V
Analog bench top shaker. Same as BTS-1500, 230 V, CE approved BTS-1524 1635.00
Specifications:
5 year
warranty
Analog BTS-1500
40-400 rpm
0.75”
35 pounds
1 hr.
None
No
UL, cUL, CE
35 lb.
All J-KEM controllers precisely regulate reaction block temperatures. The 200-Series controllers
(page 32) are always a good choice providing 0.1o C regulation of any heater, including reaction blocks.
o
The Model 150 controller is an affordable alternative which also provides 0.1 C regulation of reaction
blocks. The Model 150 is available with or without a 100 hr. timer to turn heating On/Off at a user set
time. Optional RS232 serial communications for PC control and data logging (page 36).
Digital Temperature Controllers. Model 150
Description
Thermocouple Range (oC)
Model 150 temperature controller with ramp-to-setpoint
Type T
-200 to 250
digital meter. 120 V, 1200 watts.
Type J
0 to 800
Type K
-50 to 1200
Model 150/Timer temperature controller with 100 hr. timer Type T
-200 to 250
to turn heating On/Off at user set time. Ramp-to-setpoint
Type J
0 to 800
digital meter. 120 V, 1200 watts.
Type K
-50 to 1200
Recirculating
Chillers
Reaction Block Thermocouple
Reaction Block Thermocouples
Description
Cat #
Spring loaded bayonet
RBTC-T
thermocouple connects to
RBTC-J
mating port on the reaction
RBTC-K
block providing continuous
and reliable temperature
readings of shaking blocks.
J-KEM Scientific
BTS-1500
Rotational speed:
15-500 rpm
Orbital diameter:
0.75”
Load capacity:
35 pounds
Timer duration:
100 hr.
Unbalance sensor:
Automatic stop
RS232 serial interface: Yes
Certifications:
UL, cUL, CE
Dimensions: 17.4” x 13.5” x 6.4” Weight:
Digital BTS-3500
Temperature
Controllers
BTS-3500
Toll-free: (800) 827-4849
Price
64.00
64.00
64.00
Fax: (314) 863-6070
www.jkem.com
Cat #
Price
150-T
$512.00
150-J
512.00
150-K
512.00
150/Timer-T 660.00
150/Timer-J 660.00
150/Timer-K 660.00
Circulating chillers
attach to the cooling
ports on cooled
reaction blocks to
provide the cooling to
run chilled reactions.
Temperature as low
as -90o C.
See page 24 for a
complete selection.
[email protected]
Page 19
Custom Reaction Blocks
J-KEM makes custom reaction blocks for virtually any application.
Examples of custom blocks from J-KEM.
Features include:
Built-in stirring
Multiple temperature zones
High temperatures
Multiple vial sizes
·
·
·
·
Three temperature zone block (240o C) secured to a low profile shaker.
Used to test the effectiveness of surfactants for oil/water separations
250 mL Erlenmeyer flask block
KEM-Lab Reactor (see p. 23) with insert
blocks for 4 vial sizes
Two temperature zone block
for multiple vial sizes
Large block for 15 quart jars
See-through block for
crystallization studies in glass
titer plates. High temperature
in insulating frame
High temperature block (300o C)
inside insulated frame
Six temperature zone block for SPS synthesis columns
Two temperature
zone block for
heating & cooling
inside insulating
frame
Heated & cooled reaction block with
inserts to fit a selection of vial sizes
Page 20
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
High temperature block inside insulating
frame with inert gas cover
www.jkem.com
[email protected]
Custom Solutions for Demanding Chemistry
Even more to feed the imagination
High temperature see-through block for 4 mL
vials. Heated & cooled design.
Block on hotplate stirrer
for organic chem lab
Reflux block for multiple vial sizes
Four temperature zone Peltier regulated block for 125 mL bottles
Heater with built-in digital
controller for DNA hybridization
Two heated & cooled pockets built into Gilson rack
Half liter block with
digital over-head stirrer
and digital controller for
formulations testing
Saponification reactor with high pressure stainless
steel reaction tubes. Insulated reactor inside
explosion resistant housing
Heated
& cooled
block inside
insulating
frame
J-KEM Scientific
Oven for
four deep
well titer
plates.
Cover not
shown
Heated
block to
mate with
multiposition
stirrer
16-position microtiter plate heater
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 21
Multi-Temperature Zone Reaction Blocks
Multi-zone reaction blocks allow independent temperature control
of each block position. Each block can be a different style (heated,
cooled, reflux) and can fit different size vials. Multi-zone reaction
blocks are an indispensable tool for parallel synthesis, process
development, and formulations research.
6-Position reaction block with 6-position temperature controller
·
4-Zone block heats 4 titer plates each
2, 4, or 6 Independent temperature zones
Heat, cool, and reflux capability
Multiple vial sizes
·
4-position block with 3 vial sizes
·
6-zone block for 2 vial sizes.
Four heated/cooled positions
and 2 heated only positions
Ordering a Multi-Zone Reaction Block
There are literally hundreds of configurations for 2, 4, and 6-position
reaction block systems. For this reason, it’s necessary to request a quote
that assigns a unique product number to your unique block. To receive
a quote, call or e-mail a description that answers these questions:
E-mail: [email protected]
1) Do you want a block with 2-, 4-, or 6-temperature zones?
2) What size vial does each block (temperature zone) fit?
3) What style (heated, heated/cooled, reflux) is each block position?
4) Any custom features? Vial spacing, hole depth, special shapes?
Phone: (800) 827-4849 or (314) 863-5536
Fax: (314) 863-6070
Prices
The price of a multi-zone block depends on the block style selected for each
of the temperature zones (the vial size does not matter). The price of a
block can be calculated from this price list.
Multi-Temperature Zone Reaction Blocks
Description
Two zone reaction block
Base price for two heated zones:
For each cooled zone add:
For each reflux zone add:
Four zone reaction block
Base price for four heated zones:
Six zone reaction block
Base price for six heated zones:
Price
$1620.00
320.00
820.00
2425.00
230.00
650.00
2765.00
230.00
650.00
Multi-Position Temperature Controllers
Two zone digital temperature controller. Ramp-to-setpoint, USB
Four zone digital temperature controller. Ramp-to-setpoint, USB
Six zone digital temperature controller. Ramp-to-setpoint, USB
Number of Vial Positions in Each Zone of a
Multi-Zone
The number of vials that fit in each
Reaction Block temperature zone depends on the vial
size and the block style selected.
2-Zone
Reaction
Block
4-Zone
Reaction
Block
6-Zone
Reaction
Block
Vial Size:
Heated style
Cooled style
Reflux style
Heated style
Cooled style
Reflux style
Heated style
Cooled style
Reflux style
2 mL
96
96
48
72
72
24
45
25
19
4 mL
72
48
48
42
42
24
28
19
19
8 mL
48
48
24
42
24
12
28
19
8
$925.00
1820.00
2475.00
Multi-Temperature Pocket Blocks
Multi-temperature zone pocket blocks fit aluminum
inserts that fit various vial sizes and microtiter plates.
· Transfer inserts between a robotic deck and the
heated pocket block.
· Purchase insert blocks for any vial size.
Page 22
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
20 mL
32
24
24
12
12
12
9
6
6
KEM-Lab Parallel Reactors
Compact * Convenient * Precise Temperature Control
The perfect tool for synthesis, formulations, and incubations
KEM-Lab reactors are an ideal addition to
a research laboratory.
·
·
·
·
Compact design minimizes the bench
space needed
Temperature ramping for both
heating and cooling
Multiple styles: heating, cooling,
and reflux
KEM-Lab shaker provides vigorous
mixing for KEM-Lab reactors.
KEM-Lab Reactors for: Titer plates * Vials * Custom racks
Three styles of reactors to choose from:
Heated * Heated & Cooled * Reflux
Heated KEM-Lab Reactors
Reactor
fits
(vial dim.)
(# of vials)
Description
2 mL vial (12 x 32 mm)
(24)
(24)
(20)
16 mL vial (21 x 70 mm) (15)
20 mL vial (28 x 61 mm) (12)
Shallow well titer plate
(1 plate)
Deep well titer plate
(1 plate)
J-KEM’s glass titer plate (1 plate)
Heated & Cooled KEM-Labs
Reactor
fits
(# of vials )
Reflux KEM-Labs
Reactor
fits (# of vials)
Cat #
Price
Cat #
Price
Cat #
Price
KLS-2-H
$725.00 2 mL vial
(24)
KLS-2-C $980.00 2 mL vial (18) KLS-2-R $1320.00
KLS-4-H
725.00 4 mL vial
(24)
KLS-4-C
980.00 4 mL vial (16) KLS-4-R 1320.00
KLS-8-H
725.00 8 mL vial
(20)
KLS-8-C
980.00 8 mL vial (12) KLS-8-R 1320.00
KLS-16-H
725.00 16 mL vial (15)
KLS-16-C 980.00
KLS-20-H
725.00 20 mL vial (12)
KLS-20-C 980.00 20 mL vial (6) KLS-20-R 1320.00
KLS-SW-H 725.00 Shallow
(1 plate) KLS-SW-C 980.00
All reactors are for 120 V use.
KLS-DW-H 725.00 Deepwell (1 plate) KLS-DW-C 980.00
230 V reactors available on request.
KLS-GP-H 725.00 Glass
(1 plate) KLS-GP-C 980.00
KEM-Lab Reactor Shaker & Accessories
KEM-Lab bench top shaker Provides vigorous mixing for KEM-Lab reactors. Specifications: 100 to 2000 rpm.
