JTBaker® CYCLE-TAINER™ Solvent Delivery System

Transcription

J.T.Baker ®
CYCLE-TAINER™
Solvent Delivery System
User’s Manual
Contents
Section 1 Warnings and Cautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Section 2 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
2.1 CYCLE-TAINER™ Solvent Delivery System Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
2.2 Definitions and Terminology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
2.3 CYCLE-TAINER Solvent Delivery System Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.4 Signal Statements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Section 3 Components and Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
3.1 Parts of the Container . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
3.1.1 Container Body . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
3.1.2 Chime of the Container . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
3.1.3 Dispense Head . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
3.1.4 Forklift Channels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
3.2 Container Body Specifications by Size . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
3.3 Dispense Head Assembly/Specifications by Size . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.4 Container Body and Dispense Head Diagrams . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Section 4 Pre-Installation Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
4.1 CYCLE-TAINER System Performance and Regulatory Compliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
4.2 Performance and Regulatory Chart by Size . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
4.3 Initial Preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.3.1 Gas Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.3.2 Venting the Container . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.3.3 Grounding the Container . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.3.4 Tubing Requirements — Permanently Installed System (Type A) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.3.5 Tubing Requirements — Container Directly Fed to Process or Instrumentation (Type B) . . . . . . . . . . . . . . . . . . . . . . . . . . 18
4.3.6 Tubing Requirements — Direct feed from a CYCLE-TAINER System to a J.T.Baker® CYCLE-TAP Dispenser. (Type C) . . 18
4.3.7 Pre-Installation Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
4.4 Recommendations for Initial Facility Design and Start-Up . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
CYCLE-TAINER™ Solvent Delivery System User’s Manual
1
Section 5 Preparation for Use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
5.1 Incoming Container Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
5.2 Inspection Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
5.3 Sampling the CYCLE-TAINER System for Quality Control Purposes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
5.4 Handling and Storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Section 6 Installation and Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
6.1 Basic Installations for 4 L, 18 L, 52 L, and 215 L CYCLE TAINER Systems and
1250 L CYCLE-TOTE Systems Manufactured after October 1998 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
6.2 Basic Installations for 1250 L CYCLE-TOTE System Manufactured prior to October 1998 . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
6.3 General Parts List to Hookup the CYCLE-TAINER System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
6.4 Hooking Up Tubing to the Female Quick-Connects — General Guidelines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
6.5 Preparing the CYCLE-TAINER System for Hookup (All Types of Installations) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
6.6 Hooking Up the J.T.Baker® CYCLE-TAP Dispenser to the CYCLE-TAINER System (Type C Installation) . . . . . . . . . . . . . . . . 24
6.7 Hooking Up the J.T.Baker® CYCLE-TAP Sampler to the CYCLE-TAINER System (Type C Installation) . . . . . . . . . . . . . . . . . . 24
6.8 Hooking Up the CYCLE-TAINER System to Your Process, Instrumentation
or as a Permanently Installed System (Type A and B Installations) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
6.9 Daisy Chaining Multiple CYCLE-TAINER Systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Section 7 CYCLE-TAINER System Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
7.1 With the CYCLE-TAP Dispenser (Type C Installation) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
7.2 With the CYCLE-TAP Sampler (Type C Installation) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
7.3 With Your Process, Instrumentation, or as a Permanently Installed System (Type A and B Installation) . . . . . . . . . . . . . . 28
Section 8 Temporary System Shutdown (Overnight or Short-term Shutdown) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
8.1 When Hooked to the CYCLE-TAP Dispenser (Type C Installation) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
8.2 When Hooked to Your Process, Instrumentation or as a Permanently Installed System (Type A and B Installation) . . 29
Section 9 Empty Container Shutdown and Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
9.1 Container Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
Section 10 Return Shipment of CYCLE-TAINER System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
10.1 Return Shipment Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
10.2 Regulatory Requirements for Returning Containers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
10.3 The SHaRE Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
10.4 Return Shipment of a Trial CYCLE-TAINER System or System Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
10.5 Product Shipping Information, Physical Data and Container Weights Shipping Information1 . . . . . . . . . . . . . . . . . . . . . . 31
2
Section 11 Maintenance and Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
11.1 Customer Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
11.2 Container Malfunctions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
11.3 CYCLE-TAINER System Troubleshooting Guide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
Section 12 Appendix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
12.1 System Accessories — Items and Source Listings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
12.2 Container and Pallet Handling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
12.2.1 Table: Approximate weight requirement for lifting device (based on filled containers of methylene chloride) . . . . . 38
12.2.2 Table: Recommended equipment to accomplish task . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
12.3 Maintaining ULTRA RESI-ANALYZED™ Quality in Piping Systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
12.4 CYCLE-TAINER System Weight Conversion Tables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
12.5 Engineering Drawings for Basic Installations (Type A and B) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
12.6 How to Contact Us . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
3
Warnings and Cautions
Throughout this manual, there are Caution, Warning and
Note signal statements. Please read carefully and observe
the information and/or directives in these statements. See
below for an explanation of these statements.
• CAUTION – Statements will indicate potentially hazardous operating procedures.
• WARNING – Statements will highlight regulatory requirements.
• NOTE – Statements will indicate procedures that might cause product contamination.
CAUTION: Do not pressurize the container with
compressed air or oxygen. Failure to observe this caution
could result in an explosive situation, which can cause severe
injuries to personnel.
CAUTION: Check the weight restrictions for your forklift or
hand-operated fork truck before moving the CYCLE-TAINER
system. Most lifting equipment is designed to lift up to a
designated weight.
WARNING: Local regulatory agencies, building codes, and
safety policies may require that you attach the container
to vent lines during operation. The vent lines attach to the
Pressure Relief Valve (PRV) and the Pressure Rupture Disk
(PRDA) (if applicable)
CAUTION: EXPLOSION HAZARD- You must ground the
CYCLE-TAINER system during operation.
CAUTION: Ensure that CYCLE-TAINER systems are secure
during handling to prevent accidental loss of control of
the container. This may result in injury to personnel and/or
damage to the container
CAUTION: Never mount or store a container horizontally.
Do not stack containers on top of each other
CAUTION: DO NOT DROP CONTAINER. This may damage
the container or burst the rupture disk rendering the
container inoperable
CAUTION: All metal supply and distribution lines should
be electrically earth grounded. Storage areas must provide
electrical earth ground connections for all containers while
in use.
4
CAUTION: Ensure your gas supply is routed through a
high quality stainless steel pressure regulator. The regulator
output pressure must not exceed 40 psig for ASME-certified
containers; 15 psig for non-ASME certified containers; 5 psig
for 1250 L containers manufactured prior to October 1998; 19
psig for 1250 L containers manufactured after October 1998.
These pressures represent maximum working pressures of
the CYCLE-TAINER systems as set forth in this manual.
CAUTION: To avoid possible ignition or explosion to toxic/
flammable vapors, we recommend the pressure relief output
be directed to a hood or other proper venting location. If an
external vent line is used, ensure it does not restrict gas flow
from the pressure relief device or create a vacuum against
the pressure relief device.
CAUTION: Initially turn on the toggle valve slowly to release
gas trapped inside the hose. When you release the lever,
solvent flow will stop.
CAUTION: Do not exceed operating pressure of the CYCLETAINER system. Refer to Section 3.2 for operating pressures
of various container sizes and types.
WARNING: WHEN USING THE CYCLE-TAP SAMPLER,
NEVER DEPRESS THE PLUNGER WHEN THE SYRINGE IS
ATTACHED TO THE SAMPLER. THIS MAY INTRODUCE
CONTMINANTS INTO THE CYCLE-TAINER SYSTEM.
CAUTION: Do not exceed operating pressure of the
CYCLE-TAINER system.
CAUTION: When direct feeding to instrumentation,
DO NOT OVERPRESSURIZE the input line to the instrument
- damage to the instrument may occur. Consult the
instrument manufacturer operation manual or a technical
service representative for the proper feed pressure.
WARNING: If you know or suspect that foreign substances
were introduced into the container, quarantine the container
and call Customer Service at 1-855-AVANTOR for assistance.
Do not return the container without first contacting Avantor
to avoid violations of Federal and/or State laws.
WARNING: Never tamper with the container components.
Promptly report any container malfunctions to Customer
Service at 1-855-AVANTOR
Section 2 Introduction
2.1 CYCLE-TAINER™ Solvent Delivery System Purpose
The CYCLE-TAINER™ solvent delivery system is designed to
conveniently store and dispense large volumes of J.T.Baker®
brand solvents with no degradation of quality. Solvents are
dispensed from the container to the point of use without
exposure to the atmosphere. This feature is particularly
important for moisture- or oxygen-sensitive materials. The
CYCLE-TAINER solvent delivery system allows solvents to
be delivered from local or remote solvent storage locations
directly to instrumentation or process areas.
This manual will familiarize you with the CYCLE-TAINER
solvent delivery system components and provide guidelines
on how to install the system to meet your needs. In this
manual, you will find engineering illustrations of typical
plumbing systems for distributing solvents from CYCLETAINER systems to points of end use. The facility hookup
designs are generalized and are based on experience
with various customer set-ups. We have found that some
customers’ designs may vary considerably, depending
on their individual application and facility requirements.
The facility designs illustrated herein are guidelines only.
The customer must make the ultimate decision as to the
appropriate system and design to use in their particular
application.
2.2
Definitions and Terminology
American Society of Mechanical Engineers (ASME)
— An organization that certifies pressure vessels. ASMEcertified containers may be operated at pressures above
15 psi. Refer to Section 3.2 for operating pressures for 52 L,
215 L, and 225 L CYCLE-TAINER systems. Higher operating
pressures provide higher flow rates and the ability to plumb
from a remote location or separate storage area.
Basic Startup Kit — A hook up kit that is provided to new
customers. The kit is equipped with components necessary
to hookup your tubing to the CYCLE-TAINER system. The kit
consists of two Quick-Connect bodies (one for solvent and
one for gas), two female tube connectors (one for solvent
and one for gas), and a liquid level indicator (on 52 L, 215 L,
A typical CYCLE-TAINER system connection to an HPLC instrument.
and 225 L sizes only). You will need to specify either a 1/8”,
1/4”, or 1/2” female tube connector for your solvent line.
(One kit is provided at no charge per customer fleet.)
Chime — The uppermost section of the container body. It
protects the dispense head from damage.
Container Body — The side of the container.
CYCLE-TAP™ Dispenser — An accessory device that
connects to the dispense head of the CYCLE-TAINER
system. It allows you to dispense out of the container
without hooking the container to an instrument or specially
engineered process. It is available for sale as an accessory
to the CYCLE-TAINER system. See Section 12.1 for ordering
information.
CYCLE-TOTE™ System — A 1250 L solvent delivery system.
It is part of the CYCLETAINER system family. CYCLE-TOTE
containers manufactured prior to October 1998 are not
designed to be pressure vessels and require the use of a
pump for dispensing solvent. Containers manufactured after
October 1998 can be pressure dispensed.
Dispense Head — The top section of the container, within
the chime, that includes the valves, pressure gauge, fittings,
and connectors of the CYCLE-TAINER system.
5
EPA-HW — Abbreviation for the Environmental Protection
Agency Hazardous Waste Number listed in Section 10.5.
Factory Mutual (FM) — Independent organization that
tests and reviews equipment according to their set of
guidelines. FM is recognized by many insurance agencies.
FM approval may be required for equipment such as the
CYCLE-TAINER system by your insurance carrier. Please
note, however, that all CYCLE-TAINER systems
manufactured after July 1, 2014 will not be approved
by FM.
Female Tube Connector — On the CYCLE-TAINER system,
this fitting connects your tubing to the 1/4” male NPT thread
on the Quick-Connect body.
Ferrule — Piece inside a fitting, such as the female tube
connector. It slides onto the tubing, crimps down on it, and
holds the tubing against the connector/fitting body.
Five 9’s Gas — A high purity gas that is 99.999% pure. Do
not pressurize the container with compressed air or oxygen.
Failure to observe this caution could result in an
explosive situation, which can cause severe injuries
to personnel.
Gross Weight — The total weight of the CYCLE-TAINER
system and the solvent.
