Gama completa de equipos para análisis químicos de referencia
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Gama completa de equipos para análisis químicos de referencia
Gama completa de equipos para análisis químicos de referencia Dedicated Analytical Solutions Preparación de la muestra Para obtener unos buenos resultados es imprescindible preparar la muestra correctamente. La mayoría de los errores se producen en el proceso de elaboración de la muestra, mientras que los fallos en los equipos son prácticamente inexistentes. Una preparación incorrecta de la muestra ocasiona graves errores en el análisis. No existe ninguna solución estándar válida para todo tipo de muestras. La mayoría de los laboratorios precisan diferentes molinos trituradores dependiendo de la muestra y el tipo de análisis. El molino triturador, a pesar de que muchas veces no se tiene en cuenta, es un elemento importante en el proceso analítico. FOSS lo considera imprescindible, por eso lo ha incluido como parte integral del sistema analítico. Cemotec™ 1090 El sistema Cemotec ™ Sample Mill es un molino triturador especialmente diseñado para triturar el grano y las semillas de las muestras sin pérdida de humedad. Es un triturador excelente para preparar todo tipo de muestras que no requieran que el tamaño del grano sea muy fino y uniforme. • Mantiene la humedad • Aprobado por el Departamento Sueco de Agricultura Disponibles repuestos del disco de corte (10003965) y vasos de muestras de 150 ml en cajas de 100 (10003923) o en cajas de 500 (10003924). Cyclotec™ 1093 El sistema Cyclotec ™ Sample Mill es un molino triturador diseñado para triturar de forma rápida y uniforme una gran variedad de alimentos, granos, hojas... etc, además de productos químicos, farmacéuticos y similares. El sistema Cyclotec ™ nos ofrece una solución rápida y práctica para preparar con precisión muestras para una gran variedad de técnicas de análisis como por ejemplo, digestión, extracción, fibra y NIR. • Gran velocidad- 4 g/s con granos • Distribución del tamaño de la partícula poco dispersa • Válido para la preparación NIR (AOAC 4.2.10 16th ed.) Repuestos: Botellas de muestra de 125 ml (10003679) de 52 o 104 (1000893) unidades por caja. Un lio dispositivo de entrada amplio (10002485) facilita el proceso para triturar forraje, ensilaje, paja, hojas... etc. El ensamblaje de la botella (10009833) tiene una capacidad para una botella de 500 ml (10013478). A variety of blades for different applications. Homogeneizador 2094 (monofásico, 1500 rpm) Homogeneizador 2096 (trifásico, 1500/3000 rpm) Los Homogeneizadores 2094 y 2096 están diseñados para macerar y homogeneizar una gran variedad de muestras altas en grasas, fibra y humedad en unos 20-60 segundos. Ejemplos de aplicación: reducción del forraje, de la comida seca y productos químicos; homogeneización de carne, pescado, fruta, verduras y comida precocinada, incluyendo pizza, empanadas y comida congelada. • Muestras desde 0,2 a 2,5 kg (3,5 kg con el Homogenizador 2096) • El diseño de las cuchillas aseguran la homogenización vertical y horizontal. • Modo a pulsos para tratar las muestras congeladas. Knifetec ™ 1095 ( 20.000 rpm, refrigerado) El sistema Knifetec ™ 1095 Sample Mill es un molino triturador que ha siso diseñado para preparar muestras con alto contenido en grasa, humedad y fibra como por ejemplo: semillas y plantas oleaginosas, comida precocinada, cárnicos, fruta, verduras, granos, semillas, piensos y comida de animales domésticos. • Triturador de alta velocidad con cronómetro automático. • 100 ml de muestra en 2,5 o 10 ciclos de segundos. Selección del rotor de cuchillas para diferentes aplicaciones estándar- 10005980 incluido, afilado- 10008651, pequeño- 10013135 y gránulos- 10013136) y bandeja de acero inoxidable ( 10008467). Para más información sobre molinos trituradores consulte la hoja de datos 99990730. Digestión El sistema de digestión Tecator ™ para Kjeldahl y otros procesos de mineralización o reflujo se compone de un digestor con un control de precisión de la temperatura, hasta 440ºC, y soportes de 8 o 20 tubos de 100 ml o 250 ml . Para cumplir la normativa BPL (Good Practice Laboratory) y Salud y Seguridad (H&S) recomendamos que los digestores se usen junto con el colector del extractor de humos o el cabezal de reflujo, ambos situados en la cabina de gases. El soporte de tubos, el extractor o el cabezal de reflujo se colocan encima del digestor sin ocupar un espacio adicional en el laboratorio. Sistemas autoelevadores Los sistemas autoelevadores facilitan los procesos automatizados y eliminan el peso y el riesgo que conlleva el manejo de productos químicos calientes. El soporte de 8 o 20 tubos se coloca en el elevador. La aplicación seleccionada en el software controla por completo todo el proceso. El exhaust se acopla con el soporte de tubos según desciende hasta el digestor pre-calentado y el Scrubber, en caso de estar conectado, se pone en marcha. El software de comunicación del digestor con el PC es bidireccional por medio del cable RS232 que se incluye con el sistema. También se puede conectar con un módulo opcional Bluetooth. Es posible registrar constantemente datos de tiempo, temperatura, aplicación que se usa, operador, número de lote y número de identificación. Sistemas de soportes “autorack” Cuando se usa un sistema de soporte autorack en lugar de un sistema autoelevador se sigue el mismo procedimiento que en el sistema autoelevador, exceptuando que en el sistema autorack la colocación del exhaust en el digestor y su separación se hace de forma manual al oír la señal. La aplicación seleccionada controla todas las funciones al igual que en el sistema autoelevador. Sistemas básicos La temperatura y el tiempo para el proceso de digestión se seleccionan en el panel principal. Todos los demás procedimientos, incluyendo la conexión de la unidad de limpieza, son manuales. Sistemas de extracción y contención de humos Los sistemas de extracción de humos especialmente diseñados para cada Unidad de Digestión facilitan la eliminación y contención de humos. Recomendamos su uso en todos los procesos de digestión, evita el tener que reemplazar la cabina de gases. Se recomienda el uso de los sistemas de digestión y extracción de humos dentro de cabinas de gases. De esta forma cumple con la normativa BPL (Good Practice Laboratory) y de Salud y Seguridad (H&S). Unidad de Neutralización y Limpieza de humos (Scrubber) La Unidad Scrubber de Tecator ™ es compacta, de succión independiente y por tanto no se ve afectada por el flujo de agua. Durante la digestión los gases ácidos se eliminan mediante la Unidad de Neutralización/Limpieza. Primero los vapores se condensan y se diluyen en una amplia trampa para ácidos, después, se limpian y se neutralizan antes de pasar por una segunda trampa para ácidos que protege la bomba de vacio en caso de que los neutralizantes se agoten. Después el aire limpio sale por la salida del tubo. Para cumplir con la normativa BPL (Good Practice Laboratory) y de Salud y Seguridad (H&S) dicho tubo de ventilación debería orientarse a la cabina de gases. Cuando el Scrubber se conecta a un sistema automático el programa controlará por completo toda la función incluyendo los ajustes de mayor o menor aspiración. Para más información sobre la gama de digestores consulte la hoja de datos 99990720. Destilación Las sistemas Kjeltec han sido diseñados para conseguir la mayor precisión posible en los análisis Kjeldahl y otras destilaciones. Para cumplir con los diferentes requisitos analíticos, la gama Kjeltec incluye una gran variedad de equipos, desde unidades simples de destilación hasta sistemas con automuestreador completamente automáticos. La prestación patentada SAFE (Steam Addition for Equilibration) reduce la capacidad de reacción entre los ácidos concentrados y el álcali. Todos los equipos tienen un cabezal de expansión de polipropileno resistente al álcali y bombas de fuelle para dispensar reactivos con precisión. Las aplicaciones químicas optimizadas le proporcionan un coste muy reducido en cada análisis realizado. Kjeltec ™ 2100 Es una unidad económica y semiautomática para análisis Kjeldahl y otras destilaciones químicas como por ejemplo, dióxido de azufre, alcohol, fenoles, ácidos volátiles...etc. La muestra digerida en el tubo se puede diluir manualmente, en caso necesario, y luego se coloca en la unidad. El álcali (u otro reactivo) se dispensa automáticamente iniciándose la destilación automática que se produce durante el tiempo seleccionado. Una válvula de antiretorno evita que el destilado retroceda al final del ciclo. La muestra destilada se valora manualmente o con un valorador externo. Para más información sobre Kjeltec ™ 2100 consulte la hoja de datos 99990217. Kjeltec ™ 2200 Es una unidad versátil y completamente automática para el análisis Kjeldahl y otras destilaciones . El tubo que contiene la muestra digerida se coloca en la unidad y se cierra la puerta de seguridad. El sistema diluye automáticamente la muestra, controla el agua de refrigeración, añade álcali (u otro reactivo), destila la muestra en el periodo de tiempo seleccionado y vacía el vaso de reactivo al final del ciclo. Se puede añadir solución receptora de forma automática con el kit opcional (10000041). Una válvula de antiretorno evita que el destilado retroceda al final del ciclo. La muestra destilada se valora manualmente o con un valorador externo que se puede conectar con el kit opcional (10011403). Para más información sobre Kjeltec 2200 consulte la hoja de datos 99990213. Kjeltec ™ 2300 Es un analizador completamente automático para el análisis Kjeldahl y otros procesos similares..Incluye todas las prestaciones el Kjeltec ™ 2200 además de la valoración automática on-line que se produce simultáneamente a la destilación, ahorrando de este modo un tiempo valioso. Los resultados aparecen en pantalla en las unidades deseadas. La impresora opcional (10007913) le proporciona una copia impresa de los resultados. Permite descargar datos a un PC . Un test de recuperación incorporado permite validar los resultados con patrones conocidos para que de este modo genere datos fiables. Para más información sobre Kjeltec 2300 consulte la hoja de datos 99990214 Kjeltec ™ 2400 con Autosampler (Automuestreador) automático de 60 muestras Es un analizador completamente automático con automuestreador para el análisis automático de las digestiones Kjeldahl y otros procesos similares. El analizador Kjeltec ™ 2400, sin muestreador, tiene las mismas prestaciones que el analizador Kjeltec ™ 2300 además de la posibilidad de añadir el muestreador y la conexión a una balanza de precisión. El Autosampler 2460 tiene capacidad para tres gradillas de veinte muestras. Se pueden añadir gradillas nuevas en cualquier momento y analizar muestras urgentes independientes. Una vez que todas las muestras se han procesado el sistema realiza de forma automática un ciclo de limpieza antes de apagarse. Para más información sobre Kjeltec 2400/2460 consulte la hoja de datos 99990218 Equipos para extracción con disolvente e hidrólisis La gama de equipos de extracción Soxtec ™ es muy amplia, desde el sistema básico Soxtec 2045- de dos posiciones manual, hasta el sistema totalmente automático Soxtec 2050 de seis posiciones. En todos los casos las muestras se manejan por lotes para que el proceso de análisis sea lo más fácil y seguro posible. No importa el tipo de extracción que requiera su sistema Soxhlet, siempre tenemos la solución adecuada que puede reemplazarlo consumiendo menos disolvente y entre tres y cinco veces más rápido. No existe ningún otro extractor Soxhlet que gaste tan poco disolvente. Normalmente, gracias a la recuperación de disolvente, se consumen solo unos 16 ml de disolvente por muestra, lo que reduce el coste por prueba y la eliminación de disolvente. La seguridad siempre ha sido muy importante para nosotros, por tanto, la única parte eléctrica de la unidad de Extracción, que es la placa caliente, está diseñada a prueba de chispas. Los sensores dobles de seguridad evitan que, en ningún caso, se alcance la temperatura de ignición del disolvente.. Soxtec ™ 2045 – Sistema de extracción manual de 2 muestras Incluye una unidad de extracción de 2 muestras y una unidad de control independiente. Emplea de 50 a 60 ml de disolvente por prueba (se recupera hasta el 80%). El sistema estándar incluye: Vasos de extracción de aluminio (juego de 2) Dedales de celulosa de 33 mm (65 ml) caja de 25 Opcional: Vasos de extracción de cristal (juego de 2) Dedales de celulosa de 45 mm (120 ml) caja de 25 Dedales de celulosa de 26 mm (30 ml) caja de 25 Para más información sobre Soxtec 2045 consulte la hoja de datos 99990310. Soxtec ™ 2043 – Sistema de extracción manual de 6 muestras Incluye una unidad de extracción de 6 muestras y una unidad de control independiente. Emplea de 40 a 50 ml de disolvente por prueba (se recupera hasta el 80%). El sistema estándar incluye: Vasos de extracción de aluminio (juego de 6) Dedales de celulosa de 26 mm (30 ml) (caja de 25) Opcional: Vasos de extracción de cristal (juego de 6) Para más información sobre Soxtec 2043 consulte la hoja de datos 99990312 Soxtec ™ 2055 – Sistema de extracción semiautomática de muestras Incluye una unidad de extracción de 6 muestras y una unidad de control independiente y programable. Emplea de 70 a 90 ml de disolvente por prueba (se recupera hasta el 80%) El sistema estándar incluye: Vasos de extracción de aluminio (3 juegos de 6) Dedales de celulosa de 33 mm (65 ml) (caja de 25) Opcional: Vasos de extracción de cristal (juego de 6) Dedales de celulosa de 26 mm (30 ml) (caja de 25) Para más información sobre Soxtec 2055 consulte la hoja de datos 99990306. Soxtec ™ 2050 – Sistema de extracción automática de 6 muestras Incluye una unidad de extracción de 6 muestras, una unidad de control independiente y programable y una unidad de operación para facilitar el proceso automático. Emplea de 70 a 90 ml de disolvente por prueba (recuperación de hasta el 80%). El sistema estándar incluye: Vasos de extracción de aluminio (3 juegos de 6) Dedales de celulosa de 33 mm (65 ml) (caja de 25) Para más información sobre Soxtec 2050 consulte la hoja de datos 99990306. SoxCap ™ 2047 – Sistema manual de hidrólisis ácida de 6 muestras. Análisis de grasa total. El sistema SoxCap ™ 2047 forma parte de los sistemas Soxtec ™. Dicho sistema permite determinar la grasa total siguiendo los métodos reconocidos. El sistema SoxCap realiza la hidrólisis, filtración y lavado sin ninguna transferencia de muestra. Esta técnica patentada ofrece un alto rendimiento y evita, en la mayoría de los casos, la manipulación manual usando herramientas para el manejo por lotes. El sistema SoxCap es compatible con Soxtec 2045, 2050 y 2055. Para más información sobre SoxCap 2047 consulte la hoja de datos 99990311. Análisis de fibra cruda, detergente y alimentaria Con los métodos tradicionales de análisis de fibra hay que realizar repetidos tratamientos de la muestra, transferir y filtrar, así como manejar varios reactivos, en ocasiones calientes. Cada uno de estos procesos implica un margen alto de error y un riesgo para el usuario. Los sistemas Fibertec ™ reducen el porcentaje de error y mejoran la seguridad. La muestra no sufre ninguna transferencia durante todos los procesos lo que reduce la manipulación de reactivos y se asegura la filtración rápida y eficaz usando los sistemas integrados de vacio y presión. Los sistemas de análisis de fibra cruda y detergente relacionados con la nutrición animal y la fibra dietética son la solución a sus necesidades. Sistema Fibertec™ 2021/2023 Fibercap de 6 o 18 muestras Los sistemas manuales de bajo coste se basan en el principio de una única cápsula de inmersión para determinar las fracciones de fibra cruda o detergente (NDF, ADF Y ADL) siguiendo los procedimientos oficiales según lo indica la normativa AOAC, ISO, AACC, AOCS y EC. Para más información sobre Fibertec 2021/2023 consulte la hoja de datos 99990407. Fibertec™ M6- Sistema manual de 6 muestras Determina la cantidad de fibra según Weende, Van Soest, etc, incluyendo el proceso de ebullición usando reactivos externos precalentados, el proceso de aclarado y filtración en condiciones de reproducibilidad controladas. Incluye las siguientes unidades: Fibertec ™ 1020 Hot Extraction Unit – Sistema de extracción en caliente de 6 muestras para hidrólisis y extracción con sistemas integrados para calentar y filtrar reduciendo el contacto con los reactivos. Fibertec™ 1021 Cold Extraction Unit – Sistema de extracción en frío de 6 muestras para desengrasado y extracción a temperatura ambiente, por ejemplo, determinación de lignina y desengrasado de residuos de fibras. Para más información sobre Fibertec M6 consulte la hoja de datos 99990401. Fibertec™ 2010 – Sistema automático de 6 muestras El sistema Fibertec ™ 2010 se compone de los siguientes módulos básicos: Fibertec ™ 2010 Hot Extraction Unit- Sistema de extracción en caliente para los procesos de hidrólisis y filtración con precalentamiento automático y adición de reactivos, ebullición y filtración. El sistema cumple los requisitos del inicio del tiempo de ebullición para fibra cruda siguiendo la normativa ISO y EC. La unidad controla de forma automática el agua de refrigeración. Fibertec ™ 1021 Cold Extraction Unit- Sistema de extracción en frío de 6 muestras para desengrasado y extracción a temperatura ambiente, por ejemplo, determinación de lignina y desengrasado de residuos de fibras. Para más información sobre Fibertec 2010 consulte la hoja de datos 99990405. Fibertec™ E El sistema Fibertec ™ E ha sido diseñado para determinar de forma rápida y práctica la cantidad total de fibra alimentaria soluble e insoluble según los métodos enzimáticos establecidos, incluidos los aprobados por AOAC, AACC, NMKL y Asp. También es un sistema práctico en la preparación de la muestra para realizar estudios detallados de las fracciones de fibra, por ejemplo, mediante técnicas colorimétricas o cromatográficas. El sistema incluye: una Unidad de Filtración para filtrar varias fracciones de forma rápida durante el análisis; la unidad Shaking Water Bath 1024, baño de agua con agitación, empleado para los procesos incubación enzimática. Se requiere también un sistema de baño maría ( no incluido). Para más información sobre Fibertec E 1023 consulte la hoja de datos 99990403. Análisis mediante sistemas de inyección de flujo (FIA) La unidad FIAstar 5000 es un sistema totalmente automático para determinar la cantidad de amonio, nitrato/nitritos, nitrógeno total, fosfatos, fósforo total y otros parámetros mediante métodos utilizados y aprobados por la normativa ISO. Se pueden analizar hasta 3 parámetros de forma simultánea. Cada analizador lleva incorporado un detector digital de doble longitud de onda para suprimir el efecto de índice de refracción y las burbujas de aire, un termostato, una válvula de inyección y una bomba. Todo el sistema se controla mediante el software SoFIA ™ en Windows ®, incluyendo los ajustes rutinarios según la normativa ISO 8466. Sistema FIAstar™ – mono canal Sistema básico para analizar un parámetro con presentación manual de la muestra. Se pueden determinar diferentes parámetros intercambiando el casete de método. Es necesario un PC para que funcione el software y el sistema. Requisitos del PC PC con Windows 98, 2000 o XP. Al menos 32 Mb de memoria RAM y 40 mb de espacio disponible en el disco duro, diskette de 1,44 mb o CD. Puerto USB para cada módulo FIA que se conecte. Puerto RS232 para conectar el Sampler 5027 (Muestreador 5027) Puerto adicional RS 232 para transferir datos a LIMS. Casetes de método “conectar y analizar” Los casetes de método configurados previamente se insertan y/o se intercambian fácilmente en el modulo, la conexión y desconexión es simple y rápida.. Tan solo se tarda unos minutos en iniciar y cerrar el sistema. Existe un casete de método en blanco para configurar aplicaciones especiales. Sistema FIAstar™ – 3 canales con Sampler (Muestreador) Sistema completamente automático para analizar 3 parámetros simultáneamente en una única muestra. Gracias a la función stand-by se alarga la duración de los tubos de la bomba y se ahorra una gran cantidad de reactivos (< 3 ml de reactivo/ 24 h), teniendo la posibilidad de realizar el análisis automático y desatendido incluso durante toda la noche. Autosampler 5027 (Automuestreador 5027) Bandejas de muestras: para 64 o 120 muestras Bandeja segmentada: 4 rejillas individuales Tamaño de la muestra: 12,30 ml Bandeja lateral: 10 posiciones para patrones y QC Software SoFIA Puntos de calibración: hasta 10 patrones Ajuste de la curva de calibración: lineal o de segundo orden según la normativa ISO Rutinas de seguridad y buen uso del laboratorio: comprobar las muestras, ejecutar muestras múltiples y estándar, recalibración automáti ca, advertencias de ausencia de reactivo, de muestra y fuera de rango. Biblioteca de méto dos predefinidos. Para más información sobre FIAstar 5000 consulte la hoja de datos 99990912. Consumibles, accesorios y piezas de repuesto We consider consumables, accessories and original spare parts as an integral part of our support to our customers. Everything is specially designed and manufactured to fit your systems and to ensure safe, accurate and simple laboratory work. Kjeltabs Amplia selección de catalizadores en forma de pastilla para los procesos de digestión ácida. Tubos de digestión y destilación para Kjeltec™ Los tubos para Kjeldahl y otros análisis se emplean en los sistemas de digestión Tecator ™ y Kjeltec . Capacidad disponible: 100,250 y 750 ml. Paredes rectas, aforados y juntas esféricas. Dedales de celulosa para Soxtec™ Celulosa pura de grosor simple o doble. Disponible en 26 (30), 33 (65) y 45 (120) mm (ml). Versión de pureza extra para aplicaciones medioambientales. FiberCap™ para Fibertec 2021/2023 Cápsula de un solo uso para mayor seguridad , rapidez y simplificar el análisis. Disponible en envases de 100 y 500. FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk FOSS ESPAÑA Josep Tarradellas, 8-10 08029-Barcelona Tel. 934949940 Fax: 4052176 [email protected] Catálogo de consumibles, accesorios y piezas de repuesto Para facilitarle la búsqueda de nuestros productos y resolver sus necesidades de recambios y consumibles, en este catálogo encontrará los listados por grupos de productos de los componentes para sus sistemas CA, incluyendo los correspondientes a equipos discontinuados. P/N 9999 0502, Issue 1 ES, Oct 2005 Crisoles para Fibertec™ Crisoles de cristal de varias porosidades para Fibertec™ M6, 2010 y 1023. Compass Software de gestión de datos Software Compass para el registro rápido y fiable y trazabilidad de las muestras según las rutinas GLP, incluyendo la conexión sin problemas de todos los periféricos, como balanza, impresora y