KLS-HD $1845.00
Continuous and pulsed shaking modes. Weight limit: 4 pounds. 120 V. Dimensions: 16” x 7” x 8.75” (WxDxH)
Septum cover plate provides an air-tight seal and needle access port for each vial in the reactor to add reagents or
KLS-SC-# 210.00
sample reactions. Includes a Teflon faced septum sheet. To specify the cover, replace the ‘#’ in the catalog number with
the number of vial positions in the block. Example: KLS-SC-12 fits the KLS-20-H, KLS-20-C, and KLS-8-R reactors.
Replacement septum sheet Teflon faced sheet for septum cover.
KLS-SEP
32.80
Digital temperature controller for KEM-Lab reactors. Controller provides 0.1o C
KLS-150 $520.00
regulation of any KEM-Lab reactor. 120 V Optional RS232 communications.
Digital temperature controller with 100 hour timer. Same as KLS-150 but includes a
KLS-150/T 678.00
100 hour timer to turn heating Off (or On) at a user set time. Optional RS232 port.
Replacement power cable between reactor and KLS controller.
KLS-Cable
85.00
KEM-Lab Reactor Evaporators
Evaporation head Fits on top of the
reactor to direct a jet of nitrogen gas
into each vial. Apply mild heating
from the reactor to rapidly evaporate
even high boiling point solvents. To
specify the evaporator, replace the
‘#’ in the catalog number with the vial
positions in the block. Example:
KLS-VAP-20 fits KLS-8-H and
KLS-8-C reactors.
Cat # KLS-VAP-’#’
Price: $860.00
Glass Plates for KLS-GP Reactors
J-KEM’s glass plates are individual tubes
held rigidly in a polypropylene holder. Ideal
for compound storage or chemical syntheses
that require the chemical resistance of glass.
The KLS-GP reactor has milled positions
surrounding each tube providing outstanding
temperature homogeneity. Volume discounts.
Plate with 0.5 mL reactors
Plate with 1.0 mL reactors
Teflon cap mat. Solid plug in each tube for air tight seal
Teflon cap mat. Hollow plug for needle penetration
GP1
GP2
KLS-CM
KLS-CMX
$45.95
45.95
25.50
25.50
Circulating Chillers/Heaters
J-KEM’s circulating chiller/heaters are optimized for use with J-KEM’s
reaction blocks and parallel equipment. With both pressure and suction
pumps, these circulators generate higher pumping pressures to provide rapid
heating and cooling of attached equipment. All circulators have digital
temperature entry, PID control for 0.05o C regulation, and over-temperature
protection. Models with RS232 serial ports allow PC data logging and
control of temperature ramps.
Quality
in the Details
·
·
·
·
-40.0o C chiller with
J-KEM’s KEM-Prep
reactor
Programmable
Controller
Programmable - Stores 10 programs of 50 steps each
Remote temperature probe option
Graphic LCD readout
Dual display of set point and actual bath temperature
Serial communications (RS232)
Includes PC control software (data logging, temp. ramps)
Dual pressure and suction pumps
Temperature stability
Circulator
Model 9100
Model 9500
Model 9700
Series
Standard
Digital
Programmable
Standard
Digital
Programmable
Standard
Digital
Programmable
Temperature
Range (o C)
-20 to 150
-20 to 200
-20 to 200
-30 to 150
-30 to 200
-30 to 200
-40 to 150
-40 to 200
-40 to 200
Dual pressure & suction pumps provide high
coolant flow rates for rapid cooling
Inert gas purge fitting blankets the cooling fluid to
prevent condensation build-up
Easy temperature entry
Large digital display
Standard
Controller
Digital
Controller
Yes
Yes
Yes
Yes
Yes
Yes
Yes
0.01o C
No
No
Yes
Yes
Yes
Yes
Yes
0.01o C
Circulating Chillers
Cooling power at:
Pressure and
0o -10o -30o
Suction Pumps
140 100
-No
watts
Yes
Yes
480 360 100
No
watts
Yes
Yes
450 380 160
No
watts
Yes
Yes
Flow
Rate
15 lpm
30 lpm
30 lpm
15 lpm
30 lpm
30 lpm
15 lpm
30 lpm
30 lpm
Bath
Capacity
6 liters
No
No
No
No
No
No
No
0.05o C
Weight
60 lb.
13 liters
140 lb.
13 liters
150 lb.
Cat #
Price
9100-E $2379.00
9100-SC 3042.00
9100-P
3771.00
9500-E
2784.00
9500-SC 3319.00
9500-P
4048.00
9700-E
3369.00
9700-SC 3904.00
9700-P
4633.00
Circulating Chillers Accessories
Dynatherm $125.00
Heat Transfer Fluid. Dynatherm is a low viscosity fluid with a high heat capacity for rapid heat transfer.
Compatible with water condensation that contaminates other transfer fluids. Range: -50 to 218o C. 4 L bottle.
RC-CTH
570.00
Cryogenic Transfer Hose. Flexible cryogenic transfer hose connects chiller to external equipment. Length: 5 feet.
Temperature range: -90 to 300o C. Terminal fitting: 1/8” NPTM (same as reaction blocks).
Price for 1 pair.
294.00
Quick Connect Fittings. Stainless steel fittings for rapid connection of cryogenic hose to equipment. Includes a set of RC-QCC
4 fittings (1 each on the ends of the inlet and outlet hoses, and 1 each on the inlet and outlet of the equipment).
Chiller Specifications
Note
The heat transfer fluid used with the chiller
is as important as the chiller itself. A good
transfer fluid must remain non-viscous at
the lowest possible temperature for efficient cooling. J-KEM’s
Dynatherm retains its low viscosity even at -50o C.
Tech
Page 24
J-KEM Scientific
Toll-free: (800) 827-4849
Series
9100
9500
9700
Fax: (314) 863-6070
Dimensions
(LxWxH)
16.8” x 8.3” x 22.5”
17” x 15.5” x 24.8”
17” x 15.5” x 24.8”
www.jkem.com
Power
(@ 120 V)
1100 watts
1100 watts
1100 watts
Fluid
Connections
1/4 NPTF
1/4 NPTF
1/4 NPTF
[email protected]
Miniature Overhead Stirrer
Power - More power than stirrers 10 times its size and weight!
less than 1 pound!
Convenience -- Weighs
Hand-sized
·
·
Safety
The light weight of the motor makes it easy to assemble and align
the stirrer with the reaction flask
Side mount clamp on digital speed controller
- Sparkless - Sealed housing
- 14 Vdc motor
Compare the Value
Efficient stirring of a 5 L flask
Manufacturer
J-KEM
Cole-Parmer
Arrow
IKA
Glas-Col
Model
OHS-1
Servodyne (R-50003-20)
Agitator
Eurostar
HST30N
Max Torque
91 in-oz
70 in-oz
40 in-oz
85 in-oz
101 in-oz
Overhead Stirrer
Description
Complete System. Includes the motor, digital speed controller, and chuck for
10 mm stirring rod.
Motor only for OHS-1 stirrer. Includes 10 mm stirring rod chuck.
Digital speed controller only for miniature OHS-1 motor.
Replacement inserts to secure 10 mm stirring rods in motor chuck. (Package of 6)
Chuck for 6 mm stirring rods. Chuck replaces the standard 10 mm chuck.
Weight
0.95 pounds
11 pounds
10 pounds
9 pounds
20 pounds
Cat #
OHS-1
OHS-1M
OHS-DSC
OHS-P10
OHS-6C
Price
$955.00
640.00
320.00
12.50
43.40
Price
$955.00
1,980.00
836.00
1,775.00
2,052.00
Specifications
Input voltage: 100-120 Vac
Voltage to motor: 14 Vdc max
Maximum torque: 91 in-oz
Rotational speed: 10 - 380 rpm
Rotational control: 1 rpm
Custom Laboratory Controllers
We’re glad to work with our
customers to make one-of-a-kind
instruments for temperature and
pressure control. Shown are
examples of recent projects.
Six position temperature controller with
three independent
digital vacuum regulators
Sixteen position temperature controller
J-KEM Scientific
Four position temperature controller
designed to fit on the front face of a
research hood
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 25
Solid Phase Synthesis Reactor
No
Mechanical
Valves
Fully Automated SPS Reactor
Solvent is held in the reactor by computer controlled nitrogen back pressure.
Single key stroke commands provide the functionality to:
·
·
·
·
Set up a new reaction
Mix the reactants and resin
Filter & wash the resin
Cleave and collect final products
The SPS reactor works by pressurizing the reactor base with nitrogen gas until it exactly offsets the pull of gravity.
In this way, solvent can be added to a single reactor with none of it dropping through the frit. As reactors are
sequentially filled, the SPS computer regulator precisely controls the flow of nitrogen to maintain the reactor’s back
pressure to +-0.001 psi. Using nitrogen back pressure to hold solvent in the reaction tube eliminates the need for
mechanical valves or other mechanical devices which prevents automation of the SPS process. Reactions are
mixed by placing the reactor on a bench top shaker, or by increasing the pressure in the base to cause continuous
or intermittent bubbling up through the frit mixing the resin and reactants. Reaction setup, mixing, washing, and
filtration are accomplished by a single key stroke on the computer pressure regulator. Can be combined with
J-KEM’s Eclipse robot for fully automated, multi-step SPS reactions.