Keyed Quick-Connect — A Quick-Connect that is “keyed”
and has a color-band on the body. The Quick-Connect will
only couple when the male and female
components have the same color
band on their bodies. A keyed QuickDo not
Connect is used for the Solvent Port on CAUTION:
pressurize the container
the CYCLE-TAINER system and prevents with compressed air
or oxygen. Failure to
cross-contamination of solvents. See
observe this caution
Section 12.1 for ordering information.
could result in an
explosive situation,
Liquid Level Indicator — An
which can cause severe
injuries to personnel.
indicating device that has a digital
readout. The readout shows the
approximate volume of solvent left in the system (available
only for the 52 L, 215 L, and 225 L CYCLE-TAINER systems).
Model C and Model S — These terms differentiate
containers that have either different components or
specifications. A Model C container has a “manufactured
6
by Cryodyne®” plate on it. A Model S container has a
“manufactured by Sharpsville” plate on it. This plate
refers to the manufacturing site of the container, not the
manufacturing site of the chemical inside.
Net Weight — The weight of the solvent only.
Non-keyed Quick-Connect — A Quick-Connect that is
not keyed and has a plain silver body. The Quick-Connect
will only couple when the male and female components
are “un-keyed” or both have plain silver bodies. A non-keyed
Quick-Connect is used for the gas port on the CYCLE-TAINER
system and prevents improper hook up. You will not be able
to hook the gas line to a keyed Solvent Port.
NPT (National Pipe Thread) — A standard type of thread
that is tapered and is often used to connect to pipe.
Pressure Rupture Disk Assembly (PRDA)— A secondary
safety device that helps relieve excess pressure within
the container during an emergency, such as fire or other
unexpected source of external heat. The container will not
hold any pressure after the rupture disk has burst due to
over-pressurization or mishandling. The container must be
returned to Avantor Performance Materials™ for repair.
Reset Pressure — The pressure setting at which the
pressure relief valve (PRV) will close or reset after relieving
excess pressure from the container.
Serial Number — All containers are assigned a bar-coded
serial number. The white, serial number sticker is on the
chime of the container. The serial numbers start with 4LTXXX for the 4 L, 20C-XXXX for the 18 L, 615-AXXXX for the
52 L, 615-BXXXX for the 215 L or 225 L ,615-CXXX for 52 L
non-ASME, STO-XXXX for the 1,250 L standard base with fork
Channels, ST1-XXXX for the 1,250 L modified base suitable
for pallet jacks + step block, and ST2-XXXX for the 1,250
L modified base suitable for pallet jacks + step block and
made of 316 stainless steel.
SHaRE — The SHaRE program is a SHipping And REturn
program for the CYCLE-TAINER system. The program assists
in the proper shipment of empty containers back to Avantor
at a reduced cost..
Tare weight — The weight of the CYCLE-TAINER system
only.
Trial CYCLE-TAINER System — A CYCLE-TAINER system
that can be used by a customer for an evaluation period of
up to three (3) months.
Vapor Pressure — The pressure exerted when a solid or
liquid is in equilibrium with its own vapor at a particular
temperature.
3.1.1
Container Body
The container body is made of non-leaching 304
stainless-steel. This alloy helps preserve the high quality
of the J.T.Baker® brand solvent.
The body contains most of the solvent information such as:
2.3
CYCLE-TAINER Solvent Delivery System
Description
• J.T.Baker® brand label
The CYCLE-TAINER solvent delivery system consists of
two basic components: a stainless-steel container body
and a dispense head. The two components make up the
complete CYCLE-TAINER system. The CYCLE-TAINER system
is available in 4L, 18 L, 52 L, 215 L, 225 L, or 1,250 L (CYCLETOTE) sizes.
• Batch number information
2.4
The chime is the upper ring of the container (both inside
and out). The chime protects the dispense head from
damage. It also contains regulatory information, in addition
to a bar-coded serial number.
Signal Statements
Throughout this manual, there are Caution, Warning and
Note signal statements. Please read carefully and observe
the information and/or directives in these statements. See
below for an explanation of these statements.
CAUTION – Statements will indicate potentially hazardous operating procedures.
WARNING – Statements will highlight regulatory requirements.
NOTE – Statements will indicate procedures that might cause product contamination.
• Product number
• Bar code serial number
• Clear protective sleeve to keep the container clean
3.1.2
Chime of the Container
Information on the chime of the CYCLE-TAINER system:
• Bar-coded serial number for tracking the container.
• ASME certification tag (only on ASME 52 L and 215 L systems).
• Factory Mutual (FM) approval tag. Please note, however, that all CYCLE-TAINER systems manufactured after
July 1, 2014 will not be approved by FM.
• UN/DOT rating and marking for shipping.
Section 3 Components
and Specifications
3.1
• Operating precautions label for correct operation of
the container.
Parts of the Container
The CYCLE-TAINER system has four (4) main sections:
• Container body
• Chime of the container
• Dispense head
• Forklift channels (only 215 L, 225 L, and 1250 L sizes)
7
3.1.3
Dispense Head
The dispense head is an integral part of the CYCLE-TAINER
system. It is a positive-pressure dispense head, meaning
that gas pressure is applied into the gas port (inlet), and
the solvent comes out of the solvent port (outlet) on the
dispense head. Positive-pressure dispensing with a high
quality gas prevents solvent degradation and subsequent
contamination.
The dispense head has a number of built-in features that
offer enhanced safety during operation:
• Quick-Connect for Gas (QCG) and Quick-Connect for Solvent Ports (QCS) provide automatic shut-off during uncoupling.
• Solvent Valve (VS) is a secondary shutoff valve for the Solvent Port.
52 L Dispense Head, Model S non-ASME
• Gas Valve (VG) is a secondary shutoff valve for the Gas Port.
• Pressure Relief Valve (PRV) is an initial safety device to release excess pressure inside the container during normal operation of container. The PRV is designed to open when the venting pressure is exceeded and close/reset after relieving the excess pressure from the container.
18 L Dispense Head, Model S
Chime
Container
Body
Forklift
NOTE: 1250 L containers
manufactured before
October 1998 are not
pressure vessels and can
only be blanketed with
an inert gas up to 5 psi
and may require a pump
for dispensing. 1250 L
containers manufactured
after October 1998 can be
pressurized to 19 psi. Refer
to Sections 6.1 and 6.2
for more information on
dispensing from the
1250 L containers
Channels
4 Liter
8
18 Liter
52 Liter
215 Liter
1250 Liter
• Pressure Rupture Disk
(PRDA) is a secondary safety device to release excess pressure during an
emergency, such as fire or
other unexpected sources
of external heat, and will
rupture if container is over-pressurized.
Once ruptured, the
Intact Pressure Rupture Disk (PRDA)
container will not hold
pressure. PRDA’s are only available on the 52 L
and 215 L ASME containers.
Additional features allow
efficient operation of the
system and provide added
protection of solvent quality:
Container dust cover:
Blown Pressure Rupture Disk (PRDA)
To protect dispense head
components from damage
and maintain dispense head
cleanliness, a plastic cover is
used during shipping, handling
and storage.
Tamper evident seals to
ensure container integrity:
During shipping, the container
dust cover is held in place by
Container Dust Cover
imprinted nylon zip ties. The ties
can be removed by cutting with wire cutters
Other gauges are gas filled so the bubble does not occur.
Note: the container pressure gauge should not be used in
lieu of a source gas pressure regulator
Liquid Level Indicator
with LCD readout
to monitor solvent
volume: An electronic
Liquid Level Indicating
device can be used for
Liquid Level Indicator
52 L, 215 L, and 225 L
containers. The device is powered by two 9 volt batteries.
Refer to Section 11.3 for instructions to change the batteries.
3.1.4 Forklift Channels
The 215 L, 225 L, and
1250 L containers are
fitted with two (2) forklift
channels welded beneath
each container. The
channels are designed to
facilitate handling with
forklifts or hand operated
forklift trucks. The wide
fork channel base also
provides added upright
stability for the container.
See also Handling and
Storage in Section 5.4 and
Container and Pallet
Handling in Section 12.2.
Gas pressure gauge
to monitor container
pressure: each CYCLE-TAINER
system 52 L and greater
includes a gas pressure
gauge on the dispense
head. The pressure gauge
can be used to monitor the
approximate pressure within
the container. Some pressure
Pressure gauge on CYCLE-TAINER
gauges are filled with liquid
SYSTEM Container.
(glycerin), so you may notice
a bubble inside the gauge. This is completely normal.
CYCLE-TAINER System with
Forklift Channels
9
3.2
Container Body Specifications by Size
Specification
4L
18 L
52 L ASME
52 L
52 L
215 L
ASME
215 L
ASME
215 L
225 L
1250 L
Model
Model S
Model S
Model S
Model C*
Model S
Model S
Model C*
Model S
Model C*
Model S
ASME-certified
No
No
Yes
No
No
Yes
Yes
No
No
No
Height
11.75"
22”
29”
27.3”
28.9”
55”
60”
55”
57.5”
73”
including
fork
channels
Diameter
9.2"
11"
15.6"
15.6"
15.6"
21.7"
21"
21.77"
21"
45"
Capacity
4L
18 L
52 L
52 L
52 L
215 L
215 L
215 L
225 L
1250 L
Container
Body
304
stainless
steel
304
stainless
steel
304
stainless
steel
304
stainless
steel
304
stainless
steel
304
stainless
steel
304
stainless
steel
304
stainless
steel
304
stainless
steel
304
stainless
steel
Wall
thickness
0.052"
Wall
thickness
0.06"
Wall
thickness
0.08"
Wall
thickness
0.05"
Wall
thickness
0.05"
Wall
thickness
0.08”
Wall
thickness
0.08"
Wall
thickness
0.08"
Wall
thickness
0.08"
Wall
thickness
0.098"
Tare
Weight of
System
13 lb
24 +/- 1 lb
56 +/-1 lb
43 +/- 1 lb
57.5 lb
144 +/-1 lb
169 +/- 1 lb
141 lb
154 +/- 1 lb
496 +/- 1 lb
Container
Operating
Pressure
0-15 psi
0-15 psi
0-40 psi
0-15 psi
0-15 psi
0-40 psi
0-40 psi
0-15 psi
0-15 psi
0-5 psi
(containers
mfg before
Oct. 1998);
0-19 psi
(containers
mfg after
Oct. 1998)
Fork Truck
Channels
None
None
None
None
None
3.75" H x
8.5" W x
22” D
3.5" H x
7.5" W x
22” D
3.75" H x
8.5" W x
22” D
3.5" H x
7.5" W x
22” D
3.5" H x 8.5"
W x 46” D
Fork Truck
Base
None
None
None
None
None
22" Square
22" Square
22" Square
22" Square
41" x 46" **
* Limited availability, please check with your local sales representative.
** Please note — The 1250 L container fork channels extend beyond the diameter of the container on one side. The 1250 L container will need at least 46 inches for
clearance.