PC, con independencia del fabricante El complemento perfecto para su nuevo KjeltecTM 8400. Características •Registro de muestras, incluyendo identificación •Instrumentos controlados desde PC •Conforme a rutinas GLP •Impresión de informes •Exportación de datos, por ej. a Word, Excel, Acrobat •Importación/exportación LIMS •Conectable en red, visión de resultados en varias estaciones •Conexión simple a periféricos Descripción: El analizador Kjeltec™ 8400 tiene dos sistemas de software distintos. Uno es el software incorporado que controla el análisis y contiene todas las funciones necesarias para manejar el sistema en el día a día. Este sistema se instala en fábrica en el analizador. Dedicated Analytical Solutions El otro es un sistema opcional, Compass (Composition Analysis Software System), una aplicación de PC. Este software maneja el analizador Kjeltec 8400 y el muestreador, si existe, permitiendo el registro rápido y fiable y el rastreo de muestras según las rutinas GLP, incluyendo la conexión sin problemas de todos los periféricos, como balanza, impresora y PC, con independencia del fabricante . Compass proporciona una comunicación bidireccional con el analizador a través de Ethernet con comandos de usuario. Esta comunicación también facilita la conexión a diversos paquetes LIMS (Sistema de gestión de información de laboratorio, Laboratory Information Management System) propietarios o personalizados. Las tareas realizadas con frecuencia se pueden realizar rápidamente utilizando las nueve teclas de acceso directo de la barra de herramientas de comandos. A estos comandos se puede acceder también desde el menú principal. Aplicación Compass • Windows® 2000 Service Pack 4/Windows® Server 2003 Service Pack 1/Windows® XP Service Pack 2/Windows® Vista con SP 1 • Pentium III 600 MHz o superior (recomendado 1 GHz) • 192 MB RAM (recomendado 512 MB) • 1025 MB de espacio disponible en el disco duro • Un puerto Ethernet para comunicación con el Analizador Base de datos de Compass • Windows® 2000 Service Pack 4/Windows® Server 2003 Service Pack 1/Windows® XP Service Pack 2/Windows® Vista con SP 1 • .NET Framework 2.01) • Microsoft SQL Server 2005 Express • Pentium III 600 MHz o superior (recomendado 1 GHz) • 192 MB RAM (recomendado 512 MB) • 1025 MB de espacio disponible en el disco duro • Un puerto Ethernet para comunicación con la aplicación Compass 1) Se puede descargar de la página web de Microsoft®. .NET Framework 2.0 debe instalarse antes que Microsoft® SQL Server 2005 Express FOSS Analytical Slangerupgade 69 DK-3400 Hilleroed Dinamarca Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk Comunicación con la balanza: El PC debe conectarse a la balanza mediante un cable serie (RS-232) (no incluido) según las especificaciones del fabricante de la balanza para la comunicación con el PC. Los comandos enumerados son compatibles con los siguientes modelos de balanzas: Modelos Sartorius A120S, A200S, A210P GetWeight: ESC P CR LF GetStableWeight: ESC P CR LF Modelos Sartorius CP, GC y GP GetWeight: ESC P CR LF GetStableWeight: ESC P CR LF Modelos Mettler Toledo Excellence Plus XP (XP105DR, XP205, XP205DR, XP204, XP504, XP504DR) GetWeight: SI CR LF GetStableWeight: S CR LF Comunicaciones LIMS Exportación de datos de resultados a archivos con formato *.txt, *.xml o *.csv para lectura por LIMS Importación de datos de muestras de archivos con formato *.xml creados por LIMS Cables necesarios, no suministrados en el paquete Compass: • Cable serie – (RS-232) conexión a la balanza conforme a las especificaciones del fabricante de la misma • Cable de red – Instalación en red • Cable cruzado – Conexión directa al Analizador P/N 1026228, Edición 1 ES, Enero 2009 Número de pedido: 60031632 Compass Data Management Software Requisitos de sistema del PC: Por favor, tenga en cuenta que los requisitos indicados a continuación son únicamente para la Aplicación/Base de datos Compass y que los requisitos del sistema operativo del usuario podrían ser superiores. Tecator™ Digestion Systems Tecator™ Digestion Unit Auto Lift 20 together with the Scrubber, for fully unattended operation. Features and benefits: Tecator™ Digestion units, with integrated programmable controllers, can be combined with a range of accessories offering: • fully automated digestion with user interface adapting to actual product configuration • convenient, safe and flexible operation • GLP-support through two way PC communication • economy of chemicals, energy, labour, space and time • efficient fume containment through optional exhaust • efficient fume removal through optional scrubber The systems, with extensive application support, are compatible with Kjeltec™ Distilling Units. General Description: The products described in this brochure can be combined to match individual needs, from units capable of handling just a few samples a day up to fully automated systems for high sample throughput. Three configurations; Auto Lift, Auto Rack, and Basic; are available for either 250 ml or 100 ml digestion tubes; which must be specified when ordering; dependant on the application required. A Digestion System is based on a Digestion Unit and tube rack with capacity for either eight or twenty tubes. For most Kjeldahl digestions straight 250 ml tubes are recommended. To comply with GLP and Health & Safety requirements we recommend that all Digestion Units are used with an Exhaust Manifold or Reflux Head, and are located in a fume cupboard. An optional Scrubber Unit creates a fully integrated system. Dedicated Analytical Solutions Auto Lift versions, with exhaust docking facility, allow fully automated unattended operation contributing to safety and convenience by eliminating handling of hot chemicals and saving valuable bench space. Auto Rack versions allow automated digestions but require manual placement of Tube Rack and Exhaust Manifold which are stored above the Digestion Unit in a similar position to the Auto Lift. All Auto models have an integrated programmer which precisely controls temperature(s) and timing together with connected components. The analysis cycle is clearly monitored on the graphical display. Auto models can be connected to a PC for data logging and downloading of standard, and user defined, applications. The programmer has various password protected access levels to prevent unauthorised modification and comply with accreditation procedures. Basic versions have built in, user definable, temperature and time control clearly viewed on the display. Auto Rack versions can be upgraded to Auto Lift systems to spread the investment across fiscal periods. The Basic version can be fitted with a rack system at any time to save valuable bench space. Various accessories are available to make routine analysis safe and simple. They include a range of test tubes, tube racks, retainer plates for washing, fume removal systems, boiling rods and catalyst tablets. Digestion system products and accessories are described in more detail on the following pages. All Digestion Systems are based on one of the “four” Digestion Units for either 250 ml or 100 ml tubes*. * Tube volume to be specified when ordering your digestion unit. Digestion Units The Digestion Units are insulated to minimise heat transfer to the surroundings and allow fast, even heating, thus giving good working conditions as well as saving energy. They are designed for batches of either eight or twenty test tubes with three different levels of control. The Auto versions have an integrated all activity controller, that adapts to the actual product configuration and is programmable using the software supplied. When a Lift or Scrubber Unit is connected they are controlled by the selected application program, which is stored in the Digestion Unit memory, allowing fully unattended operation. The Basic versions have a built in, user definable, time and temperature controller and display. Software for Auto Lift and Auto Rack systems There are two separate software systems in Auto versions. The embedded software controls all necessary functions of the digestion system on a routine basis. The PC Application software, delivered on CD, is system management software which enables default values to be modified according to the needs of the authorised user. To process different type of samples a wide range of Tecator™ applications can be downloaded from the database included on the CD. Up to 254 Applications can be stored in the digestion unit at any one time, of which half can be standard Tecator™ format and half can be user defined. Each application can control up to 23 steps including all Temperature; ramp and time; Lift and Scrubber steps. The software supports Good Laboratory Practice (GLP) routines and accreditation procedures. Data for date, time, temperature, application used, operator, batch number, and ID number are constantly logged. The 32 most recent Data Logs can be stored in the Digestion Unit. All this information can be transferred to a PC for archiving and generation of up to seven different reports. Original Tecator™ Applications cannot be changed. They can be adapted and saved as different files or the user can design their own applications. To prevent unauthorised changes, and comply with GLP routines, the software is password protected at different authority levels. Audible alerts Audible ‘’ready’’ or ‘’cycle over’’ alerts advise the user when the digestion application is completed Audible ‘’alarm’’ alerts advise the user when errors/interruptions occur within the running application program Alerts can be adjusted High, Low or Off. Power failure or interruption of power supply In the event of power failure the digestion unit operation is automatically handled in the safest way. If the failure or interruption occurs at any time up to or during preheating, before digestion has started, the cycle will continue when power is restored. Following a power failure or interruption, after the digestion cycle has started, the unit stops heating immediately and the Lift goes to the cooling position with exhaust in place, upon restoration of power. This complies with GLP and Health & Safety routines. These interruptions will be recorded in the data logging function. Communication with PC The PC Application software has two way communication with the Digestion Unit via the serial RS232 cable supplied as standard. Alternatively communication can be achieved through Bluetooth TDK blu2i modules, or equivalent, available from your computer supplier. Language versions The software is available in the following languages:Chinese (simplified), Dutch, English, French, German, Italian, Japanese, Korean, Polish, Russian, Spanish, and Swedish. Other languages can be accommodated in co-operation with your local supplier. Auto Lift Systems Auto Lift systems facilitate highly automated procedures, eliminating heavy and risky handling of hot chemicals. Valuable bench space is saved, as the Tube Rack and Exhaust Manifold are positioned above the Digestion Unit. A Tube Rack with 8 or 20 tubes is placed in the Lift. The application selected then fully controls the entire process. The Exhaust Manifold docks automatically with the Tube Rack as they move down into the preheated Digestion Unit; and the Scrubber Unit, if connected, starts. The scrubber capacity is automatically adjusted during the cycle to contain fumes and minimise acid losses. When the digestion is completed the combined Tube Rack and Exhaust Manifold move to the cooling position with the Scrubber Unit still running until no further fumes are evolved. An adjustable audible signal in the Digestion Unit indicates “cycle over”. To avoid any spillage a drip tray, supplied with the Exhaust Manifold, is inserted underneath the Exhaust Manifold when it is separated from the Tube Rack after cooling. The Lift eliminates heavy handling. The Rack System saves space. Auto Rack Systems When an Auto Rack system is used in place of an Auto Lift system the typical procedure is as with the Auto Lift system with the exception that the combining/separating of Tube Rack and Exhaust Manifold and the movement to the cooling position is performed manually when the signal is heard. The application selected controls all other functions as with the Auto Lift system. Basic Systems The temperature and time for the digestion are selected on the front panel. All other procedures, including operation of a connected scrubber, are then performed by the operator once the digestion unit has reached the selected temperature. Fume Removal and Containment Systems Exhaust Manifolds Many digestion applications, e.g. Kjeldahl, produce fumes that are unpleasant and corrosive. Exhaust Manifolds designed for each Digestion Unit facilitate fume removal and containment and are strongly recommended for use with all digestion procedures. The cost of replacement of a fume cupboard which has been corroded by inefficient fume handling is very much greater than the relatively low cost of an approved exhaust. Whilst many users choose to operate integrated systems in the open laboratory, we strongly recommend the use of both exhaust systems and fume cupboards for these operations. This is simply Good Laboratory Practice (GLP) and avoids conflict with local Health & Safety (H&S) requirements. The Exhaust Manifolds should be connected to the water aspirator supplied, or to a suitable Scrubber Unit. Scrubber Unit Where water is a scarce or expensive commodity, or simply when a higher level of automation is desired, the water aspirator should be replaced with an efficient Scrubber Unit. Exhaust Manifolds and Scrubber Units which require an external water source are subject to variation in vacuum efficiency due to fluctuations in local water pressure. The compact bench top Tecator™ Scrubber Unit is self contained and is therefore unaffected by water supply issues. During digestion moist, acidic fumes from the connected exhaust are drawn through the Scrubber Unit. Acid vapours are first condensed and diluted in a large acid trap. Any residual fumes are collected, washed and neutralised before passing through a second small acid trap which protects the vacuum pump in the event that the scrubbing agents are exhausted. The cleaned air is then There is an Exhaust for each Digestion Unit. The Scrubber neutralizes the corrosive fumes. vented via a tubing outlet. In the interest of GLP and H&S this venting tube should be directed into a fume cupboard. When the Scrubber Unit is connected to an Auto Lift or Auto Rack system the program will fully control the function including switching from high to low aspiration settings. Reflux Heads When a digestion unit is used for reflux chemistries, such as Chemical Oxygen Demand (COD), a Reflux Head connected to a suitable cold water supply should be used in place of the Exhaust Manifold. Tecator™ Reflux Heads are conveniently mounted in handling racks which match the tube rack in the Digestion Unit. The ball jointed condensers are designed for use with ball jointed digestion tubes. The Reflux Heads are compatible with Auto Lift, Auto Rack and Basic systems. There are Reflux Heads for 250 ml Digestion Units. Select the correct tube for your application. Kjeltabs, salt and catalyst in tablet form. Digestion Tubes To suit different applications and manual/automatic handling systems, tubes for the Digestion Units are available in two sizes (250 ml and 100 ml) and three shapes. Straight sided tubes are recommended for the majority of digestion applications. Volumetric tubes with a constriction at the neck are recommended for applications where the digestate requires dilution to a fixed volume before analyses such as FIA, SFA, and AA etc. Ball jointed tubes, available in 250 ml size only, are required for reflux chemistries using the reflux condenser heads. The larger 250 ml straight sided tubes are recommended for Kjeldahl, as they can hold samples of widely varying sizes. Samples of heterogeneous material often need to be fairly large to ensure that they are representative. There is no lower limit of sample size in the 250 ml tubes; they simply allow greater flexibility for most type of samples. The 100 ml straight sided tubes can be used where the material is homogeneous and small samples are fully representative or where they are specified by the approved method. Kjeltabs A salt, to increase the boiling point, and a catalyst, to increase the speed of reaction, are used for Kjeldahl digestions. As a convenient way to obtain the correct dosage, FOSS supplies Kjeltabs – tablets containing Potassium Sulphate and a catalyst (Copper, Selenium, or Copper/Titanium). Digestion time may depend on the catalyst used. Historically Mercury has been used as the most efficient catalyst. Today it has been replaced largely by Copper, or other metals, due to safety and environmental considerations. Kjeltabs are supplied in two sizes; 3.5 g and 1.5 g. One or more tablets are combined with the acid to obtain an optimal salt/acid ratio. The smaller 1.5 g size is designed for the 100 ml tubes. Ordering information:* Digestion Units: All models are delivered with a Tube Rack with integrated heat shields. They should always be combined with a matching Exhaust Manifold or Reflux Head and Test Tubes – 100 or 250 ml volume. For Kjeldahl digestions the 2501-001 Scrubber Unit should always be considered for safe and efficient neutralisation of corrosive gases. This replaces the water aspirator, supplied as standard. Auto Lift models, complete with 2515-001 Lift and integrated controller for fully automatic control of digestion applications, including the operation of the Lift and a 2501-001 Scrubber Unit (optional extra). The digestion unit can be connected to PC for application updates, traceability and logging purposes. NOTE. An appropriate exhaust manifold or reflux head MUST be added for an automatic system. Auto Rack models, complete with 2515-011 Rack and integrated controller for full control of digestion applications, including the operation of a 2501-001 Scrubber (optional extra). The digestion unit can be connected to PC for application updates, traceability and logging purposes. Can be upgraded to an Auto Lift system by addition of the 2515-001 Lift. NOTE. An appropriate exhaust manifold or reflux head MUST be added for an automatic system. Basic models, with built in electronics for control of temperature and time only. Can not be upgraded to Auto models but are compatible with 2515-011 Rack. Tecator™ Auto Digestion Units Auto models with integrated all activity controller and graphical display. Versions for 250 ml tubes 2508-001 Tecator™ Digestion Unit 8 – Auto Lift system, 250 ml tubes, 230 V 50-60 Hz 2508-002 Same as above but for 110 V 50-60 Hz 2508-011 Tecator™ Digestion Unit 8 – Auto Rack system, 250 ml tubes, 230 V 50-60 Hz 2508-012 Same as above but for 110 V 50-60 Hz 2520-001 Tecator™ Digestion Unit 20 – Auto Lift system, 250 ml tubes, 230 V 50-60 Hz 2520-011 Tecator™ Digestion Unit 20 – Auto Rack system, 250 ml tubes, 230 V 50-60 Hz Versions for 100 ml tubes 2508-006 Tecator™ Digestion Unit 8 – Auto Lift system, 100 ml tubes, 230 V 50-60 Hz 2508-007 Same as above but for 110 V 50-60 Hz 2508-016 Tecator™ Digestion Unit 8 – Auto Rack system, 100 ml tubes, 230 V 50-60 Hz 2508-017 Same as above but for 110 V 50-60 Hz 2520-006 Tecator™ Digestion Unit 20 – Auto Lift system, 100 ml tubes, 230 V 50-60 Hz 2520-016 Tecator™ Digestion Unit 20 – Auto Rack system, 100 ml tubes, 230 V 50-60 Hz Tecator™ Digestion Units Basic models with built in electronics for control of temperature and time. Versions for 250 ml tubes 2508-051 Tecator™ Digestion Unit 8 – Basic, 250 ml tubes, 230 V 50-60 Hz 2508-052 Same as above but for 110 V 50-60 Hz 2520-051 Tecator™ Digestion Unit 20 – Basic 250 ml tubes, 230 V 50-60 Hz Versions for 100 ml tubes 2508-056 Tecator™ Digestion Unit 8 – Basic, 100 ml tubes, 230 V 50-60 Hz 2508-057 Same as above but for 110 V 50-60 Hz 2520-056 Tecator™ Digestion Unit 20 – Basic 100 ml tubes, 230 V 50-60 Hz Fume Removal & Containment Systems 2508-020 Exhaust Manifold for Digestion Units 2508, if 250 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2508-021 Exhaust Manifold for Digestion Units 2508, if 100 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2520-020 Exhaust Manifold for Digestion Units 2520, if 250 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2520-021 Exhaust Manifold for Digestion Units 2520, if 100 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2501-001 Scrubber Unit 110/230 V 50-60 Hz. For neutralization of fumes in acid digestions. It can be combined with any of the Exhaust Mani folds. Up to 100 samples without changing of reagent. Fully automatic operation when connected to an Auto Digestion Unit. Lift & Rack Systems 2515-001 LIFT for the AUTO version of Digestion Unit 2508 and 2520. The Application run in the Digestion Unit fully controls the LIFT. The Lift can only be connected to Auto version Digestion Unit. 2515-011 RACK System for all versions of Digestion Unit 2508 and 2520 without LIFT. Enables manual positioning of components in a similar way as the Auto Lift. Reflux condensers 2508-030 Reflux Head COD Digestion Unit 2508. Water-cooled Condensers for 8x250 ml tubes. 2520-030 Reflux Head COD Digestion Unit 2520. Water-cooled Condensers for 20x250 ml tubes. 10000254 Reflux Condenser, Air Cooled. 700 mm. With ground joint for 250 ml tubes. Cont. Ordering information:* Handling Systems Digestion Units are delivered complete with one Tube Rack. It may be found convenient to order extra so that all tubes normally in use in the laboratory are placed in a rack. All Tube Racks fit the Kjeltec 2460 Sampler. 10014245 Tube Rack for 8 Digestion Tubes 250 ml. 10014248 Tube Rack for 8 Digestion Tubes 100 ml. 10014240 Tube Rack for 20 Digestion Tubes 250 ml. 10014246 Tube Rack for 20 Digestion Tubes 100 ml. 10014006 Retainer Plate for Washing; Digestor 2520, 250 ml Tubes. 10014007 Retainer Plate for Washing; Digestor 2520, 100 ml Tubes. 10000460 Boiling Rod To avoid bumping when digesting large volumes of water. 10000897 Handling Device for Digestion Tube 10007117 Dispenser 2-10 ml, 1000 ml Bottle 10007118 Dispenser 10-30 ml, 2000 ml Bottle Test tubes Straight model Test Tubes, often used for Kjeldahl determination. 10014311 Digestion Tubes Straight 100 ml 8/pkg 10014312 Digestion Tubes Straight 100 ml 20/pkg 10014278 Digestion Tubes Straight 250 ml 8/pkg 10000158 Digestion Tubes Straight 250 ml 20/pkg With constriction and volume mark, used in applications where the digest is diluted to volume and an aliquot is taken for analysis. 10014313 Digestion Tubes With Mark 100 ml 8/pkg 10014314 Digestion Tubes With Mark 100 ml 20/pkg 10014315 Digestion Tubes With Mark 250 ml 8/pkg 10000157 Digestion Tubes With Mark 250 ml 20/pkg With ground joint for air-cooled Reflux Condensers. 