Automation Ready
SPS reactor with reactor
reflux heater and digital
temperature controller
Reactor Reflux Heater
surrounds each reactor
to provide heating to the
reaction solvent and cooling
to the top half of the reactor.
Sample concentrator
cover
Page 26
Gas coming up through
the bottom frit to
promote mixing
See J-KEM’s solid phase synthesis robot on page 3.
Solid Phase Synthesis Reactor.
Basic Components
Description
Reactor Base. Polypropylene base fits collection block and secures reactor top plate.
Reactor Support Plate with luer fittings to secure 48 SPS reactors.
Reactor Support Plate with lure fittings to secure 96 SPS reactors
Sample Collection Block positions sample collection tubes beneath reaction tube outlets.
Collection blocks are customized to fit your vial or tube. Contact J-KEM with specifications.
SPS Pressure Regulator. Computerized controller regulates the back pressure applied to
the reaction tubes. Automates reaction setup, resin washing, and sample collection.
Pressure Proportioning Valve for SPS pressure regulation. For 48 position reactor.
Pressure Proportioning Valve for SPS pressure regulation. For 96 position reactor.
Waste Valve filters reaction tubes and sweeps wash and reaction solvents to waste.
Inlet Gas Pressure Regulator. High flow rate nitrogen gas inlet pressure regulator.
SPS Reactors
Fritted SPS Reactor, 6 mL capacity, PP column with 20 µm PE frit. (Package of 100)
Optional SPS Components
Reactor Reflux Heater. Heats the bottom half of each reaction tube, and cools the top half
with a chilled condenser plate to create a sustained reflux inside the reaction tubes.
Reactor Port Plugs. Male luer plug seals unused reactor positions. (Package of 12)
Replacement O-ring for reactor base. Teflon impregnated AFLAF.
Short Reactor Base. Useful for robotic systems to minimize height of reactor.
Inert Gas Reactor Cover. Creates an inert atmosphere for all reactors, septum port access.
Cat #
Price
SPS-TB
$2450.00
SPS-SP48
748.00
SPS-SP96
940.00
SPS-CB
750.00
SPS-REG
2750.00
PSV-5
PSV-5TEK
SPS-WV
SPS-HCR
485.00
987.00
285.00
130.00
SPS-RX6
SPS-RX12
SPS-RX35
SPS-RX60
$122.50
145.00
161.25
193.50
SPS-RB
$1880.00
SPS-PP
59.90
SPS-ORING
56.00
SPS-SB
1720.00
SPS-EC
1680.00
SPS Concentrator Components
Concentrator for 48-position SPS system directs a jet of N2 gas into each collection tube.
SPS-CC48 $1350.00
Concentrator for 96-position SPS system directs a jet of N2 gas into each collection tube.
SPS-CC96 1390.00
Nitrogen Gas Heater warms the N2 to promote faster evaporation. Includes controller (p. 29) NGH-120
2220.00
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
KEM-Vap Solvent Evaporator
Evaporate solvents from:
·
·
·
·
Deepwell plates
Vial racks
Gilson racks
Custom Racks
Evaporates both volatile
and nonvolatile solvents
Fast
Acetone • DMSO • TFA
DMF • Water
Efficient
Solvent Evaporation
The KEM-Vap Solvent Evaporator uses heated
nitrogen gas and variable vacuum pressures to rapidly
evaporate volatile and nonvolatile solvents in the
same evaporator. The evaporator cover directs a jet of nitrogen gas
into each cell of a titer plate or vial in a vial rack for uniform and
consistent evaporations. For nonvolatile solvents, a combination of
vacuum and heated nitrogen removes solvents in a fraction of the
time needed when vacuum or heated gas is used alone. Made from
stainless steel and ultra high density polypropylene the evaporator
is not harmed by organic or aqueous solvents. Custom evaporators
made on request.
KEM-Vap SOLVENT EVAPORATOR
Description
Cat #
Price
SC1
$2285.00
Solvent concentrator base for 4 deep well
plates.
SC3
1115.00
Solvent concentrator base for 4 shallow well
plates.
SC4
2380.00
Solvent concentrator base for 1 Gilson rack.
1115.00
Solvent concentrator base for 1 deep well plate. SC5
SC-IN1
325.00
Insert blocks for SC1 to elevate shallow well
plates for evaporation. (Set of 4)
SC10
1640.00
Solvent evaporator cover for SC1 & SC3.
For 96-position titer plates.
SC11
1640.00
SC12
1640.00
SC13
1640.00
Solvent evaporator cover for SC4.
SC15
970.00
Solvent evaporator cover for SC5.
SC20
185.00
High capacity vacuum solvent trap. Dry ice
trap with 1000mL receiving flask.
NGH-120 2220.00
Nitrogen gas heater. Includes digital
temperature controller. See p. 29 for details.
J-KEM Scientific
Toll-free: (800) 827-4849
SC4 Gilson rack evaporator
SC5 Single plate evaporator
Nitrogen gas heater
Need Custom Solvent Evaporators?
Contact J-KEM
to design
a solvent
evaporator for
any rack or
application
Fax: (314) 863-6070
www.jkem.com
KEM-Lab
evaporators
on page 23
Reaction block
evaporators on p. 18
[email protected]
Page 27
Laboratory Safety Instruments
Lab Safety Controller
NEW
USB Communications &
GLP/GMP software
The Lab Safety Controller combines all the features of J-KEM’s Digital Temperature
Monitor and Water Flow Monitor, then adds a temperature limit controller into a
single versatile instrument. Plug any piece of equipment into the monitor,
then if the water flow rate falls below the user set level, or the reaction
temperature goes above or below the set limits, outlet power is turned off
until the controller is manually reset. The controller also disconnects power
following recovery from a power failure. USB communications and free
KEM-Net software provide GLP/GMP data and alarm logging.
Description
Lab Safety Controller. 120 V, 1800 watts.
Requires a flow sensor.
Protects against: • Coolant flow failure
• Over-temperature condition
• Under-temperature condition - Protects against
TC Type
T
J
K
Lab Safety Controller. 230 V, 2300 watts.
Flow sensor. Flow rate: 0.1 to 2.5 L/min
Flow sensor. Flow rate: 1 to 10 L/min
Water shut off valve. Turns off flow during an alarm
Digital Alarm Outlet. Open collector (170 ma) outlet
Specifications:
flask breaking or TC falling out of the flask.
Cat #
Price
LS-120T $595.00
LS-120J
595.00
LS-120K
595.00
LS-230K
615.00
WFM-01
220.00
WFM-02
230.00
WFM-03
230.00
250WV
158.50
WFM-OC
32.00
Dim. 3.25” x 5.25” x 7.25” (H x W x D).
USB 2.0
NEW
USB Communications &
GLP/GMP software
Monitors and displays the temperature of an attached piece of
equipment on a bright LED display. Built-in USB 2.0 serial
communications and free KEM-Net data logging software (page 37) provides remote
temperature monitoring and records time & temperature data to a GLP/GMP compliant
log file. Kem-Net provides email notification of an over or under-temperature condition.
Large digital display
0.1o C Resolution
Description
120 Vac input. USB communications
with KEM-Net data logging software
230 Vac input. USB communications
with KEM-Net data logging software
TC Type
T
J
K
T
J
K
Optional audible alarm
Range (o C)
-200 to 250
0 to 800
-50 to 1200
-200 to 250
0 to 800
-50 to 1200
Cat #
DM120-T
DM120-J
DM120-K
DM230-T
DM230-J
DM230-K
Price
$375.00
375.00
375.00
385.00
385.00
385.00
Specifications: 120 or 230 Vac input, 50 watts USB 2.0
Dim. 2.5” x 3.75” x 5.4” (H x W x D)
Water Flow Monitor
Precisely monitors the flow rate of water through a condenser, water bath, or other piece of
equipment. If the flow rate falls below the minimum rate set by the user (i.e. loss of
pressure, broken hose), power is turned off to the monitor’s output receptacle and any equipment plugged into it. Power remains off until
being manually reset. The optional water shut off valve stops water flow during an alarm condition preventing a flooded lab. With safety as
its primary goal, the J-KEM Water Flow Monitor measures the actual water flow rate,
rather than back pressure as in commonly measured by lower quality instruments.
• Digital sensor measures
actual coolant flow rate
Prevents heating accidents
due to water flow failures
Page 28
J-KEM Scientific
• Optional audible
and digital alarms
Description
Water flow monitor. 120 V, 1800 watts. Requires a flow sensor.
Water flow monitor. 230 V, 2300 watts. Requires a flow sensor.
Flow sensor. Flow rate: 0.1 to 2.5 L/min
Water shut off valve. Turns off water flow during an alarm.
Audible Alarm. Alarm (70 dB) sounds during under flow condition.
Digital Alarm Outlet. High current (170 ma) open collector output.
Toll-free: (800) 827-4849
Specifications:
Fax: (314) 863-6070
Cat #
Price
WFM-120 $345.00
WFM-230 365.00
WFM-01
220.00
WFM-02
230.00
WFM-03
230.00
250WV
158.50
WFM-AA
65.00
WFM-OC
32.00
Dimensions: 2.5” x 3.75” x 5.4” (H x W x D)
www.jkem.com
[email protected]
Laboratory Safety Instruments
Replace an existing electrical outlet
Solid state electronics makes this variac the perfect instrument for research, and is especially
useful in teaching labs. Safety features include sparkless solid state regulation of voltage for oil
baths, heating mantles, heat lamps, and many other devices. Offered in two configurations, the
Trinity-1 replaces an existing receptacle for installation directly in hoods or other outlets. The
Trinity-2 comes in its own case with an attached power cord. Both the Trinity-1 and Trinity-2
are offered with and without a built in analog voltage meter.