Note — If you are not sure if you have a Model C or a Model S container, see Definitions and Terminology Section 2.2 for assistance
10
3.3
Dispense Head Assembly/Specifications by Size
Specification
4L
18 L
52 L and 225 L
52 L
215 L
215 L
52 L and 215 L
1250 L
Model
Model S
Model S
Model C*
Model S
Model S
ASME Model C
ASME Model S
Model S
Container
Head
Assembly
304 stainless
steel
316 stainless
steel
316 stainless
steel
316 stainless
steel
316 stainless
steel
316 stainless
steel
316 stainless
steel
316 stainless
steel
On/Off
Diaphragm
Valve
1 valve for
solvent
Diaphragm
Packless Valve
1 valve for
solvent
Diaphragm
Packless Valve
2 valves - one
for solvent and
one for gas
Diaphragm
Packless Valve
2 valves - one
for solvent and
one for gas
Diaphragm
Packless Valve
2 valves - one
for solvent and
one for gas
Diaphragm
Packless Valve
2 valves - one
for solvent and
one for gas
Diaphragm
Packless Valve
2 valves - one for
solvent and one
for gas
Diaphragm
Packless Valve
None
Gas Port
(non-keyed)
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2 or QT-4
Quick-Connect
¼”or ½ “male
NPT connection
respectively
Solvent Port
(color-coded,
keyed QuickConnect)
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-2
Quick-Connect
¼” male NPT
connection
QT-8
Quick-Connect
¾” male NPT
connection
Pressure
Relief Valve
1/4” Nupro
Valve, Male
Thread
Venting Pressure:
50 psi
Reset Pressure:
35-38 psi
Venting Pressure:
50 psi
Reset Pressure:
35-38 psi
Venting Pressure:
50 psi
Reset Pressure:
38-40 psi
Relief valve
outlet
integrated w/
rupture disk
Venting Pressure:
50 psi
Reset Pressure:
38-40 psi
Relief valve
outlet
Venting Pressure:
50 psi
Reset Pressure:
38-40 psi
Relief valve
outlet
Venting Pressure:
50 psi
Reset Pressure:
38-40 psi
Venting Pressure:
50 psi
Reset Pressure:
38-40 psi
Venting Pressure:
(25 psi)1
Reset Pressure:
(16-22 psi)1
Pressure
Rupture Disk
None
None
None
None
None
Rupture
Pressure:
70 psi 1”
Tri-clover
clamp
connection
Rupture
Pressure:
56 psi 1”
female thread
connection
Rupture
Pressure:
35 psi1 2”
female thread
connection
Venting
Capacity
50 SCFM @
50 psi (relief
valve)
50 SCFM @
50 psi (relief
valve)
21-24 SCFM @
62 psi (relief
valve)
21-24 SCFM @
62 psi (relief
valve)
21-24 SCFM @
62 psi (relief
valve)
>1,000 SCFM
@ 70 psi (disk
rupture)
717 SCFM @
61 psi (disk
rupture)
1460 SCFM
@ 24 psi (disk
rupture)
Dispense
Rate of
Solvent
N/A
~3.5 L/min.
typical @ 15
psi
~3.5 L/min.
typical @ 15 psi
~4.9 L/min.
typical @ 15
psi
~4.9 L/min.
typical @ 15
psi
~3.5 L/min.
typical @ 15
psi
~3.5 L/min.
typical @ 15 psi
Diaphragm
pump usage
will affect flow
rate
Gas Pressure
Gauge
N/A
N/A
–30 to 100 psi
compound
gauge
0 to 15 psi
0 to 15 psi
–30 to 100 psi
compound
gauge
–30 to 100 psi
compound
gauge
N/A
Level
Indicator
N/A
N/A — if needed,
a small scale may
be used
LED liquid level
cube
LED liquid
level cube
LED liquid
level cube
LED liquid
level cube
LED liquid level
cube
N/A
Inert Gas
Filter
N/A
N/A
Internal
2 micron
sintered SS
Internal
2 micron
sintered SS
Internal
2 micron
sintered SS
Internal
2 micron
sintered SS
N/A
N/A
Tamper
Evident Seals
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
* Limited availability, please check with your local sales representative.
Specifications of containers manufactured after 10/98.
N/A- Not Applicable
Note — If you are not sure if you have a Model C or a Model S container, see Definitions and Terminology Section 2.2 for assistance.
1
11
3.4
Container Body and Dispense Head Diagrams
*
ASME Certification
(if applicable)
*
*
Forklift Channel
4 Liter CYCLE-TAINER
Container
Container
Container
Container
* Please note that all CYCLE-TAINER systems manufactured after July 1, 2014 will not be approved by FM and
will not carry the FM approval marking.
12
4
13
14
15
Section 4 Pre-Installation Information
4.1
CYCLE-TAINER System Performance and Regulatory Compliance
Most products sold in the Avantor CYCLE-TAINER solvent
delivery system are regulated hazardous materials. Obtain
and consult current Material Safety Data Sheets for all
materials you will be using. Check with your local regulatory
agencies regarding safety, storage, handling, and facility
engineering requirements for these material(s) prior to use.
Material Safety Data Sheets (MSDS) can be obtained from
our web site at www.avantormaterials.com or by calling
1-855-AVANTOR.
4.2
For flammable or hazardous materials, ensure your local
fire marshal or fire department has been contacted. Ensure
your facility CYCLE-TAINER system installation plan meets all
appropriate fire codes and has been reviewed and approved
by that office, if required.
All CYCLE-TAINER systems are labeled in accordance with
DOT/UN 49 CFR, OSHA 29 CFR 1910.1200 and ANSI Z 129.1
requirements and Avantor product and hazard labeling
systems.
Performance and Regulatory Chart by Size
4L
Model S
18 L
Model S
52 L
Model S
52 L, 215 L
Model C
215 L
Model S
52 and
215 L
Model S
215 L
Model C
225 L
Model C
1250 L
Model S
UN Rating
1A1X
1A1X
1A1X
1A1X
1A1X
1A1X
1A2X
1A1X
31A
Meets
NFPA 30
Yes
Yes
Yes
No
Yes
Yes
Yes
No
No
ASME-certified
No
No
No
No
No
Yes
Yes
No
No
FM
Approved
Yes*
Yes*
No
Yes*
No
Yes*
Yes*
Yes*
Yes*
*Please note that all CYCLE-TAINER systems manufactured after July 1, 2014 will not be approved by FM.
16
4.3
Initial Preparation
Typical CYCLE-TAINER system installations are of three (3)
basic types:
• Type A — Permanently Installed System — distribution from a remote storage location through a main line to a manifold and multiple points of use (Figure 4 in the Appendix).
• Type B — Direct feed from the CYCLE-TAINER system to a process or instrumentation (Figure 5 in the Appendix).
• Type C — Direct feed from the CYCLE-TAINER system to a J.T.Baker® CYCLE-TAP dispenser.
In the Appendix, Section 12.5, there are engineering drawings
of typical plumbing designs with the necessary hardware
recommended to maintain the purity and performance
of these high purity products. These system designs are
meant as guidelines only. The design requirements may vary
depending on the facility layout and application.
4.3.1
Gas Supply
For basic operation of the CYCLE-TAINER system, your lab
needs to have a gas supply (Nitrogen, Argon or Helium)
for blanketing and dispensing that is 99.999% pure and
can deliver regulated pressures to at least 15 psi. The ASME
containers should not be pressurized above 40 psi. If your
application requires high flow rates or you need to plumb
from a distance, you need a gas supply that goes up to 40
psi and ASME-certified containers.
A pressure regulator designed for high purity gases must
be used to regulate your gas supply. These regulators
have stainless-steel diaphragms and inert seals that do not
introduce contamination into the system. DO NOT USE
STANDARD INDUSTRIAL TYPE GAS REGULATORS.
4.3.2
Venting the Container
Local regulatory agencies, building codes, and safety
policies may require that you attach the container to vent
lines during operation. The vent lines attach to the Pressure
Relief Valve (PRV) and the Pressure Rupture Disk (PRDA) (if
applicable). The lines should go from the container directly
to the outside or to an appropriate exhaust system or
laboratory hood. Any exhaust system used for venting the
Pressure Rupture Disk Assembly (PRDA) must not create
a vacuum against the
rupture disk because
this will cause the disk to
rupture.
Stainless-steel or PTFE
tubing may be used as
vent lines depending
on local regulations. If
your regulations require
stainless-steel vent lines,
you may want to use
flexible stainless-steel
tubing for adaptability
and ease of use.
WARNING: Local regulatory agencies,
building codes, and safety policies may
require that you attach the container to
vent lines during operation. The vent lines
attach to the Pressure Relief Valve (PRV)
and the Pressure Rupture Disk
(PRDA) (if applicable)
NOTE: Care should be taken to ensure
that the Pressure Rupture Disk (PRDA) is
not compromised by the vent tubing or
fitting. The fitting must not touch the
PRDA membrane.
Check with your local
CAUTION: EXPLOSION HAZARD- You
must ground the CYCLE-TAINER system
regulatory agencies
during operation.
regarding safety, storage,
handling, and
facility engineering
requirements for these material(s) as well.
4.3.3Grounding
the Container
A grounding cable or grounding device is needed for
operation of the CYCLE-TAINER system. Failure to use a
ground connection on the containers will allow a static
electricity explosion hazard to exist with the use of
flammable solvents. The originating end of the grounding
wire must be attached to a proper ground per standard
facility procedure.
4.3.4
Tubing Requirements —
Permanently Installed System (Type A)
Permanent installation is recommended for rigorous
processes, plumbing long distances, and high-pressure
applications.
All permanently installed product supply lines should be
high quality 316 stainless-steel with a minimum ½” I.D..
Valves, pressure regulators, flow meters, and fittings should
be high quality 316 stainless-steel or PTFE. In-line valves
should be high quality packless diaphragm valves with
PTFE stem inserts to avoid lubricant contamination within
the lines.
17
Some site installations may require “line within a line” main
feed or distribution lines from the CYCLE-TAINER system
storage area to point(s) of end use. A site may also require
special preventative spill control measures. Check with your
local fire marshal and applicable building codes on these
requirements.
• Pump with polytetrafluoroethylene (PTFE) diaphragm for high purity solvents (for 1,250 L CYCLE-TOTE systems manufactured prior to October 1998 only).
4.3.5
• Design the system to meet your local fire, safety, materials handling and other regulatory codes.
4.4
Tubing Requirements — Container Directly Fed to Process or Instrumentation (Type B)
CYCLE-TAINER systems can be directly connected
to analytical and production processes. This type of
configuration is usually found in laboratories where one or
more instruments or small-scale processes are being fed
from a single CYCLE-TAINER system in near proximity. Check
with your facility safety officer on storage requirements,
design, and location of your intended system set-up.
• Keep all product lines dedicated to a single product to maintain reliability and purity.
4.3.6 Tubing Requirements — Direct feed from a CYCLE-TAINER System to a J.T.Baker®
CYCLE-TAP Dispenser. (Type C)
CYCLE-TAINER systems can be dispensed by the CYCLE-TAP
Dispenser accessory. Check with your facility safety officer on
storage requirements, design, and location of your intended
system set-up.
5.1
• Gas supply of high quality gas (purity of 99.999%).
• Gas regulator for high purity gases.
• Tubing for solvent.
• Tubing for gas.
18
Incoming Container Checklist
• Verify the proper product
was received. The product name, grade, product
number, and lot number are shown on the product
label on the outside of the container.
Pre-Installation Checklist
• Vent line for PRDA installed (if applicable).
For first time system start-up, you should purge the entire
plumbing system with the product of intended use,
including any dispensing device. Continue to purge until
all air and contamination in the lines are removed. Solvent
should be tested to ensure it meets product specifications
at the point of end use prior to use. Be sure to schedule
time for this step before you begin critical usage of the
Section 5 Preparation for Use
We suggest the use of flexible stainless-steel or high quality
PTFE tubing for gas lines. If PTFE tubing is used, ensure it is
rated for the supply pressures you intend to use. See System
Accessories, Section 12.1, for tubing sources and CYCLE-TAP
dispenser options.
• Vent line for PRV installed (not applicable on 215 L — Model C).
NOTE: Solvent should be tested
to ensure it meets product
specifications at the point of end
use prior to use.
• All valves, pipes and fittings should be de-greased before installation to maintain solvent purity.
We suggest the use of flexible stainless-steel or high quality
PTFE tubing for gas and solvent lines. If PTFE tubing is used,
ensure it is rated for the supply pressures you intend to use.
See System Accessories, Section 12.1, for tubing sources.
4.3.7
Recommendations for Initial Facility Design and Start-Up
NOTE: Do not apply labels
directly to the container surface.
Any labels that customers apply
should be applied to the plastic
protective sleeve that covers
every CYCLE-TAINER system.
• Check and record the
container serial numbers (bar-coded number on
white sticker).
• Verify the containers are part of your assigned fleet.
• Do not add any labels, stickers, or marks to the container itself. If you must add labels, stickers, or marks please only put them on the clear protective sleeve.
5.2
Inspection Checklist
• Verify that the tamper
evident straps securing the
dust cover on container are intact.
• Remove the tamper evident straps and dust cover.
CAUTION: Ensure that CYCLETAINER systems are secure during
handling to prevent accidental
loss of control of the container.
This may result in injury to
personnel and/or damage to the
container
• Inspect for any product leakage or obvious damage
to dispense head including valves, gauges, fittings
and seals.