10014316 Digestion Tubes - Ground Joint 250 ml 8/pkg 10000159 Digestion Tubes - Ground Joint 250 ml 20/pkg With ball joint for water-cooled Reflux Condensers. 10014317 Digestion Tubes - Ball Joint 250 ml 8/pkg 10000611 Digestion Tubes - Ball Joint 250 ml 20/pkg Kjeltabs: Most types are delivered in boxes of 1000. 15270001 Selenium, Tablets with 1.5 g K2SO4 + 7.5 mg Se. 15270002 Selenium, Tablets with 5 g K2SO4 + 5 mg Se. 15270003 Selenium, Tablets with 3.5 g K2SO4 + 3.5 mg Se. 15270056 Selenium, Tablets with 1 g Na2SO4 + 0.05 g Se. 15270010 Copper/Titanium, Tablets with 5 g K2SO4 + 0.15 g CuSO4.5H2O + 0.15 g TiO2 . 15270020 Copper/Titanium, Tablets with 3.5 g K2SO4 + 0.105 g CuSO4.5H2O + 0.105 g TiO2 . 15270018 Copper, Tablets with 3.5 g K2SO4 + 0.4 g CuSO4.5H2O. 15270034 Copper, Tablets with 1.5 g K2SO4 + 0.15 g CuSO4.5H2O. 15270057 Copper, Tablets with 4.5 g K2SO4 + 0.5 g CuSO4.5H2O. Other types are available upon request Installation requirements: Digestion Unit 2508 Auto Power Supply: 200 - 240 V or 100 - 115 V, 50 - 60 Hz Power consumption: 1100 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 10 kg Dimensions, W × D × H: 300 × 500 × 697 mm (incl. Rack system) Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Lift or Racking System is used Digestion Unit 2508 Basic Power Supply: 200 - 240 V or 100 - 115 V, 50 - 60 Hz Power consumption: 1100 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 10 kg Dimensions, W × D × H: 300 × 390 × 140 mm Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Racking Sys tem is used Digestion Unit 2520 Auto Power Supply: 200 - 240 V, 50 - 60 Hz Power consumption: 2300 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 18 kg Dimensions, W × D × H: 300 × 660 × 697 mm (incl. Rack system) Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Lift or Rack System is used Digestion Unit 2520 Basic Power Supply: 200 - 240 V, 50 - 60 Hz Power consumption: 2300 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 18 kg Dimensions, W × D × H: 300 × 550 × 140 mm Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Rack System is used Scrubber Power Supply: 100 to 240 V, 50 - 60 Hz, Self selecting Power consumption: 50 W Water supply: No Weight: 19 kg Dimensions, W × D × H: 335 × 485 × 395 mm Ambient temperature: max 40°C Ventilation requirement: Outlet tubing preferably into sink in fume hood Recommended bench space: 0.6 m Exhaust 2508 Water supply: 3 - 5 l/min for 5 minutes, then 1 l/min Exhaust 2520 Water supply: 10 - 12 l/min for 5 minutes, then 3 - 5 l/min Lift Power Supply: None. Powered from the Diges tion Unit Auto Power consumption: 10 W Weight: 7 kg Dimensions, W × D × H: 300 × 550 × 697 mm (Mounted on Digestion Unit) Ambient temperature: max 40C Ventilation requirement: No Recommended bench space: 0 m. Lift is mounted on the Digestion Unit Performance data: 2508 Auto 2508 Basic 2520 Auto 2520 Basic Temperature range Ambient - 440°C 100 - 440°C Ambient - 440°C 100 - 440°C Temperature setting repeatability 1°C 1°C 1°C 1°C Temperature readout Digital Digital Digital Digital Heater indication LED LED LED LED Heater warning Text in display Text in display Text in display Text in display Over temperature protection Yes Yes Yes Yes Temperature stability at ± 2°C 100°C ± 5°C ± 2°C ± 5°C Temperature stability at ± 1°C 400°C ± 2°C ± 1°C ± 2°C Heating time 20 to 400°C at 230 V ~35 min ~35 min ~40 min ~40 min Time setting per step 1 - 999 min 1 - 1199 min 1 - 999 min 1 - 1199 min Ramp control (Rate of heating) Yes No Yes No Digestion applications memory Up to 254 No Up to 254 No Digestion steps per application Up to 23 1, Manual control Up to 23 1, Manual control Lift connection Yes, full control No Yes, full control No Scrubber Yes, full control Yes, man control Yes, full control Yes, man control Tubes / batch 8 8 20 20 Tube size 250 ml 250 ml 250 ml 250 ml Sample size* solids up to 5 g up to 5 g up to 5 g up to 5 g Sample size* liquids up to 15 ml up to 15 ml up to 15 ml up to 15 ml Tube size 100 ml 100 ml 100 ml 100 ml Sample size* solids up to 1 g up to 1 g up to 1 g up to 1 g Sample size* liquids up to 3 ml up to 3 ml up to 3 ml up to 3 ml Typical sample capacity FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0720E, Issue 2 GB, August 2005 *Note: Larger samples require special procedures. Please see the relevant Application Notes or consult our Customer Service Laboratory. FIAstar® Analizador 5000 Analizador FIAstar 5000. ”Conectar y Analizar”, la máxima sencillez en análisis químicos por vía húmeda. ® Características y Beneficios Beneficioso inclusive con lotes pequeños de muestras, debido a: - Puesta en marcha y apagado rápido (10 min.). - Resultados inmediatos (menos de 1 min.). Casetes de Método ”Conectar y Analizar” rápido y sencillo. ® Software Windows 98/2000 incluyendo rutinas de calibración según ISO 8466. Detector Digital de Doble Longitud de Onda (DDW) para eliminar los efectos del índice de refracción y de las burbujas de aire. Rango dinámico amplio y bajos límites de detección. Función de stand-by (<3mL de reactivo/24 h) permite la operación nocturna sin supervisión. El módulo básico de FIAstar en operación. Descripción del sistema El FIAstar 5000 es un sistema totalmente automatizado para la determinación de Amonio, Nitrato / Nitrito, Nitrógeno Total, Fosfato, Fósforo Total y otros parámetros, utilizando los últimos métodos aprobados por ISO. Se pueden analizar hasta tres parámetros simultáneamente. Cada Módulo Analizador incluye un detector DDW, termostato, válvula de inyección y bomba. Todo el sistema se controla mediante el software SoFIA del sistema FIAstar 5000. Casetes de Método Los Casetes de Método pre-configurados se colocan y/o intercambian en una sola operación y se conectan / desconectan automáticamente. La puesta en marcha y apagado del sistema es una cuestión de minutos. Se dispone de un Casete de Método en blanco para configurar aplicaciones que no sean estándar. Software SoFIA Los métodos predefinidos y botones rápidos para funciones utilizadas frecuentemente permiten un procesamiento de muestras rápido y fácil. Las rutinas de control de calidad (QC) y de GLP para la detección de errores analíticos contribuyen a obtener resultados exactos. El programa también soporta un lector de código de barras para el registro simplificado de muestras, importación de archivos de registro de muestras e incluye una interface LIMS para la exportación de resultados de muestras. Analizador FIAstar 5000 para Nitritos / Nitratos, con 1 Módulo Analizador FIAstar 5000, 1 software SoFIA, 1 casete NO2 / NO3, 1 Muestreador 5027 (120 posiciones). Analizador FIAstar 5000 de Dos Canales para Nitrógeno en Suelos, con 2 Módulos Analizadores FIAstar 5000, 1 software SoFIA, 1 hub USB, 1 casete NO2 /NO3, 1 casete NH4 y 1 Muestreador 5027 (120 posiciones). 5000-700 Sistema FIAstar 5000 de Tres Canales para Análisis de Agua, con 3 módulos Analizadores FIAstar 5000, 1 software SoFIA, 1 hub USB, 1 casete NO2 / NO3, 1 casete NH4, 1 casete P y 1 muestreador 5027 (120 posiciones). Accesorios y consumibles 50003139 50000295 50002875 10004593 5000-050 Columnas de Cadmio pre-empaquetadas, caja de 3 unidades Mezcla indicadora para Amonio Membranas de Difusión de Gases para Amonio Membranas de Difusión de Gases para TKN Casete de Método en blanco para otras aplicaciones, con tubos de la bomba y conjunto de bucles de mezcla. Los filtros deben ser pedidos separadamente Datos de Operación: Analizador FIAstar® 5000 Principio de operación: Inyector: Volumen de muestras: Bomba: Termostato: Casete de Método: Detector: Análisis por Inyección en Flujo (FIA) Inyector rotatorio de 6 vías, volumen variable 20 - 400 µl Bomba peristáltica de 2 ´ 4 canales con velocidad variable y función de alerta Termostato incorporado, 30°C - 90°C ± 1°C Consumo de reactivos 0.3 - 2 mL/ muestra Fotómetro Digital de Doble Longitud de Onda con corrección automática de fondo Paso 10 mm; volumen 18 µL 400 - 1,000nm Celda de Flujo: Rango de Longitud de Onda: Intervalo de Absorbancia: 0 - 2.5 UA Requerimientos de Instalación ® Analizador FIAstar 5000 Suministro eléctrico: Dimensiones: Peso: Consumo de energía: Conexión a PC: 100 - 240 V CA, 50-60 Hz (26 V CC) 450 ´ 310 ´ 145 mm (con soporte de reactivos 625 ´ 310 ´ 145) 8,7 kg 70 vatios USB (Universal Serial Bus) Resolución: Reproducibilidad: Software SoFIA Puntos de Calibración: Ajuste de curva de calibración: Rutinas QC y GLP: Principio de operación: Bandejas de muestras: División de la bandeja: Tamaño de muestra: Bandeja lateral: Tel: +46 42 36 15 00 Fax: +46 42 34 03 49 e-mail [email protected] Página web: www.foss.dk Representantes en 100 países Lineal o segundo orden ISO 8466 Verificación de muestras; análisis estándar y muestras múltiples; recalibración automática; alarmas de falta de reactivo, falta de muestras y fuera de rango Métodos pre-definidos Circular Para 64 o 120 muestras 4 gradillas individuales 12, 30 mL 10 posiciones para patrones y QC Espacio disponible en disco duro 40 MB Disquetera de 1.44 Mb o lector de CD Una puerta USB para cada módulo FIA conectado Una puerta RS 232 para comunicación con el muestreador 5027 Puerta RS 232 adicional para transferencia de datos a un sistema LIMS Muestreador 5027 Suministro eléctrico: Dimensiones: Peso: Consumo de energía: *Información de pedidos: Utilice los Números de Catálogo y texto correspondiente detallados arriba. Foss Tecator AB Box 70, SE-263 21 Höganäs, Suecia Hasta 10 patrones Muestreador 5027 Especificaciones del PC: Ordenador en entorno Windows® 98 o 2000 instalado Mínimo 32 Mb de memoria RAM 0.001 mUA Mejor que 1% r.s.d. In the interest of product development we reserve the right to alter specifications without prior notice. Sistemas completos 100/115/130/200/240 V, 50-60 Hz 450 ´ 400 ´ 260 mm (con bandeja separada 625 ´ 400 ´ 260) 14 kg 20 vatios Part no 9999 0912ES / 0006 DOT Graphic AB, Malmö, Sweden Información de Pedidos*: 5000-001 Módulo Analizador FIAstar 5000 (26 V DC), unidad de análisis con válvula de inyección, bomba, soporte de casete, termostato incorporado, detector DDW, conexión USB y adaptador de voltaje (100-240 V, 50-60 Hz). 5000-010 Casete de Método Nitrato/Nitrito y Nitrógeno Total, con filtros, tubos de la bomba, columnas de reducción, botellas para reactivo / enjuague y soporte de casete. 5000-020 Casete de Método Amonio, con filtros, tubos de la bomba, membranas de difusión de gas, mezcla indicadora, botellas para reactivo / enjuague y soporte de casete. 5000-030 Casete de Método Fosfato/Fósforo Total, con filtros, tubos de la bomba, botellas para reactivo / enjuague y soporte de casete. 5000-040 Casete de Método TKN (Nitrógeno Kjeldahl Total), con filtros, tubos de la bomba, membranas de difusión de gas, mezcla indicadora, botellas de reactivo / enjuague y porta casete. 5000-100 Programa SoFIA para FIAstar 5000 en entorno Windows® 5027-003 Muestreador 5027 para FIAstar con bandeja para 120 muestras, vasos de 12 mL y bandeja separada para patrones de calibración y de QC. 5027-004 Ídem, pero con bandeja para 64 muestras, 30 mL FiberCap™ 2021/2023 Fibre Analysis System A modular system for simple analysis of crude and detergent fiber. Features and benefits •18 & 6 position systems for crude fibre, NDF, ADF & ADL •Results in agreement with official procedures •Low investment cost giving unique performance/ price ratio •FiberCap™ capsule design ensures accurate analysis and superior precision •Batch handling with no sample transfer •Rapid filtration for all sample types saves time •Multiple systems are easily operated for high throughput •Small bench space needed Description The FiberCap system is specifically designed to provide a low cost, high capacity solution for fibre determination in accordance with the Weende and van Soest methods. Batch handling, with no sample transfer, is used throughout the procedure. Defatting, boiling, rinsing and filtration are performed under reproducible and controlled conditions. Dedicated Analytical Solutions The system offers substantial savings both in manual handling and time as well as improved analytical precision compared to manual methods. The capsule is a polypropylene container with a simple snap on lid, once sealed, there is no sample transfer. The different chemical properties of the membranes used in the capsule and the lid ensure free flow of reagent through the FiberCap during analysis. This feature guarantees repeatable conditions for all sample types, even high starch samples can easily be determined. Filtration or washing is done in seconds for all sample types. Two versions of capsules are available, having different mesh size, offers the possibility to match results either with the filter paper method (white capsule) or the crucible method (green capsule). The FiberCap is available in either 18 or 6 position systems and one operator can easily handle several systems simultaneously giving a very high throughput. For example, 4 batches with the 18 position system give 72 finished extractions in 1,5 h. Weighing De-fatting Batch transfer Extraction System description 2021 0001 FiberCap 2021 (6 position) 230 V, 50 Hz. Including all accessories necessary for analysis whereof 100 pcs of capsules (white) 2021 0004 FiberCap 2021, 115 V, 50-60 Hz. As above. 2021 0011 FiberCap 2021 230 V, 50 Hz. Including all accessories necessary for analysis whereof 100 pcs of capsules (green) 2021 0014 FiberCap 2021, 115 V, 50-60 Hz. As above. 2023 0001 FiberCap 2023 (18 position) 230 V, 50 Hz. Including all accessories necessary for analysis whereof 100 pcs of capsules (white) 2023 0003 FiberCap 2023, 115 V, 50-60 Hz. As above. 2023 0011 FiberCap 2023 230 V, 50 Hz. Including all accessories necessary for analysis whereof 100 pcs of capsules (green) 2023 0013 FiberCap 2023, 115 V, 50-60 Hz. As above. Accessories: 1524 0010 2022 Hot Plate 230 V, 50 Hz 1524 0011 2022 Hot Plate 115 V, 50 - 60 Hz 1001 0332 Boiling Stand 1001 0224 Capsule Tray, 6 position 1001 0334 Capsule Tray, 18 position 1001 0137 Extraction Beaker, 6 position 1001 0546 Extraction Beaker, 18 position 1001 0331 Drying Stand 1001 0347 FiberCap capsules, 100 pcs 1001 0346 FiberCap capsules, 500 pcs 1001 0262 Stopper, 6 position 1001 0335 Stopper, 18 position Performance data: Sample size: Measuring range: Capacity per batch: Capacity per day: (6 batches) Repeatability: 0,5 - 3 g 0,1 - 100 % 6 samples or 18 samples simultane- ously � � � � � � � � Up to 216 analyses (Crude fibre) using six Fibertec 2021 Systems in parallell, 108 analyses (Crude fibre) using one Fibertec 2023. ± 1 % relative at 5 - 30 % fibre level Installation requirements: Equipment Power supply Power consumption Dimensions Weight Water supply w× d×h 2022 Hot Plate 230 V, 50 Hz 500 W 20 × 30 × 35 cm 2,5 kg 0,4 l/min 115 V, 50 - 60 Hz Furnace Note; the furnace used during the analysis must be well ventilated, due to the build up of smoke. Applications: • Crude Fibre • NDF (Neutral Detergent Fibre) • ADF (Acid Detergent Fibre) & ADL (Acid Detergent Lignin) The Fibertec™ 2021 and 2023 System are also suitable for use with almost any chemical. Materials used are glass, PTFE; PEEK, PP, PET & PA. FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0407, Issue 2 GB, Nov 2007 * Ordering information: See separate price-list Fibertec™ M6 Fibre Analysis System Extraction System for simple determination of Crude Fibre, Detergent Fibre, Cellulose, Hemicelluloses, Lignin and related Parameters in plant materials, compound feed, food, etc. Benefits • Six samples processed simultaneously. • Accessories for batch handling. • Integral extraction and filtration. • No sample transfer and no loss of sample. • Separate unit for solvent dehydration, lignin determination and defatting. • Extensive application service. • High reproducibility of conditions and results. • Saves time, energy and laboratory space. • Official approval: ISO 6865, 92/89 EEC and AOAC 2002.04 (feed). Description The Fibertec™ System M6 is dedicated for fibre determinations according to Weende, van Soest, etc. Single or sequential extractions including boiling, using externally preheated reagents, rinsing and filtration are performed under reproducible and controlled conditions. Dedicated Analytical Solutions The basic modules of a Fibertec M6 are: • 1020 Hot Extraction Unit, for hot hydrolysis and extraction with built-in systems for heating and filtration • 1021 Cold Extraction Unit, for defatting samples, extraction at ambient temperature e.g. lignin determination, and for solvent dehydration of fibre residues. Both units are adapted to the same crucible system that permits the sample, whenever required, to be dried and weighed between extractions. In the system the samples are handled in specially designed filter crucibles, which are used both as an integral part of an extraction assembly during extraction, rinsing and filtering, and as a sample vessel during the weighing, drying and ashing steps. The Fibertec M6 permits handling of six samples at a time by the use of accessory tools for batch handling. Filtration problems are overcome by the unique vacuum/reverse air flow system. The Fibertec M6 offers a most time saving and convenient solution for more reproducible fibre determinations. System description: Fibertec™ M6 (200-230V): • Hot Extraction Unit comprising: Hot Extractor, Reflector, Reagent Bottles, Hot Water Sprayer, Beaker, Funnel, Water Suction Pump, Antifoaming Agent, Tubing, Holder for 6 crucibles, Stand for 6 crucibles, Crucibles (P2 standard, 2 sets of 6), Manual. • Cold Extraction Unit comprising: Cold Extractor, Spray Bottle, Tubing, T-tube, Spare Part Kit, Stand for 6 crucibles, Crucibles (P2 standard 40 - 100 µm, set of 6), Antifoaming Agent (octanol), Celite, 1 l Performance data: Sample size: Measuring range: Repeatability: Accuracy: 0.5 - 3 g (1 g normal) 0.1 - 100% < 1% relative at 5 - 30 % fibre level According to official methods Installation requirements: Equipment Power supply 1020 Hot Extraction Unit 200 - 230V ± 10% 50 - 60 Hz 1021 Cold Extraction Unit - Also choose from the following accessories: 1093 Cyclotec™ Sample Mill, cyclone mill 1090 Cemotec™ Sample Mill, moisture mill 2094 Homogenizer, blender type 2096 Homogenizer, blender type 1095 Knifetec™, water cooled sample mill Hot plate 2022 Filter Crucibles: Crucible, P1 (100 - 160 µm), set of 6 Crucible, P2 (40 - 100 µm), set of 6, standard Crucible, P3 (16 - 40 µm), set of 6 Crucible, P0 (160 - 250 µm), set of 6 Crucible P2 US, (40 - 60 µm) set of 6 Capacity per batch: Capacity per day: 6 samples simultaneously Up to 36 analyses (Crude Fibre method acc. to Weende) per day Power consumption 1 000 kW Dimensions w× d×h 56 × 38 × 57 Weight - 56 × 38 × 28 4 kg 28 kg Water supply Tap water for condensors (appr. 2 l/min) and water aspirator (during filtration) Tap water for water aspira tor (during filtration) Applications: • Crude Fibre (acc. to Weende). • Neutral Detergent Fibre. • Acid Detergent Fibre. • Acid Detergent Lignin. In addition, most other chemical extraction methods except methods including acetic acid, trichloracetic acid and/or nitric acid, may be employed. For specific method information, please ask for detailed FOSS Analytical Application Notes. Fibertec™ Systems for any fibre determination needs: Low fat samples 1093 Cyclotec™ Mill Medium fat samples 1090 Cemotec™ Mill Enzymatic Balance Method High fat samples 2094/2096 Homogenizer 1095 Knifetec™ Chemical Fibertec™ E High workloads Fibertec™ 2010 Medium workloads Fibertec™ M6 Drying Oven Balance Muffle furnance Balance FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0401E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Fibertec™ E Dietary Fibre Analysis System Semi-automated incubation and separation system for quantitative determination of dietary fibre in processed food, cereal products, fruits and vegetables, health food, feedstuffs, plant materials, etc. Benefits • Free choice of methods like AOAC, AACC, NMKL and Asp. • Determines total, soluble and insoluble dietary fibre. • Rapid filtration of six samples simultaneously. • Specially designed incubation flasks • High incubation and separation capacity. • Repeatable readings, S.D. < 0.5% absolute. • Easy and convenient to use. • Saves time, space and manual work. Description The Fibertec™ E is designed for rapid and rational determination of dietary fibre according to established enzymatic methods, including those approved by AOAC, AACC, NMKL and Asp. The Fibertec E determines total dietary fibre as well as the insoluble and soluble fibres separately. It is also useful in sample preparation for detailed studies of fibre fractions, e.g. by chromatographic or colorimetric techniques. Dedicated Analytical Solutions The basic Fibertec E includes a Shaking Water Bath and a Filtration Module. The Shaking Water Bath incubates 12 samples in each batch. The temperature range is from ambient to 80°C and it is possible to preset three temperatures. The shaking frequency and amplitude are continously adjustable. The Filtration Module filters and collects 6 sample solutions batchwise and includes a system for rapid dehydration. The filtration step is speeded up through built-in “Pressure Mode”. Reversed pressure is applied to facilitate filtration by breaking up clogged filter residues during filtration. Filtration time varies according to sample type, but on average it is 2-4 minutes for 100 ml of digested solution. The reproducibility (standard deviation) of the Fibertec E in determining total, insoluble and soluble dietary fibre is < 0.5% absolute. System description: Fibertec™ E • Filtration Module complete, comprising: Filtration Module, Incubation Flasks (4 sets of 6), Standard Crucibles (P2, 2 sets of 6), Basket for Incubation Flasks, 2 Stands for Crucibles, 2 Spray bottles, 2 Water aspiration pumps, Filter aid, Tubing, Shaking Water Bath, complete, comprising: a tray for 12 Incubation Flasks and a hinged inclined lid. In addition, we recommend: Incubation Flask (set of 6), at least 4 sets Crucible, P2 (40 - 100 µm) set of 6, at least 2 sets Basket for 12 Incubation Flasks, at least 1 Total Dietary Fibre Kit for 200 determinations Termamyl 300 L, 100 ml Boiling Water Bath Pipette 100 µl Muffle or incineratron furnace ~525°C Performance data: Filtration Module: Filtration and dehydration capacity: 6 samples/batch Filtration rate: 2-4 ml/100 ml of digested solution, depending on sample type Repeatability: S.D. < 0.5% absolute Flask volume: 600 ml Installation requirements: Equipment Power supply Accessories: Alternative filter crucibles: Crucible, P0 (160 - 250 µm), set of 6 Crucible, P1 (90 - 150 µm), set of 6 Crucible, P3 (15 - 40 µm), set of 6 Stand for 6 Crucibles 1093 Cyclotec™ Sample Mill 1090 Cemotec™ Sample Mill 1095 Knifetec™ Sample Mill for high fat, high fibre samples