Trinity-1
Installs
in hood
Trinity-2
Nitrogen Gas Heater
J-KEM’s Nitrogen Gas Heater regulates the temperature of nonflammable gases providing
an intrinsically safe heat source for safety critical laboratory applications. An ideal
instrument for solvent evaporation or for any heating application where a traditional heater
is unsafe or inconvenient to use. Includes a digital temperature controller for
0.5o C regulation of outlet gas temperature. A minimum flow rate of 1 liter/minute must
be maintained when power is applied to the heater. To avoid burning out the heater
element, an optional flow switch can be built into the heater to turn power off when gas
flow falls below the minimum safe level.
•
•
•
•
Convenience of a built-in variac
Frees up bench space
Solid state design
Affordable price
Installs
Built-in
in Hood
Meter
Cat #
Price*
Yes**
Yes
Trinity-1M
$138.00
Yes**
No
Trinity-1P
118.00
No
Yes
Trinity-2M
148.00
No
No
Trinity-2P
128.00
Specifications: 120vac, 5 amps, 600 watts
* Academic and volume discounts
** Requires 1.625” junction box depth
Maximum Gas Temperature as a Function of Flow Rate
Maximum Temperature (oC)
Air Flow
(L/min)
50
75
150
225
375
Voltage: 120 V
230 V
700 watts 900 watts 2000 watts
820
820
820
590
660
820
330
400
820
230
280
570
150
175
350
Intrinsically safe heating, even for flammable substances
Nitrogen Gas Heater
Description
Heater with digital controller, 120 Vac. 700 watt heater core.
Accessories
Flow switch turns heating off if air flow falls below a minimum safe rate.
Cat #
NGH-120
NGH-130
NGH-230
Price
$2220.00
2250.00
2275.00
NGH-FS
610.00
Specifications: Temperature range: See chart above
Minimum flow range: 1 liter per minute
Fittings:
3/8” female NPT
Handheld Meter &
Data Logger
These versatile meters provide convenient temperature readings from a variety of
thermocouples. Features include two thermocouple inputs, large dual temperature displays,
data logging and automatic MIN/MAX temperature storage. Data can be transferred in
real-time or after a run is complete on the optional PC interface.
Feature
Thermocouples
Resolution
Data points stored
Optional printer
Scale oF and o C
Automatic MIN/Max
Built-in stand
J-KEM Scientific
Toll-free: (800) 827-4849
HHM-20
T, J, K, E
0.1o
25
No
Yes
Yes
Yes
HHM-40
T, J, K, E
o
0.1
1000
Yes
Yes
Yes
Yes
Fax: (314) 863-6070
Hand Held Temperature Meters
Description
Dual channel hand held meter
Dual channel meter with extended
memory to store 1000 data points
Hand Held Meter Options
RS232 interface for PC data logging
www.jkem.com
Cat #
HHM-20
Price
$185.00
HHM-40
260.00
HHM-232
125.00
[email protected]
Page 29
Digital Vacuum Regulator
Features: * No Mercury
· 100% digital pressure entry and control
· Wetted parts are 100% stainless steel and Teflon
· Vacuum ramping feature eliminates bumping
· USB port and free software for PC control
Resists:
· All organic solvents
· Acids
· Bases
· Water
The Digital Vacuum Regulator is an ideal instrument for laboratory
vacuum regulation. Connect the regulator to any vacuum pump or
vacuum source and then to any piece of equipment to regulate pressure
in most cases to ± 1 torr. A pressure ramp feature (standard) evacuates
equipment at a user defined rate to eliminate bumping due to solvent degassing or over-evacuation. The vacuum regulator is ideally suited
for large volume distillations, rotary evaporators and vacuum chambers. The DVR-200 is not recommended for small volume distillations or
applications which involve a continuous purge with gas. These are better
performed by J-KEM’s Precision Vacuum Regulator, the DVR-1000.
Two Styles of Regulator to Choose From
DVR-200
Recover > 99% of solvent
from rotary evaporators
Solvent
Ether
CH2Cl2
CH2Cl2
EtOAc
Toluene
DVR Pressure
(mm Hg)
475 torr
300 torr
100 torr
90 torr
50 torr
Solvent
Volume
340 mL
360 mL
255 mL
316 mL
273 mL
Time to
Dryness
14.6 min
21.9 min
5.9 min
17.0 min
15.7 min
Percent
Recovery
99.6%
99.8%
99.5%
99.9%
99.4%
A Note About Quality
The DVR-200 is designed for continuous vacuum sources, such as
oil-filled vacuum pumps, aspirators, or systems that are “always
on”, like in-house vacuum systems. The DVR-200 regulates
pressure by opening and closing a valve that separates the vacuum
source from the system being evacuated. In most cases, the
DVR-200 is the best choice.
DVR-280
The DVR-280 is designed for use with diaphragm vacuum
pumps. In some systems, pressure is regulated by turning on and
off the vacuum pump itself. The DVR-280 extends the life of
diaphragm pumps by not exposing the diaphragm to full vacuum
pressures when starting, which increases pump life by 100%.
J-KEM uses the highest quality components available. For example, most vacuum
controllers use a silicone filled vacuum transducer (because they cost less), but J-KEM
uses a stainless steel diaphragm transducer. Also, rather than a standard vacuum valve
with Viton seals, J-KEM uses a custom stainless steel valve with Teflon seals. These,
and other enhancements provide the chemical resistance needed in chemistry laboratories.
NEW!! USB +
Free KEM-Net software. (see p. 37)
Digital Vacuum Regulators and Monitors
Description
Vacuum Regulator, Model DVR-200. Includes built-in SS transducer. 120V
Vacuum Regulator, Model DVR-300. Same as DVR-200 but for 230V. CE Approved.
Vacuum Regulator, Model DVR-280. SS transducer and pump controller. 120V
Vacuum Regulator, Model DVR-380. Same as DVR-280 but for 230V. CE Approved.
Vacuum Regulator with large capacity valve for large volume equipment.
Digital Vacuum Monitor. Continuous display of system pressure, no regulation. 120V
Digital Vacuum Monitor. Same as DVM-100 but for 230V. CE Approved.
Cat #
DVR-200
DVR-300
DVR-280
DVR-380
Call
DVM-100
DVM-140
Price
$1175.00
1195.00
1280.00
1295.00
1560.00
920.00
940.00
Vacuum Regulator Accessories
Stainless Steel Needle Valve. Improves regulation in small pieces of equipment.
Analog pressure output. External 0-20 mV analog output. Useful for data logging.
Condenser body for dry ice condenser. 35/25 joint.
Condenser receiving flask. 1000 mL flask with 35/25 joint.
Condenser receiving flask. 2000 mL flask with 35/25 joint.
DVR-PNV
DVR-JH
JCE-1000
MTE-1000
MTE-2000
$108.50
95.00
268.00
65.00
72.00
Dry ice trap
JCE-1000
Specifications: 120 & 230 Vac @ 100 watts. Vacuum fittings: 1/8” NPTM. Dim. 3.4” x 5.4” x 7.4” (H x W x D)
* Academic discounts. Warranty: Electronics: 2 yr; transducer and vacuum valve: 6 mo., but void if due to chemical buildup.
Page 30
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Precision Vacuum & Pressure Regulators
Precise regulation of ±0.1 torr of
volumes as small as 1 mL
·
·
·
Perfect for vacuum distillations
Automatically compensates for leaks in the
equipment under test
Maintains constant precise pressure, even in
systems with a continuous gas purge
Standard Features:
·
·
0.1 Torr Regulation - No Mercury
J-KEM’s computer (built-in) controlled vacuum and pressure regulators maintain
pressure to 0.1 torr in test instruments with volumes as small as 1 mL. Built
from J-KEM’s Infinity Computer, this series of instruments can be customized to
automate virtually any laboratory or quality control task involving the regulation
of vacuum or pressure. The DVR-1000 regulates vacuums, the DPR-1100
regulates positive pressures, and the DDR-1200 regulates both vacuum and
positive pressures.
Precision Vacuum and Pressure Regulators
Description
Digital Vacuum Regulator. Precise regulation of vacuum pressures in the range of
0.1 to 760.0 torr (atm pressure). Requires the selection of one PSV valve (below)
Digital Pressure Regulator. Precise regulation of positive pressures in the range
of 0 psi (atm pressure) to 50 psi. The maximum pressure of the controller is user
selectable. Replace the ‘#’ in ‘DPR-1100-#’ with the selected maximum pressure.
Ranges: 1, 5, 15, 30, 50 psi. Requires the selection of one PSV valve (below). Gage
transducer is standard, but absolute is available on request.
Dual Range Vacuum & Pressure Regulator. Precisely controls both vacuum and
positive pressures. The DDR-1200 is built with a dual range pressure transducer
capable of accurately measuring pressures from full vacuum to the pressure limit of
the transducer selected. The maximum pressure of the controller is user selectable.
Replace the ‘#’ in ‘DDR-1200-#’ with the selected maximum pressure above ATM.
Ranges: 15 and 35 psi. Requires the selection of two PSV valves (below), one for
vacuum and one for pressure regulation. Contains an absolute pressure transducer.
Back-Fill Option. The DVR-1000 and DPR-1100 can be equipped to operate a
second valve used to back fill the evacuated or pressurized reactor. Requires the
selection of a second PSV valve (below).