• Make sure the dust caps are on the Solvent and Gas Ports.
• Replace the container’s dust cover.
• If any damage or tampering is evident, please report it immediately to our Customer Service department at 1-855-AVANTOR.
Be sure to have the container serial number and
specific information about the damage or tampering
readily available.
5.3
Sampling the CYCLE-TAINER System for Quality Control Purposes
If sampling of the CYCLE-TAINER system is necessary, the
CYCLE-TAP dispenser (sold separately) may be used during
the sampling process. See Section 6.6, 7.2, and 8.1 for stepby-step procedures. See Section 12.1 System Accessories for
ordering information.
We recommend that you pressurize the container before
removing a sample from the CYCLE TAINER system. The
CYCLE-TAINER system is blanketed with an inert gas at the
time of filling. The blanket of gas may not provide sufficient
pressure to dispense a sample from the container.
5.4
Handling and Storage
• Individual 4 L CYCLE-TAINER systems are light enough to lift by hand or by a hand truck.
• The 18 L and 52 L CYCLE-TAINER systems can be moved to its storage or system hookup area using a hand truck
or dolly. CYCLE-TAINER™ Solvent Delivery System User’s Manual
19
• A motorized forklift or hand truck can be used for the transport of the 215 L, 225 L, 1250 L CYCLE-TAINER
systems. The 215 L and 1250 L systems are fitted with two forklift channels. See also Container and Pallet Handling in Section 12.2.
• Ensure all CYCLE-TAINER systems are mounted upright and securely at their storage site.
• Return all valves and components to the closed position before attempting to move the container. Prior to moving a container, please refer to Section 8 and Section 9 for proper container shut down and removal procedures.
• Refer to Section 12.2 Container and Pallet Handing for equipment guidance and recommendations.
Section 6 Installation and Connections
6.1
Basic Installations for 4 L, 18 L, 52 L, and 215 L CYCLE TAINER Systems and 1250 L
CYCLE-TOTE Systems Manufactured after
October 1998
The CYCLE-TAINER system is designed as a portable product
supply tank, which uses inert gas pressure to transfer
solvents from the CYCLE-TAINER system, through solvent
supply lines, to point(s) of end use. Product may also be
drawn by demand from a CYCLE-TAINER system by a pump,
such as that from an HPLC or another pump used for high
purity solvents. If pumps are employed, apply a low interior
gas pressure (< 0.5 psig) to blanket the solvent and protect
the solvent from the atmosphere.
Typical CYCLE-TAINER system installations are of three (3)
basic types:
• Type A — Permanently Installed System — distribution from a remote storage location through a main line to a manifold and multiple points of use (Figure 4 in the Appendix).
• Type B — Direct feed from a CYCLE-TAINER system to a process or instrumentation (Figure 5 in the Appendix).
• Type C — Direct feed from a CYCLE-TAINER system to a J.T.Baker® CYCLE-TAP dispenser.
20
In Section 12 of the Appendix, there are engineering
drawings of typical plumbing designs with the necessary
hardware recommended to maintain the purity and
performance of these high-purity products. These
system designs are meant as guidelines only. The design
requirements may vary depending on the facility layout and
application. Throughout this section, references are made to
the engineering drawings
in Section 12. The
corresponding
CAUTION: This section assumes that gas
engineering drawing
and solvent lines have been installed to
component is listed in
the instrument or process. If applicable,
parenthesis after the
the setup should have its main
solvent supply valve closed to prevent
component description
unintentional solvent surges or down-line
in the hookup
releases when the CYCLE-TAINER system
Instructions (i.e. Regulated is pressurized.
Gas Shutoff (V2G)).
6.2 Basic Installations
for 1250 L
CYCLE-TOTE System Manufactured
prior to
October 1998
Product must be drawn
by demand from this
1250 L CYCLE-TOTE
System. You will need
to use a pump that is
acceptable for use with
high-purity solvents.
A stainless-steel pump
with a PTFE diaphragm
will work for most
applications. During
operation, you will need
to apply minimal gas
pressure (<5 psig) to
blanket and protect
the solvent from the
atmosphere. The pump
will pull the solvent out
of the container and
dispense it to the point
CAUTION: DO NOT PRESSURIZE THE
CONTAINER WITH COMPRESSED AIR OR
OXYGEN. Failure to observe this caution
could result in an explosive situation,
which can cause serious or fatal injuries
to personnel.
NOTE: For first time start-up or if there
is contamination suspected in plumbing
system, a total solvent purge of your
facility lines should be carried out before
placing the CYCLE-TAINER system in
service.
CAUTION: All metal supply and
distribution lines should be electrically
earth grounded. Storage areas must
provide electrical earth ground connections
for all containers while in use.
CAUTION: Ensure your gas supply is
routed through a high quality stainless
steel pressure regulator. The regulator
output pressure must not exceed 40 psig
for ASME-certified containers; 15 psig for
non-ASME certified containers; 5 psig for
1250 L containers manufactured prior to
October 1998; 19 psig for 1250 L
containers manufactured after October
1998. These pressures represent maximum
working pressures of the CYCLE-TAINER
systems as set forth in this manual
of use. In order to adhere to DOT regulations, this
intermediate bulk container was not designed as a pressure
vessel that operates at higher pressures.
Typical CYCLE-TOTE system installations are of two (2) basic
types:
• Type A — Permanently installed system with distribution from a remote storage location through a main line to a manifold and multiple points of use (Figure 4 in the Appendix).
• Female tube connector with ferrule for solvent line (size specific for the solvent tubing)
• Female tube connector with ferrule for gas line (1/4”)
• Liquid Level Indicator cube (52 L and 215 L only). Model C containers will require an additional adapter for the Liquid Level Indicator cube. Model S containers do not require this adapter.
• 316 stainless-steel tubing or PTFE tubing
• Type B — Direct feed from a CYCLE-TOTE system to
a process or instrumentation (Figure 5 in the Appendix).
• PTFE tape
In Section 12 of the Appendix, there are engineering
drawings of typical plumbing designs with the necessary
hardware recommended to maintain the purity and
performance of these high purity products. These
system designs are meant as guidelines only. The design
requirements may vary depending on the facility layout and
application.
• Gas filter (2 micron)
6.3
General Parts List to Hookup the
CYCLE-TAINER System
CYCLE-TAINER system basic hook-up kit:
• Keyed, female Quick-Connect body (contains color band) for solvent
• Non-keyed, female Quick-Connect body (no color band) for gas
• Grounding strap
• Diaphragm pump for dispensing (for non-pressurized
1250 L CYCLE-TOTE system only)
• Also see pre-installation checklist, Section 4.3.7.
6.4
Hooking Up Tubing to the Female Quick-
Connects — General Guidelines
These steps will guide you in
the hookup of your solvent and
gas lines to the female QuickConnect body.
NOTE: See System Accessories
Section 12.1 for ordering
information on components
listed on this page.
1. Wrap the male threads of the
Quick-Connect body with
PTFE tape in the direction of the threads.
(1)
21
(2)
(6)
2. Open the female tube connector to ensure that the
ferrule is inside. Gently tighten it back together upon
verification.
3. Hand-tighten the female tube connector onto the male
thread of the Quick-Connect.
4. Insert either stainless-steel or PTFE tubing into the
aperture on the tube connector.
(7)
6. Thread the male Quick-Connect stem into the female
tube connector and hand tighten. Use a wrench to gently
tighten the female tube connector onto the QuickConnect body.
7. The tubing is now connected to the Quick-Connect body.
Repeat above steps for the other Quick-Connect.
(5)
5. While holding the tubing inside the tube connector,
gently tighten the nut on the tube connector with a
wrench. This will set or crimp the ferrule onto the tubing
and create a connection that should be “leak free.” The
tubing must be seated properly in order to prevent fitting
leaks.
22
6.5
Preparing the CYCLE-TAINER System for Hookup (All Types of Installations)
1. Remove the dust cover:
CYCLE-TAINER systems are
shipped with a plastic dust
cover held in place by printed
tamper evident zip ties. Cut
the zip ties and remove the
container dust cover from the
container chime.
2. Ground the container:
Securely fasten the grounding
cable to the container chime
or Grounding Terminal (GT).
Ensure the container shows
continuity to earth ground.
3. Remove the dust caps:
The Solvent and Gas Ports
are protected by plastic caps.
Remove the dust caps from
the gas port (QCG) and
Solvent Port (QCS). Inspect
the ports to ensure the male
stems are free of dirt and
residue.
4. Remove the transport
plugs: The Pressure Relief Valve
(PRV) and Pressure Rupture
Disk Assembly (PRDA) are protected during transport by
plastic caps and plugs. Remove all transportation plugs
from the container’s Pressure Relief Valve (PRV) and/or the
Pressure Rupture Disk Assembly (PRDA). Do not discard
the transport plugs since they will be needed for return
shipment of the empty container.
5. Close the gas and solvent valves: Ensure the Gas Valve
(VG) and Solvent Diaphragm Valve (VS) on the
CYCLE-TAINER system are closed.
7. Connect the Liquid Level
Indicator: Connect the
five or six-pin, Liquid Level
CAUTION: To avoid possible
Indicator to the Liquid Level
ignition or explosion to
toxic/flammable vapors, we
Indicator connection (LC) on
recommend the pressure relief
the dispense head (applicable output be directed to a hood or
other proper venting location.
for 52 L and 215 L sizes only).
If an external vent line is used,
For Model C containers, an
ensure it does not restrict gas
adapter is needed in order
flow from the pressure relief
device or create a vacuum
to connect the Liquid Level
against the pressure relief device.
Indicator cube cable to
the Liquid Level Indicator
connection (LC) on the
NOTE: not all container types
dispense head. Note: Care
have pressure rupture disk
assemblies. Non-ASME
should be taken to avoid
containers and 4 L and 18 L
bending the pins on the
containers do not have pressure
connector cable. Bent pins
rupture disks.
can result in improper or no
reading on the indicator cube.
To successfully connect the
liquid level cube, the cable must
be properly oriented. The cable
will not connect if the cable
connector is not oriented with
the connector on the dispense
head.
8. Connect the vent lines:
Connect your facility vent lines
to the Pressure Relief Valve
(PRV) and/or Pressure Rupture
Disk Assembly (PRDA) on the
container.
9. Attach the gas line to the
container: Connect the gas
supply Quick-Connect body
(female) to the gas port
Quick-Connect male stem of
the CYCLE-TAINER system gas
port (QCG).
6. Close the gas supply valves and solvent supply
valves: Ensure the Regulated Gas Shutoff (V2G) valve on
your regulator and the main liquid supply (V5L) valves are
both closed, if applicable
23
6.6
Hooking Up the J.T.Baker® CYCLE-TAP Dispenser to the CYCLE-TAINER System
(Type C Installation)
The CYCLE-TAP dispenser is a solvent dispense unit designed
for unmetered manual dispensing of solvents from the
CYCLE-TAINER system. The dispenser is available with either
a toggle valve for dispensing into laboratory containers or
with a needle connector to dispense into reaction vessels for
oxygen or water sensitive applications.
1. Close the gas and solvent valves: Ensure that the gas
(VG) and solvent valves (VS) on the CYCLE-TAINER system
are in the “closed” positions.
2. Close the dispenser valve: Turn the arrow/handle on
the three-way ball valve (CYCLE-TAP dispenser) to the
“off” position (horizontal, perpendicular to the fittings and
Quick-Connect).
3. Connect the CYCLE-TAP dispenser: Attach the solvent
Quick-Connect body (female) to the matching color
Quick-Connect stem (male) of the CYCLE-TAINER system
solvent port (QCS).
24
6.7
Hooking Up the J.T.Baker® CYCLE-TAP Sampler to the CYCLE-TAINER System
The CYCLE-TAP sampler is a device for sampling small
quantities of solvent from the CYCLE-TAINER system.
1. Close the gas and
solvent valves:
Ensure that the gas
(VG) and solvent valves
(VS) on the CYCLETAINER system are in
the “closed” positions.
2. Adjust the gas
pressure: Connect the
appropriate gas supply
to the CYCLE-TAINER
system, following the
instructions outlined
in this manual. Set the
pressure regulator to
approximately 5 psig.