For protein determination we recommend our Kjeltec analyzers. Alternative flask trays for other applications, e.g. biochemical work: Tray for E**-flasks, 50 ml Tray for E**-flasks, 100 ml Tray for E**-flasks, 250 ml Tray for E**-flasks, 500 ml ** Erlenmeyer Shaking Water Bath: Capacity: Temperature range: Temperature accuracy: Shaking frequency: Stroke length: Power consumption 12 flasks/batch ambient to 80°C ± 0.1°C 0-150 strokes/minute 0-50 mm 1023 Filtration Module 100-120 V, 50-60 Hz 210-230 V, 50-60 Hz 8 Dimensions w× d×h 770 × 280 × 500 1024 Shaking Water Bath 100-120 V, 50-60 Hz 210-230 V, 50-60 Hz 1500 890 × 370 × 320 Weight, kg 24 24 A comple analytical scheme for dietary fibre determination consists of: Samples with a low fat content 1093 Cyclotec™ Mill 1090 Cemotec™ Mill Balance Samples with a high fat content 2094 Homogenizers 1095 Knifetec™ Water Bath Boiling Shaking Water Bath 1024 Filtration Module 1023 Drying Oven Balance Correction Muffle furnance Kjeltec™ FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0403E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Fibertec™ 2010 Auto Fibre Analysis System A semi-automated extraction system for simple determination of crude fibre, detergent fibre and related parameters in plant materials, compound feeds, foodstuffs etc. Features and benefits Safety • Automated heating of reagents in an integrated, closed system • Automated addition of preheated reagents Precision • Fulfils boiling start time requirements for crude fibre specified in ISO and EC standards • Enhances precision thanks to integrated extraction and filtration, thus avoiding sample transfer • Ensures same extraction condition in each analysis by means of timer function • Official approval: ISO 6865, 92/89 EEC and AOAC 2002.04 (feed). Value • Automatic water filling/topping up • Batch handling devices for simple transfer of samples to balance, furnace etc • Water-saving device reduces consumption Dedicated Analytical Solutions Description The Fibertec™ 2010 is specifically designed for fibre determination in accordance with the Weende, van Soest and other recognized methods. Single or sequential extractions including boiling, use of internally preheated reagents, rinsing and filtration are performed under reproducible and controlled conditions. The Fibertec 2010 is available with the following basic modules: Fibertec 2010 Hot Extraction Unit, for hot hydrolysis and extraction, featuring built-in systems for heating and filtration, and for automatic preheating and addition of reagents Fibertec 1021 Cold Extraction Unit, for de-fatting samples, extraction at ambient temperatures (e.g. in lignin determination) and solvent dehydration of fibre residues Both modules use the same crucible system, permitting samples to be dried and weighed between extractions if required. Samples are handled in specially designed filter crucibles. Crucibles are used both as an integral part of the assembly during extraction, rinsing and filtration and as sample vessels during weighing, drying and ashing. The Fibertec method is as described in the relevant ISO and EC standards. It is thus the reference method and is a sound choice for the future. System description: • Fibertec 2010, 240V, 50 Hz comprising; Hot Extraction Unit, Cold Extraction Unit, crucibles, crucible stand, crucible holder, reflector, spray bottle, tubing, anti-foaming agent and water supply tank, crucible seals • Fibertec 2010, 240V, 60 Hz specifications. As above. • Fibertec 2010, 240V, 60 Hz specifications • Fibertec 2010 Hot Extraction Unit (240V, 50 Hz) same as 2010 but without Cold Extraction Unit Accessories: Crucible stand for 6 crucibles. At least two stands recommended. Crucible holder for 6 crucibles Water Aspirator Pump Performance data: Sample size: Measuring range: Capacity per batch: Capacity per day: 2010 Hot Extraction Unit Power supply Optional accessories: Crucibles, P0 (porosity 160-250 µm), set of 6 Crucibles, P1 (porosity 100-160 µm), set of 6 Crucibles, P2 standard (porosity 40-100 µm), set of 6 Crucibles, P3 (porosity 16-40 µm), set of 6 Sample preparation equipment: 1093 Cyclotec™, Sample mill 1090 Cemotec™, Sample mill 2094 Homogenizer, blender type 2096 Homogenizer, blender type 1095 Knifetec™, water cooled Repeatability: ±1 % relative at 5% - 30% fibre level Reagent preheating time: 10-20 min Heating-up time from preheated temperature to boiling: 5-7 min 0,5 - 3 g 0,1% - 100% Up to 6 samples simultaneously Up to 36 analyses (crude fibre method). Up to 60 analyses using modified procedure Installation requirements: Equipment Anti-foaming agent (octanol) Filtering agent (celite 545), 1 l Power Dimensions consumption w × d × h 200 - 240V ± 10% 50 Hz or 200 - 240V ± 10% 60 Hz 2.3 kW 75 × 40 × 68 1021 Cold Extraction Unit with water aspirator 58 × 38 × 28 * When Fibertec 2010 is in standby mode the tap water supply is closed down. Weight Water supply 65 kg Tap water* appr. 2 l/min 14 kg Tap water Applications: • Crude Fibre (acc. to Weende). • Neutral Detergent Fibre. • Acid Detergent Fibre. • Acid Detergent Lignin. The Fibertec™ 2010 is also suitable for use with most other chemical extraction methods except those that involve the use of acetic acid, trichloracetic acid and/or nitric acid. For specific method information, please ask for detailed FOSS Analytical Application Notes. Fibertec™ Systems for any fibre determination needs: Low fat samples 1093 Cyclotec™ Mill Medium fat samples 1090 Cemotec™ Mill Enzymatic Balance Method High fat samples 2094/2096 Homogenizer 1095 Knifetec™ Chemical Fibertec™ E High workloads Fibertec™ 2010 Medium workloads Fibertec™ M6 Drying Oven Balance Muffle furnance Balance FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0405E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Fibertec™ E Dietary Fibre Analysis System Semi-automated incubation and separation system for quantitative determination of dietary fibre in processed food, cereal products, fruits and vegetables, health food, feedstuffs, plant materials, etc. Benefits • Free choice of methods like AOAC, AACC, NMKL and Asp. • Determines total, soluble and insoluble dietary fibre. • Rapid filtration of six samples simultaneously. • Specially designed incubation flasks • High incubation and separation capacity. • Repeatable readings, S.D. < 0.5% absolute. • Easy and convenient to use. • Saves time, space and manual work. Description The Fibertec™ E is designed for rapid and rational determination of dietary fibre according to established enzymatic methods, including those approved by AOAC, AACC, NMKL and Asp. The Fibertec E determines total dietary fibre as well as the insoluble and soluble fibres separately. It is also useful in sample preparation for detailed studies of fibre fractions, e.g. by chromatographic or colorimetric techniques. Dedicated Analytical Solutions The basic Fibertec E includes a Shaking Water Bath and a Filtration Module. The Shaking Water Bath incubates 12 samples in each batch. The temperature range is from ambient to 80°C and it is possible to preset three temperatures. The shaking frequency and amplitude are continously adjustable. The Filtration Module filters and collects 6 sample solutions batchwise and includes a system for rapid dehydration. The filtration step is speeded up through built-in “Pressure Mode”. Reversed pressure is applied to facilitate filtration by breaking up clogged filter residues during filtration. Filtration time varies according to sample type, but on average it is 2-4 minutes for 100 ml of digested solution. The reproducibility (standard deviation) of the Fibertec E in determining total, insoluble and soluble dietary fibre is < 0.5% absolute. System description: Fibertec™ E • Filtration Module complete, comprising: Filtration Module, Incubation Flasks (4 sets of 6), Standard Crucibles (P2, 2 sets of 6), Basket for Incubation Flasks, 2 Stands for Crucibles, 2 Spray bottles, 2 Water aspiration pumps, Filter aid, Tubing, Shaking Water Bath, complete, comprising: a tray for 12 Incubation Flasks and a hinged inclined lid. In addition, we recommend: Incubation Flask (set of 6), at least 4 sets Crucible, P2 (40 - 100 µm) set of 6, at least 2 sets Basket for 12 Incubation Flasks, at least 1 Total Dietary Fibre Kit for 200 determinations Termamyl 300 L, 100 ml Boiling Water Bath Pipette 100 µl Muffle or incineratron furnace ~525°C Performance data: Filtration Module: Filtration and dehydration capacity: 6 samples/batch Filtration rate: 2-4 ml/100 ml of digested solution, depending on sample type Repeatability: S.D. < 0.5% absolute Flask volume: 600 ml Installation requirements: Equipment Power supply Accessories: Alternative filter crucibles: Crucible, P0 (160 - 250 µm), set of 6 Crucible, P1 (90 - 150 µm), set of 6 Crucible, P3 (15 - 40 µm), set of 6 Stand for 6 Crucibles 1093 Cyclotec™ Sample Mill 1090 Cemotec™ Sample Mill 1095 Knifetec™ Sample Mill for high fat, high fibre samples For protein determination we recommend our Kjeltec analyzers. Alternative flask trays for other applications, e.g. biochemical work: Tray for E**-flasks, 50 ml Tray for E**-flasks, 100 ml Tray for E**-flasks, 250 ml Tray for E**-flasks, 500 ml ** Erlenmeyer Shaking Water Bath: Capacity: Temperature range: Temperature accuracy: Shaking frequency: Stroke length: Power consumption 12 flasks/batch ambient to 80°C ± 0.1°C 0-150 strokes/minute 0-50 mm 1023 Filtration Module 100-120 V, 50-60 Hz 210-230 V, 50-60 Hz 8 Dimensions w× d×h 770 × 280 × 500 1024 Shaking Water Bath 100-120 V, 50-60 Hz 210-230 V, 50-60 Hz 1500 890 × 370 × 320 Weight, kg 24 24 A comple analytical scheme for dietary fibre determination consists of: Samples with a low fat content 1093 Cyclotec™ Mill 1090 Cemotec™ Mill Balance Samples with a high fat content 2094 Homogenizers 1095 Knifetec™ Water Bath Boiling Shaking Water Bath 1024 Filtration Module 1023 Drying Oven Balance Correction Muffle furnance Kjeltec™ FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0403E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Fibertec™ M6 Fibre Analysis System Extraction System for simple determination of Crude Fibre, Detergent Fibre, Cellulose, Hemicelluloses, Lignin and related Parameters in plant materials, compound feed, food, etc. Benefits • Six samples processed simultaneously. • Accessories for batch handling. • Integral extraction and filtration. • No sample transfer and no loss of sample. • Separate unit for solvent dehydration, lignin determination and defatting. • Extensive application service. • High reproducibility of conditions and results. • Saves time, energy and laboratory space. • Official approval: ISO 6865, 92/89 EEC and AOAC 2002.04 (feed). Description The Fibertec™ System M6 is dedicated for fibre determinations according to Weende, van Soest, etc. Single or sequential extractions including boiling, using externally preheated reagents, rinsing and filtration are performed under reproducible and controlled conditions. Dedicated Analytical Solutions The basic modules of a Fibertec M6 are: • 1020 Hot Extraction Unit, for hot hydrolysis and extraction with built-in systems for heating and filtration • 1021 Cold Extraction Unit, for defatting samples, extraction at ambient temperature e.g. lignin determination, and for solvent dehydration of fibre residues. Both units are adapted to the same crucible system that permits the sample, whenever required, to be dried and weighed between extractions. In the system the samples are handled in specially designed filter crucibles, which are used both as an integral part of an extraction assembly during extraction, rinsing and filtering, and as a sample vessel during the weighing, drying and ashing steps. The Fibertec M6 permits handling of six samples at a time by the use of accessory tools for batch handling. Filtration problems are overcome by the unique vacuum/reverse air flow system. The Fibertec M6 offers a most time saving and convenient solution for more reproducible fibre determinations. System description: Fibertec™ M6 (200-230V): • Hot Extraction Unit comprising: Hot Extractor, Reflector, Reagent Bottles, Hot Water Sprayer, Beaker, Funnel, Water Suction Pump, Antifoaming Agent, Tubing, Holder for 6 crucibles, Stand for 6 crucibles, Crucibles (P2 standard, 2 sets of 6), Manual. • Cold Extraction Unit comprising: Cold Extractor, Spray Bottle, Tubing, T-tube, Spare Part Kit, Stand for 6 crucibles, Crucibles (P2 standard 40 - 100 µm, set of 6), Antifoaming Agent (octanol), Celite, 1 l Performance data: Sample size: Measuring range: Repeatability: Accuracy: 0.5 - 3 g (1 g normal) 0.1 - 100% < 1% relative at 5 - 30 % fibre level According to official methods Installation requirements: Equipment Power supply 1020 Hot Extraction Unit 200 - 230V ± 10% 50 - 60 Hz 1021 Cold Extraction Unit - Also choose from the following accessories: 1093 Cyclotec™ Sample Mill, cyclone mill 1090 Cemotec™ Sample Mill, moisture mill 2094 Homogenizer, blender type 2096 Homogenizer, blender type 1095 Knifetec™, water cooled sample mill Hot plate 2022 Filter Crucibles: Crucible, P1 (100 - 160 µm), set of 6 Crucible, P2 (40 - 100 µm), set of 6, standard Crucible, P3 (16 - 40 µm), set of 6 Crucible, P0 (160 - 250 µm), set of 6 Crucible P2 US, (40 - 60 µm) set of 6 Capacity per batch: Capacity per day: 6 samples simultaneously Up to 36 analyses (Crude Fibre method acc. to Weende) per day Power consumption 1 000 kW Dimensions w× d×h 56 × 38 × 57 Weight - 56 × 38 × 28 4 kg 28 kg Water supply Tap water for condensors (appr. 2 l/min) and water aspirator (during filtration) Tap water for water aspira tor (during filtration) Applications: • Crude Fibre (acc. to Weende). • Neutral Detergent Fibre. • Acid Detergent Fibre. • Acid Detergent Lignin. In addition, most other chemical extraction methods except methods including acetic acid, trichloracetic acid and/or nitric acid, may be employed. For specific method information, please ask for detailed FOSS Analytical Application Notes. Fibertec™ Systems for any fibre determination needs: Low fat samples 1093 Cyclotec™ Mill Medium fat samples 1090 Cemotec™ Mill Enzymatic Balance Method High fat samples 2094/2096 Homogenizer 1095 Knifetec™ Chemical Fibertec™ E High workloads Fibertec™ 2010 Medium workloads Fibertec™ M6 Drying Oven Balance Muffle furnance Balance FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0401E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Kjeltec™ – el estándar para el análisis preciso, seguro y fácil de la proteína EXACTITUD Con el enfoque en la exactitud Alcanzar la mayor exactitud posible es el objetivo de todo análisis. Ésta ha sido siempre la pauta de FOSS en el desarrollo de nuevos instrumentos y sistemas. Hoy, 30 años después de que se lanzara el primer Kjeltec™, FOSS mantiene una posición líder en el análisis de nitrógeno/proteína. 2 Nuestra meta fundamental es usar la tecnología disponible para eliminar los factores humanos y técnicos que causan errores en los resultados, o que cambian el funcionamiento de los analizadores con el tiempo. Un Kjeltec de FOSS hace fácil y fiable el análisis de rutina. La generación Serie Azul de Kjeltec esta diseñada para lograr la mayor exactitud y precisión posible en el análisis Kjeldahl de nitrógeno. Para corresponder a todos los tipos de requisitos analíticos, la gama cuenta con varios instrumentos, desde unidades de destilación manual a sistemas totalmente automatizados, con auto-muestreo, para el funcionamiento desatendido. Una de las características que aseguran la más alta exactitud es el software interactivo, que ayuda al operario a evitar errores. El funcionamiento del analizador puede verificarse fácilmente usando el test de recuperación de rutina incorporado. Otro ejemplo es la posibilidad de predefinir un amplio número de procedimientos automatizados, especialmente útil en laboratorios que usan varios métodos de destilación. El único con tritación colorimétrica incorporada proporciona una exactitud incomparable y es la metodología recomendada por las recientes normas AOAC, ISO/IDF y otras organizaciones de estandarización. Las bombas de fuelle miden el volumen real de reactivo que se dosifica, lo que asegura la exactitud constantemente. Las ventajas adicionales son la estabilidad a largo plazo, el amplio rango de trabajo, velocidad de respuesta, simplicidad y ninguna necesidad de calibraciones. El método Kjeldahl es la técnica más versátil disponible para el análisis de nitrógeno. De hecho, éste es el único método que puede ser usado para análisis tanto de amonio como contenido de nitrógeno/ proteína en todo tipo de muestras Las superiores prestaciones se basan en el uso de que una precisa reacción ácido-base para la detección del punto final de la valoración. Esta reacción será la misma día a día y año a año. No está afectada por factores externos como el tiempo, la deriva o el factor humano 3 SEGURIDAD La seguridad es una responsabilidad La seguridad en su trabajo diario en el laboratorio es su responsabilidad. Sin embargo, es nuestra responsabilidad desarrollar instrumentos que hagan su tarea tan simple como sea posible para lograr sus objetivos. Cuanta más seguridad incorporemos en el instrumento, menos tendrá usted que preocuparse al manejarlo. Un Kjeltec™ de FOSS hace el análisis rutinario más seguro. 4 La gama de Kjeltec de FOSS cumple con las normas de seguridad en el análisis de nitrógeno/proteína por método Kjeldahl. Los instrumentos están equipados con un conjunto de elementos de seguridad incorporados, tales como sensores que detectan si el tubo está en su sitio o no, si la puerta y/o la tapa frontal están abiertas, y si el nivel de reactivo es demasiado alto o bajo. También están equipados con un rápido y fiable sistema de vaciado de tubos, que sustituye el manejo manual de reactivos calientes después de la destilación. Cuando cualquiera de los sensores se activa, el sistema se detiene y muestra en la pantalla y/o imprime la razón de esta interrupción. El mensaje obtenido indica la acción correctiva necesaria. El analizador Kjeltec™ contiene numerosos sensores para asegurar un manejo seguro. Cuando los sensores del sistema indican un error, el sistema se detiene y muestra la razón de la interrupción por pantalla y/o por listado. Además, la nueva tecnología patentada SAfE (Steam Addition for Equilibration) mejora la seguridad del analizador a través de un procedimiento de mezclado de los reactivos especial que reduce la reacción exotérmica cuando se añade el álcali a la mezcla de digestión, y elimina la necesidad de predilución manual de muestras. Las pastas semisólidas de la mezcla sal/ácido restantes de la digestión, se disuelven con suavidad. Si un instrumento puede funcionar con sus puertas y cubiertas abiertas, no garantiza la seguridad durante la operación . Si el instrumento continúa con el análisis incluso si no hay tubo en la posición, ese instrumento es inseguro tenga puertas o no. DELAY La tecnología patentada SAfE (Steam Addition for Equilibration) mejora la seguridad del analizador a través de un procedimiento de mezclado de los reactivos especial. Después de la adición del agua, comienza el vapor, se mezclan los contenidos del tubo, y las gradientes de concentración se reducen al mínimo. Se agrega el álcali y se produce un cambio gradual de ácido a las condiciones alcalinas, mientras la pasta de sal se disuelve. El procedimiento SAfE ahorra tiempo, mejora la seguridad y previene la pérdida potencial de nitrógeno. AGUA SAfE PATENTED AGUA/ÁLCALI ÁLCALI SAL/ÁCIDO Los gradientes de reactivos permanecen SAL/ÁCIDO La mezcla de reactivos minimiza el gradiente 5 ... Esto es lo que obtiene Un coste más bajo del análisis Gracias a aplicaciones de rutina optimizadas los costes de funcionamiento se mantienen bajos. Eficacia más alta El tiempo de inactividad y gastos de mantenimiento se reducen al mínimo gracias al empleo de una cuidadosa selección de componentes de larga duración. El equipo está construido de modo que las superficies expuestas a reactivos están fabricadas con plásticos resistentes a materiales químicos y libres de corrosión, etiquetados para el reciclaje. Naturalmente todas las partes que son expuestas a las sustancias químicas son fáciles para limpiar. Los programas de mantenimiento rutinario se estipulan de acuerdo con las rutinas GLP. Rendimiento más alto Las muestras se pueden manejar en lotes, lo que simplifica la carga y la capacidad de trazabilidad de las muestras. En combinación con nuestro sistema de automuestreo, Kjeltec asegura el proceso de hasta 60 muestras, sin transferencia de la muestra. Simplemente cargue los porta-muestras directamente desde el bloque de digestión y el Kjeltec realizará el análisis exacto y desatendido durante 4 horas. Hay que mencionar de nuevo, que al ser el único equipo con titración colorimétrica incorporada no requiere esfuerzos de calibración. Conocimiento mejorado Además, cuando usted escoge FOSS como su compañero en el laboratorio adquiere algo que puede significar la diferencia entre éxito y fracaso. Adquiere acceso a toda la experiencia de una empresa de análisis líder mundial dentro del campo de alimentos, piensos y análisis de agua. FOSS está representado en más de 100 países. El Kjeltec de FOSS ofrece una relación calidadprecio sin igual y hace beneficioso el análisis rutinario. Con un Analizador Kjeltec, el análisis rutinario se hace muy sencillo. La documentación y el soporte técnico de FOSS aseguran resultados exactos, disminuyen el tiempo de inactividad y reducen gastos operacionales. Simplemente cargue los porta-muestras directamente desde el bloque de digestión y el Kjeltec realizará el análisis exacto y desatendido durante 4 horas. Se pueden cargar hasta un máximo de 60 muestras. Un 1% de Diferencia La precisión es el criterio más importante para una buena economía de por vida. El ejemplo está en la industria de la alimentación, donde el coste de materia prima afecta a la rentabilidad del productor considerablemente. COMPONENTE Materia Prima Costes Fijos Costes Mano de Obra Beneficio (%) SOBRE PRECIO VENTA 80 10 5 5 79 10 5 6 (=20% aumento beneficio) 7 KJELTEC ™ 2200 KJELTEC ™ 2300 KJELTEC ™ 2400 KJELTEC ™ 2400/2460 estándar 1 programa estándar estándar estándar 5 programas estándar estándar estándar 10 programas estándar estándar estándar 10 programas estándar estándar estándar 5 programas estándar estándar – <4 Min Manual Automático Manual estándar – estándar estándar – – estándar <3 Min 30 s Automático Automático estándar/opcional estándar estándar estándar estándar estándar estándar estándar estándar – opcional – – – – – – estándar – – 2200W 1 l/min a 15°C estándar – estándar <3 Min 30 s Automático Automático Automático estándar estándar estándar estándar estándar estándar estándar estándar estándar – 400 estándar opcional – estándar estándar estándar opcional – 2200W 1 l/min a 15°C estándar – estándar <3 Min 30 s Automático Automático Automático estándar estándar estándar estándar estándar estándar estándar estándar estándar – 1600 estándar opcional estándar estándar estándar estándar opcional opcional 2200W 1 l/min a 15°C estándar estándar estándar <3 Min 30 s Automático Automático Automático estándar estándar estándar estándar estándar estándar estándar estándar estándar – 800 estándar opcional estándar estándar estándar estándar opcional estándar 2200W 1 l/min a 15°C estándar estándar Seguridad de reinicio – – – – – – – – – – – – 1900W 1 l/min a 15°C – – Dedicated Analytical Solutions FOSS Analytical AB Box 70 SE-263 21 Höganäs, Sweden. Tel +46 42 36 15 00. Fax +46 42 34 03 49. E-mail [email protected] Representatives in 100 countries. www.foss.dk Laholms Tryckeri AB, Laholm, Sweden KJELTEC ™ 2100 Generador automático de vapor Programable Sistema de ahorro de agua Cabezal de expansion de polipropeno Recipiente de vaciado de tubos de polipropeno Tiempo de destilación Adición de agua de dilución Adición de álcali Adición de solución receptora Bombas de fuelle para reactivos Alarmas de reactivo Bandeja de goteo removible Seguridad en la puerta interactiva Puerta de seguridad removible Seguridad de “tubo de posición” Sensor reemplazo de tubo Vaciado de tubo / recogida residuos Sistema de tritación colorimétrica Conexión a valorador externo Almacenaje datos crudos Cálculo resultados Impresora Interface para balanza Interface para PC Bureta intercambiable Software de servicio Bypass de la tritación Sistema de automuestreo Potencia Consumo de agua cuando sólo destila Multilenguaje SW Ajustes protegidos por clave Part No. 99990222ES/0412 UNIDAD DE DESTILACION In the interest of product development we reserve the right to alter specifications without prior notice. La gama Kjeltec™ de FOSS Kjeltec™ 8100 Unidad de destilación manual Unidad de destilación sencilla de utilizar para el análisis Kjeldahl de nitrógeno/proteína, amonio-nitrógeno, TKN, Destilación directa (DD), ácidos/bases volátiles, etc.