16-Step programmable pressure ramp
Serial communication for PC control and
logging
Custom Features:
·
·
·
·
Custom programming to meet any research
requirement
Add a temperature control channel.
Add User programmable digital and analog
inputs and outputs
Use the built-in Infinity computer to automate
a complex test sequence or any process
involving pressure control
Cat #
Price
DVR-1000 $2980.00
DPR-1100-# 3145.00
Transducer
Diaphragm:
DDR-1200-# 3615.00
Microflow proportioning valves, call to discuss your application.
For reactor volumes: 1 mL to 2 L
Cv: 0.033 Orifice: 0.040”
For reactor volumes: 25 mL to 4 L Cv: 0.055 Orifice: 0.055”
For reactor volumes: 100mL to 22L Cv: 0.068 Orifice: 0.063”
For reactor volumes: 1 L to 50 L.
Cv: 0.12
Orifice: 0.093”
Large capacity valve.
Cv: 0.37
Orifice: 0.147”
Cv: 0.7
Orifice: 0.234”
Cv: 1.3
Orifice: 0.316”
Cv: 2.0
Orifice: 0.375”
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
Accuracy:
Stainless steel
DVR-1000: 0.1%
DPR-1100: 0.25%
DDR-1200: 0.25%
Proof Pressure: 200%
OPT-DV
220.00
Stainless Steel Proportioning Valves
The optimal PSV value depends on the exact conditions of the procedure. The volume guides below are helpful
for closed systems. For applications with a continuous purge of gas, call J-KEM for assistance.
Proportioning Valve.
Specifications:
PSV-Micro
PSV-2
PSV-3
PSV-4
PSV-5
PSV-5TEK
PSV-6
PSV-7
PSV-8
www.jkem.com
Call
$485.00
485.00
485.00
485.00
987.00
1097.00
1097.00
1097.00
Controller
Regulation: 0.015% of range
Resolution: 0.1 torr or 0.01 psi
Vapor Path Materials:
Stainless steel and Teflon
Ramp Rates:
100 torr/sec to 0.1 torr/hr.
Serial Communications: RS232
(RS485 or USB on request)
Power: 100 watts.
Fittings
1/4” SS Compression fittings
Warranty:
Electronics: 2 years.
Transducer and proportioning
valve is 6 mo. but void if failure
is due to chemical buildup.
[email protected]
Page 31
Model 210
The Model 210 is J-KEM’s most compact, research-grade controller, yet packed with 1200 watts of power.
Sufficient for heating mantles up to 5 L in size and most laboratory ovens, hot plates, reaction blocks and other
heaters. Contains J-KEM’s patented power control computer which provides 0.1o C regulation of anything.
NEW!!
— 0.1o C Regulation & Display —
· NIST traceable
· Advanced PID algorithm
230VAC, CE approved
Model 310 available
Controller Only
Cat #
Price*
210-T
$840.00
210-J
840.00
210-K
840.00
210-Pt
850.00
Complete System §
Cat #
Price*
210-T-S
$925.00
210-J-S
925.00
210-K-S
925.00
210-Pt-S
995.00
USB port and Free
KEM-Net data logging
& control software
Thermocouple Temperature
Type
Range (oC)
T
J
K
RTD
-200 to 250
0 to 800
-50 to 1200
-200 to 400
Specifications: 120vac, 10 amps, 1200 watts. Dim. 3.25” x 5.25” x 7.4” (H x W x D)
* Academic and volume discounts available.
2 Year warranty
§ Complete system includes: controller, Teflon TC, TC cord, and adapter (see p. 33)
Model 210/Timer
Same power and versatility as the Model 210, but also contains a 100 hour digital timer to turn
heating OFF (or ON) at a user specified time. A new safety feature automatically disconnects
power from the heater following recovery from a power failure. Contains J-KEM’s patented power control
NEW!!
computer which provides 0.1o C regulation of anything.
USB port and Free
NIST traceable
Advanced PID algorithm
& control software
·
·
Controller Only
Cat #
Price*
210/Timer-T
$935.00
210/Timer-J
935.00
210/Timer-K
935.00
210/Timer-Pt
945.00
Complete System §
Cat #
Price*
210/Timer-T-S $1020.00
210/Timer-J-S
1020.00
210/Timer-K-S
1020.00
210/Timer-Pt-S 1090.00
Type
Range (oC)
T
J
K
RTD
-200 to 250
0 to 800
-50 to 1200
-200 to 400
Specifications: 120vac, 10 amps, 1200 watts. Dim. 3.25” x 6.7” x 6” (H x W x D)
2 Year warranty
New in 2009
At the heart of J-KEM’s 200-Series
controllers is a new, high
speed microprocessor that
performs 3 functions:
1. Power Regulation
J-KEM’s original
power control computer is replaced by a next generation
microprocessor. The power control computer is J-KEM’s
patented technology that adjusts power to the heater 2048
times per second resulting in 0.1o C regulation.
2. USB Communications
PC communications and free
KEM-Net software enables remote PC control, GLP/GMP compliant data
collection, and multi-temperature ramps built in an Excel-like table.
3. Upgradable Programming
Software modules can be uploaded to the
processor, at no charge, adding new capabilities
to the controller. For example, automatic
detection of exothermic reactions. You
may not see the exotherm in this plot (and
it was a big one), but the microprocessor
does. You can’t see it because as it occurred,
the temperature controller stopped powering
the heater to compensate for the heat being
generated by the reaction.
Page 32
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Model 250
The Model 250 has both heating and cooling outlets for maximum versatility. Two heating outlets supply
1800 watts of power for large equipment and heating mantles up to 22 L. The third outlet (1800 watts),
normally used for cooling, is programmable to supply power below, above, or at the setpoint. Contains J-KEM’s
patented power control computer which provides 0.1o C regulation of anything.
NEW!!
· NIST traceable
o
— 0.1 C Regulation & Display —
Controller Only
Cat #
Price*
250-T
$935.00
250-J
935.00
250-K
935.00
250-Pt
945.00
USB port and Free
& control software
Complete System §
Cat #
Price*
250-T-S
$1025.00
250-J-S
1025.00
250-K-S
1025.00
250-Pt-S
1095.00
Model 250 Accessories
Thermocouple
Type
T
J
K
RTD
Temperature
Range (oC)
-200 to 250
0 to 800
-50 to 1200
-200 to 400
Coolant valve turns On/Off flow in cooling applications.
Cat# 250WV $142.50
2 Year warranty
Model 260/Timer
Designed for processes requiring an extra measure of safety. The Model 260/Timer
disconnects outlet power if the process temperature exceeds the setpoint by a user specified
amount, or following recovery from a power failure. Power remains off until the controller is manually reset. Over temperature is signalled
by both an indicator lamp and an audible alarm. Contains a 100 hour digital timer to turn heating OFF (or ON) when the time expires. The
Model 260 has two power outlets (1800 watts) for large equipment or heating mantles up to 22 L. Contains
J-KEM’s patented power control computer which provides 0.1o C regulation of anything.
230VAC, CE approved
Model 360 available
Controller Only
Cat #
Price*
260/Timer-T $1175.00
260/Timer-J
1175.00
260/Timer-K
1175.00
260/Timer-Pt
1185.00
·
·
NEW!!
NIST traceable
Advanced PID algorithm
Complete System §
Cat #
Price*
260/Timer-T-S $1265.00
260/Timer-J-S
1265.00
260/Timer-K-S
1265.00
260/Timer-Pt-S 1335.00
USB port and Free
& control software
Thermocouple
Type
T
J
K
RTD
Temperature
Range (oC)
-200 to 250
0 to 800
-50 to 1200
-200 to 400
2 Year warranty
The Complete System
1. Temperature
Controller
Types T & K
have the best
corrosion resistance
J-KEM Scientific
2. Thermocouple
Extension Cord
Toll-free: (800) 827-4849
3. Teflon Probe
Adapter
4. Teflon Coated
Thermocouple
(14/20 joint)
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 33
Multi-Channel Controllers
Gemini
Features two temperature controllers in a single cabinet to regulate two independent reactions. The Gemini is among
J-KEM’s most versatile controllers featuring high power outlets and a 100 hour digital timer (on channel 1) to turn
heating OFF (or ON) at a user entered time. Features include: over-temperature protection circuits with audible alarms, dual temperature
displays, selectable operating modes, double fused, and 100% solid state design. Contains J-KEM’s patented power control computer which
provides 0.1o C regulation of anything.
Gemini controls TWO independent reactions!
230VAC, CE approved
Gemini-CE available
Controller Only
Cat #
Price*
Gemini-T
$1365.00
Gemini-J
1365.00
Gemini-K
1365.00
Gemini-Pt
1375.00
NEW!!
· NIST traceable
Complete System §
Cat #
Price*
Gemini-T-S
$1540.00
Gemini-J-S
1540.00
Gemini-K-S
1540.00
Gemini-Pt-S
1680.00
USB port and Free
& control software
Thermocouple
Type
T
J
K
RTD
Temperature
Range (oC)
-200 to 250
0 to 800
-50 to 1200
-200 to 400
Specifications: 120vac, 15 amps, 1800 watts total, 1200 watts maximum per channel.
Dim. 3.5” x 7.75” x 9.25” (H x W x D)
2 Year warranty
§ Includes: controller, plus two each of: Teflon TC, TC cord, and adapter (see p. 33)
Apollo
Features two independent temperature controllers in a single cabinet to regulate two reactions at the same time. Each
temperature controller channel has a high power outlet and a 100 hour digital timer to turn heating OFF (or ON) at a
user set time. Features include: over-temperature protection circuits, dual temperature displays, selectable operating modes, double fused, and
100% solid state design. Contains J-KEM’s patented power control computer which provides 0.1o C
regulation of anything.