3. Close the sampler
valve: Turn the
arrow/handle on the
three-way ball valve
(CYCLE-TAP sampler)
to the “closed”
position (horizontal,
perpendicular to the
fittings and QuickConnect).
NOTE: See System Accessories Section 12.1
for CYCLE-TAP ordering information.
NOTE: The color bands on the quickconnects should be the same color.
CAUTION: Initially turn on the toggle
valve slowly to release gas trapped inside
the hose. When you release the lever,
NOTE: For first time use of the CYCLE-TAP
dispenser, you should purge the entire
plumbing system with the solvent from
the container. Continue to purge until all
air in the lines is removed. Solvent should
be tested to ensure it meets product
specifications at the point of end use.
Before use in your application, be sure
to schedule time for this step before you
begin critical usage of the CYCLE-TAINER
system.
CAUTION: Do not exceed operating
pressure of the CYCLE-TAINER system.
Refer to Section 3.2 for operating
pressures of various container sizes
and types.
4. Connect the CYCLETAP sampler: Attach
the solvent QuickWARNING: NEVER DEPRESS THE PLUNGER
Connect body of the
WHEN THE SYRINGE IS ATTACHED TO
sampler (female) to
THE SAMPLER. THIS MAY INTRODUCE
the matching color
CONTMINANTS INTO THE CYCLE-TAINER
SYSTEM.
Quick-Connect
stem (male) of the
CYCLE-TAINER system Solvent Port (QCS). Note: The
three-way ball valve is designed to completely inhibit flow
in the “off” position. However, for added safety, always
be sure the syringe connection port is pointed away
from laboratory personnel and ignition sources when
connecting the sampler.
6.8
Hooking Up the CYCLE-TAINER System to
Your Process, Instrumentation or as a Permanently Installed System
(Type A and B Installations)
1. Prepare the gas and solvent lines: Your tubing for
both solvent and gas should already be attached to
the female Quick-Connect bodies. See Section 6.4 for
guidelines on hooking your tubing to the Quick-Connect
bodies.
2. Close the purge line valve: If you have a purge line
installed, ensure the Purge Shutoff Valve (V7L) is in the
fully closed position and the three-way purge bypass
valve (V6L) is in the bypass position.
3. Connect the gas supply line: Insert the gas QuickConnect that is attached to your gas tubing onto the gas
port (QCG) on the CYCLE-TAINER system. The gas QuickConnects will not have a color band.
4. Connect the solvent line: Insert the solvent QuickConnect that is attached to your solvent tubing onto the
Solvent Port (QCS) on the CYCLE-TAINER system. The color
band on the Quick-Connects should be the same color. See
Section 12.1 System Accessories for product color codes.
6.9
Daisy Chaining Multiple CYCLE-TAINER
Systems
Multiple CYCLE-TAINER systems can be connected together
in series, or “daisy chained.” Daisy chaining allows for
continuous operation through a smooth transition from an
empty container to a full container. It also allows the user to
increase the overall solvent volume for applications requiring
continuous solvent delivery volumes beyond that of a single
container. For each additional daisy chained container you
will need:
1. An additional length of PTFE tubing
2. A keyed solvent Quick-Connect body
3. A non-keyed gas Quick-Connect body
4. Two (2) tube fittings
End Use
“Daisy Chaining” CYCLE-TAINER System Diagram
25
See Section 12.1 of the System Accessories Section for
ordering information on components listed above.
Section 7 CYCLE-TAINER System Operation
The steps for daisy chaining CYCLE-TAINER systems are:
7.1
1. Close the gas and solvent valves: Ensure that the gas
(VG) and solvent valves (VS) on the CYCLE-TAINER systems
are in the “off” positions.
2. Prepare the solvent and gas lines: An additional
length of tubing will be needed to connect the partial
CYCLE-TAINER system to the full CYCLE-TAINER system.
Ensure that one end of the tubing has the appropriate
keyed solvent Quick-Connect body attached and
the other end has a non-keyed Quick-Connect body
attached. Refer to Section 6.4 for guidelines on hooking
the tubing to Quick-Connect.
3. Connect the gas supply line: Connect the gas QuickConnect from the gas supply line to the gas port on the
partial CYCLE-TAINER system.
4.Connect the containers together: Connect the solvent
Quick-Connect on the additional tubing piece (see above)
to the Solvent Port (QCS) of the partial CYCLE-TAINER
system. Connect the non-keyed Quick-Connect on the
additional tubing piece to the gas port (QCG) on the full
5. Connect the solvent line: Connect the solvent QuickConnect of the solvent line to the Solvent Port (QCS) on
the full CYCLE-TAINER system.
With the CYCLE-TAP Dispenser
See Section 6.6 for
connecting the CYCLETAP dispenser.
1. Adjust gas pressure
regulator:
a.
Set regulator
pressure below operating pressure of container.
b.
Ensure the
regulated gas
shutoff valve (V2G) on the regulator
is closed.
c.
Set the gas
pressure regulator
(GPR1) to the
desired pressure.
NOTE: See System Accessories Section 12.1
for CYCLE-TAP ordering information.
NOTE: The color bands on the quickconnects should be the same color.
CAUTION: Initially turn on the toggle
valve slowly to release gas trapped inside
the hose. When you release the lever,
NOTE: For first time use of the CYCLE-TAP
dispenser, you should purge the entire
plumbing system with the solvent from
the container. Continue to purge until all
air in the lines is removed. Solvent should
be tested to ensure it meets product
specifications at the point of end use.
Before use in your application, be sure
to schedule time for this step before you
begin critical usage of the CYCLE-TAINER
system.
CAUTION: Do not exceed operating
pressure of the CYCLE-TAINER system.
Refer to Section 3.2 for operating
pressures of various container sizes
and types.
WARNING: NEVER DEPRESS THE PLUNGER
WHEN THE SYRINGE IS ATTACHED TO
THE SAMPLER. THIS MAY INTRODUCE
CONTMINANTS INTO THE CYCLE-TAINER
SYSTEM.
26
2. Close the dispenser valve: Ensure that the three-way
valve on the dispenser is in the off position with arrow
pointing to the right.
3. Turn on gas supply: Turn on the gas supply to the
CYCLE-TAINER system by opening the regulated gas
shutoff valve (V2G).
4. Open the gas valve: Open gas diaphragm valve (VG)
on the dispense head to begin pressurizing the CYCLETAINER system.
5. Open the solvent valve: Open the solvent diaphragm
valve (VS) on the dispense head to begin solvent flow out
of the container.
6. Open the dispenser valve: Turn the three-way ball
valve pointing down toward the container. Solvent will fill
the dispenser.
7. Dispense solvent: To begin solvent flow from the
dispenser, push the lever of the toggle valve down.
27
7.2 With the CYCLE-TAP Sampler (Type C Installation)
See Section 6.7 for connecting the CYCLE-TAP sampler.
Select a Luer lock syringe of appropriate size and material of
construction with an on/off valve for sampling the solvent.
Before use, thoroughly clean and dry the syringe, ensuring
the barrel, plunger and Luer lock valve assembly are free of
residue and moisture.
from the CYCLE-TAINER system by extracting the plunger.
Once the desired volume of solvent has been withdrawn,
immediately turn the three-way ball valve to the “off”
position.
7. Disconnect the syringe: Turn the syringe valve to the
“off” position and remove the syringe from the sampler.
8. Purge the sampler: Purging the sampler is
recommended. Discard the first one or two volumes of
solvent to purge the sampler of residue.
7.3
CYCLE-TAP Sampler and Optional Syringe
1. Adjust gas pressure regulator: Set regulator pressure
to below 5 psig.
2. Close the sampler valve: Ensure that the three-way
valve on the sampler is in the off position.
3. Turn on gas supply: Turn on the gas supply to the
CYCLE-TAINER system by opening the regulated gas
shutoff valve (V2G).
4. Open the gas valve: Open gas diaphragm valve (VG)
on the dispense head to begin pressurizing the CYCLETAINER system.
5. Connect the syringe to the Sampler: Depress the
syringe plunger until it is completely inserted in the barrel.
Attach the syringe to the syringe connection port of the
sampler.
With Your Process, Instrumentation,
or as a Permanently Installed System
(Type A and B Installation)
1. Pressurize the system
by opening the
regulated gas shutoff
valve (V2G) on the
regulator. See
Section 3 for operating
pressure. Open
the container’s gas
valve (VG). Open the
container’s solvent
valve (VS). (If
necessary, adjust the
gas pressure regulator
(GPR1) until the
desired solvent
pressure is obtained.)
CAUTION: When direct feeding to
instrumentation, DO NOT
OVERPRESSURIZE the input line to the
instrument - damage to the instrument
may occur. Consult the instrument
manufacturer operation manual or a
technical service representative for the
proper feed pressure.
NOTE: Product may also be drawn by
demand from a CYCLE-TAINER system by
a pump such as that from an HPLC or
a stainless-steel pump with a PFA
diaphragm. If pumps are used, apply a
low (<0.5 psig) interior gas pressure
to maintain solvent isolation from the
atmosphere.
2. For first time start up,
purge your facility’s
lines with product until all air is expelled. Slowly open
the purge line shutoff valve (V7L) and vent any gas from
the lines until only solvent emerges into the purge/waste
tank. Fully close the purge shutoff valve (V7L).
3. If applicable, open the main liquid supply valve (V5L).
6. Withdraw sample: Turn the three-way ball valve to
the “on” position while holding the plunger and syringe
(the pressure within the CYCLE-TAINER system may fill
the syringe and push out the plunger). Withdraw solvent
28
Section 8 Temporary System Shutdown (Overnight or Short-term Shutdown)
8.1
When Hooked to the CYCLE-TAP Dispenser
1. Shut off the solvent valve (VS) on the container.
5. Disconnect the liquid level indicator connection (LC), and
the pressure relief vent lines from the container.
6. Replace the transport cap for the pressure relief valve
(PRV).
7. Replace the transport cover for the pressure rupture disk
assembly (PRDA), if applicable.
2. Shut off the gas valve (VG) on the container.
8. Disconnect the facility grounding cable from the CYCLETAINER system grounding terminal (GT).
3. Turn off the gas supply to the container.
9. Reseat the container dust cover.
4. Push the lever on the CYCLE-TAP Dispenser toggle valve
to remove small amount of solvent from the hose.
10. Reseal the container cover with tamper evident straps
that arrived in the chime at time of receipt.
5. To restart, ensure that the proper feed pressure is set on
the gas regulator and then reverse the above steps.
The container can now be moved to your shipping area
for return shipment. Before shipping the empty container,
complete the return shipment checklist (Section 10.1) to
ensure proper shipment (keep for your records).
8.2
When Hooked to Your Process, Instrumentation or as a Permanently
Installed System (Type A and B Installation)
1. Close solvent valve (VS) first to prevent back flushing into
the container.
2. Close the gas valve (VG).
3. Close the regulated gas shutoff valve (V2G).
4. To restart, ensure that the proper feed pressure is set on
the gas regulator and then reverse the above steps.
Section 9 Empty Container Shutdown and Removal
9.1
Container Removal
Section 10Return Shipment of
CYCLE-TAINER System
10.1
Return Shipment Checklist
1. Gas diaphragm (VG)
and solvent diaphragm
valves (VS) closed.
2. All tamper-evident
seals are intact.
3. Container emptied
and purged.
WARNING: If you know or suspect that
foreign substances were introduced into
the container, quarantine the container
and call Customer Service at
1-855-AVANTOR for assistance. Do
not return the container without first
contacting Avantor to avoid violations
of Federal and/or State laws.
4. Container pressure
gauge reading is zero or within operating pressure for
shipment.
1. Close the solvent valve (VS) first to prevent back flushing
into the container.
5. Transport caps placed over Quick-Connect gas port (QCG)
and Quick-Connect Solvent Port (QCS) male stems.
2. Close the gas valve (VG).
6. Transport cap in place over pressure relief valve (PRV).
3. Remove all customer-owned equipment.
7. Transport cover in place over pressure rupture disk (PRDA),
if applicable.
4. Disconnect the gas and solvent Quick-Connects (QCG
and QCS) and replace the dust caps on both QuickConnect male stems on the container.