(en la foto también se muestra; TecatorTM Digestor 20 Auto Elevador y el Lavador) Funciones & Ventajas: • Facilidad de uso con la dilución, adición de álcali, destilación y vaciado del tubo automáticos. Descripción: La Unidad de Destilación Kjeltec™ 8100 es una solución simple y fiable de destilación segura y semiautomática. • El generador variable del vapor de salida amplía el área de aplicación a otros componentes volátiles. La posibilidad de preprogramar los tiempos de la adición de álcali y de la destilación ayuda a conseguir resultados precisos con independencia del operador. • Procedimientos oficiales y precisos (ISO, AOAC, EPA, DIN, etc.) que simplifican la validación. • Función SAfE* patentada para la destilación segura de tubos con presencia de precipitados. • Sistemas de seguridad incorporados para protección de usuarios. • El control con ajuste automático del agua de refrigeración ahorra agua y reduce costes. • Bombas de fuelle para la dispensación precisa de reactivos. • Cabezal de expansión de plástico resistente al álcali para larga vida útil. Las bombas de fuelle de precisión proporcionan una estabilidad a largo plazo en la dispensación de reactivos. La unidad va equipada de sensores para la puerta de seguridad, plataforma del tubo y temperatura del destilado, así como sensores de nivel y sobrepresión para el generador variable del vapor de salida. La tecnología patentada SAfE* mejora la seguridad mediante un procedimiento de mezclado, reduciendo la reacción exotérmica entre el álcali y el ácido durante la destilación. El usuario está totalmente protegido por la puerta de seguridad de rotación única que debe estar cerrada con un tubo en su sitio antes de que la unidad puede funcionar. La puerta de seguridad y la bandeja de goteo pueden extraerse fácilmente para su limpieza. El agua de refrigeración se utiliza únicamente durante el análisis lo que permite ahorros adicionales mediante la función automática de control de flujo. El conjunto de aplicaciones optimizadas hace que los costes de ejecución se reduzcan aún más. Mediante la utilización de componentes seleccionados se minimizan los costes de parada y mantenimiento. El programa de mantenimiento rutinario permite incluir rutinas de Buenas Prácticas de Laboratorio (BPL). * Adición de vapor para homogenización Dedicated Analytical Solutions Accesorios opcionales: Para instalar un sistema Kjeldahl completo, debe seleccionarse un Digestor con los accesorios adecuados, como Aspirador, Lavador, tubos de de muestra y pastillas catalizadoras. Los detalles se pueden encontrar en la hoja de datos técnicos de los sistemas Tecator™ Digestor. 60032042 Tanque 20 l (álcali/agua/residuos) sin sensores de nivel 60032043 Kit de sensor de nivel para residuos 60032044 Kit de sensor de nivel para reactivos 1002-022 Unidad de valoración completa, 50 ml 60030343 Adaptador para tubos Büchi 10000089 Cesta para 20 matraces de receptor (250 ml) 10000164 Matraces de receptor, 250 ml (juego de 10) 10000897 Dispositivo para manejar tubos de digestión Datos de funcionamiento a 230 V: Tiempo de destilación: 3,5 min a 30 mg N (6,5 min a 200 mg N) Capacidad destilación: ~ 40 ml/min Rango medición: 1 – 200 mg N Reproducibilidad: 1% RSD (incluyendo paso de digestión) Recuperación: > 99,5 % a niveles nitrógeno entre 1 - 200 mg N Drenaje del tubo: 200 ml en menos de 10 s Volúmenes bomba reactivos: 0 - 150 ml en intervalos de 10 ml Retardo: 0 - 1800 s SAfEPatented: 0 - 15 s Requisitos de instalación: Fuente de alimentación: 200 - 240 V, 50 - 60 Hz Consumo eléctrico: 2.200 W Consumo de agua: 2 l/min a temperatura de agua de 30ºC (sólo durante destilación) 1 l/min a temperatura de agua de 15ºC Temperatura ambiente: máx. 40ºC Humedad ambiente: máx. 80 % relativa Peso neto: 30 kg Dimensiones: A × P × Al = 480 × 580 × 690 mm Drenaje: Sólo para agua de refrigeración FOSS Analytical Slangerupgade 69 DK-3400 Hilleroed Dinamarca Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 1026210, Edición 1 ES, Enero 2009 Números de pedido: 81000001 Unidad de Destilación Manual, 200 – 240 V, 50 – 60 Hz que incluye: Unidad de destilación controlada por microprocesador con drenaje de tubo y adición automática de agua y álcali. Generador de vapor incorporado para agua deionizada o agua corriente. Completa con tanques de álcali/agua/residuos con sensores de nivel, matraz de receptor, adaptador combi para tubos de 100, 250, 400 & 750 ml y tubos de digestión de 100 & 250 ml. Kjeltec™ 8200 Unidad de Destilación Automática Destilación automática para el análisis Kjeldahl de nitrógeno/proteína, amonio-nitrógeno, TKN, Destilación directa (DD), ácidos/bases volátiles, etc. (En la foto tambien se muestra; TecatorTM Digestor 20 Auto Elevador y el Lavador) Funciones & Ventajas: • Facilidad de uso con la destilación automática totalmente programable, que incluye la dilución de muestras, adición de álcali & receptor, destilación y drenaje del tubo. • El generador variable del vapor de salida amplía el área de aplicación a otros componentes volátiles. • Procedimientos oficiales y precisos (ISO, AOAC, EPA, DIN, etc.) que simplifican la validación. • Función SAfE* patentada para la destilación segura de tubos con presencia de precipitados. • Sistemas de seguridad incorporados para protección de usuarios. • El control con ajuste automático del agua de refrigeración ahorra agua y reduce costes. • El control de temperatura del destilado asegura la precisión de los resultados. • Bombas de fuelle para la dispensación precisa de reactivos. • Cabezal de expansion de plástico/recipiente de drenaje de tubos resistentes al álcali para una larga vida útil. • Sistema del analizador y muestreador actualizables de forma modular. Descripción: La unidad de Destilación Automática Kjeltec™ 8200 es la solución más avanzada de destilación automática y segura. Las bombas de fuelle de precisión proporcionan una estabilidad a largo plazo en la dispensación de reactivos. La unidad va equipada con sensores para la puerta de seguridad, plataforma del tubo y temperatura del destilado, así como sensores de nivel y sobrepresión para el generador variable del vapor de salida. La tecnología patentada SAfE* mejora la seguridad mediante un procedimiento de mezclado, reduciendo la reacción exotérmica entre el álcali y el ácido durante la destilación y eliminando la necesidad de predilución manual. Un sistema rápido de drenaje de tubos elimina la necesidad de manipular reactivos calientes tras la destilación. El usuario está totalmente protegido por la puerta de seguridad de rotación, única en el mercado, que debe estar cerrada con un tubo en su sitio antes de que la unidad puede funcionar. La puerta de seguridad y la bandeja de goteo pueden extraerse fácilmente para su limpieza. El agua de refrigeración se utiliza únicamente durante el análisis lo que permite ahorros adicionales mediante la función automática de control de flujo. El Kjeltec 8200 ofrece la opción de actualizar la unidad a un analizador Kjeltec 8400 completo cuando lo requiera su negocio. También se puede añadir al analizador un cambiador de muestras de 20 o 60 posiciones, lo que proporciona un funcionamiento desatendido totalmente automático. * Adición de vapor para homogenización Dedicated Analytical Solutions Números de pedido: 82000001 Unidad de Destilación Automática, 200 – 240 V, 50 – 60 Hz que incluye: Unidad de destilación controlada por microprocesador con drenaje de tubo y adición automática de agua, álcali y solución receptora. Generador de vapor incorporado para agua deionizada o agua corriente. Completa con tanques de álcali/agua/receptor/residuos con sensores de nivel, matraz de receptor, adaptador combi para tubos de 100, 250, 400 & 750 ml y tubos de digestión de 100 & 250 ml, dispositivo de manejo de tubos de digestión. 60032041 Kit para by pass de la destilación 60032073 Cable para conexión de valorador externo 60032040 Kit para actualización de la unidad de Destilación Kjeltec 8200 a la unidad Analizador Kjeltec 8400 Accesorios opcionales: Para instalar un sistema Kjeldahl completo, debe seleccionarse un Digestor con los accesorios adecuados, como Aspirador, Lavador, tubos de muestra y pastillas catalizadoras. Los detalles se pueden encontrar en la hoja de datos técnicos de los sistemas Tecator™ Digestor. Datos de funcionamiento a 230 V: Tiempo de destilación: 3,5 min a 30 mg N (6,5 min a 200 mg N) Capacidad destilación: ~ 40 ml/min Rango medición: 1 – 200 mg N Reproducibilidad: 1% RSD (incluyendo paso de digestión) Recuperación: > 99,5 % a niveles nitrógeno entre 1 - 200 mg N Drenaje del tubo: 200 ml en menos de 10 s Volúmenes bomba reactivos: 0 - 150 ml en intervalos de 10 ml Retardo: 0 – 1800 segundos SAfEPatented: 0 – 15 segundos Requisitos de instalación: Fuente de alimentación: 200 - 240 V, 50 - 60 Hz Consumo eléctrico: 2.200 W Consumo de agua: 2 l/min a temperatura de agua de 30 ºC (sólo durante destilación) 1 l/min a temperatura de agua de 15 ºC Temperatura ambiente: máx. 40ºC Humedad ambiente: máx. 80 % relativa Peso neto: 30 kg Dimensiones: A × P × Al = 480 × 580 × 690 mm Drenaje: Sólo para agua de refrigeración Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 1026216, Edición 1 ES, Enero 2009 FOSS Analytical Slangerupgade 69 DK-3400 Hilleroed Dinamarca 60032042 Tanque 20 l (álcali/agua/residuos) sin sensores de nivel 60032043 Kit de sensor de nivel para residuos 60032044 Kit de sensor de nivel para reactivos 1002-022 Unidad de valoración completa, 50 ml 60030343 Adaptador para tubos Büchi 10000089 Cesta para 20 matraces de receptor (250 ml) 10000164 Matraces de receptor, 250 ml (juego de 10) 10000897 Dispositivo para manejar tubos de digestión Kjeltec™ 8400/8420/8460 Sistemas automáticos de muestreo Análisis totalmente automático de nitrógeno/proteínas o TKN en digestiones Kjeldahl, nitrógeno de amoniaco, destilación directa (DD) etc. (En la foto también se muestra: Tecator™ Digestor 20 Auto Elevador y el Lavador) Funciones & Ventajas: • Procesos totalmente automáticos de dilución, manejo de reactivos, destilación, valoración, cálculo e informes • El cambiador de muestras opcional de 20 o 60 posiciones proporciona un funcionamiento totalmente desatendido • Sistema de valoración colorimétrico acreditado oficialmente (AOAC, EPA, DIN, ISO) que simplifica la validación. • Sistemas de seguridad incorporados para protección de usuarios. • Función SAfE* patentada para la destilación segura de muestras que forman precipitados. • El control de temperatura del destilado asegura resultados precisos • El autoajuste del control de agua de enfriamiento ahorra agua • Bombas de fuelle para la dispensación precisa de reactivos • Cabezal de expansión de plástico/recipiente de drenaje de tubos resistentes al álcali para una larga vida útil • Bureta intercambiable para el cambio sencillo del valorante • La conexión Ethernet elimina los problemas de comunicación con impresoras y balanzas • Control completo del PC de todos los registros e informes a través del software opcional de gestión de datos Descripción: Los sistemas Analizador Kjeltec™ 8400 y los Muestreadores 8420 o 8460 son las soluciones más avanzadas de automatización en el laboratorio Kjeldahl con independencia de la producción de muestras. El desarrollo de rutinas de Buenas Prácticas de Laboratorio (BPL) se realiza mediante rutinas de registro de muestras y pruebas de rendimiento y la documentación completa de todos los eventos realizados durante el análisis a través de la conexión Balanza/ Impresora/LIMS. Las bombas de fuelle y una bureta rellenable de gran precisión proporcionan estabilidad a largo plazo en la dispensación de reactivos. El flujo de agua de enfriamiento se controla automáticamente y un sensor de temperatura detiene la unidad si el destilado está demasiado caliente. Dispone de sensores que monitorizan que los tubos están en su sitio, puertas de seguridad, niveles de reactivos, nivel de agua y sobrepresión en el generador de vapor, proporcionando todo ello condiciones seguras para los usuarios. La tecnología SAfE* reduce la reacción exotérmica entre el álcali y el ácido, lo que elimina la necesidad de predilución manual de las muestras. Un sistema rápido de drenaje de tubos elimina la necesidad de manipular reactivos calientes. Los sistemas de muestreador toman los tubos directamente en sus bandejas de digestión original, lo que limita la manipulación y los errores de transferencia de muestras. * Steam Addition for Equilibration (Adición de vapor para homogenización) Dedicated Analytical Solutions Números de pedido: 84000001 Unidad Analizador Kjeltec™ 8400, 200 – 240 V, 50 - 60 Hz que consta de: Unidad automática de destilación / valoración con drenaje de tubo y generador de vapor incorporado para agua deionizada o agua corriente, completa con tanques de álcali/agua/receptor/residuos con sensores de nivel, adaptador combi de tubos de 100, 250, 400 y 750 ml para dispositivo de manejo de 100 & 250 ml 84200001 Kjeltec 8400 / Muestreador Kjeltec 8420 200 – 240 V, 50 - 60 Hz que consta de: Kjeltec 84000001 y 84200011 Muestreador Kjeltec 8420 para 20 muestras 84600001 Kjeltec 8400 / Muestreador Kjeltec 8460 200 – 240 V, 50 - 60 Hz que consta de: Kjeltec 84000001 y 84600011 Muestreador Kjeltec 8460 para 60 muestras Accesorios opcionales: Para instalar un sistema Kjeldahl completo, debe seleccionarse un Digestor con los accesorios adecuados, como Aspirador, Lavador, tubos de muestra y pastillas catalizadoras. Puede encontrar información adicional en la hoja de datos técnicos aparte de los sistemas Tecator™ Digestion. 60031631 Compass, software de PC para la unidad Analizador Kjeltec 8400 60028286 Tanque para valorante, completo con tubos 60032074 Dispositivo de Dosificación de Bureta para la calibración de la bureta. 10011512 Sensor de nivel para tanque de residuos 10011513 Sensor de nivel para tanque de reactivos 60032042 Tanque 20 l (álcali/agua/residuos) sin sensores de nivel 60032043 Kit de sensor de nivel para residuos 60032044 Kit de sensor de nivel para reactivos 60030343 Adaptador para tubos Büchi 10000897 Dispositivo para manejar tubos de digestión 84200011 Muestreador Kjeltec 8420 200 – 240 V, 50 – 60 Hz con accesorios necesarios para conectarse y funcionar con Kjeltec 8400 Muestreador Kjeltec 8460 200 – 240 V, 50 – 60 Hz con accesorios necesarios para conectarse y fun- cionar con Kjeltec 8400 Con tanque de agua integrado Datos de funcionamiento a 230 V: Capacidad automuestreador: Muestreador Kjeltec 8420, 1 bandeja con 20 tubos Kjeldahl de 250 ml o 400 ml Muestreador Kjeltec 8460, 3 bande- jas con 20 tubos Kjeldahl de 250 ml o 400 ml Capacidad almacenaje: 40 lotes (ilimitado con Compass) Tiempo de análisis: 3,5 min a 30 mg N (6,5 min a 200 mg N) Capacidad destilación: ~ 40 ml/min Rango medición: 1 – 200 mg N Reproducibilidad: 1% RSD (incluyendo paso de digestión) Recuperación: > 99,5 % a niveles nitrógeno entre 1 - 200 mg N Drenaje del tubo: 200 ml en menos de 10 segundos Volumen probeta: 35 ml Resolución probeta: 2.4 μl/intervalo Velocidad probeta: >0.5 ml/segundo Retardo: 0 – 1800 segundos SAfEPatented: 0 – 15 segundos FOSS Analytical Slangerupgade 69 DK-3400 Hilleroed Dinamarca Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk Requisitos de instalación: Fuente de alimentación: 200 - 240 V, 50 - 60 Hz Variación tolerable tensión: ± 10 % Consumo eléctrico: 2.200 W Consumo de agua: 2 l/min a temperatura de agua de 30ºC (sólo durante destilación) 1 l/min a temperatura de agua de 15 ºC Temperatura ambiente: máx. 40°C Humedad ambiente: máx. 80 % relativa Drenaje: Sólo para agua de refrigeración Peso neto: Kjeltec 8400 35 kg Muestreador Kjeltec 842071 kg Muestreador Kjeltec 846089 kg Dimensiones (A x P x Al): Kjeltec 8400 480 × 580 × 690 mm Muestreador Kjeltec 8420645 × 840 × 900 mm Muestreador Kjeltec 84601000 × 800 × 900 mm P/N 1026222, Edición 1 ES, Enero 2009 84600011 Mill Collection The Mill collection Introduction Good results starts with sample preparation. Errors caused by analytical instruments are very small compared to the errors associated with sample preparation. Badly prepared samples will automatically result in large analytical errors. The laboratory sample mill is an important but often overlooked link in the chain of analysis; so important that at FOSS Tecator we regard it as an integral part of the analytical system. We have therefore developed mills of our own to assure the best analytical results. They are convenient and safe to use and they cover a broad range of grinding applications, including preparation for both traditional wet chemistry and NIR/NIT analyses, with assured high repeatability and reproducibility. General description This Mill collection folder presents high quality products that can ensure reliability and reproducibility of the analysis. The Cemotec™ is optimized for solid samples with a high moisture content, and the Cyclotec™ Dedicated Analytical Solutions for dry samples that require a uniform particle size. The Knifetec™ is suitable for small (100 ml) samples of dry, moist or wet materials, and the robust Homogenizer for larger (0.2-2.5 kg) samples with a high fat or oil content. Various accessories and consumables are available to make routine sample preparation simple. They include a range of sample bottles, grinding rings, blades and impellers. Sample preparation is an important step in all analytical procedures. It is for example crucial to grind properly to obtain the highest quality of the analytical results. Analytical errors are more easily reduced in the sample preparation step than in any of the subsequent steps of the analysis. All samples should be prepared under the same conditions. On the following pages we show how our Mill collection can crush, grind, mix and homogenize dry samples to a consistency suitable for chemical analysis. Cemotec™ 1090 Sample Mill Sample grinding without moisture loss. Features: • Reliable classic working principle • Adjustable particle size • Low noise level Benefits: • No loss of moisture • Officially approved by the Swedish National Board of Agriculture for sample preparation prior to moisture analysis • Low maintenance demand Cemotec™ Mill Cemotec™ Accessories Description: The Cemotec™ Sample Mill is specially designed to grind grain and seed samples without losing any of the moisture content. It is however an excellent mill for all types of sample preparation where the requirements for fineness and uniformity of particle size are moderate. The Cemotec works on the tried-and-true principle of grinding between two discs, one stationary and one turning. The sample is introduced at the centre of the stationary disc and is crushed between the discs. The distance between the discs is easily adjusted by a graduated knob to control the fineness of the grist. The Cemotec works silently and effectively at relatively low speed. The rate of grinding is about 3 grams per second. Low speed means low noise, and dust is effectively contained by the seal between the outlet and the sample container. Cyclotec™ 1093 Sample Mill Rapid sample preparation for general laboratory analysis. Features: • High grinding speed, 4 grams per second • Adjustable particle size • Low noise level (75 dBA) Benefits: • No thermal degradation of the sample • Uniform particle size distribution • Easy handling of samples • High operator safety • Low maintenance demand • Recommended by the Canadian Grain Commission prior to NIR analysis • Approved by AOAC prior to NIR analysis (4.2.10 16th Ed.) Description: The Cyclotec™ Sample Mill is designed for rapid, uniform grinding of a wide variety of feeds, grains, leaves, etc. and also for grinding of chemicals, pharmaceuticals and similar products. Recovery of the sample is complete. Through its unique design the Cyclotec grinds samples by a high speed action. This action rolls the sample against the inner circumference of a durable grinding surface and then passes it through a fine mesh screen. The high volume air flow provides self cleaning action and minimum temperature rise; whole series of samples can be ground with minimal cross contamination and without cleanout between samples. Thermal degradation is minimized to provide more accurate results. The Cyclotec offers a very rapid and convenient solution to accurate sample preparation for a variety of analytical techniques, e.g. Kjeldahl, Infrared Reflectance, Direct Distillation, Crude Fibre and Extraction. Cyclotec™ Mill Cyclotec™ filled with holder for 500 ml sample bottle 2094 and 2096 Homogenizers Rapid maceration and homogenization of a variety of samples. Features: • Powerful cutting action at one or two speeds: 1500 or 1500/3000 rpm • Sample size from 0.2 to 2.5 kg • A variety of angled knives for different sample types • Knives and bowl in stainless steel • Safety switch • Sample preparation of meat products according to AOAC 983.18 Benefits: • Rapid and reproducible homogenization • Easy to clean • Robust construction Homogenizers The cutters Description: The 2094 and 2096 Homogenizers are designed for macerating and homogenizing of a variety of highmoisture, high-fat and fibrous samples. Application examples include: size reduction of forage and dry food and chemical products; homogenization of meat, fish, fruit, vegetables, prepared foods (such as pizza, meat pies and frozen meals) and chemical and pharmaceutical formulations. The Homogenizers allows frozen food samples to be homogenized in a short period of time, providing more accurate analyses of unstable constituents such as vitamins. A reproducible degree of homogenization is achieved by the mixing action obtained by the angled knives. Homogenization is accomplished through the high speed combined with a powerful cutting action. Angled knife blades produce a vertical flow within the batch and facilitate rapid and thorough homogenization. Complete homogenization is normally achieved in 20 to 60 seconds. A magnetic safety switch prevents the 2094 and 2096 Homogenizers from being operated without the transparent cover in the locked position. The 2094 and 2096 Homogenizers comes with a multipurpose micro-teeth cutter. For additional convenience extra stainless steel bowls and smooth blade cutters are available for both Homogenizers. For the 2096 Homogenizer a scalloped cutter is also available. 