LEADING ANALYTICAL INSTRUMENTATION
Transcription
LEADING ANALYTICAL INSTRUMENTATION
LEADING ANALYTICAL INSTRUMENTATION LABORATORY INSTRUMENTATION PROCESS SOLUTIONS INSTALLATION SUPPORT www.mep.net.au SERVICE Metrohm Anton Paar Analytik Jena DropSens Metrohm Applikon Metrohm Autolab Metrohm NIRs Retsch Retsch Technology Ion Analysis Titration (Potentiometric, Thermometric) Automation Tiamo Software tiBase Data Management Touch Control Karl Fischer Titration Coulometer pH, Ion, Conductivity Meters Electrodes (pH, Conductivity, Redox, ISE) Ion Chromatography UV-Vis Detection Amperometric Detection Separation Columns Combustion IC 4 5 6 6 6 7 7 8 9 10 10 10 11 11 Electrochemistry Trace Analysis, Voltammetry Cyclic Voltammetry Stripping Standardised Stability Measurement Potentiostats, Galvanostats Screen-printed Electrodes CONTENT Spectroscopy ICP MS Atomic Absorption High-Res ICP OES High Res CS AAS SUM Parameters 12 12 12 13 13 AOX/TX TOC/TNb UV-Vis Elemental Analysis Titration ISE VA Heavy Metal Colorimetry Total Organic Carbon TOC Turnkey Solutions Ambient Air Analysis (continuous) C,N,S,Cl in Solids 14 14 14 14 15 15 16 Particle Characteristics Density and Sound Sensors Beverage Analysers Inline Viscometers Sample Preparation Density Meters (benchtop, handheld) 18 Beverage Alcohol Measurement 19 CO2 /O219 Refractometry 20 Polarimetry 20 Material Testing 21 21 22 22 22 23 23 23 23 26 NIR for the Laboratory and Process Lines 27 Raman Spectroscopy 27 Sieve Analysis Size and Shape (dynamic image) Density and Concentration 26 Near-Infrared Spectroscopy Process Measuring Solutions 17 17 17 25 25 UV-Vis Spectroscopy Online Process Ion Analysis Rheology Viscometry Nanostructure Analysis Zeta Potential Surface Mechanical Properties Fuel and Bitumen Testing Flash-Point (Pensky-Martens) Penetration Automatic Distillation 24 24 24 24 Milling Grinding Assisting 28 29 30 30 31 Microwave Chemistry Microwave Digestion Microwave Synthesis 32 33 Service MEP Service Packages MEPCare™ Seminars, Workshops, Training Application Notes, Publications Newsletters 34 35 36 36 36 Laboratory Service Application Testing Application Development Applications and Methods Overview 37 37 38 MEP Instruments MEP is a joint venture company of Metrohm and Anton Paar set up to serve the scientific industry in Australia and New Zealand with first class products and services. Represented in all major cities we aim to exceed your expectations when it comes to instrument quality, technical advice and strong after sales support. MEP is proud to represent many world-leading companies and their technologies. Metrohm Metrohm is a worldwide leading manufacturer of precision instruments for chemical analysis. In the field of electrochemical ion analysis Metrohm has been the unchallenged world number one for many years. Metrohm is the only manufacturer with a sole focus on ion analysis from titration to pH, from ion chromatography to voltammetry. Metrohm Autolab With a strong background and in-depth knowledge in electrochemistry Metrohm-Autolab’s mission is to serve the research community by supplying modern, affordable potentiostats/galvanostats, software and accessories. Metrohm Applikon Metrohm Applikon delivers sophisticated solutions for at-line and on-line wet chemical analysis, including total organic carbon, to measure ion concentrations in various processes, using techniques such as colorimetry, ISE, standard addition, titration and voltammetric analysis. Metrohm NIRSystems More than 50 years’ spectroscopy experience with more than 50 patents – that is Metrohm NIRSystems. Our enlarged portfolio of NIRS laboratory and process spectrometers as well as our ready-to-analyse Raman spectrometers in smartphone size let you experience the lightness of measuring. We offer you an unparalleled accuracy, even for intricate samples. Discover our complementary spectroscopy families, NIRS and Raman. Anton Paar Anton Paar GmbH produces high-end measuring laboratory and process instruments for industry and research. With its innovative solutions in measurements of density, concentration and CO2 and in the field of rheometry Anton Paar has secured its leading position