8. Container dust cover placed on top of chime.
9. Tamper-evident straps in place.
29
10. Completed bill of lading paperwork attached to the
container.
• Company name and address—including the building name, if applicable.
11. Any problems with this container? If so, please refer to
Section 11.
• Contact name for shipment.
12. Carrier contacted for return shipment of container.
Date_____________________
13. Ship containers to the return address noted on the
container.
10.2
Regulatory Requirements for
Returning Containers
Empty CYCLE-TAINER systems must be returned under the
same DOT shipping requirements as full containers of the
solvent. The containers are DOT approved for shipping and
must ship as a hazardous material.
10.3
The SHaRE Program
To make the process of returning empty containers
easier, Avantor developed the SHaRE program. SHaRE is
an acronym for Shipping and Return. Through a contract
with Old Dominion Freight Line, Inc. (ODFL), you can take
advantage of Avantor’s low freight costs for the return of
empty containers. This simple and economical program
makes the return efficient and trouble-free. The steps are
listed below. For more information, please contact your local
Avantor Sales Representative or the Avantor CYCLE-TAINER
System Administrator by telephone at 1-855-AVANTOR, ext. 32675
or by e-mail at [email protected].
SHaRE Process Overview:
1. To enlist in the SHaRE program, make contact with
Avantor’s CYCLE-TAINER System Administrator and provide
your contact information and preferred billing method.
2. Empty and prepare containers for shipment in accordance
with Section 9.1 of this manual.
3. Contact Old Dominion Freight Line, Inc. by telephone at
1-800-800-7770 ext-3933 or by e-mail at AvantorSHaRE@
ODFL.com between the hours of 9 A.M. and 5 P.M. EST
to schedule a container shipment. Indicate that you are a
participant in the SHaRE program for the CYCLE-TAINER
system. ODFL’s customer service representative will need
the following information
30
• Telephone and fax number or e-mail address.
• Pick-up hours.
• Special arrangements and/or equipment needs.
• Purchase order (same PO Number provided to Avantor during enlistment.
• The total number of containers and whether they are full or empty.
• Product number and serial number of the
CYCLE-TAINER system container(s).
4. Attach completed Bills of Lading with pre-assigned pro
number (faxed or e-mailed from ODFL) to container(s).
5. ODFL will pick up containers within 48 hours and return
them to Avantor.
6. Avantor consolidates and re-bills the shipping charges on
a monthly basis.
10.4
Return Shipment of a Trial CYCLE-TAINER
System or System Accessories
The trial CYCLE-TAINER systems may be shipped back using
the SHaRE program. Contact Old Dominion Freight Line,
Inc. by telephone at 1-800-800-7770 ext-3933 or by e-mail
at [email protected] between the hours of 9 A.M.
and 5 P.M. EST and mention that you are returning a trial
container. The cost of the freight will be covered by Avantor.
Please return the Trial Container Hookup Kit and Accessories
in the chime of the container. If you have already shipped
the container, please ship the accessories back in a separate
box and note your company name and the product code
that you purchased. If hookup kits and accessories are not
returned, you will receive an invoice for their replacement. In
this situation, return all accessories to: Avantor Performance Materials
Attn: CYCLE-TAINER Prep Group
600 North Broad Street
Phillipsburg, NJ 08865
10.5
1
Product Shipping Information, Physical Data
and Container Weights Shipping Information1
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
DOT Class
3
3
3
Combustible
Liquid
Combustible
Liquid
3
3
3
6.1
3
EPA-HW
U002
U003
D001
NA
U112
D001
U154
U080
U213
U220
IMO Class
3
3
3
NA
3
3
3, 6.1
6.1
3
3
CAS
Number
67-64-1
75-05-8
68-12-2
67-68-5
141-78-6
110-54-3
67-56-1
75-09-2
109-99-9
108-88-3
UN
Number
UN1090
UN1648
UN2265
NA 1993
UN1173
UN1208
UN1230
UN1593
UN2056
UN1294
Accurate at the time of publication.
Physical Data
12
3
4
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Formula
Wt.
58.08
41.05
73.10
78.14
88.11
86.18
32.04
84.93
72.11
92.14
Boiling
Point2
56
82
153
189
77
69
65
40
65
111
Flash
Point3
-19
6
57
88
-4
-22
11
NA
-14
4
Vapor
Pressure4
31
11.8
0.53
0.08
12.6
20
17
58
22
3.8
Density1
1 L=0.791 kg
1 L=0.791 kg
1 L=0.949 kg
1 L=1.10 kg
1 L=0.900 kg
1 L=0.659 kg
1 L=0.791 kg
1 L=1.327 kg
1 L=0.888 kg
1 L=0.867 kg
Boiling Point Temperature in °C
Flash Point Temperature in °C
Vapor Pressure at 25 °C in kPa (1kPa = 7.50 torr)
31
Container Weights (in pounds)
18 L Model S
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Gross
55
55
62
68
60
50
55
77
59
58
Tare
24
24
24
24
24
24
24
24
24
24
Net
31
31
38
44
36
26
31
53
35
34
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Gross
134
133
152
169
146
119
134
195
145
142
Tare
43
43
43
43
43
43
43
43
43
43
Net
91
90
109
126
103
76
91
152
102
99
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Gross
147
146
165
182
159
132
147
208
158
155
Tare
56
56
56
56
56
56
56
56
56
56
Net
91
90
109
126
103
76
91
152
102
99
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Gross
544
540
619
690
596
481
544
798
590
580
Tare
169
169
169
169
169
169
169
169
169
169
Net
375
371
450
521
427
312
375
629
421
411
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Gross
519
517
594
665
571
456
519
773
565
555
Tare
144
144
144
144
144
144
144
144
144
144
Net
375
371
450
521
427
312
375
629
421
411
52 L Model C
52 L Model S
215 L Model C
215 L Model S
Full/Gross = product + CYCLE-TAINER system
Net = product only
Tare = CYCLE-TAINER system only
32
Container Weights (in pounds)
225 L Model C
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Gross
546
544
625
700
601
481
546
812
595
584
Tare
154
154
154
154
154
154
154
154
154
154
Net
392
390
471
546
447
327
392
658
441
430
Acetone
Acetonitrile
DMF
DMSO
Ethyl
Acetate
Hexane
Methanol
Methylene
Chloride
THF
Toluene
Gross
2676
2662
3112
3528
2977
2312
2676
4154
2944
2886
Tare
496
496
496
496
496
496
496
496
496
496
Net
2180
2166
2616
3032
2481
1816
2180
3658
2448
2390
1250 L Model S
Full/Gross = product + CYCLE-TAINER system
Net = product only
Tare = CYCLE-TAINER system only
Section 11 Maintenance and Troubleshooting
11.1
Customer Maintenance
Due to the high purity
requirements of products
shipped in CYCLE-TAINER
systems, we ask that
our customers regularly
maintain the physical
cleanliness of containers
while in their care. This
would include:
WARNING: Never tamper with the
container components. Promptly report
any container malfunctions to Customer
Service at 1-855-AVANTOR.
CAUTION: Tampering with container may
result in a severe health hazard.
• Storage indoors whenever possible in cool, clean, covered areas.
• Periodic exterior wipe downs of the containers to remove any accumulated dirt or dust.
• All customer labels should be placed on the protective
plastic sleeve only and not directly on the metal surface of the container. Examples: Quarantine, QC, in-plant destination or other labels not affixed by Avantor.
Other maintenance, such as tampering with dispense head
seals, relief valves, gauges, tightening of valve stem or
removal of dispense head from the container should never
be attempted. Such tampering may invalidate container
compliance with DOT/UN codes rendering the container
un-shippable or result in charges for parts replacement and
container refurbishing.
11.2
Container Malfunctions
If any components of a CYCLE-TAINER system malfunction:
1. Refer to Section 11.3 to find a potential remedy for the
problem.
2. Visit our online customer support portal at
www.askavantor.com and search our knowledgebase of
technical information related to CYCLE-TAINER systems to
find a remedy for the problem.
3. Contact our technical support group for assistance online
at www.avantormaterials.com/askavantor or by calling
1-855-AVANTOR.
33
11.3
CYCLE-TAINER System Troubleshooting Guide
Problem
Caused by
Resolution
Product purity fails
specifications
When sampled directly from
the container
Contamination in the sampling
device
Resample the container. Make sure your sampling apparatus
has been thoroughly flushed or rinsed with the product you are
using.
specifications
When sampled directly from
the container
Problem with analytical
methods or techniques
Contact the Technical Services department to obtain the
analytical method used by Avantor. Resample and retest using
the same analytical method used by Avantor.
specifications
When sampled at point of
end use, i.e., after solvent has
flowed through your
plumbing system.
Contamination within the
plumbing system
Sample material directly from the container and analyze. If the
sample meets requirements, there is contamination within your
plumbing system. Flush your plumbing lines thoroughly with the
product and purity grade you will be using. Continue flushing
until it meets analytical specifications at the end use location. For
new plumbing installations, see note below. Note: Most valves,
fittings, and regulators contain trace amounts of lubricants when
received from the factory. We recommend disassembly and
thorough cleaning of these items with the product you will be
using before their installation in your system.
Product flow problems
No or low product flow
No or low inert gas supply
Check the pressure gauges on gas cylinder or source to ensure an
adequate supply is available. Replace the gas tank, if needed.
Gas or solvent supply valves
closed
Check to ensure the gas and solvent valves in your system are
open. Open the valves, if needed.
Pressure regulator malfunction
Check both the inlet and outlet pressures on all solvent and
gas regulators. Adjust pressure regulator controls. If adequate
pressure is seen on inlet side of regulator and outlet pressure
does not respond to adjustment, repair or replace regulator.
Clogged in-line gas or solvent
filter
Check all solvent and gas filters for proper flow. Replace any that
might be clogged or malfunctioning.
Obstruction in solvent lines
Verify the solvent flow at various points throughout your
plumbing system. Start with a point closest to the container
and work your way toward the dispensing area. This will help
you pinpoint the area that is obstructed. Repair or replace any
obstructed tubing and/or pipes.
Malfunctioning Pressure
Relief Valve or Rupture Disk
Assembly
Check to see if gas is leaking from the PRV or PRDA. If gas is
leaking from these areas turn the gas supply off and contact
Avantor Technical Service Department for assistance.
Gas, instead of solvent, is
discharged from the container
dispenser
Empty CYCLE-TAINER
container
Check to see if there is any solvent left in the container. If it is
empty, replace the empty container with a full container.
Excessive gas bubbles in
product supply lines
The type of inert gas used
(Argon, helium, nitrogen)
Check to see which type of gas is being used. Argon is the least
soluble of the three recommended gases. If helium and nitrogen
are being used and excessive bubbling is observed, try argon gas
since it is least likely to cause bubbling.
Outgassing of dissolved gas
from the solvent
Pressurize and dispense product from the CYCLE-TAINER
containers at the same temperature as the end use. Cool
temperatures at a storage and pressurization point promote
higher gas solution. This can result in outgassing (bubbles) at a
warmer end use location.
Gas pressure is too high
If solvent pressure regulation is used in your system, minimize
the pressure drop between the container gas pressure and the
regulated solvent pressure. If the container gas pressure is too
high, it unnecessarily increases gas solution in the product.
from the solvent
Install a gas accumulator in your solvent line as close to the point
of end use as practical.
34
Problem
Caused by
Resolution
from the solvent
Install a 1 micron or smaller dispersion filter in the solvent line.
Incorrect container
instrument readings
Volume readings are erratic or
display is blank on the Liquid
Level Indicator (LLI) cube
Incompatible LLI cube for the
container
Check the label on the front of the LLI to see which container
type (C or S) the cube is designed for. If the label says S, then a
type S container must be used. If the cube is labeled type C, then
it should only be used with a type C container.
Incorrect container
instrument readings
display is blank on the LLI
Poor plug connection
Check to ensure male and female connectors on the container
and LLI signal line are properly mated. Reconnect the cable, if
needed, to re-secure the connection.
Incorrect container
instrument readings
Bent pins on the LLI cable
Check to ensure male connectors on the LLI signal line are not
bent or broken. If they are bent or broken, please call Avantor
Customer Service at 1-855-AVANTOR for a replacement.