1095 Knifetec™ Sample Mill Rapid sample preparation of high-fat, high-moisture and fibrous samples. Features: • 20 000 rpm rotor blade for rapid grinding • Timer controlled • Sample size up to 100 ml initial volume • Water cooled • Safety switch stops rotor in less than 1 second Benefits: • Integral tilting system, fully removable lid and rotor blade to facilitate cleaning • Chamber cooling option reduces adhesion of sample to the wall of the grinder • No heat generated, making samples suitable for moisture analysis Description: The 1095 Knifetec™ Sample Mill is designed for the preparation of high fat, high moisture and fibrous samples prior to analysis. Oilseeds, prepared foods, meat products, fruit, vegetables, grains, seeds and feed samples are examples of suitable sample types. The high speed rotor blade and timer control ensure very fast and reproducible sample preparation time after time. The normal time to prepare samples is from two to ten seconds. A safety switch located in the lid prevents accidental operation of the mill with the lid removed. The Knifetec is equipped with a grinding chamber cooling feature which enables it to be connected to a cold water tap or other laboratory chilling devices. Samples containing high levels of fat have a tendency to stick to the wall of the chamber as the fat softens during grinding, preventing adequate homogenisation. Fibrous samples may generate heat due to friction. Utilizing the cooling option overcomes both these problems, ensuring satisfactory sample preparation. The fully removable lid, the stainless steel chamber and the removable rotor blade of the Knifetec simplify sample removal and cleaning between samples. This saves a considerable amount of time compared to other techniques. An integral tilting system also simplifies emptying and cleaning. The design of the 1095 Knifetec ensures rapid, reproducible and safe preparation. Knifetec™ The sample tray and rotor blades Ordering information: Cemotec™ 1090 Sample Mill: 1090-001 Cemotec 1090 Sample Mill complete with hardened Grinding Discs, disposable Sample Bottles (20), Allen Keys 4 and 5 mm, Hopper with cover, Users’ Manual, 200-230 V, 50-60 Hz 1090-002 Same as above but for 115 V, 50-60 Hz Homogenizer 2094 2094-001 Homogenizer complete with stainless steel bowl (3.5 l), multipurpose cutter with microteeth blades, transparent lid and User’s Manual, 1 500 rpm, 1 × 230 V, 50 Hz 2094-002 Same as above but for 1 × 115 V, 60 Hz Accessories 10003923 Disposable Sample Bottles (150 ml) of polypro pylene with snap-on lid 100/pkg 10003924 Disposable Sample Bottles (150 ml) of polypro pylene with snap-on lid 500/pkg 10003965 Grinding Discs (1 pair) 10003922 Seal for Sample Bottle Accessories 19000660 Stainless steel bowl. 3,5 l 19000662 Transparent lid 19000654 Cutter with smooth blades 19000659 Cutter with microteeth blades 19000634 Grindstone for blades Cyclotec™ 1093 Sample Mill 1093-001 Cyclotec 1093 Sample Mill complete with Sample Bottles (125 ml) with snap-on lid (2), screens 0.5 and 1.0 mm, Allen Keys 4 and 6 mm, Seal for Grinding Chamber, Paper Bag for Dust Collection, Seal for Sample Bottle, Users’ Manual, 200-230 V, 50 Hz 1093-002 Same as above but for 115 V 60 Hz 1093-003 Same as above but for 200-230 V 60 Hz 1093-004 Same as above but for 115 V 50 Hz Accessories 10000893 Sample Bottles, dark glass for UV protection, 125 ml, case of 104 10003679 Sample Bottles, dark glass for UV protection, 125 ml, case of 52 15220023 Lid for Sample Bottles 10002485 Large Inlet/Forage Assembly Kit 10002488 Dust Collection with external connection 10002537 Paper Bags for Dust Collection, pack of 10 10002000 Dust Filter Pad 10014484 Screen 0.3 mm (use together with 1 or 2 mm Screen) 10000820 Screen 0.5 mm 10005864 Screen 0.8 mm 10001989 Screen 1.0 mm 10002715 Screen 2.0 mm 10001990 Seal for Sample Bottle 10001992 Seal for Grinding Chamber 10001993 Seal for Dust Filter Cover 10008180 Seal Kit 10001991 Impeller, Standard 10002666 Impeller, Nickel-plated for mineral analysis 10009833 Holder for 500 ml sample bottle 10013478 Sample bottle 500 ml with lid, 1 pcs 10004463 Grinding Ring, made of tungsten carbide Standard 10013810 Grinding Ring for Hard sample 10006680 Grinding Ring Heavy Metals 3/set Homogenizer 2096 2096-001 Homogenizer complete with stainless steel bowl (5.5 l), multipurpose cutter with microteeth blades, transparent lid with integrated scraper and Users’s Manual, 1 500 / 3 000 rpm, 3 × 400 V, 50 Hz 2096-002 Same as above but only 1 500 rpm for 1-phase, 115 V, 60 Hz Accessories 19000605 Stainless steel bowl. 5,5 l 19000655 Transparent lid with scraper 19000656 Cutter with smooth blades 19000657 Cutter with scalloped blades 19000658 Cutter with microteeth blades 19000634 Grindstone for blades Knifetec™ 1095 Sample Mill 1095-001 Knifetec Sample Mill complete with rotor blade, PVC tubing 4m, tubing clamp, Users’ Manual, 230 V, 50-60 Hz 1095-002 Same as above and also including Transformer for 115 V operation, 50-60 Hz Accessories 10005980 Rotor blade standard, complete 10008651 Rotor blade with sharp knives complete 10013135 Rotor blade for small volume 10013136 Rotor blade for pellets 10005960 Distance for Rotor blade 10003923 Disposable Sample Bottles (150 ml) of polypro pylene with snap-on lid 100/set 10003924 Disposable Sample Bottles (150 ml) of polypro pylene with snap-on lid 500/set 10008467 Stainless steel tray *Ordering information: Use the above specified Cat. Nos. together with the text. Installation requirements: Cemotec™ 1090 Sample Mill Power supply: 200-230 V, 50-60 Hz 115 V, 50-60 Hz Power consumption: 600 W Net weight:18 kg Dimensions, L × D × H: 220 × 400 × 400 mm Rotor speed, grinding disc 3 000 rpm Homogenizer 2096 Power supply: Power consumption: Net weight: Capacity: Rotor speed: Dimensions, L × D × H: Cyclotec™ 1093 Sample Mill Power supply: 200-230 V 50 Hz 115 V 60 Hz 200-230 V 60 Hz 115 V 50 Hz Power consumption: 600 W Net weight: 18 kg Dimensions, L × D × H: 220 × 300 × 400 mm Rotor speed, impeller 10 000 rpm Homogenizer 2094 Power supply: Power consumption: Net weight: Capacity: Rotor speed: Dimensions, L × D × H: 230 V 50 Hz 1-phase 115 V 60 Hz 1-phase 500 W 15 kg 3,5 l bowl. Do not exceed 1,5 l liquid content 1 500 rpm 250 × 410 × 300 mm 400 V 50 Hz 3-phase 115 V 60 Hz 1-phase 750 W 1-phase / 1400 W 3-phase 25,5 kg 5,5 l bowl. Do not exceed 2,5 l liquid content 1 500 rpm (1-phase) / 1 500 & 3 000 rpm (3-phase) 270 × 460 × 400 mm Knifetec™ 1095 Sample Mill Power supply: 230 V 50-60 Hz incl Transformer 115/230V Power consumption: 120 W Net weight: 7.5 kg Dimensions, L × D × H: 190 × 290 × 250 mm Rotor speed: 20 000 rpm Water supply: 2 l/min, 8-10°C Performance data: Feature Cemotec™ Cyclotec™ Homogenizer Knifetec™ Sample Type Dry samples prior to moisture analysis, up to 20 % moisture and/or 20% fat Dry samples prior to wet chemistry or IR analysis, up to 15% moisture and/or fat content up to 20% High-moisture, highfat and fibrous samples High-moisture, highfat and fibrous samples Applications Grains, seeds, feed, beans, dry granular foods, fertilizer, tablets Grains, seeds, cereals, forage, feed, leaves, tablets, tobacco, lime, coal Forage, dry food, meat, fish, vegetables, prepared foods, chemical and pharmaceutical formulations Oilseeds, prepared foods, meat products, fruit, vegetables, grains, seeds, and feed Sample Size Up to 14 mm ∅ Up to 10 mm, large inlet up to 40 mm 0.2 - 2.5 kg Maximum 100 ml (50 - 150 g) Grinding Principle Two discs, one rotating one stationary Turbine and sieve Rotor knives Rotor blade Grinding Rate/Time Appr. 3 g/s Appr. 4 g/s 20 to 60 s 2 to 10 seconds Grinding Speed Grinding disc 3 000 rpm Impeller 10 000 rpm Blade 1 500 or 1 500 / 3 000 rpm Blade 20 000 rpm Particle Size Coarse grist Fine and uniform grist with 0.5 mm screen: max 0.45 mm with 1.0 mm screen: max 0.75 mm Depending on sample Depending on sample Timer No No No Yes Safety Microswitch Microswitch Magnetic switch Microswitch Cleaning Low cross contamination Low cross contamination Manual Manual Application overview Application Cemotec™ Cyclotec™ Homogenizer Knifetec™ +++ +++ + +++ Soya beans + + + +++ Rapeseed + + + +++ +++ +++ + ++ Grains of wheat, oats, barley, rye Feed pellets Hay/Straw ++ + Vegetables/Fruit +++ + Meat ++ Meat products +++ + Mixed food +++ + Subsequent analysis Application Cemotec™ Cyclotec™ Homogenizer Knifetec™ Protein +++ +++ +++ +++ Fat low Fat high +++ +++ ++ +++ +++ +++ Fibre crude Fibre dietary +++ +++ + ++ Moisture low & low fat Moisture low & high fat Moisture high & low fat Moisture hig & high fat +++ +++ ++ +++ +++ ++ +++ +++ +++ +++ +++ Reference methods ++ NIR/NIT ++ very good FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk +++ + good P/N 9999 0730E, Issue 2 GB, Nov 2005 +++ excellent + Tecator™ Digestion Systems Tecator™ Digestion Unit Auto Lift 20 together with the Scrubber, for fully unattended operation. Features and benefits: Tecator™ Digestion units, with integrated programmable controllers, can be combined with a range of accessories offering: • fully automated digestion with user interface adapting to actual product configuration • convenient, safe and flexible operation • GLP-support through two way PC communication • economy of chemicals, energy, labour, space and time • efficient fume containment through optional exhaust • efficient fume removal through optional scrubber The systems, with extensive application support, are compatible with Kjeltec™ Distilling Units. General Description: The products described in this brochure can be combined to match individual needs, from units capable of handling just a few samples a day up to fully automated systems for high sample throughput. Three configurations; Auto Lift, Auto Rack, and Basic; are available for either 250 ml or 100 ml digestion tubes; which must be specified when ordering; dependant on the application required. A Digestion System is based on a Digestion Unit and tube rack with capacity for either eight or twenty tubes. For most Kjeldahl digestions straight 250 ml tubes are recommended. To comply with GLP and Health & Safety requirements we recommend that all Digestion Units are used with an Exhaust Manifold or Reflux Head, and are located in a fume cupboard. An optional Scrubber Unit creates a fully integrated system. Dedicated Analytical Solutions Auto Lift versions, with exhaust docking facility, allow fully automated unattended operation contributing to safety and convenience by eliminating handling of hot chemicals and saving valuable bench space. Auto Rack versions allow automated digestions but require manual placement of Tube Rack and Exhaust Manifold which are stored above the Digestion Unit in a similar position to the Auto Lift. All Auto models have an integrated programmer which precisely controls temperature(s) and timing together with connected components. The analysis cycle is clearly monitored on the graphical display. Auto models can be connected to a PC for data logging and downloading of standard, and user defined, applications. The programmer has various password protected access levels to prevent unauthorised modification and comply with accreditation procedures. Basic versions have built in, user definable, temperature and time control clearly viewed on the display. Auto Rack versions can be upgraded to Auto Lift systems to spread the investment across fiscal periods. The Basic version can be fitted with a rack system at any time to save valuable bench space. Various accessories are available to make routine analysis safe and simple. They include a range of test tubes, tube racks, retainer plates for washing, fume removal systems, boiling rods and catalyst tablets. Digestion system products and accessories are described in more detail on the following pages. All Digestion Systems are based on one of the “four” Digestion Units for either 250 ml or 100 ml tubes*. * Tube volume to be specified when ordering your digestion unit. Digestion Units The Digestion Units are insulated to minimise heat transfer to the surroundings and allow fast, even heating, thus giving good working conditions as well as saving energy. They are designed for batches of either eight or twenty test tubes with three different levels of control. The Auto versions have an integrated all activity controller, that adapts to the actual product configuration and is programmable using the software supplied. When a Lift or Scrubber Unit is connected they are controlled by the selected application program, which is stored in the Digestion Unit memory, allowing fully unattended operation. The Basic versions have a built in, user definable, time and temperature controller and display. Software for Auto Lift and Auto Rack systems There are two separate software systems in Auto versions. The embedded software controls all necessary functions of the digestion system on a routine basis. The PC Application software, delivered on CD, is system management software which enables default values to be modified according to the needs of the authorised user. To process different type of samples a wide range of Tecator™ applications can be downloaded from the database included on the CD. Up to 254 Applications can be stored in the digestion unit at any one time, of which half can be standard Tecator™ format and half can be user defined. Each application can control up to 23 steps including all Temperature; ramp and time; Lift and Scrubber steps. The software supports Good Laboratory Practice (GLP) routines and accreditation procedures. Data for date, time, temperature, application used, operator, batch number, and ID number are constantly logged. The 32 most recent Data Logs can be stored in the Digestion Unit. All this information can be transferred to a PC for archiving and generation of up to seven different reports. Original Tecator™ Applications cannot be changed. They can be adapted and saved as different files or the user can design their own applications. To prevent unauthorised changes, and comply with GLP routines, the software is password protected at different authority levels. Audible alerts Audible ‘’ready’’ or ‘’cycle over’’ alerts advise the user when the digestion application is completed Audible ‘’alarm’’ alerts advise the user when errors/interruptions occur within the running application program Alerts can be adjusted High, Low or Off. Power failure or interruption of power supply In the event of power failure the digestion unit operation is automatically handled in the safest way. If the failure or interruption occurs at any time up to or during preheating, before digestion has started, the cycle will continue when power is restored. Following a power failure or interruption, after the digestion cycle has started, the unit stops heating immediately and the Lift goes to the cooling position with exhaust in place, upon restoration of power. This complies with GLP and Health & Safety routines. These interruptions will be recorded in the data logging function. Communication with PC The PC Application software has two way communication with the Digestion Unit via the serial RS232 cable supplied as standard. Alternatively communication can be achieved through Bluetooth TDK blu2i modules, or equivalent, available from your computer supplier. Language versions The software is available in the following languages:Chinese (simplified), Dutch, English, French, German, Italian, Japanese, Korean, Polish, Russian, Spanish, and Swedish. Other languages can be accommodated in co-operation with your local supplier. Auto Lift Systems Auto Lift systems facilitate highly automated procedures, eliminating heavy and risky handling of hot chemicals. Valuable bench space is saved, as the Tube Rack and Exhaust Manifold are positioned above the Digestion Unit. A Tube Rack with 8 or 20 tubes is placed in the Lift. The application selected then fully controls the entire process. The Exhaust Manifold docks automatically with the Tube Rack as they move down into the preheated Digestion Unit; and the Scrubber Unit, if connected, starts. The scrubber capacity is automatically adjusted during the cycle to contain fumes and minimise acid losses. When the digestion is completed the combined Tube Rack and Exhaust Manifold move to the cooling position with the Scrubber Unit still running until no further fumes are evolved. An adjustable audible signal in the Digestion Unit indicates “cycle over”. To avoid any spillage a drip tray, supplied with the Exhaust Manifold, is inserted underneath the Exhaust Manifold when it is separated from the Tube Rack after cooling. The Lift eliminates heavy handling. The Rack System saves space. Auto Rack Systems When an Auto Rack system is used in place of an Auto Lift system the typical procedure is as with the Auto Lift system with the exception that the combining/separating of Tube Rack and Exhaust Manifold and the movement to the cooling position is performed manually when the signal is heard. The application selected controls all other functions as with the Auto Lift system. Basic Systems The temperature and time for the digestion are selected on the front panel. All other procedures, including operation of a connected scrubber, are then performed by the operator once the digestion unit has reached the selected temperature. Fume Removal and Containment Systems Exhaust Manifolds Many digestion applications, e.g. Kjeldahl, produce fumes that are unpleasant and corrosive. Exhaust Manifolds designed for each Digestion Unit facilitate fume removal and containment and are strongly recommended for use with all digestion procedures. The cost of replacement of a fume cupboard which has been corroded by inefficient fume handling is very much greater than the relatively low cost of an approved exhaust. Whilst many users choose to operate integrated systems in the open laboratory, we strongly recommend the use of both exhaust systems and fume cupboards for these operations. This is simply Good Laboratory Practice (GLP) and avoids conflict with local Health & Safety (H&S) requirements. The Exhaust Manifolds should be connected to the water aspirator supplied, or to a suitable Scrubber Unit. Scrubber Unit Where water is a scarce or expensive commodity, or simply when a higher level of automation is desired, the water aspirator should be replaced with an efficient Scrubber Unit. Exhaust Manifolds and Scrubber Units which require an external water source are subject to variation in vacuum efficiency due to fluctuations in local water pressure. The compact bench top Tecator™ Scrubber Unit is self contained and is therefore unaffected by water supply issues. During digestion moist, acidic fumes from the connected exhaust are drawn through the Scrubber Unit. Acid vapours are first condensed and diluted in a large acid trap. Any residual fumes are collected, washed and neutralised before passing through a second small acid trap which protects the vacuum pump in the event that the scrubbing agents are exhausted. The cleaned air is then There is an Exhaust for each Digestion Unit. The Scrubber neutralizes the corrosive fumes. vented via a tubing outlet. In the interest of GLP and H&S this venting tube should be directed into a fume cupboard. When the Scrubber Unit is connected to an Auto Lift or Auto Rack system the program will fully control the function including switching from high to low aspiration settings. Reflux Heads When a digestion unit is used for reflux chemistries, such as Chemical Oxygen Demand (COD), a Reflux Head connected to a suitable cold water supply should be used in place of the Exhaust Manifold. Tecator™ Reflux Heads are conveniently mounted in handling racks which match the tube rack in the Digestion Unit. The ball jointed condensers are designed for use with ball jointed digestion tubes. The Reflux Heads are compatible with Auto Lift, Auto Rack and Basic systems. There are Reflux Heads for 250 ml Digestion Units. Select the correct tube for your application. Kjeltabs, salt and catalyst in tablet form. Digestion Tubes To suit different applications and manual/automatic handling systems, tubes for the Digestion Units are available in two sizes (250 ml and 100 ml) and three shapes. Straight sided tubes are recommended for the majority of digestion applications. Volumetric tubes with a constriction at the neck are recommended for applications where the digestate requires dilution to a fixed volume before analyses such as FIA, SFA, and AA etc. Ball jointed tubes, available in 250 ml size only, are required for reflux chemistries using the reflux condenser heads. The larger 250 ml straight sided tubes are recommended for Kjeldahl, as they can hold samples of widely varying sizes. Samples of heterogeneous material often need to be fairly large to ensure that they are representative. There is no lower limit of sample size in the 250 ml tubes; they simply allow greater flexibility for most type of samples. The 100 ml straight sided tubes can be used where the material is homogeneous and small samples are fully representative or where they are specified by the approved method. Kjeltabs A salt, to increase the boiling point, and a catalyst, to increase the speed of reaction, are used for Kjeldahl digestions. As a convenient way to obtain the correct dosage, FOSS supplies