NEW!!
Controls TWO independent reactions!
USB port and Free
& control software
· NIST traceable
o
— 0.1 C Regulation & Display —
Controller Only
Cat #
Price*
Apollo-T
$1515.00
Apollo-J
1515.00
Apollo-K
1515.00
Apollo-Pt
1535.00
Complete System §
Cat #
Price*
Apollo-T-S
$1695.00
Apollo-J-S
1695.00
Apollo-K-S
1695.00
Apollo-Pt-S
1825.00
Type
Range (oC)
T
J
K
RTD
-200 to 250
0 to 800
-50 to 1200
-200 to 400
Dim. 4” x 8.2” x 9” (H x W x D)
2 Year warranty
§ Includes: controller, plus two each of: Teflon TC, TC cord, and adapter (see p. 33)
The Quad
Because we’ve never met a chemist with too much bench space, the Quad packs four independent temperature
controllers into a single compact unit. Each of the four controller channels has 1200 watts of power, an
independent display, and an over-temperature protection circuit. Contains J-KEM’s patented power control
NEW!!
Think of the Quad as a Model 210 on steroids
0.1o C Regulation
and Display
Controller Only
Cat #
Price*
Quad-T
$2355.00
Quad-J
2355.00
Quad-K
2355.00
Quad-Pt
2355.00
· NIST traceable
Complete System §
Cat #
Price*
Quad-T-S
$2695.00
Quad-J-S
2695.00
Quad-K-S
2695.00
Quad-Pt-S
2955.00
USB port and Free
& control software
Type
Range (oC)
T
J
K
RTD
-200 to 250
0 to 800
-50 to 1200
-200 to 400
Dim. 5.25” x 7” x 7.5” (H x W x D)
2 Year warranty
§ Includes: controller, plus four each of: Teflon TC, TC cord, and adapter (see p. 33)
Page 34
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
High Safety Controllers
Model 270
Designed for processes requiring uncompromised safety. The only temperature controller available with a
built-in, independent, backup controller to guard against heating accidents from equipment failure. The desired
temperature is entered into the main temperature controller which regulates heating, and then a high temperature cut-off is entered into the
backup limit controller. If the reaction reaches the high temperature limit or a thermocouple breaks, power is turned off to the heater until the
controller is manually reset. Both meters independently monitor the reaction temperature. In the event that one meter fails, the other takes
over to prevent a heating accident. J-KEM’s design provides independent, 100% redundant control.
NEW!!
Contains J-KEM’s patented power control computer which provides 0.1o C regulation of anything.
USB port and Free
& control software
· NIST traceable
* * 0.1o C Regulation & Display * *
Controller Only
Cat #
Price*
270-T
$1530.00
270-J
1530.00
270-K
1530.00
Type
Range (oC)
Complete System §
Cat #
Price*
270-T-S
$1680.00
270-J-S
1680.00
270-K-S
1680.00
T
J
K
-200 to 250
0 to 800
-50 to 1200
Specifications: 120vac, 15 amps, 1800 watts.
Requires a dual element
Dim. 3.4” x 7.75” x 9.25” (H x W x D)
thermocouple (see below)
* Academic and volume discounts available. 2 Year warranty
§ Includes: controller, dual element Teflon TC, TC cord, and adapter (see p. 33)
High Power Controllers
NEW!!
USB port and Free KEM-NEt data logging
& control software
Three Models of HCC to choose from
HCC 130 Voltage: 110-120 V
Model HCC
The line of HCC controllers are
designed to power large scale
equipment with volumes up to 100 L. Built with the same
uncompromising commitment to safety as our Model 270, the HCC is
available in 3 models for 120 and 230 volt operations. In addition to
the features of the Model 270, these high power controllers incorporate
a 100 hour timer to turn heating OFF (or ON) at a user set time. The
HCC is readily customized to meet unique research or additional safety
needs. Call for details. Contains J-KEM’s patented power control
Power:
Description
Model HCC-130 controller only.
Requires a dual element thermocouple and
thermocouple extension cord (see below).
30 amps; 3600 watts
Cat #
Price
HCC-130-T $1865.00
HCC-130-J 1865.00
HCC-130-K 1865.00
HCC 215 Voltage: 208-240 V Power:
15 amps; 3600 watts
HCC-215-T $1890.00
HCC-215-J 1890.00
HCC-215-K 1890.00
HCC 230 Voltage: 208-240 V Power:
30 amps; 7200 watts
HCC-230-T $1985.00
HCC-230-J 1985.00
HCC-230-K 1985.00
Dimensions:
5.5” x 12” x 12.5”
(H x W x D)
Temperature range
of all HCC
controllers
T
J
K
-200 to 250o C
0 to 800o C
-50 to 1200o C
Thermocouples for Model 270 and HCC Controllers
Dual element thermocouples contain two independent thermocouples in a single probe.
Model 270 and HCC controllers require either 1 dual-element or 2 single-element thermocouples.
Teflon Coated Dual Element Thermocouples
Probe
Thermocouple
Diameter (in.)
Length (in.)
1/8
12
Probes listed are
Teflon coated.
1/4
12
Stainless steel and
1/4
24
glass probes are
1/4
36
also available.
Probes of any length are available.
J-KEM Scientific
Cat #
TC270-(*)-18T12
TC270-(*)-14T12
TC270-(*)-14T24
TC270-(*)-14T36
Toll-free: (800) 827-4849
Dual Element Thermocouple Extension Cords
Price
$103.00
115.00
137.00
151.00
Length
10 ft.
25 ft.
Cat #
EXT-10-270-(*)
EXT-25-270-(*)
Price
$45.00
70.00
* Specify thermocouple type T, J, or K
* Specify thermocouple type T, J, or K
Fax: (314) 863-6070
www.jkem.com
[email protected]
Page 35
Oil Bath Controller
Variable
Voltage Output
Model 410
The Model 410 is designed for heaters that cannot be operated at 120 Vac, such as some styles of oil baths. The
maximum output voltage of the Model 410 is selected using the Power Output knob on the front of the controller.
Selectable output voltage limits provide precise power and temperature control while protecting low voltage
heaters. Contains J-KEM’s patented power control computer which provides 0.1o C regulation of anything.
NEW!!
Output Voltages of:
10, 20, 40, 60, 120 Vac
Controller Only
Cat #
Price*
410-T
$815.00
410-J
815.00
410-K
815.00
410-Pt
825.00
· NIST traceable
Complete System §
Cat #
Price*
410-T-PKG
$885.00
410-J-PKG
885.00
410-K-PKG
885.00
410-Pt-PKG
915.00
USB port and Free
& control software
Type
Range (oC)
T
J
K
RTD
-200 to 250
0 to 800
-50 to 1200
-200 to 400
2 Year warranty
§ Complete system includes: controller, stainless steel TC, and TC cord (see p. 33)
Economy Temperature Controllers
Model 150
An ideal controller for applications that don’t require the precise regulation of J-KEM’s 200-Series controllers.
This compact unit packs 1200 watts of power, sufficient for 5 L heating mantles, many ovens, and other devices.
Built with J-KEM’s state-of-the-art PID process controller, but does not contain J-KEM’s power control computer. See comparison below.
· NIST traceable
· Ramp-to-setpoint feature standard
Controller Only
Cat #
Price*
150-T
$512.00
150-J
512.00
150-K
512.00
Model 150 Options
Complete System §
Cat #
Price*
150-T-S
$598.00
150-J-S
598.00
150-K-S
598.00
Type
Range (oC)
T
J
K
Cat #
-200 to 250
0 to 800
-50 to 1200
Price
RS232 Serial Port for PC control and data logging.
add “-RS232” $110.00
High Power Output. 1800 watts @ 120 Vac
add “-HC”
85.00
2 Year warranty
Model 150/Timer
· NIST traceable
· Ramp-to-setpoint feature standard
Same power and versatility as the Model 150, but also contains a 100 hour digital timer to turn
heating OFF (or ON) at a user set time. See comparison to the 200-Series at bottom of page.
Controller Only
Cat #
Price*
150/Timer-T
$660.00
150/Timer-J
660.00
150/Timer-K
660.00
Model 150 Options
Complete System §
Cat #
Price*
150/Timer-T-S
$746.00
150/Timer-J-S
746.00
150/Timer-K-S
746.00
Type
Range (oC)
T
J
K
Cat #
-200 to 250
0 to 800
-50 to 1200
Price
RS232 Serial Port for PC control and data logging.
add “-RS232” $110.00
High Power Output. 1800 watts @ 120 Vac
add “-HC”
85.00
2 Year warranty
What’s the difference
between J-KEM’s 200-Series
controller and the 150-Series?
Feature
Temperature regulation
Smallest regulated volume
USB port & software
200-Series
0.1o C
0.01 mL
Free
150-Series
1o C
250 mL
Optional
J-KEM’s 200-Series controllers have our patented power control computer with technology that provides
0.1o C regulation of any instrument or volume as small as 100 µL. The 150-Series combines a state-of-the-art
PID process controller with solid state circuitry to provide unparalleled performance in its price range.
The 150-series is ideal for equipment such as reaction blocks, ovens, or heating mantles 500 mL or larger.