Incorrect container
instrument readings
Dead batteries
Open the Indicator by
unscrewing the four
recessed screws on the
front panel. Replace the
two batteries with 9-volt
alkaline batteries.
CAUTION: Do not
tamper with or remove
electronic chip from
its holder. Reattach front
panel.
Incorrect container
instrument readings
Pressure gauge reads zero
upon container receipt
Conditions during transit
Container is shipped with a blanket of high purity gas on the
solvent. Gas going into solution and temperature fluctuations
during transit may cause the gauge to read near zero (0). The
solvent integrity will be maintained as long as the container will
hold pressure upon use.
Incorrect container
instrument readings
Pressure gauge reads zero
upon applying gas to the
container
Various
Refer to "product flow problems" above.
Quick-Connect problems
Quick-Connects will not easily
connect or will not connect
at all
Vapor lock
Hydroscopic pressure between the valve and the male stem
may have built up. Open the valve and let the container sit a few
minutes. Then try to reconnect the Quick-Connects.
Quick-Connect problems
Quick-Connects will not easily
connect or will not connect
at all
Incompatible Quick-Connect
bodies
For solvent connections, if the color band on the male QuickConnect stem does not match that on the female Quick-Connect
body the parts will not connect together. Use a female QuickConnect body that is the same color as the male stem.
Container malfunction
Quick-Connects or container
valves malfunction or leak
Defective or broken part or
accessory
Contact Avantor Customer Service to obtain assistance with
returning the container for repair.
Container pressure relief valve
malfunctioning or leaking
accessory
Other damages to container
(other than normal wear and
tear)
accessory
35
Section 12 Appendix
12.1
System Accessories — Items and Source Listings
Item
Part Number
Source
Female Quick-Connect Bodies
Gas Port
Solvent Ports (not for 1250 L)
High Purity Solvents
Acetone
Acetonitrile
Ethyl Acetate
Hexane
Methanol
Methylene Chloride
THF
All Reagent Grade Solvents
High Purity Solvents – 1,250 L
Acetonitrile
Methanol
Avantor Performance Materials
1-855-AVANTOR
www.avantormaterials.com
Color Code
J.T.Baker®
Part #
SWAGELOK
Part #
None
9801-00
SS-QT2-B-4PM
WHITE
BLACK
PURPLE
YELLOW
ORANGE
GREEN
BLUE
BROWN
9802-06
9802-00
9802-07
9802-04
9802-01
9802-02
9802-05
9802-03
BLACK
ORANGE
9804-00
9804-01
(¼” male NPT)
SS-QT2-B-4PMK6
SS-QT2-B-4PMK1
SS-QT2-B-4PMK7
SS-QT2-B-4PMK4
SS-QT2-B-4PMK2
SS-QT2-B-4PMK3
SS-QT2-B-4PMK5
SS-QT2-B-4PMK8
(¾” male NPT)
SS-QT8-B-12PMK1
SS-QT8-B-12PMK2
Tube Fittings (fits QT2 above) P-NPT Female
Tube’s O.D.
1/2”
1/4”
1/8”
3/4”
3/8”
1/2”
1-855-AVANTOR
Pipe Size
1/4”
1/4”
1/4”
1/2”
3/4”
3/4”
9809-03
9809-02
9809-01
N/A
9809-04
9809-05
SS-810-7-4
SS-400-7-4
SS-200-7-4
SS-1210-7-8
SS-600-7-12
SS-810-7-12
1/4”
1/4”
1/4”
Inlet/Outlet
Male NPT/Female NPT
SWAGELOK
SWAGELOK
SS-DLTM4F4A
SS-DLTS4
SS-43GF4-1466
Valves
Diaphragm Valve
Ball Valve
Inline Filters
SWAGELOK
1-908-232-4444
Compact Stainless Steel Inline Particulate Filters
Tube’s O.D.
1/2”
1/4”
Part Numbers
SS-8F-2
SS-4F-2
SS-2F-2
Filter
2 micron
2 micron
2 micron
Teflon® Tubing
Tube’s O.D.
1/2”
1/4”
1/4”
1/8”
www.plastics.saint-gobain.com
Tube’s I.D.
3/8”
1/8”
3/16”
1/16”
Part Numbers
AXH00027
AXJ00007
AXJ00011
AXJ00002
Thread Sealant Tape
800
Goldend Tape
Sealant Tape
36
A.W. Chesterton Co.
A.W. Chesterton
1/2” X 180’
1/2” X 540’
1/2” X 1296’
Part Numbers
000801
000802
000803
CYCLE-TAP DISPENSER and CYCLE-TAP Sampler
9814-24
Methanol, High Purity
toggle valve, 10 ft., orange
The J.T.Baker® CYCLE-TAP dispenser is a stainless steel solvent
dispense unit with a hose designed for unmetered manual
dispensing of solvents from the Avantor CYCLE-TAINER
solvent delivery system. The dispenser is available with either
a toggle valve for dispensing into laboratory containers or
with a needle connector to dispense into reaction vessels
for oxygen and water sensitive applications. Shown below
is a listing and description of the different configurations of
CYCLE-TAP dispensers.
9814-25
9814-26
DCM (dichloromethane)
High Purity
toggle valve, 4 ft., green
9814-27
DCM, High Puritytoggle valve, 10 ft., green
9814-28
DCM, High Puritytoggle valve, 15 ft., green
9814-29
THF, High Purity, Low Water toggle valve, 4 ft., blue
9814-30
9814-31
9814-32
THF, Ultra Low Water
needle valve, 4 ft., blue
9814-33
THF, Ultra Low Water
needle valve, 6 ft., blue
9814-34
needle valve, 4 ft., orange
9814-35
DCM, High Purityneedle valve, 6 ft., green
The J.T.Baker® CYCLE-TAP sampler is a device for sampling
small quantities of solvent from the CYCLE-TAINER system.
The sampler is designed to eliminate solvent exposure
to the atmosphere when used with a Leur lock syringe1.
Shown below is a listing and description of the different
configurations of the CYCLE-TAP sampler.
CYCLE-TAP Dispenser
CYCLE-TAP Sampler
Part #
SolventDescription
9815-01
THF, High Purity, Low
and Ultra Low Water
9815-02
Acetonitrile, High Purity,
Low WaterBlack QC
9815-03
Methanol, High Purity,
Low WaterOrange QC
9815-04
DCM, High Purity,
Low WaterGreen QC
9815-05
All ReagentBrown QC
9815-06
Hexanes, High PurityYellow QC
Part #
SolventDescription
9814-04
Acetone, High Purity
toggle valve, 4 ft, white
9814-05
toggle valve, 10 ft., white
9814-06
toggle valve, 15 ft., white
9814-07
Acetonitrile, High Purity
toggle valve, 4 ft., black
9814-08
9814-09
9814-10
Acetonitrile, low water
needle valve, 4 ft., black
9814-11
Acetonitrile, low water
needle valve, 6 ft., black
9814-12
All Reagent Grade
toggle valve, 4 ft., brown
9814-13
All Reagent Grade
Luer Lock Syringe with Valve
9814-14
All Reagent Grade
Vendor: SGE Analytical Science
9814-15
All Reagent Grade
needle valve, 4 ft., brown
9814-16
All Reagent Grade
needle valve, 6 ft., brown
9814-17
Ethyl Acetate, High Purity
toggle valve, 4 ft., purple
9814-18
9814-19
9814-20
Hexanes, High Purity
toggle valve, 4 ft., yellow
009472 (Syringe Pre-fitted with Luer Lock Valve)
1-800-945-6154
9814-21
031870 (Replacement Plunger)
9814-22
031910 (Replacement Valve)
9814-23
25MR-VLLMA-GT (Syringe Code)
Blue QC
Syringe must be purchased separately. Avantor does not sell the Leur lock syringe.
1
25 mL Syringe Pre-fitted with Luer Lock Valve
www.sge.com
Part Number: CYCLE-TAINER™ Solvent Delivery System User’s Manual
37
12.2 Container and Pallet Handling
Individual 4 L and 18 L CYCLE-TAINER system containers
can be moved to its storage or system hookup area using
a hand truck or dolly. Pallets containing multiple 4 L or 18 L
containers should be moved with an appropriate pallet jack
or motorized fork lift. A motorized fork lift or hand truck can
be used for the transport of the 215 L, 225 L, 1250 L CYCLETAINER systems. The 215 L and 1250 L systems are fitted
with two fork lift channels. There are three basic container
handling tasks that end-users and distribution partners may
need to accomplish: moving pallets of containers, lifting
containers off of pallets, and moving individual containers.
The information below will give you guidance for selecting
equipment for each of these basic tasks.
NOTE: Ensure all CYCLE-TAINER systems
are positioned upright and securely at
their storage site. Ensure all valves and
components are in the closed position
before attempting to move the container.
Prior to moving a container, please refer
to Section 8 and Section of this manual
for system shut-down and removal
guidance.
NOTE: The table listed below shows
recommendations for handling and
moving containers throughout your
facility. It is important that you
understand and follow the United States
Department of Labor Occupational
Safety and Health Administration (OSHA)
guidelines for Powered Industrial Trucks
(29 CFR 1910.178) for safe operation of
fork lifts and jacks.
NOTE: Distributors and/or end-users
must have the ability to unload common
carrier trucks. Most facilities have a
loading dock to enable unloading; it is
also possible to unload trucks from
street-level using the lifting mechanism
of a fork truck or other mechanized
lifting device. If the distributor and/or
end user is not able to unload a common
carrier truck, then a delivery truck with
a lift gate must be requested.
12.2.1 Table: Approximate weight requirement for
lifting device (based on filled containers of methylene chloride)
4L
18 L
52 L
215 - 225 L
1,250 L
Lift individual
container off of a
pallet
25 lbs.
80 lbs.
210 lbs.
800 lbs.
Not Applicable
Move an individual
container
25 lbs.
80 lbs.
210 lbs.
800 lbs.
4000 lbs.
Move a pallet of one
or more containers
300 lbs.
720 lbs.
900 lbs.
1650 lbs.
Not Applicable
38
12.2.2 Table: Recommended equipment to accomplish task
Task \ Size
4L
18 L
52 L
215 - 225 L
1250 L
(< 3750 lbs..)
1250 L
(> 3750 lbs..)
N/A
N/A
Lift individual
container off of a
pallet
Move an
individual
container
Move a pallet
with one or more
containers up to a
full pallet
IMAGE DESCRIPTIONS
Dolly - size matched for 52 L
rubbermaidforless.com
Brute 2640 Cost = $ Hand Truck - curved for cylinders
HandTrucks.com
Item# BEM058
Cost = $
Walkie Stacker
Adjustable Base legs
Can get adjustable Forks
E or EE rated
Capacity = 2,500 lb
Cost - $$
Hand Pallet Truck rated to 5,000 lbs..
Fork width = 20.5
Length = 36” – 215 L Individual move
Length = 48” - Pallet move
Capacity up to 5,000 lb
Cost - $
Walkie Stacker
Counterbalanced
E or EE Rated
Capacity = 4000 lb
Cost - $$$
4-Wheel AC Drive - Electric
E or EE Rated
Capacity = 6500 lb
Cost - $$$$
Pictures depict Toyota®1 brand mechanized devices
For more information on these products and local dealers, visit www.toyotaforklift.com.
Many other manufacturers offer similar and acceptable mechanized devices
1 – Toyota is a trademark of Toyota Jidosha Kabushiki Kaisha TA Toyota Motor Corporation Japan
It is important that you understand and follow the United States Department of Labor Occupational Safety and Health Administration (OSHA) guidelines for Powered Industrial
Trucks (29 CFR 1910.178) for safe operation of fork lifts and jacks.
39
12.3
hexane to 500-X. It is recommended that a final verification
of the system and/or components be done with the
ULTRA RESI-ANALYZED solvent to be used in the system
(Note: do not inject halogenated solvents directly into GCECD instrument).
Maintaining ULTRA RESI-ANALYZED™
Quality in Piping Systems
The quality of the ULTRA RESI-ANALYZED product is easily
affected by trace impurities present in piped transfer
systems (see chromatograms below). These impurities may
interfere with GC-ECD analyses, and to a lesser extent, trace
GC-FID analyses.