worldwide. Petroleum, fuel and bitumen testing solutions and highly sophisticated nano-scale surface mechanical properties testing instruments are also included in the group’s impressive portfolio. Analytik Jena Germany-based Analytik Jena has a long tradition in developing high-performance precision analytical systems dating back to the inventions made by Ernst Abbe and Carl Zeiss. They have become one of the most innovative manufacturers worldwide. Analyik Jena excels in the fields of optical and mass spectroscopy, sum parameters and elemental analysis. Retsch Since 1915 Retsch has developed consistently within the fields of solids homogenization and sieve analysis. Its unparalleled product lines have won Retsch the position of world leader in the market of milling and sieving equipment. Retsch Technology Based on the experience and know-how of the parent company Retsch GmbH and in cooperation with partners Jenoptik and Horiba, Retsch Technologies offer highly innovative instruments for particle size and shape analysis. DropSens DropSens is an innovative technology-based firm specialised in the design and manufacture of instruments and screen-printed electrodes, based on thick-film hybrid technology for electrochemistry research. 3 Ion Analysis TITRATION AT ITS BEST Intuitive, intelligent, sophisticated Titrando – the flagship of titration Titration systems à la carte The 906/907 can perform SET, MET, DET, KFT and STAT titrations, as well as Ion Concentration Measurement. A sophisticated control algorithm, combined with the increased volume resolution of the Intelligent Exchange Units, guarantees highly precise results. Touch control or mouse click? Whether you operate the Titrando with touch control or via PC and mouse, appearance and operation are practically identical. The system’s operator guidance is exemplary. Intelligent dosing The Titrando automatically reads from its chip all the data (type of reagent, titre, last titre determination and much more) that it needs to carry out the titration properly. Thermometric Titration 916 Ti-Touch reduced to the max! Thermometric titration is a very versatile determination method and an ideal complement to potentiometric titration. Suitable for any reaction that produces a sufficiently large temperature change in the sample solution. The 916 Ti-Touch comes with a complete package system for Oil, Food/Wine and Salt/Chloride analysis. •Ultrafast • Paperless pdf reports • One sensor only for all • Direct connection to applications 4 • Maximum system integration, in-built colour touch-pad screen • Uses patented Dosino technology intranet and LIMS www.mep.net.au Ion Analysis AUTOMATION AT THE HIGHEST LEVEL From titration to complex liquid handling Automate your liquid handling tasks The efficient Robotic USB Sample Processor XL carries out complex laboratory automation tasks in combination with a Titrando. When used with the revolutionary 786 Swing Heads its capacity can be increased, e.g. up to 100 samples of 75 mL each. 786 Swing Heads are true masters of precision • They move pipetting tips to microtitre plates with millimetre accuracy or take up disposable filters • High sample volumes • High numbers of samples • Working in parallel • Automated liquid handling • Automated pipetting, diluting • Karl Fischer automation • Automatic sample preparation • Up to two external titration stations Customised automation systems Space saving automation All-in-one 855 Titrosampler For large sample series Get correct and dependable results faster! The 855 Robotic Titrosampler is an automated titrator that combines the highest quality standards in titration: • 40% less lab space The 898 XYZ Sample Changer provides automation to the analysis of large sample series with utmost precision. Plenty of space for 82 samples and the 898’s high operating speed mean that you save considerable amounts of time in routine analysis. • Unique and outstanding • Controlled by Tiamo, the leading titration software • Easy to handle and user friendly • Rack change during operation • Based on the Titrando technology • With top performance automation • Robust and reliable • Large sample numbers MEP