Kjeltabs – tablets containing Potassium Sulphate and a catalyst (Copper, Selenium, or Copper/Titanium). Digestion time may depend on the catalyst used. Historically Mercury has been used as the most efficient catalyst. Today it has been replaced largely by Copper, or other metals, due to safety and environmental considerations. Kjeltabs are supplied in two sizes; 3.5 g and 1.5 g. One or more tablets are combined with the acid to obtain an optimal salt/acid ratio. The smaller 1.5 g size is designed for the 100 ml tubes. Ordering information:* Digestion Units: All models are delivered with a Tube Rack with integrated heat shields. They should always be combined with a matching Exhaust Manifold or Reflux Head and Test Tubes – 100 or 250 ml volume. For Kjeldahl digestions the 2501-001 Scrubber Unit should always be considered for safe and efficient neutralisation of corrosive gases. This replaces the water aspirator, supplied as standard. Auto Lift models, complete with 2515-001 Lift and integrated controller for fully automatic control of digestion applications, including the operation of the Lift and a 2501-001 Scrubber Unit (optional extra). The digestion unit can be connected to PC for application updates, traceability and logging purposes. NOTE. An appropriate exhaust manifold or reflux head MUST be added for an automatic system. Auto Rack models, complete with 2515-011 Rack and integrated controller for full control of digestion applications, including the operation of a 2501-001 Scrubber (optional extra). The digestion unit can be connected to PC for application updates, traceability and logging purposes. Can be upgraded to an Auto Lift system by addition of the 2515-001 Lift. NOTE. An appropriate exhaust manifold or reflux head MUST be added for an automatic system. Basic models, with built in electronics for control of temperature and time only. Can not be upgraded to Auto models but are compatible with 2515-011 Rack. Tecator™ Auto Digestion Units Auto models with integrated all activity controller and graphical display. Versions for 250 ml tubes 2508-001 Tecator™ Digestion Unit 8 – Auto Lift system, 250 ml tubes, 230 V 50-60 Hz 2508-002 Same as above but for 110 V 50-60 Hz 2508-011 Tecator™ Digestion Unit 8 – Auto Rack system, 250 ml tubes, 230 V 50-60 Hz 2508-012 Same as above but for 110 V 50-60 Hz 2520-001 Tecator™ Digestion Unit 20 – Auto Lift system, 250 ml tubes, 230 V 50-60 Hz 2520-011 Tecator™ Digestion Unit 20 – Auto Rack system, 250 ml tubes, 230 V 50-60 Hz Versions for 100 ml tubes 2508-006 Tecator™ Digestion Unit 8 – Auto Lift system, 100 ml tubes, 230 V 50-60 Hz 2508-007 Same as above but for 110 V 50-60 Hz 2508-016 Tecator™ Digestion Unit 8 – Auto Rack system, 100 ml tubes, 230 V 50-60 Hz 2508-017 Same as above but for 110 V 50-60 Hz 2520-006 Tecator™ Digestion Unit 20 – Auto Lift system, 100 ml tubes, 230 V 50-60 Hz 2520-016 Tecator™ Digestion Unit 20 – Auto Rack system, 100 ml tubes, 230 V 50-60 Hz Tecator™ Digestion Units Basic models with built in electronics for control of temperature and time. Versions for 250 ml tubes 2508-051 Tecator™ Digestion Unit 8 – Basic, 250 ml tubes, 230 V 50-60 Hz 2508-052 Same as above but for 110 V 50-60 Hz 2520-051 Tecator™ Digestion Unit 20 – Basic 250 ml tubes, 230 V 50-60 Hz Versions for 100 ml tubes 2508-056 Tecator™ Digestion Unit 8 – Basic, 100 ml tubes, 230 V 50-60 Hz 2508-057 Same as above but for 110 V 50-60 Hz 2520-056 Tecator™ Digestion Unit 20 – Basic 100 ml tubes, 230 V 50-60 Hz Fume Removal & Containment Systems 2508-020 Exhaust Manifold for Digestion Units 2508, if 250 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2508-021 Exhaust Manifold for Digestion Units 2508, if 100 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2520-020 Exhaust Manifold for Digestion Units 2520, if 250 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2520-021 Exhaust Manifold for Digestion Units 2520, if 100 ml tubes are used. Complete with Water Aspirator and Drip Tray. 2501-001 Scrubber Unit 110/230 V 50-60 Hz. For neutralization of fumes in acid digestions. It can be combined with any of the Exhaust Manifolds. Up to 100 samples without changing of reagent. Fully automatic operation when connected to an Auto Digestion Unit. Lift & Rack Systems 2515-001 LIFT for the AUTO version of Digestion Unit 2508 and 2520. The Application run in the Digestion Unit fully controls the LIFT. The Lift can only be connected to Auto version Digestion Unit. 2515-011 RACK System for all versions of Digestion Unit 2508 and 2520 without LIFT. Enables manual positioning of components in a similar way as the Auto Lift. Reflux condensers 2508-030 Reflux Head COD Digestion Unit 2508. Water-cooled Condensers for 8x250 ml tubes. 2520-030 Reflux Head COD Digestion Unit 2520. Water-cooled Condensers for 20x250 ml tubes. 10000254 Reflux Condenser, Air Cooled. 700 mm. With ground joint for 250 ml tubes. Cont. Ordering information:* Handling Systems Digestion Units are delivered complete with one Tube Rack. It may be found convenient to order extra so that all tubes normally in use in the laboratory are placed in a rack. All Tube Racks fit the Kjeltec 2460 Sampler. 10013896 Tube Rack for 8 Digestion Tubes 250 ml. 10013981 Tube Rack for 8 Digestion Tubes 100 ml. 10013895 Tube Rack for 20 Digestion Tubes 250 ml. 10013982 Tube Rack for 20 Digestion Tubes 100 ml. 10014006 Retainer Plate for Washing; Digestor 2520, 250 ml Tubes. 10014007 Retainer Plate for Washing; Digestor 2520, 100 ml Tubes. 10000460 Boiling Rod To avoid bumping when digesting large volumes of water. 10000897 Handling Device for Digestion Tube 10007117 Dispenser 2-10 ml, 1000 ml Bottle 10007118 Dispenser 10-30 ml, 2000 ml Bottle Test tubes Straight model Test Tubes, often used for Kjeldahl determination. 10014311 Digestion Tubes Straight 100 ml 8/pkg 10014312 Digestion Tubes Straight 100 ml 20/pkg 10014278 Digestion Tubes Straight 250 ml 8/pkg 10000158 Digestion Tubes Straight 250 ml 20/pkg With constriction and volume mark, used in applications where the digest is diluted to volume and an aliquot is taken for analysis. 10014313 Digestion Tubes With Mark 100 ml 8/pkg 10014314 Digestion Tubes With Mark 100 ml 20/pkg 10014315 Digestion Tubes With Mark 250 ml 8/pkg 10000157 Digestion Tubes With Mark 250 ml 20/pkg With ground joint for air-cooled Reflux Condensers. 10014316 Digestion Tubes - Ground Joint 250 ml 8/pkg 10000159 Digestion Tubes - Ground Joint 250 ml 20/pkg With ball joint for water-cooled Reflux Condensers. 10014317 Digestion Tubes - Ball Joint 250 ml 8/pkg 10000611 Digestion Tubes - Ball Joint 250 ml 20/pkg Kjeltabs: Most types are delivered in boxes of 1000. 15270001 Selenium, Tablets with 1.5 g K2SO4 + 7.5 mg Se. 15270002 Selenium, Tablets with 5 g K2SO4 + 5 mg Se. 15270003 Selenium, Tablets with 3.5 g K2SO4 + 3.5 mg Se. 15270056 Selenium, Tablets with 1 g Na2SO4 + 0.05 g Se. 15270010 Copper/Titanium, Tablets with 5 g K2SO4 + 0.15 g CuSO4.5H2O + 0.15 g TiO2 . 15270020 Copper/Titanium, Tablets with 3.5 g K2SO4 + 0.105 g CuSO4.5H2O + 0.105 g TiO2 . 15270018 Copper, Tablets with 3.5 g K2SO4 + 0.4 g CuSO4.5H2O. 15270034 Copper, Tablets with 1.5 g K2SO4 + 0.15 g CuSO4.5H2O. 15270057 Copper, Tablets with 4.5 g K2SO4 + 0.5 g CuSO4.5H2O. Other types are available upon request Installation requirements: Digestion Unit 2508 Auto Power Supply: 200 - 240 V or 100 - 115 V, 50 - 60 Hz Power consumption: 1100 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 10 kg Dimensions, W × D × H: 300 × 500 × 697 mm (incl. Rack system) Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Lift or Racking System is used Digestion Unit 2508 Basic Power Supply: 200 - 240 V or 100 - 115 V, 50 - 60 Hz Power consumption: 1100 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 10 kg Dimensions, W × D × H: 300 × 390 × 140 mm Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Racking System is used Digestion Unit 2520 Auto Power Supply: 200 - 240 V, 50 - 60 Hz Power consumption: 2300 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 18 kg Dimensions, W × D × H: 300 × 660 × 697 mm (incl. Rack system) Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Lift or Rack System is used Digestion Unit 2520 Basic Power Supply: 200 - 240 V, 50 - 60 Hz Power consumption: 2300 W Water supply: See Exhaust Manifolds. If Scrubber connected - None Weight: 18 kg Dimensions, W × D × H: 300 × 550 × 140 mm Ambient temperature: max 40°C Ventilation requirement: Exhaust system and Fume hood Recommended bench space: 1 m, or 0.4 m if a Rack System is used Scrubber Power Supply: 100 to 240 V, 50 - 60 Hz, Self selecting Power consumption: 50 W Water supply: No Weight: 19 kg Dimensions, W × D × H: 335 × 485 × 395 mm Ambient temperature: max 40°C Ventilation requirement: Outlet tubing preferably into sink in fume hood Recommended bench space: 0.6 m Exhaust 2508 Water supply: Exhaust 2520 Water supply: Lift Power Supply: 3 - 5 l/min for 5 minutes, then 1 l/min 10 - 12 l/min for 5 minutes, then 3 - 5 l/min None. Powered from the Digestion Unit Auto Power consumption: 10 W Weight: 7 kg Dimensions, W × D × H: 300 × 550 × 697 mm (Mounted on Digestion Unit) Ambient temperature: max 40�C Ventilation requirement: No Recommended bench space: 0 m. Lift is mounted on the Digestion Unit Performance data: 2508 Auto 2508 Basic 2520 Auto 2520 Basic Temperature range Ambient - 440°C 100 - 440°C Ambient - 440°C 100 - 440°C Temperature setting repeatability 1°C 1°C 1°C 1°C Temperature readout Digital Digital Digital Digital Heater indication LED LED LED LED Heater warning Text in display Text in display Text in display Text in display Over temperature protection Yes Yes Yes Yes Temperature stability at ± 2°C 100°C ± 5°C ± 2°C ± 5°C Temperature stability at ± 1°C 400°C ± 2°C ± 1°C ± 2°C Heating time 20 to 400°C at 230 V ~35 min ~35 min ~40 min ~40 min Time setting per step 1 - 999 min 1 - 1199 min 1 - 999 min 1 - 1199 min Ramp control (Rate of heating) Yes No Yes No Digestion applications memory Up to 254 No Up to 254 No Digestion steps per application Up to 23 1, Manual control Up to 23 1, Manual control Lift connection Yes, full control No Yes, full control No Scrubber Yes, full control Yes, man control Yes, full control Yes, man control Tubes / batch 8 8 20 20 Tube size 250 ml 250 ml 250 ml 250 ml Sample size* solids up to 5 g up to 5 g up to 5 g up to 5 g Sample size* liquids up to 15 ml up to 15 ml up to 15 ml up to 15 ml Tube size 100 ml 100 ml 100 ml 100 ml Sample size* solids up to 1 g up to 1 g up to 1 g up to 1 g Sample size* liquids up to 3 ml up to 3 ml up to 3 ml up to 3 ml Typical sample capacity FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0720E, Issue 1 GB, May 2005 *Note: Larger samples require special procedures. Please see the relevant Application Notes or consult our Customer Service Laboratory. Shaking Water Bath 1024 High capacity laboratory Shaking Water Bath for precise and reproducible control of chemical and biochemical reactions, e.g. incubations, fermentations, extractions, dialyses, diffusions, etc. Benefits • High incubation capacity • Protection against overheating • Digital read out of actual temperature • Flexible shaking capacity • Easy to combine with the FOSS Analytical 1023 Filtration Module • Circulating water for temperature stability Description The FOSS Analytical Shaking Water Bath is designed for accurate temperature control and continuous mixing of liquids and suspensions. A series of exchangeable flask trays provide high incubation capacity for a wide range of sample sizes. The specially developed container system makes the Shaking Water Bath particularly useful in combination with the FOSS Analytical 1023 Filtration Module for rapid filtration of incubated solutions as e.g. in dietary fibre determination. Dedicated Analytical Solutions The Shaking Water Bath is an electronically controlled thermostatic bath with a mechanically driven shaking trolley. It includes a transparent lid to ensure temperature stability and minimize evaporation loss. The water tank is designed to minimize splashing. A digital display gives the actual water temperature. A cut out device prevents overheating due to low water level or thermostat malfunction. The speed and stroke length of the shaking trolley are continuously adjustable to ensure adequate mixing in a broad range of applications. The Shaking Water Bath has a constant flow of circulating water. This ensures temperature stability also when the shaking trolley is not in use. System description: The FOSS Analytical Shaking Water Bath comprises: • Shaking Water Bath 1024, 230V, equipped with a shaking trolley, facilities for manual and automatic temperature setting, temperature control and a transparent hinged lid. The interior of the water bath is made of polished stainless steel. Flask tray are avilable as accessories (see below). • Shaking Water Bath 1024, 115V. As above. Choose from the following accessories: Standard tray for Erlenmeyer flasks: holds 33 × 50 ml flasks holds 22 × 100 ml flasks holds 12 × 250 ml flasks holds 8 × 500 ml flasks Special flaks tray, holds 12 × 600 ml 1000 2081 Incubation Flasks Incubation Flasks (set of 6) A special flask tray and a container system combines the FOSS Analytical Shaking Water Bath with the FOSS Analytical 1023 Filtration Module for incubation followed by filtration of suspensions, e.g. in dietary fibre determination. Performance data: Max. water volume: Overall dimensions (L×W×D): Weight: Power supply: Power consumption: Maximum flask immersion: Temperature range: Temperature stability: Shaking speed: Stroke length: 20 litres 89×37×32 cm 24 kg 115-230 V ±10%, 50/60 Hz 1500W/230 V (800W/115V) 65 mm Ambient to 80ºC ±0.1ºC 10-150 strokes/minute 0-50 mm FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0704E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list SoxCap™ 2047 Hydrolysis Unit The SoxCap™ 2047 is a simple solution for total fat analysis prior to solvent extraction using the Soxtec™ Systems. Features and benefits • No sample transfer in combination with batch handling tools improves measurement precision and speeds up analysis • Low system investment cost • For operator safety and convenience acid fumes are automatically removed • Fast filtration and washing of samples thanks to SoxCap™ capsule* design • Minimum use of Celite** • No contact with hot acid during hydrolysis, filtration or washing. The entire analysis takes place in a closed vessel • Compact system requiring minimum bench space System description The SoxCap 2047 features a new technique combining superior performance with low investment. It offers a solution for hydrolysis of food and feed samples, in accordance with recognized methods, prior to solvent extraction. The SoxCap system performs hydrolysis, filtration and washing without any sample transfer, with minimum manual handling using batch handling tools. The system does not require to be placed in a fume hood, as it has a built in fume removal system. After hydrolysis, filtration and washing is done inside the beaker within minutes, ensuring no contact with the hot hydrolysis solution. The sample is weighed into a SoxCap glass capsule fitted with a disposable filter. After hydrolysis the glass capsule is simply turned upside down, a cellulose thimble is fitted on top and the capsule is placed in the Soxtec Avanti for the solvent extraction step. The patented technique is based on the SoxCap capsule’s ability to hold the fat present in the sample during hydrolysis and release it during solvent extraction. * patent pending ** only with liquid samples and very fine particle size samples Dedicated Analytical Solutions Hydrolysis in a SoxCap™ 2047 Microwave drying System description: • SoxCap™ 2047, 230 V, 50-60 Hz comprising:* Ceramic Hot Plate 2022, Condenser holder with valve plate, Condenser, Hydrolysis Beaker, Beaker, Boiling Stand, Capsule Tray (set of 2), Drying Stand, Glass Capsules (2 sets of 6), Filters (set of 100), Thimbles (set of 25), Adapters (set of 6), Cotton, Water Aspirator, User Manual • SoxCap™ 2047, 115 V, 50-60 Hz. As above. Solvent extraction in a Soxtec™ System Accessories: Filters, set of 100 Cellulose Thimbles 28 × 22 mm, set of 25 Hydrolysis Beaker Beaker, Low Condenser Condenser Holder Boiling Stand Drying Stand Capsule Tray Adapters, set of 6 Glass Capsules, set of 6 Cotton, defatted Performance data: Sample size: 0,5 - 3 g Hydrolysis time: 60 min Measuring range: 0,1 - 100 % fat Capacity per batch: 6 samples simultaneously Capacity per day: Up to 36 analyses Installation requirements: Equipment Power supply 2022 Hot Plate Power consumption 230 V, 50 - 60 Hz 115 V, 50 - 60 Hz 500 W Dimensions w× d×h 19 × 30 × 11 cm Weight Water supply 2,5 kg 2 taps needed: 0,4 l/min Tap water for vacuum pump FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0311E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Soxtec™ 2043 Fat Extraction System Solvent extraction system for fast, safe determination of soluble material in food, feed, soil, polymers, textiles, paper, pulp, etc. Features and benefits • Only ~10 ml of solvent used per sample with the recovery system • Separate timer functions for each extraction step make programming and procedure conveniently repeatable • Accessories for batch handling improve laboratory efficiency • Official approvals AOAC 991.36 (meat), AOAC 2003.05, 2003.06 (feed), SCAN-CM 49:93 (paper/pulp), EPA method 3541 (PAH in soil) System description The Soxtec™ 2043 is designed for rapid, safe and economic extraction of solid and semisolid materials. This has been achieved by applying a patented version of the Soxhlet extraction technique. It is designed for maximum user convenience through batch handling of six samples at a time. Dedicated Analytical Solutions The Soxtec 2043 is CE approved according to the LVD and EMC Directives. It consists of an Extraction Unit and a Control Unit. The extraction unit must be installed in a well ventilated fume hood (air flow 0,5 m/s). The sample to be analyzed is weighed into thimbles and inserted in the Extraction Unit. The cups are heated by the electrical heating plate. The 3-step extraction procedure consists of boiling, rinsing and recovery. The system is flexible and suitable for a wide variety of applications in the food, feed, environmental and industrial segments. It is designed to work with all common solvents used for solvent extraction (we do not recommend the use of Diethyl ether due to the explosion risk when handling it.) Typical solvent recovery is 80%, only ~10 ml solvent is used per sample. Sample preparation prior to GC/HPLC work is also possible using a specially designed seal. The repeatability is equal to traditional technique (1% rel. or better). System description Soxtec™ 2043 comprises: • Soxtec 2043, 230 V 1 ea Soxtec 2043 Extraction Unit 1 ea Soxtec 2046 Control Unit 1 ea Food/Agri routine accessories kit comprising: Extraction cups (1 set of 6), cup holder, thimbles (set of 25), thimble adaptors, thimble stand, seals in viton and butyl, Manual and Application Note AN 301. • Soxtec 2043, 115 V. As above. In addition, we recommend: Cellulose thimbles, ∅ 26mm (set of 25) Cellulose thimbles, ∅ 26mm (set of 25) for sample preparation Thimble handler Thimble support Holder for thimble support Performance data: Thimble size: Solvent volume: Extraction time: Capacity per batch: Capacity per day: Measuring range: Accuracy: Repeatability: Heating up time: 26 × 60 mm. Approx. 