• For inert gas supply, use pressure regulators designed for
high purity gases. Diaphragms should be stainless steel with inert seals and seats.
It is practically impossible to rinse contaminated systems to
an acceptable purity level. The best approach is to design
and install a clean system. Given below are a few things that
will help ensure URA quality in the installation of the piped
system.
• Use diaphragm valves.
• Use no lubricants, cutting oils, grease, etc.
• Eliminate threaded joints, where possible.
• Do not use any pipe dope on the pipe threads. Use thread sealant tape.
• Eliminate pockets or dead legs in piping. Run piping so it can drain completely.
ULTRA RESI-ANALYZED Hexane
500-X Concentration on GC-ECD
• Use SWAGELOK® Quick-Connect fittings (QT series). These have stainless steel and wetted parts.
• Transfer hoses should be lined with a stainless steel outer braid.
• The interior material finish for dedicated piping system
finish should be at least #180 grit for valves and other equipment (foundry finish-investment casting).
• If a piping component is suspect in terms of possible
contamination, do not install it on the pipeline until its
cleanliness has been ascertained. Contaminated equipment should be cleaned with solvent or replaced.
• The following procedure may be used to verify component cleanliness.
Rinse the wetted surfaces of the component several
times with J.T.Baker® ULTRA RESI-ANALYZED grade hexane
(product number 9262). Test the final rinse with a neat
injection of the hexane on a gas chromatograph equipped
with an Electron Capture Detector (GC-ECD). Compare
this chromatogram to that of the starting solvent. Higher
levels of detection may be obtained by concentrating the
40
ULTRA RESI-ANALYZED Solvent contaminated by fluorocarbon
grease from ball valve
500-X Concentration on GC-ECD
Column: 30m, 0.53 mm ID DB-5
Oven Temp.: 40°C to 250°C
Carrier gas: Nitrogen
Flow rate: 5 mL/min.
Split Ration: 25:1
Detector: Electron Capture Detector (ECD)
12.4
CYCLE-TAINER System Weight Conversion Tables
ACETONE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Model S Model C Model S Model C Model S Model CModel S
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
Weight Volume (pounds)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
Weight Volume Weight Volume
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
272
462
592
172 2
1472
1572
4992
335
578
70 8
186 10
16110
17110
51310
388
6714
8014
195 15
17015
18015
54830
4110
7820
9120
221 30
19630
20630
57445
4713
8826
10126
247 45
22245
23245
60160
5015
9731
11031
274 60
24960
25960
62775
5518
10837
12137
300 75
27575
28575
65390
11843
13143
326 90
30190
31190
670100
12849
141 49
343 100
318100
328100 1019300
13452
147 52
370 115
345115
355115 1368500
396130
371130 381130 1717700
422145
397145 407145 2066
900
448160
423160 433160 2415
1100
474175
449175 459175 2676
1250
500190
475190 485190
527205
502205 512205
544215
519215 529215
546225
41
ACETONITRILE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
272
462
592
172 2
1472
1572
4992
335
578
70 8
186 10
16110
17110
51310
388
6714
8014
195 15
17015
18015
54830
4110
7820
9120
221 30
19630
20630
57445
4713
8826
10126
247 45
22245
23245
60060
5015
9731
11031
273 60
24860
25860
62675
5518
10737
12037
299 75
27475
28475
65290
11843
13143
325 90
30090
31090
669100
12849
141 49
342 100
317100
327100 1016300
13352
146 52
368 115
343115
353115 1363500
394130
369130 379130 1709700
420145
395145 405145 2056
900
446160
421160 431160 2402
1100
472175
447175 457175 2662
1250
498190
473190 483190
524205
499205 509205
542215
517215 527215
42
544225
CHLOROFORM
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
312
502
632
176 2
1512
1612
5032
405
698
82 8
202 10
17710
18710
52910
508
8914
10214
218 15
19315
20315
59430
5710
10820
12120
267 30
24230
25230
64345
6613
12826
14126
316 45
29145
30145
69260
7315
14431
15731
365 60
34060
35060
74175
8318
16437
17737
414 75
38975
39975
79090
18343
19643
463 90
43890
44890
822100
203 49
216 49
495 100
470 100
480 100
1475 300
21552
228 52
544 115
519115
529115 2128500
593130
568130 578130 2780700
642145
617145 627145 3433
900
691160
666160 676160 4086
1100
740175
715175 725175 4575
1250
789190
764190 774190
838205
813205 823205
871215
846215 856215
888225
43
DIMETHYLFORMAMIDE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
282
472
602
173 2
1482
1582
5002
345
608
73 8
190 10
16510
17510
51710
418
7214
8514
200 15
17515
18515
55930
45 10
8520
98 20
232 30
207 30
217 30
590 45
5113
9726
11026
263 45
23845
24845
62260
5515
10831
12131
295 60
27060
28060
65375
6218
12037
13337
326 75
30175
31175
68490
13343
14643
357 90
33290
34290
705100
14649
159 49
378 100
353100
363100 1124300
15252
165 52
410 115
385115
395115 1542500
441130
416130 426130 1961700
472145
447145 457145 2379
900
504160
479160 489160 2798
1100
535175
510175 520175 3112
1250
567190
542190 552190
598205
573205 583205
619215
594215 604215
44
625225
DIMETHYLSULFOXIDE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
292
482
612
174 2
1492
1592
5012
365
628
75 8
193 10
16810
17810
52010
438
7714
9014
205 15
18015
19015
56930
4810
9220
10520
242 30
21730
22730
60545
5613
10626
11926
278 45
25345
26345
64260
6015
11831
13131
315 60
29060
30060
67875
6818
13337
14637
351 75
32675
33675
71490
14743
16043
387 90
36290
37290
739100
16249
175 49
412 100
387100
397100 1224300
16952
182 52
448 115
423115
433115 1709500
484130
459130 469130 2194700
521145
496145 506145 2679
900
557160
532160 542160 3164
1100
593175
568175 578175 3528
1250
630190
605190 615190
666205
641205 651205
690215
665215 675215
700225
45
ETHYL ACETATE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
282
472
602
173 2
1482
1582
5002
345
598
72 8
189 10
16410
17410
51610
408
7114
8414
199 15
17415
18415
55630
4410
8320
9620
229 30
20430
21430
58545
50 13
9526
108 26
258 45
233 45
243 45
615 60
5415
10531
11831
288 60
26360
27360
64575
6018
11637
12937
318 75
29375
30375
67590
12843
14143
348 90
32390
33390
694100
14049
153 49
367 100
342100
352100 1091300
14052
159 52
397 115
372115
382115 1488500
427130
402130 412130 1885700
457145
432145 442145 2282
900
487160
462160 472160 2679
1100
516175
491175 501175 2977
1250
546190
521190 531190
576205
551205 561205
596215
571215 581215
46
601225
HEPTANE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
272
462
592
172 2
1472
1572
4992
315
558
68 8
184 10
15910
16910
51110
368
6414
7714
191 15
16615
17615
54130
3910
7320
8620
214 30
18930
19930
56345
4313
8226
9526
236 45
21145
22145
58660
4615
8931
10231
259 60
23460
24460
60875
5118
9837
11137
281 75
25675
26675
63190
10743
12043
304 90
27990
28990
646100
11649
129 49
319 100
294100
304100
946300
12352
137 52
341 115
316115
326115 1246500
364130
339130 349130 1546700
386145
361145 371145 1845
900
409160
384160 394160 2145
1100
431175
406175 416175 2370
1250
454190
429190 439190
476205
451205 461205
491215
466215 476215
491225
47
HEXANE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
272
462
592
172 2
1472
1572
4992
315
558
68 8
184 10
15910
16910
51110
368
6314
7614
191 15
16615
17615
54030
39 10
7220
85 20
213 30
188 30
198 30
561 45
4313
8126
9426
234 45
20945
21945
58360
4615
8831
10131
256 60
23160
24160
60575
5018
9737
11037
278 75
25375
26375
62790
10543
11843
300 90
27590
28590
641100
11449
127 49
314 100
289100
299100
932300
11952
132 52
336 115
311115
321115 1223500
358130
333130 343130 1513700
380145
355145 365145 1804
900
401160
376160 386160 2094
1100
423175
398175 408175 2312
1250
445190
420190 430190
467205
442205 452205
481215
456215 466215
48
481225
METHANOL
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
272
462
592
172 2
1472
1572
4992
335
578
70 8
186 10
16110
17110
51310
388
6714
8014
195 15
17015
18015
54830
4110
7820
9120
221 30
19630
20630
57445
4713
8826
10126
247 45
22245
23245
60160
5015
9731
11031
274 60
24960
25960
62775
55 18
10837
121 37
300 75
275 75
285 75
653 90
11843
13143
326 90
30190
31190
670100
12849
141 49
343 100
318100
328100 1019300
13452
147 52
370 115
345115
355115 1368500
396130
371130 381130 1717700
422145
397145 407145 2066
900
448160
423160 433160 2415
1100
474175
449175 459175 2676
1250
500190
475190 485190
527205
502205 512205
544215
519215 529215
546225
49
METHYLENE CHLORIDE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
302
492
622
175 2
1502
1602
5022
395
668
79 8
198 10
17310
18310
52510
47 8
8414
97 14
213 15
188 15
198 15
584 30
5310
10220
11520
257 30
23230
24230
62845
6213
11926
13226
301 45
27645
28645
67260
6815
13431
14731
345 60
32060
33060
71575
7718
15137
16437
388 75
36375
37375
75990
169 43
182 43
432 90
407 90
417 90
789 100
18649
199 49
462 100
437100
447100 1374300
19552
208 52
505 115
480115
490115 1959500
549130
524130 534130 2544700
593145
568145 578145 3129
900
637160
612160 622160 3715
1100
681175
656175 666175 4154
1250
725190
700190 710190
769205
744205 754205
798215
773215 783215
50
812225
TETRAHYDROFURAN
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
282
472
602
173 2
1482
1582
5002
345
598
72 8
189 10
16410
17410
51610
408
7014
8314
198 15
17315
18315
55530
4410
8220
9520
228 30
20330
21330
58445
4913
9426
10726
257 45
23245
24245
61360
5315
10431
11731
286 60
26160
27160
64375
5918
11537
12837
316 75
29175
30175
67290
12743
14043
345 90
32090
33090
692100
139 49
152 49
365 100
340 100
350 100
1083 300
14552
158 52
394 115
369115
379115 1475500
424130
399130 409130 1867700
453145
428145 438145 2258
900
482160
457160 467160 2650
1100
512175
487175 497175 2944
1250
541190
516190 526190
570205
545205 555205
590215
565215 575215
595225
51
TOLUENE
18 L
52 L
52 L 215 L
215 L 225 L 1250 L
Weight Volume
(pounds)
(Ls)
Weight Volume
(pounds)
(Ls)
(Ls)
Weight Volume
(pounds)
(Ls) Weight Volume
(pounds)
(Ls)
(pounds )
(Ls)
(pounds)
(Ls)
240
430
560
169 0
1440
1540
4960
282
472
602
173 2
1482
1582
5002
345
588
71 8
188 10
16310
17310
51510
398
7014
8314
198 15
17315
18315
55330
4310
8120
9420
226 30
20130
21130
58245
4913
9326
10626
255 45
23045
24045
61160
5315
10231
11531
284 60
25960
26960
63975
5818
11437
12737
312 75
28775
29775
66890
12543
13843
341 90
31690
32690
687100
13749
150 49
360 100
335100
345100 1070300
14252
155 52
389 115
364115
374115 1452500
418130
393130 403130 1834700
446145
421145 431145 2217
900
475160
450160 460160 2599
1100
504175
479175 489175 2886
1250
532190
507190 517190
561205
536205 546205
580215
555215 565215
52
584225
12.5 Engineering Drawings for Basic Installations
Figure 4 (Type A and B)
Facility Solvent Distribution Lines
53
Figure 5
54
Figure 6
55
Figure 7
56
12.6
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JTBaker® CYCLE-TAINER™ Solvent Delivery System

Transcription

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