Instruments • A company of Metrohm and Anton Paar 5 Ion Analysis TIAMO™ Unparalleled titration software tiamo™ – Titration and more tiamo™ is the result of Metrohm’s largest and most modern software project for ion analysis. tiamo™ is the most powerful control and database software for titrators, dosing devices and sample changers, allowing complete laboratory automation. tiamo™ comes in three base versions for every requirement: Light, Full and Multi (Client Server) Features of Full and Multi: 900 Touch Control • Sample data export and import • Fully compliant to FDA 21 CFR Part 11 The operating unit for Titrando’s pH and Conductivity modules and Sample processors. • Parallel titration • Direct connection to intranet • Result, sensor, titrant monitoring • Unlimited number of instruments connected • Third party instruments can be connected, e.g. density meters and LIMS • Touch sensitive, high resolution display • Methods, results stored on tiBase – Intelligent data management for titration The new datalogging software from Metrohm manages all of your data directly from the 900 Touch Control, Titrino Plus and the new 915–916 Ti-Touch • Direct import of data • Determination reprocessing system as well as ability to and storage of titration store on USB stick or network curves and all instrument • PDF generator • Favourite methods can be linked to an icon on the screen for ease of use configuration data. • Data export to LIMS • Can be supplied in a client server version • Fully compliant to FDA 21 CFR Part 11 6 www.mep.net.au Ion Analysis KARL FISCHER MOISTURE ANALYSIS Moisture determination from ppm to 100% 915 KF Ti-Touch KF titration reduced to the max! The 915 KF Ti-Touch is the Karl Fischer version of Metrohm’s standalone titrator for routine analysis. In this titrator the burette, stirrer, dosing system and operation module are cased in a single, compact unit. This is not only handy but also saves valuable benchspace. • Contact-free reagent exchange • USB Interface for printer, USB stick or barcode reader • Direct access to intranet and LIMS • Paperless pdf reports • Colour touch-pad screen control with data storage Karl Fischer automation and software solutions KF automation system 851 with 874 Oven Sample Processor The 851 KF Coulometer is perfect for large sample throughput. Together with the 874 Oven Sample Processor, it combines exceptionally well with the proven reliability of Metrohm sample changers. Complete package for water determinations 890 KF Titrando for titration with the proven intelligence of the Titrando family. • Packages with Touch Control or tiamo™ software control • Intelligent dosing elements • Client/server database thanks to tiamo™ • Direct connection to intranet and LIMS • FDA 21 CFR Part 11 compliant • 20,000 pulses per cylinder volume MEP Instruments • A company of Metrohm and Anton Paar 7 Ion Analysis pH, ION AND CONDUCTIVITY METERS Precision tools for everyday Metrohm pH and ion meters designed for field, laboratory and plant «Two-in-one» – for indoors and outdoors These new Metrohm meters are «two in one»: precision instruments for measurements in the laboratory and robust companions for mobile use in the field and at the process line. Optional battery operation makes the new meters independent of a power grid. They can even be recharged on the road on the cigarette lighter with the use of an adapter. Measuring on two channels at once Parallel measurement of pH and conductivity with the 914 pH/Conductometer, parallel recording of two pH values with the 913 pH Meter. Moreover, both versions indicate the temperature(s) of the sample(s). 