25 ml 40 ml typically 40 to 60 min, depending on application 6 samples 30-36 samples 0.1-100% fat According to official approvals ± 1% rel. or better at 5-100% fat from 20°C to 280°C in 7-9 min (230 V) Installation requirements: Equipment Power supply Power consumption Extraction Unit Control Unit Accessories: Cup holder Thimble stand Extraction cups (set of 6), aluminium Extraction cups (set of 6), glass Seals for condensers, viton (set of 6) Seals for condensers, butyl (set of 6) 1090 Cemotec™ sample mill (food, feed prior to moisture analysis) 1093 Cyclotec™ sample mill (food, feed general applications) 2094 Homogenizer™, blender type 1095 Knifetec (water cooled for high fat and high fibre) - - Dimensions w× d×h 57 × 35 × 58 230 V, 50-60 Hz 115 V, 50-60 Hz 1 250 W 28 × 23 × 19 Weight Water supply Ventilation 30 kg 2 l/min 3 kg - Fume hood min. airflow 0,5 m/s (inter locked) - FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0312E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Soxtec™ 2045 Fat Extraction System Solvent extraction system for fast, safe determination of soluble material in food, feed, soil, polymers, textiles, paper, pulp, etc. Features and benefits • Only ~15 ml of solvent used per sample with the recovery system • Separate timer functions for each extraction step make programming and procedure conveniently repeatable • Accessories for batch handling improve laboratory efficiency • Official approvals AOAC 991.36 (meat), AOAC 2003.05, 2003.06 (feed), SCAN- CM 49:93 (paper / pulp), EPA method 3541 (PAH in soil) • Large thimble size, 65 ml, extends application range System description The Soxtec™ 2045 is designed for rapid, safe and economic extraction of solid and semisolid materials. This has been achieved by applying a patented version of the Soxhlet extraction technique. The Soxtec System 2045 is an electrically heated solvent extraction system which is CE approved ac- Dedicated Analytical Solutions cording to the LVD and EMC Directives. It consists of an Extraction Unit and a Control Unit where the extraction unit must be installed in a well ventilated fume hood (air flow 0,5 m/s). It is designed for user convenience through handling of two samples at a time. The sample to be analyzed is weighed into thimbles and inserted in the Extraction Unit. After the 3-step extraction procedure consisting of boiling, rinsing and recovery, the extractable matter is collected in the cup. The system is flexible and suitable for a wide variety of applications in the food, feed, environmental and industrial segments. It is designed to work with all common solvents used for solvent extraction (we do not recommend the use of Diethyl ether due to the explosion risk when handling it). Typical solvent recovery is 75%, only ~15 ml solvent is used per sample. Sample preparation prior to GC/HPLC work is also possible using a specially designed seal. The repeatability is equal to traditional technique (1% rel. or better). System description Soxtec™ 2045 comprises: • Soxtec 2045, 230 V complete with 1 ea 2045 Extraction Unit 1 ea 2046 Control Unit 1 ea Food/Agri routine accessories kit comprising: Extraction cups (1 set of 2), cup holder, thimbles (set of 25), thimble adapters (1 set of 6), thimble stand, seals in viton and butyl, Manual and Application Note AN 301. • Soxtec 2045, 115 V. As above. In addition, we recommend: Cellulose thimbles, ∅ 33mm (set of 25) single thickness Cellulose thimbles, ∅ 33mm (set of 25) double thickness Cellulose thimbles, ∅ 26mm (set of 25) double thickness Thimble adapter, ∅ 33mm (set of 6) Thimble adapter, ∅ 26mm (set of 6) Accessories: Cup holder Thimble stand Extraction cups (set of 2), aluminium Extraction cups (set of 2), glass Seals for condensers, viton (set of 2) Seals for condensers, butyl (set of 2) 1090 Cemotec™ sample mill (food, feed prior to moisture analysis) 1093 Cyclotec™ sample mill (food, feed general applications) 2094 Homogenizer, blender type 1095 Knifetec™ (water cooled for high fat and high fibre) For total fat determination, used in conjunction with Soxtec™ Extraction Systems we recommend: SoxCap™ 2047 comprises: • SoxCap 2047, 230 V, complete system for integrated boiling and filtration of samples and all accessories needed for acid hydrolysis of food and feed samples • SoxCap 2047, 115 V. As above. Performance data: Thimble size: 33 × 80 mm, 65 ml 0.5 to 15 g depending on sample Solvent volume: 60 ml Extraction time: typically 40 to 60 min, depending on application Capacity per batch: 2 samples Capacity per day: 10-12 samples Measuring range: 0.1-100% fat Accuracy: According to official approvals Repeatability: ± 1% rel. or better at 5-100% fat Heating up time: from 20 to 285°C in 10 min (230V) Installation requirements: Equipment Power supply Power consumption Extraction Unit Control Unit - - Dimensions w× d×h 34 × 27 × 58 230 V, 50-60 Hz 115 V, 50-60 Hz 600 W 28 × 23 × 19 Weight Water supply 18 kg 1-2 l/min 3 kg - Ventilation Fume hood min. airflow 0,5 m/s (inter locked). - FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0310E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Soxtec™ 2050 Auto Fat Extraction System Soxtec™ 2050 Auto Fat Extraction System - the fully automated solvent extraction system for safe determination of soluble material in food, feed, soil, polymers, textiles, paper pulp, etc. Features and benefits • Fully automatic for unattended operation • Accessories for batch handling offer operator convenience • Closed solvent addition limits operator’s exposure to solvent • Cooling water control reduces water costs • Automatic shutdown enables overnight operation • Official approvals; AOAC 991.36 (meat), AOAC 2003.05, 2003.06 (feed), SCAN-CM 49:93 (paper pulp), EPA No 3541 (soil) System description The Soxtec™ 2050 System represents the new generation of automated Soxhlet extraction. It is designed for maximum user convenience with full automation for unattended operation and minimum system handling. This has been achieved by applying a new patented version of the Soxhlet extraction technique Dedicated Analytical Solutions combined with integral solvent handling. The system consists of an Extraction Unit, a Control Unit and a Drive Unit. The sample to be analysed is weighed into thimbles and inserted into the extraction unit. Solvent is added to the extraction cups in a closed system. The cups are heated by the electric heating plate. The 4-step extraction consists of boiling, rinsing, solvent recovery and pre-drying. The system is flexible and suitable for a broad range of applications in the food, feed, environmental and industrial segments. It is designed to work with all common solvents used for solvent extraction (we do not recommend the use of Diethyl ether due to the explosion risk when handling it). Typical solvent recovery is 80%, only 16 ml solvent is used per sample. Sample preparation prior to GC/HPLC work is also suitable; ask for our special accessories. The repeatability is equal to traditional technique. System description: Soxtec™ 2050 comprises: • Soxtec 2050, 230V complete with 1 ea Soxtec 2050 Extraction Unit 1 ea Soxtec 2050 Control Unit 1 ea Soxtec 2050 Drive Unit 1 ea Food/Agri Routine Accessories kit comprising: Extraction cups (3 sets of 6), Cup holder, Thimble support, Thimble holder, Thimbles (set of 25), Thimble adaptors (2 sets of 6), Thimble handler, Tong for extraction cups, Thimble stand (2 sets of 6), Cup stand, seals of viton and butyl, Solvent addition tube, Solvent emptying tube, Manual and Application Note AN 301. • Soxtec 2050, 115V. As above. Accessories: Extraction Cups (set of 6), aluminium Extraction Cups (set of 6), glass Seals for condensers, viton (set of 6) Seals for condensers, butyl (set of 6) Condenser sealing ring of teflon Solvent dispenser 1090 Cemotec™ sample mill (food, feed prior to moisture analysis) 1093 Cyclotec™ sample mill (food, feed general applications) 2094 Homogenizer, blender type 2096 Homogenizer, blender type 1095 Knifetec™ (water cooled for high fat and high fibre) In addition, we recommend: Cellulose thimble, ∅ 33mm (set of 25) Cellulose thimble, ∅ 33mm (set of 25) Single thickness For total fat determination, used in conjunction with Soxtec™ Extraction Systems we recommend: SoxCap™ 2047 comprises: • SoxCap 2047, 230 V, complete system for integrated boiling and filtration of samples and all accessories needed for acid hydrolysis of food and feed samples • SoxCap 2047, 115 V. As above. Performance data: Thimble size: 33 × 80 mm, 65 ml 0.5 to 15 g depending on sample Solvent volume: 70-90 ml Extraction time: typically 40 to 60 min, depending on application Capacity per batch: 6 samples Capacity per day: 42 samples Measuring range: 0.1-100% fat Accuracy: According to official approvals Repeatability: ± 1% rel. or better (5-100% fat) Heating up time: from 20 to 280°C in 7-9 min (230V) Installation requirements: Equipment Power supply Power consumption Extraction Unit Control Unit Drive Unit - - Dimensions w× d×h 60 × 38 × 58 230V, 50-60 Hz 115V, 50-60 Hz 230V, 50-60 Hz 115V, 50-60 Hz 1550 W 40 W Closed solvent addition limits operator’s exposure to solvents. Weight Water supply Ventilation 30 kg 2 l/min. 31 × 24 × 16 3 kg - Fume hood min. airflow 0,5 m/s (inter locked) - 40 × 28 × 12 8 kg - - FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0306E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list Soxtec™ 2055 Fat Extraction System Soxtec™ 2055 Fat Extraction System - the new generation of manual solvent extraction systems for safe determination of soluble material in food, feed, soil, polymers, textiles, paper, pulp, etc. Features and benefits • Separate timer functions for each extraction step make programming and procedure conveniently repeatable • One handle moves all samples simultaneously • Accessories for batch handling offer operator convenience • Closed solvent addition limits operator’s exposure to solvents • Official approvals AOAC 991.36 (meat), AOAC 2003.05, 2003.06 (feed), SCAN-CM 49:93 (paper/ pulp), EPA method 3541 (PAH in soil) System description The Soxtec™ 2055 System represents the new generation of manual Soxhlet extraction systems. It is designed for maximum user convenience through batch handling of six samples at a time, giving a minimum of system handling. This has been achieved by applying a new patented version of the Soxhlet extraction technique Dedicated Analytical Solutions combined with integral solvent handling. The system consists of an Extraction Unit and a Control Unit. The sample to be analyzed is weighed into thimbles and inserted in the Extraction Unit. The solvent is added in a closed system. The cups are heated by the electrical heating plate. The 4-step extraction procedure consists of boiling, rinsing, recovery and pre-drying. The system is flexible and suitable for a wide variety of applications in the food, feed, environmental and industrial segments. It is designed to work with all common solvents used for solvent extraction (we do not recommend the use of Diethyl ether due to the explosion risk when handling it). Typical solvent recovery is 80%, only 16 ml solvent is used per sample. Sample preparation prior to GC/HPLC work is also possible using a specially designed seal. The repeatability is equal to traditional technique (1% rel. or better). System description Soxtec™ 2055 comprises: • Soxtec 2055, 230V Complete with 1 ea Soxtec 2055 Extraction Unit 1 ea Soxtec 2055 Control Unit 1 ea Food/Agri routine accessories kit comprising: Extraction cups (3 sets of 6), cup holder, thimble support, thimble holder, thimbles (set of 25), thimble adaptors, thimble handler, tongs for extraction cups, thimble stand, cup stand, seals in viton and butyl, solvent addition tube, solvent emptying tube, Manual and Application Notes. • Soxtec 2055, 115V. As above. Accessories: Extraction cups (set of 6), aluminium Extraction cups (set of 6), glass Seals for condensers, viton (set of 6) Seals for condensers, butyl (set of 6) Seals for condensers, RESEL (set of 6) 1090 Cemotec™ sample mill (food, feed prior to moisture analysis) 1093 Cyclotec™ sample mill (food, feed general applications) 2094 Homogenizer, blender type 1095 Knifetec™ (water cooled for high fat and high fibre) In addition, we recommend: Cellulose thimbles, ∅ 33mm (set of 25) Cellulose thimbles, ∅ 33mm (set of 25) single thickness For total fat determination, used in conjunction with Soxtec™ Extraction Systems we recommend: SoxCap™ 2047 comprises: • SoxCap 2047, 230 V, complete system for integrated boiling and filtration of samples and all accessories needed for acid hydrolysis of food and feed samples • SoxCap 2047, 115 V. As above. Performance data: Thimble size: 33 × 80 mm, 65 ml 0.5 to 15 g depending on sample Solvent volume: 70-90 ml Extraction time: typically 40 to 60 min, depending on application Capacity per batch: 6 samples Capacity per day: 36 samples Measuring range: 0.1-100% fat Accuracy: According to official approvals Repeatability: ± 1% rel. or better (5-100% fat) Heating up time: from 20 to 280°C in 7-9 min (230V) Installation requirements: Equipment Power supply Power consumption Extraction Unit Control Unit - - Dimensions w× d×h 60 × 38 × 58 230V, 50-60 Hz 115V, 50-60 Hz 1550 W 31 × 24 × 16 Closed solvent addition limits operator’s exposure to solvents. Weight Water supply 30 kg 2 l/min. 3 kg - Ventilation Fume hood min. airflow 0,5 m/s (inter locked) - FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0308E, Issue 1 GB, Dec 2004 * Ordering information: See separate price-list A Soxtec™ for every need Dedicated Analytical Solutions Just load, start and walk away For 30 years, FOSS has developed and supplied instruments with a mission: to always make routine analysis simpler. A great step forward As early as 1975, we revolutionised solvent extraction by introducing Edward Randall’s patented two-stage technique for boiling and rinsing. Six years later, FOSS launched an improved system, Soxtec™, based on Tecator™ technology, that also handled solvent recovery. Soxtec 2050 is the next great step forward in solvent extraction. A solvent extractor that needs practically no handling by lab personnel. A fully automatic Soxhlet analyzer that is the fastest on the market, using less solvent and less water. Four automatic steps 1 2 Boiling Rinsing Rapid solubilisation in boiling solvent. Efficient removal of remaining soluble matter. Fully automated, unattended operation The Soxtec 2050 utilizes a new, patented four-step solvent extraction technique. It performs boiling, rinsing and solvent recovery. In its fourth step, the sample cup lifts off the hot plate, utilizing residual heat to pre-dry while eliminating boil-dry risk. The entire process is a fully automatic, unattended operation. You just load, start and walk away. Soxtec 2050 will even shut down automatically when finished. Because it frees operators from routine tasks, Soxtec 2050 helps to improve the laboratory’s productivity. And it’s very quiet – an additional bonus for the laboratory working environment. 3 Recovery Automatic collection of distilled solvent for re-use. 4 Pre-drying Elimination of boil-dry risk. Application flexibility Soxtec systems are developed for maximum application flexibility. Users can easily design and optimise their own applications for accurate, safe determination of soluble matter within the food, feed, environmental and industrial sectors. Soxtec can handle larger sample volumes (a standard 33×80 mm thimble), and its higher temperature range even enables effective use of high-boiling point solvents, such as toluene and xylene. Furthermore, the glass/Teflon solvent interface makes it possible to run metal-sensitive applications. Built for the purpose Safety is important Minimal manual handling assures safety in the process. When the sample has been loaded, the solvent is added in a closed, secure system. The solvent dispenser, automatic solvent recovery and built-in fume hood limit solvent vapour to a minimum, thus ensuring a safe working environment. Safety has always been important to us, the only electrical part in the Extraction unit, the hot plate, is spark proof. The double temperature sensors ensure that the set temperature is kept and that the ignition point is never reach for any solvent. Soxtec™ 2050 guarantees a safe working environment – the entire analysis takes place in a closed, secure system. It is designed and built to surpass strict European safety standards. There is simply no safer solvent extraction system available. Operating convenience Soxtec 2050’s automation improves efficiency. Overall laboratory efficiency is further improved by the purpose-developed handling tools delivered with the Soxtec system. The tools for simple batch-wise sample handling save time, simplify usage and minimize risk of operator error. There is no longer any need for manual handling of thimbles or hot extraction cups. Soxtec™ 2050 and 2055 are operated through the Control Unit, with simple logic commands and a full graphical interface. The fastest on the market Typically five times faster than the classical Soxhlet technique, Soxtec Systems are the fastest Soxhlet extractors on the market. With Soxtec 2050 you can extract as many as seven batches per day, with absolutely no loss in precision or accuracy. The Soxtec systems follow officially approved methods for fat in feed (AOAC), meat (AOAC), PCB (EPA) and paper pulp (SCAN). Dramatically reduced extraction times Analyte Fat in feed Fat in food (eg. meat, cereals) PCB, PAH & Pesticides in soil Oil & Grease in water Extractable Matter in polymers & rubber Extractable Matter in paper & pulp Extractable Matter in explosives & propellants Hydrocarbons in petroleum rock Finishing Oil on textile & synthetic fibres Anti-Caking Coating on fertilisers Detergent in detergent powder Fat in leather Soxhlet Soxtec™ Extraction time Extraction time 2 h to 16 h 2 h to 16 h 17 h 4 h 2 h to 48 h 2 h to 48 h 16 h 24 h 2 h 3 h to 4 h 5 h 5 h 1h 1h 2h 45 min 1 h to 5 h 1 h to 5 h 1h 2h 30 min 1h 1h 1h A profitable solution Soxtec™ extractors range in capacity and function from the small Soxtec 2045 to the fully automatic Soxtec 2050. All Soxtec models fully utilise our batch handling concept to make sample processing as easy and safe as possible. Whatever your Soxhlet extraction need is, we can offer you the right solution. Total fat analysis The SoxCap™ 2047 is an integral part of the Soxtec systems. It offers total fat analysis in accordance with recognized methods. The SoxCap system performs hydrolysis, filtration and washing without any sample transfer. This patented technique offers high throughput together with minimum manual handling using batch handling tools. Save time and money Soxtec 2050 shortens the analysis time, increasing throughput to up to seven extractions per day. Furthermore, the automatic shutdown function enables overnight operation*. Its automatic operation frees operators from time-consuming routine tasks, thereby increasing laboratory efficiency. Most users prefer aluminium extraction cups –only environmental applications require glass cups. Aluminium cups are unbreakable, and they offer rapid heat transfer, which in turn shortens heating and drying times. The low weight of the aluminium cups also makes it possible to use a standard 120 g capacity balance. Soxtec systems utilizes environmentally sound techno logy. Compared to classical Soxhlet, the Soxtec systems uses a significantly lower solvent volume. No other Soxhlet extractor uses solvents so efficiently. Typically, thanks to solvent recovery, 16 ml of solvent is used per sample – so costs for solvent purchase and disposal can be kept to a minimum. Built-in water control minimizes water consumption. *Subject to local regulation With Soxtec™ 2050, you make the most of your laboratory – day and night! Soxtec™ Systems Soxtec™ Soxtec™ Soxtec™ Soxtec™ SoxCap™ 2045 2043 2055 2050 2047 Sample Positions 2 6 6 6 6 Capacity, samples per day 12 36 36 42 36 50–70 ml 40-50 ml 70–90 ml 70–90 ml – 80% 80% 80% 80%, automatic – Closed Solvent Addition No No Yes Yes – Solvent Volume per sample Solvent Recovery Programmable Yes Yes Yes Yes No Fully Automated No No No Yes No Overnight Operation No No No Yes No Batch Handling Yes Yes Yes Yes Yes Extraction Cups Glass & Aluminium Glass & Aluminium Glass & Aluminium Glass & Aluminium – Cellulose, Glass Cellulose, Glass Cellulose, Glass Cellulose, Glass Cellulose 26, 33, 45 26 26, 33 26, 33 30 120 ml 30 ml 65 ml 65 ml 50 ml Remotely controlled electric Remotely controlled electric Remotely controlled electric Remotely controlled electric Electric Thimbles Thimble Diameter Thimble Volume Heating Temperature Range 0–285ºC Overtemperature 145, 210 & 330ºC Protection 0–285ºC 0–285ºC 0–285ºC – 145, 210 & 330ºC 145, 210 & 330ºC 145, 210 & 330ºC – Power Consumption 1500 W 1500 W 1550 W 1590 W 500 W Water Consumption 2 l/min 2 l/min 2 l/min 2 l/min 0,4 l/min Water Saving System No No No Yes No 34×27×58 51×32×58 60×38×58 60×38×58 19×30×11 +/- 1% relative +/- 1% relative +/- 1% relative +/- 1% relative +/- 1% relative Dimensions, cm Accuracy In the interest of product development we reserve the right to alter specifications without prior notice. Solvent extraction systems for safe determination of soluble matter in food, feed, soil, polymers, textiles, paper pulp, and more. Whatever your Soxhlet extraction needs, we can offer the right solution. About FOSS FOSS provides dedicated analytical solutions that ensure optimal production of food, agricultural, pharmaceutical and chemical products. FOSS solutions analyse and control your products during production – helping you to optimise both quality and profit. FOSS is unique in offering a range of dedicated solutions based on both indirect and reference methods. FOSS solutions provide analysis and control throughout the production process, from raw material to finished product and from routine analysis to at-line and in-line process control. FOSS is a privately-owned company employing over 1100 worldwide. FOSS has manufacturing and research and development facilities in Denmark, Sweden and the USA. Solutions are sold and supported through FOSS sales and service companies in 21 countries and by more than 75 dedicated distributors. FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 99990307, Issue 2 GB, April 2006 Please visit www.foss.dk. SoxCap™ 2047 Hydrolysis Unit The SoxCap™ 2047 is a simple solution for total fat analysis prior to solvent extraction using the Soxtec™ Systems. Features and benefits • No sample transfer in combination with batch handling tools improves measurement precision and speeds up analysis • Low system investment cost • For operator safety and convenience acid fumes are automatically removed • Fast filtration and washing of samples thanks to SoxCap™ capsule* design • Minimum use of Celite** • No contact with hot acid during hydrolysis, filtration or washing. The entire analysis takes place in a closed vessel • Compact system requiring minimum bench space System description The SoxCap 2047 features a new technique combining superior performance with low investment. It offers a solution for hydrolysis of food and feed samples, in accordance with recognized methods, prior to solvent extraction. The SoxCap system performs hydrolysis, filtration and washing without any sample transfer, with minimum manual handling using batch handling tools. The system does not require to be placed in a fume hood, as it has a built in fume removal system. After hydrolysis, filtration and washing is done inside the beaker within minutes, ensuring no contact with the hot hydrolysis solution. The sample is weighed into a SoxCap glass capsule fitted with a disposable filter. After hydrolysis the glass capsule is simply turned upside down, a cellulose thimble is fitted on top and the capsule is placed in the Soxtec for the solvent extraction step. The patented technique is based on the SoxCap capsule’s ability to hold the fat present in the sample during hydrolysis and release it during solvent extraction. * patent pending ** only with liquid samples and very fine particle size samples Dedicated Analytical Solutions Hydrolysis in a SoxCap™ 2047 Microwave drying System description: 20470001 SoxCap™ 2047, 230 V, 50-60 Hz comprising:* Ceramic Hot Plate 2022, Condenser holder with valve plate, Condenser, Hydrolysis Beaker, Beaker, Boiling Stand, Capsule Tray (set of 2), Drying Stand, Glass Capsules (2 sets of 6), Filters (set of 100), Thimbles (set of 25), Adapters (set of 6), Cotton, Water Aspirator, User Manual 20470002 SoxCap™ 2047, 115 V, 50-60 Hz. As above. 20470003 20470004 SoxCap™ 2047mini, 230 V, 50-60 Hz comprising:* Ceramic Hot Plate 2022, Condenser holder with valve plate, Condenser, Hydrolysis Beaker, Beaker, Boiling Stand, Capsule Tray (set of 2), Drying Stand, Glass Capsulesmini (2 sets of 6), Filters (set of 100), Thimbles (set of 25), Adapters (set of 6), Cotton, Water Aspirator, User Manual SoxCap™ 2047mini, 115 V, 50-60 Hz. As above. Solvent extraction in a Soxtec™ System Accessories: 10012381 Filters, set of 100 15220053 Cellulose Thimbles 28 × 22 mm, set of 25 10012233 Hydrolysis Beaker 10011595 Beaker, Low 10013849 Condenser 10013840 Condenser with drip tray assembly 10012227 Boiling Stand 10012229 Drying Stand 10012230 Capsule Tray 10012379 Adapters, set of 6 10012378 Glass Capsules, set of 6 15290009 Cotton, defatted 60022802 Glass Capsulesmini, set of 6 Performance data: Sample size: 0,5 - 3 g Hydrolysis time: 60 min Measuring range: 0,1 - 100 % fat Capacity per batch:6 samples simultaneously Capacity per day: Up to 30 analyses Installation requirements: Equipment Power supply Power consumption Dimensions Weight w × d × h 2022 Hot Plate 230 V, 50 - 60 Hz 500 W 19 × 30 × 11 cm 2,5 kg 115 V, 50 - 60 Hz Water supply 2 taps needed: 0,4 l/min Tap water for vacuum pump FOSS Analytical 69, Slangerupgade DK-3400 Hilleroed Denmark Tel.: +45 7010 3370 Fax: +45 7010 3371 [email protected] www.foss.dk P/N 9999 0311, Issue 2 GB, Feb 2007 *Ordering information: Use the above specified Cat. Nos. together with the text.