Page 36
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
[email protected]
Serial Communications, PC Control, Data Logging &
The J-KEM Advantage
PC Control with Free
KEM-Net Software
The J-KEM Advantage
Research grade temperature (200-Series) and vacuum regulators contain
two next-generation FLASH programmable microprocessors.
Processor 1
The Power Control Computer
The patented power control
computer is the heart of every
J-KEM temperature controller. The
computer adjusts power to the heater
2048 times per second resulting in
0.1o C regulation of any reaction and
virtually eliminates overshoot of the entered setpoint on initial warming.
Processor 2
USB Communications
The communications
processor, new in
2009, implements PC
control, data logging, and our new web based FLASH Modules. FLASH
Modules are programs that can be downloaded from J-KEM’s web site to
your controller at no charge. An example of a FLASH module is the Exo/
Endo module that automatically quantifies, then alerts the user when an
exothermic reaction is detected.
KEM-Net software is included with all USB enabled controllers.
Features:
·
·
·
·
·
Run 16-step temperature and vacuum ramps
Easy setup using an Excel-like table input
Enter setpoints and controller parameters remotely
Real-time graphical display and data logging to Excel
Encrypted data file is tamper-proof, meeting GLP and
GMP requirements
E-mail alerts of over- & under-temperature alarms
PC Control, serial communications, networking, and data logging explained.....
J-KEM supports three serial communications standards: USB, RS-232, and RS-485. Each has advantages and limitations.
J-KEM USB This is the standard port on 200-Series
temperature controllers and the Digital Vacuum Regulator.
The advantage of USB is that it’s present on all PCs and
supports connecting multiple controllers to a single PC. The
only limitation of USB is that cable lengths cannot be longer
than 15 feet without using a USB extender (offered below).
Controllers connect to the
PC’s USB ports or a USB hub.
RS-232 A hardware RS-232 port is available, but usually not needed.
J-KEM’s USB port includes a virtual RS-232 port driver that operates with software utilizing RS-232 communications.
RS-485 has the unique advantage that cable lengths between
the instrument and PC can be as long as 4000 feet. For lab
arrangements that require long cable runs, RS-485 is a valuable
alternative. Contact J-KEM for ordering assistance. J-KEM’s
KEM-Comm software is required for RS-485 communications.
USB to RS485
converter
Serial Communication Options and Accessories
Description
USB Extender, 50-Foot. Amplifier extends USB communications to 50 feet. Includes extender and 50’ cable.
USB 4-Port Hub. Used to connect multiple controllers to a single PC USB port
RS-232 Port. Physical RS-232 port substituted for the USB port. Add as a suffix to any controller, Ex: 210-T-RS232
RS-485 Port. Physical RS-485 port substituted for the USB port. Add as a suffix to any controller, Ex: 210-T-RS485
USB to RS-485 Converter. Converts a PC USB port to RS-485 with the proper connector style for J-KEM controllers
KEM-Comms Software. PC control and data logging software for RS-232 and RS-485 ports. Not needed for USB
J-KEM Scientific
Toll-free: (800) 827-4849
Fax: (314) 863-6070
www.jkem.com
Cat #
USBC-50
USBC-100
USBC-150
USBH
RS232
RS485
USB-485
KEM-Comm
[email protected]
Price
$94.00
118.00
142.00
32.00
120.00
150.00
140.00
159.00
Page 37
Thermocouples & Accessories
NEW!
Glass
over-coated
thermocouples
Note: To read temperatures accurately, the type of the
thermocouple must match the controller’s type. On a new
controller, the type is the letter immediately following the
model number:
Thermocouple
Type
Probe Outer
Diameter (in.)
T
J
K
Pt/100
1/16
1/8
1/4
210 - K - S
On an existing controller, the thermocouple type is indicated
by the color of the thermocouple receptacle on the front.
If the receptacle is:
BLUE - - - - YELLOW - BLACK - - WHITE - - -
you must order a type T thermocouple
you must order a type K thermocouple
you must order a type J thermocouple
you must order a type Pt/100 sensor
To determine the Catalog
($0)
($0)
($0)
($60.00)
Probes are color coded
Thermocouple
Overcoating1
($33.00)
($34.00)
($38.00)
Uncoated
Teflon2
Glass3
Number of a probe:
Examples:
($0)
($30.00)
($40.00)
1- All sensors are housed in 304 stainless steel sheaths.
2- PFA coating over SS probe.
3- Borosilicate glass. Available as 1/4” probe only.
6
12
18
24
36
($0)
($0)
($11)
($15)
($28)
Probes of any
length are
available
To determine the Price of a probe:
Total the dollar value associated with each
selection made from all four columns
1. Enter the thermocouple type (T, J, K, Pt/100)
2. Enter the outer diameter of the probe (1/16, 1/8, or 1,4)
3. Enter the probe over coating (U= Uncoated, T= Teflon, G= Glass)
4. Enter the length of the probe in inches.
---
Probe Length
(inches)
T-1/8-U-12 . . . . . . . . . . . Price: $0 + 34.00 + 0 + 0 = $34.00
K-1/4-G-18 . . . . . . . . . . . Price: $0 + 38.00 + 40.00 + 11.00 = $89.00
Thermocouple Calibration J-KEM offers thermocouple calibration in standard and extended temperature ranges.
Calibrated at three points in the stated range with NIST traceable standards and supplied with a certificate of calibration. Additional calibration
points available on request.
Description
# of Points Temp. Range
Cat #
Price
Thermocouple calibration, standard temperature range
Thermocouple calibration, extended temperature range
Thermocouple calibration, low temperature range
Additional calibration points in
stated range are $35.00 each.
Coiled Cord
3
3
3
STCC
ETCC
LTCC
$105.00
150.00
240.00
Thermocouple Extension Cords
Retractable coiled cord saves
space in crowded hoods.
26 gauge multi strand wire
with PVC insulation.
Coiled Thermocouple Cords
Catalog Number
CC-10-(type)-(connector)
CC-20-(type)-(connector)
Straight Thermocouple Cords
EXT-10-(type)-(connector)
EXT-20-(type)-(connector)
Teflon insulated wire
for superior chemical
resistance. 24 gauge
single stranded wire.
J-KEM Scientific
Select type: T, J, K, or Pt/100
The cord, controller, and thermocouple
must all be of the same type.
Specify: T for a blue plug
J for a black plug
K for a yellow plug
Pt/100 for a white plug
Ordering Examples: CC-10-T-SMP
EXT-20-K-OST
Toll-free: (800) 827-4849
Fax: (314) 863-6070
Price
$26.00
44.00
(see type and connectors below)
10 feet
20 feet
$17.00
30.00
Connector
Type
Straight Cord
(see type and connectors below)
Extended Length
10 feet
20 feet
Select a connector
style
Select a connector
type
Page 38
0o C to 150o C
0o C to 300o C
-195o C to 300o C
Select plug style: SMP or OST
Style SMP
Fits all controllers
www.jkem.com
Style OST
Fits 250, 260,270, HCC
[email protected]
Thin Wire Thermocouples
Flexible yet rugged thermocouples measure difficult to reach spots such as inside
heating mantles, ovens, or around curved surfaces. Also useful to measure volumes
as small as 100 µL. Thin wire thermocouples adhere to equipment to measure surface
temperatures of hot plates, HPLC columns, photolysis or other reactors.
Teflon Coated Thin Wire Thermocouple
Teflon Coated
Description
Cat #
Price
Thin wire thermocouple (30 gauge; 36” long) completely
Type
T
Tefl
on
embedded
TEF-30-T
$89.20
sealed in Teflon for submersion in solution. Excellent for
TEF-30-K
89.20
use with small volumes (<100 µL). Inserts through rubber Type K Teflon embedded
Exposed
Junction
Thin
Wire
Thermocouple
septum for airtight seal. Extremely flexible.
Type T exposed junction
Type K exposed junction
Type J exposed junction
Exposed Junction
Teflon wire (30 gauge; 72” long) exposed junction is
ideal for rapid temperature measurement of solids, air,
or heating mantles. Not suitable for continuous liquid
contact.
TWT-T
TWT-K
TWT-J
28.00
28.00
28.00
Longer lengths and other diameters are
available on request.
Needle Tip Thermocouples
Hypodermic needle thermocouples (17 gauge) are ideal to measure and control the temperature of small volumes and
inert reactions. Temperature measuring end of the thermocouple is at the tip, so only the first 2 mm of the probe must
have liquid contact for accurate temperature measurement. Forms an air tight seal when inserted through a septum.
Needles are sealed on the end
Thermocouple Needle
Teflon Coated Needles
Uncoated Needles
for liquid tight applications.
Type
Length
Catalog #
Price
Catalog #
Price
Available in 3.5” and 7” lengths.
T
3.5”
HN-3.5-T-TEF $93.00 HN-3.5-T
$73.00
These stainless steel needles are
7.0”
HN-7-T-TEF
98.00 HN-7-T
78.00
also available with Teflon coating.
K
3.5”
HN-3.5-K-TEF
93.00 HN-3.5-K
73.00
Each comes with 72 inches of
7.0”
HN-7-K-TEF
98.00 HN-7-K
78.00
attached Teflon extension wire.
NEW
Teflon coated
needle thermocouples!
J
3.5”
7.0”
HN-3.5-J-TEF
HN-7-J-TEF
93.00
98.00
HN-3.5-J
HN-7-J
73.00
78.00
Cat #
RBTC-T
RBTC-K
RBTC-J
Price
$64.00
64.00
64.00
Reaction Block Thermocouple
Thermocouple Type
Type T
Type K
Type J
Armored cable thermocouple has a spring loaded bayonet style
connector for rapid and secure connection to reaction blocks.