912 Conductometer, 913 pH Meter, 914 pH/Conductometer German French Maintenance and Care of Metrohm Electrodes A.740.0001 English Spanish Metrosensor electrodes Portuguese Italian Metrohm AG CH-9101 Herisau, Switzerland www.metrohm.com ©Copyright 2007 Precision is not accidental, but brought about by design! The 914 pH/Conductometer shows you at a glance the pH value, the conductivity, and two temperature values. As a result of the two separate measuring inputs, conductivity and pH value can be measured in parallel, even in the same beaker. With the 913 pH Meter, you can measure two pH values and two temperature values simultaneously. Two separate measuring inputs are available here as well. The 912 Conductometer is equipped with a measuring input for conductivity, TDS, salinity, and temperature. Electrode selection and maintenance Maintenance and Care The ABC of electrode care – get precise results and a long lifetime of your electrodes. Order your free DVD copy! The Metrosensor Catalogue guides you to the right electrode for your applicaton, explains how a Metrosensor is made and introduces the theoretical fundamentals. It is free to order. Call us. All versions of the new meters are equipped with a large colour display. 8 www.mep.net.au Ion Analysis pH, CONDUCTIVITY, REDOX, ION SELECTIVE ELECTRODES Unsurpassed Swiss quality and service life Application Universal Water Waste water Soil samples Agricultural, cultivation of plants Food, stimulants Pharma industry Biology Cosmetics Detergents, surfactants Leather, paper, textile industry Paints, lacquers, solvents Electroplating, metal processing Special applications Beverages Specifics Electrode Standard laboratory, various samples, pH 0…14, T = 0…100 °C Unitrode Demineralised, drinking and sea water, weakly buffered solutions Aquatrode Plus General Unitrode Sulphide-containing waste water Profitrode Surface measurement or aqueous suspensions Flat Membrane Culture media, small volume samples Biotrode Fertilisers Unitrode Liquid manure Profitrode Nutrient solutions Viscotrode Protein-containing solutions Porotrode General Unitrode Sensors for all applications Metrohm is a leading manufacturer of a variety of sensors. From pH, ion-selective electrodes, Redox, photometric, thermometric and conductometric, Metrohm offers a full range of sensors for practically every application. • The Metrosensor Long Life reference system for pH and combined metal probes allows the system to last longer and to reduce blockage of the electrode diaphragm. • Full range of analogue and digital interface Protein-containing food, beer Porotrode Penetration measurement (dough, cheese, meat) Spearhead Drinking water Aquatrode Plus connected to non-Metrohm systems. Request Juices, wine, spirits Unitrode Creams, liquid formulations, medicinal syrup, mouthwash, raw materials the free adapter to take advantage of Viscotrode Dialysis solutions, urine Unitrode Gastric juice, serum, small volume samples Biotrode Infusion solutions Aquatrode Plus Protein-containing solutions Porotrode Shampoos, emulsions, shower gels, mouth rinse, perfumes Viscotrode Make-up Microelectrode Skin (surface measurement) Flat Membrane General Viscotrode Samples with pH >10 Profitrode Bleaching & dye baths Profitrode Dampening solutions (offset printing), glues Unitrode probes with the new iTrode and iConnect • With the correct adapter Metrosensors can be Metrohm electrodes. • Quality Swiss Made products ADAPTERS for non-Metrohm instruments available Leather, paper, textiles (surface measurement) Flat Membrane Washing liquors Viscotrode Dye baths, ink, wood stain, lacquers Profitrode Dispersions, emulsions, resins, suspensions Unitrode Paint (surface) Flat Membrane Non-aqueous, polar solvents Solvotrode General Profitrode Acidic electroplating baths Unitrode Cutting oil emulsions Viscotrode Etching baths containing fluoride/hydrofluoric acid Sb Electrode Concentrated acids Profitrode Photographic baths Profitrode Emulsions, suspensions, dispersions Unitrode Samples at pH >12 Unitrode Temperature 50…80 °C Unitrode Temperature 80…100 °C Unitrode Ion-deficient solutions, weakly buffered solutions Unitrode (Idrolyte) Non-aqueous, polar solvents Solvotrode Penetration measurement Spearhead Protein-containing solutions Porotrode Small volume samples Biotrode Surface measurements Flat Membrane Wines, beers and soft drinks Vinotrode MEP Instruments • A company of Metrohm and Anton Paar 9 Ion Analysis THE WHOLE WORLD OF ION CHROMATOGRAPHY Compact intelligence for ion chromatography 940 Professional IC Vario The amazing 940 Professional IC Vario system stands for maximum flexibility combined with most easy operation and perfect reliability. 