Flexible cable is designed for the constant shaking of reaction
blocks.
Thermocouple Adapters
Adapters enable plugging thermocouples with an SMP
(small flat pins) or OST (larger round pins) plug into
controllers with the opposite receptacle style.
Teflon Probe Adapters
Teflon probe
adapters form
air tight seals
between
thermocouple
probes and
standard taper
joints.
Not suitable for
high vacuums
J-KEM Scientific
Thermocouple Adapters
Probe
Joint
Diameter Size
Cat #
1/16”
1/16”
1/16”
1/16”
1/8”
1/8”
1/8”
1/8”
1/8”
1/4”
1/4”
1/4”
Toll-free: (800) 827-4849
10/18
14/20
24/40
29/42
10/18
14/20
19/22
24/40
29/42
14/20
24/40
29/42
1016
1416
2416
2916
1018
1418
1918
2418
2918
1414
2414
2914
Price
$32.75
34.75
39.75
43.85
30.75
24.95
49.95
24.95
43.85
22.45
24.95
43.85
Fax: (314) 863-6070
Thermocouple OST Male
SMP Male
Type
SMP Female OST Female Price
Type T
ADP-T
ADA-T
$9.75
Type K
ADP-K
ADA-K
9.75
Type J
ADP-J
ADA-J
9.75
Replacement O-Rings for Thermocouple Probes
Probe Viton (Pk of 12) Kalrez (Each) TEV* (Each)
Dia. Cat # Price Cat # Price Cat # Price
1/16”
1/8”
1/4”
1610R $9.00
1810R 9.00
1410R 9.00
1810RK $40.00
1410RK 52.00 1410RT $21.00
Replacement Adapter External O-Rings
Joint Viton (Pk of 12) Kalrez (Each)
TEV*
Size Cat # Price Cat # Price Cat #
14/20
24/40
29/42
1420E $9.00
2440E 9.00
2942E 9.00
1420EK $46.00
2440EK 56.00
2942EK 67.00
(Each)
Price
1420ET $21.00
2440ET 22.15
2942ET 23.20
* Viton O-ring encapsulated in Teflon over coating
www.jkem.com
[email protected]
Page 39
Research Heaters
Heating Mantles
Heating mantles are the
safest method of laboratory
heating because they avoid
the burn hazards associated
with other styles of heaters.
Heating mantles uniformly
heat glassware and remain
cool to the touch, even at
internal temperatures
> 300o C.
Heating Mantle
Size (mL)
5
10
25
50
100
250
500
1,000
2,000
3,000
5,000
12,000
22,000
50,000
72,000
Series-TM heating mantles
have a self-supporting
aluminum shell. The
TM mantle is stable on
bench tops, and with extra
insulation, the exterior
remains cool to touch.
Maximum internal
temperature of 450o C.
Not suitable for magnetic
stirrers.
Series-OS heating
mantles can be
placed directly on
top of magnetic
stirrers
providing
vigorous
mixing
using a stirring
bar.
120 Vac Mantles
Catalog #
Price
OS-5
$116.00
OS-10
116.00
OS-25
127.00
OS-50
122.00
OS-100
135.00
OS-250
149.00
OS-500
168.00
OS-1000
188.00
OS-2000
205.00
OS-3000
228.00
OS-5000
278.00
OS-12000
561.00
OS-22000
665.00
Not available
Not available
-
230 Vac Mantles
Catalog #
Price
Not available
Not available
Not available
Not available
Not available
OS-250/230
$161.00
OS-500/230
179.00
OS-1000/230
199.00
OS-2000/230
216.00
OS-3000/230
238.00
OS-5000/230
290.00
OS-12000/230 573.00
OS-22000/230 680.00
Not available
Not available
-
120 Vac Mantles
Catalog #
Price
Not available
Not available
Not available
TM-50
$185.00
TM-100
190.00
TM-250
181.00
TM-500
218.00
TM-1000
233.00
TM-2000
242.00
TM-3000
288.00
TM-5000
358.00
TM-12000
668.00
TM-22000
768.00
TM-50000
1216.00
Not available
-
230 Vac Mantles
Catalog #
Price
Not available
Not available
Not available
Not available
TM-100/230
$196.00
TM-250/230
201.00
TM-500/230
229.00
TM-1000/230
244.00
TM-2000/230
253.00
TM-3000/230
299.00
TM-5000/230
366.00
TM-12000/230 678.00
TM-22000/230 780.00
TM-50000/230 1227.00
TM-72000/230 1387.00
Wattage
12
20
30
60
80
180
270
380
500
500
600
2@650
2@770
3@1000
2@2000
Instatherm® Oil Baths
* Accommodates a variety of vessel sizes
and shapes
The intelligent design of the Instatherm oil bath, from Ace Glass, includes features
that make it the safest and most reliable oil bath for laboratory use. The metal alloy
* Suitable for magnetic stirrers
heating element is fused directly to the surface of the glass bath and then covered with
a tough silicone rubber layer and a glass insulation layer which serves as both
a thermal barrier and protects against physical shock. The bottom of the
Instatherm is not heated so the bath can
be placed on magnetic stirrers. The
Instatherm bath can be operated up to
250o C. Includes power cord.
Glass
Electrical connections
Fused-to-glass
Conductive heating film
Integral outer Insulation
For maximum versatility, J-KEM recommends the INS-150 and INS-190 oil baths. These
baths can be used with any 200-Series temperature controller, which can also be used with
any heating mantle (above). Thus, the same controller can be used with either heating
mantles or oil baths.
Bath Size
(Dia. x Hght.)
70 x 50 mm
100 x 50 mm
125 x 65 mm
150 x 75 mm
190 x 100 mm
-
Page 40
Max. Applied Voltage
Cap., mL (Volts/Amps)
Cat #
160 mL
20V/5A
INS-70
340 mL
40V/6A
INS-100
700 mL
40V/8A
INS-125
1200 mL
120V/5A
INS-150
2600 mL
120V/10A
INS-190
INS-PC
J-KEM Scientific
Price
$342.00
379.00
388.00
424.00
490.00
27.00
Toll-free: (800) 827-4849
Temperature Controller Compatibility
Low voltage bath compatible with Model 410 (p. 36) and Trinity controller (p. 29)
Can be used with any J-KEM Digital Controller.
Can be used with any J-KEM Digital Controller.
Replacement power cord for Instatherm oil bath
Fax: (314) 863-6070
www.jkem.com
[email protected]
The Road
We’re
On
(together)
1988
Incorporated as J-KEM Electronics.
Offering one product, the Model 260
temperature controller, we finish our
first year with sales of $784.00.
1989
Flush with cash from its first year
sales, J-KEM doubles its product line
and begins offering the Model 210.
Attended the Fall ACS meeting,
exhibiting all four of the controllers
we owned, then spent sleepless
nights worrying how we’d fill orders
if they came in.
J-KEM Scientific’s employees gathered around the fire pole of our first facility, the fire house.
1990
J-KEM’s first major customer was Dr. James
Zeller of Parke Davis. J-KEM expands its
manufacturing area 400% by moving from
just the corner to occupy the entire basement
(sorry girls about your play house).
1992
First international sale. Model 210 to Italy.
1993
Moved to our first commercial building.
Hired our first full time employee (Li, above).
Built the first power control computer
(8 bits, 4 MHz!!).
1994 - Incorporated as J-KEM Scientific
1995 - Purchased our first building,
J-KEM appreciates the relationship we’ve had with all of our
customers. It’s more than just the obvious fact that without you, J-KEM
would not be in business. We appreciate the friendships and the
ideas we’ve received from world class scientists, that without, many
of our best products wouldn’t exist. Don Korte gave us the idea for
the miniature overhead stirrer, Martyn Fordham, the Personal Reaction
Station, Dr. Bruce Hamper the Solid Phase Synthesis Regulator, and the
unknown chemist from Abbott who came to our booth at the ACS show
to say “I don’t need a temperature controller, I need a vacuum regulator
that works”. This resulted in our Digital Vacuum Regulator.
20 Years of Innovation
a 1930’s fire house.
1998 - First years sales >$1,000,000.
1999 - First robot sold to Dr. Glass
40 MHz microprocessor enables
* Exo & Endotherm analysis
* USB communications
* Enhanced safety
of Zenica.
2000+ - Emphasis in lab automation,
parallel reactors, and robotics.
Pictured are the original
(left) and new (right) Model
210-Timer circuit boards
2008 - Staying abreast with advances in
technology:
• Third generation power control
computer
• Second generation Syringe Pumps
• Two new robotic designs
• Custom lab automation
instruments and software
The first temperature controller
made by J-KEM, sold to Dr.
Kurt Moedritzer of Monsanto
(Dr. Moedritzer also purchased
controller #2. Our first loyal
customer!!)
In 2008, J-KEM completed the redesign and
implementation of the 3rd generation of its
power control computer. The new design
uses a FLASH programmable microprocessor
that can be updated with new controller
features from J-KEM’s web site.
KEM Scientific
®
Instruments for Science from Scientists
J-KEM Scientific, Inc.
6970 Olive Blvd.
St. Louis, MO 63130
USA
Phone (314) 863-5536
(800) 827-4849
Fax
(314) 863-6070
Email [email protected]
Web
www.jkem.com

NEW - J-KEM Scientific

Transcription

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