930 Compact IC Flex The outstanding 930 Compact IC Flex is the ion chromatograph of choice for routine analysis developed with a focus on the requirements of contract laboratories and QC laboratories in all kinds of industries. Rugged design, perfect ease of use and outstanding system reliability are key features of the 930 Compact IC Flex. Configure your personal IC Metrohm’s online configurator for the 940 Professional IC Vario system and the 930 Compact IC Flex allows you to put together your customized IC system. UV-Vis detection Amperometric detection The 944 Professional UV-Vis Detector enables reliable and accurate quantification of substances that absorb light in the ultraviolet or visible range. The 945 Amperometric Detector is designed for direct current (DC), amperometric (PAD), highly flexible integrated pulsed amperometric (flexIPAD) or cyclic voltammetry (CV) modes. Broad area of use The flow path of Metrohm’s IC instruments is completely metal-free. Thus, not only the standard anions and cations, but also transition metal ions and various organic substances can be detected without any problem. Even in complex matrices, e.g. biological samples, good detection limits can be achieved on the basis of the specific absorption properties of many analytes. 10 Typical applications include the determination of inorganic anions, such as cyanide, sulphide, nitrite, sulphite or iodide; carbohydrates, such as mono-, di- and polysaccharides, amino-sugars, sugar alcohols and sugar acids; and organic compounds, such as phenols or vitamins. www.mep.net.au Ion Analysis SEPARATION COLUMNS Surpassing standards The first intelligent ion chromatography column generation in the world “Insert and start” When a Metrosep separation column is used in different systems, it conveys all its information to the next IC system. This results in complete traceability and GLP surveillance for all the columns used, even on different IC instruments. This greatly facilitates system validation. Column selection for standard test methods Meeting global standards in IC is now easy. Metrohm columns are built and developed to meet compliance requirements. Metrohm application chemists remain at the forefront of science and research where new simplified and enhanced methods are being developed. • All column data is immediately available. • Active monitoring of all important column functions • Complete traceability of all column parameters COMBUSTION IC Analyse solids and viscous samples Combustion IC is the modern combination of hydropyrolysis and ion chromatography. With this coupling, it is possible to analyse solids and highly viscous samples fully automatically. In contrast to previously employed methods, Analytik Jena’s flame sensor technology in combination with Metrohm’s liquid handling capabilities enables fully automated analysis without time consuming method development, internal standards, and manual steps. Even the supply of sample is automatic. Combustion IC at a glance: • Fully automatic sample preparation for solids and liquids during sample delivery and subsequent ion chromatographic analysis • Simultaneous determination of sulfur and halogens • Differentiated determination of the concentrations of various halogens • Material tests with regard to halogen-free products (RoHS) • High sample throughput • High precision and accuracy MEP Instruments • A company of Metrohm and Anton Paar 11 Ion Analysis TRACE ANALYSIS WITH VOLTAMMETRY The versatile all-rounder for research, teaching and industry 797 VA Computrace 894 Professional CVS Analysis of heavy metals: total concentration… For specific applications where the cost of AAS or ICP is prohibitive, voltammetry can accomplish metal analysis with equivalent or even higher sensitivities. Only small quantities of reagents and pure nitrogen are required. Cyclic Voltammetry Stripping (CVS) … and speciation! With voltammetry it is also possible to differentiate between varying oxidation states of metal ions, or between free and bound metal species. This information can be used to assess biological availability and toxicity of heavy metals, making voltammetry an essential technique in environmental analysis. High ion concentrations? No problem with VA! Voltammetry is ideally suited for the analysis of: • Water, waste water and sea water • Salts and pure chemicals • Electroplating baths •Foodstuffs The 894 Professional CVS stands out for its unique flexibility. Due to the system’s entirely modular design, it can be expanded and upgraded at any time with additional units such as dosing devices, pumps and sample changers. STANDARDISED STABILITY MEASUREMENT Easy and automatic Oxidative stability of fats and oils The determination of the oxidation stability of edible oils and fats is the classical application for the 892 Rancimat. The “induction time” that is measured characterises the resistance of oils and fats to oxidation. The term Oil Stability Index (OSI) is also commonly used. The Rancimat method is incorporated in standards such as AOCS Cd 12b-92 and ISO 6886. This technique replaces the complicated Active Oxygen Method. 12 StabNet – Modern software for stability measurement StabNet is the modern and user-friendly software for carrying out stability measurements and archiving the measurement data. The characteristic features of StabNet are its ease of use and flexibility. www.mep.net.au Electrochemistry POTENTIOSTATS Developed for electrochemists by electrochemists Autolab NOVA software Autolab potentiostats The next-generation NOVA software package supports all electrochemical measurement techniques, offering accuratelytimed sequences of commands and powerful data analysis tools. NOVA is designed for multi-tasking and collaboration, with automatic database storage of all measurements and potentiostat settings. Autolab potentiostats and galvanostats offer a range of current outputs from 100 mA to 2 A and compliance voltages from 10 V to 100 V. The new Multi Autolab can control up to 12 independent channels. The capabilities of Autolab PGSTAT’s can be extended with additional modules, e.g. • Electrochemical Impedance Spectroscopy • pA current amplification for microelectrodes • Bipotentiostat and sensor electrode array • Ultra-fast (sub-μs) electrochemistry • Current boosters (10 A & 20 A) Innovative technology for miniaturised electrochemistry Portable dual- and multi-channel potentiostats Screen-printed electrodes • Voltammetric, amperometric or potentiometric measurements •Disposable • 18 electroanalytical methods • Micro-volumes of sample • • Working electrodes of carbon, platinum, gold, carbon Bluetooth™ connectivity • Optional accessories (Flow-cells) MEP Instruments • A company of Metrohm and Anton Paar nanotubes and gold nanoparticles, etc. • Dual sensors and customised chips 13 Process Analysis PROCESS ANALYSIS Laboratory analysis in the process environment ADI 2045 Process Analyzer Combining Metrohm’s knowledge in laboratory analysis and Applikon’s experience in process control instrumentation, the ADI 2045 can perform nearly every ON-line or AT-line wet chemical analysis in the most difficult environments. Its unique modular design makes it possible to adapt the analyser to the specific needs of the application. Multi-parameter and multi-stream analyses are easily implemented as well as communication with other devices. Titration •Acid/Base •Argentometric •Colorimetric •Complexometric •Iodometric • Karl Fischer •Precipitative •Redox • Thermometric Titration ISE Ion-Selective Electrodes • Analysis of most common anions and cations. Voltammetric Heavy Metal Analyser • Analysis of heavy metals in highly ionic solutions Differential Absorbance Colorimetry • Analysing heavy metals in most demanding sample matrices. Chemical species analysed on-line Acetic Acid Acidity Acrylaldehyde Alkalinity Aluminium Ammonia Aniline Anion-ActiveDetergent Arsenic Ascorbic Acid Bayer Liquor Blended Acid Boric Acid Brine (Ca & Mg) 14 Bromide Calcium Carbonate Caustic Chlorate Chloride Chlorine, Free/ Total Chlorine dioxide Chromium Citric Acid Cobalt ChemicalOxygen-Demand Copper Cyanide, Free/ Total/WAD Dithionite EDTA Fatty Acid Fluoride Formaldehyde Glucose Glycerol Heavy Metals (Cd, Cu, Pb, Zn, etc) Hydrazine Hydrochloric Acid Hydrofluoric Acid Hydroxylamine Hypochlorite Hypophosphite Indigo Iodide Iron (II) & (III) Lactic Acid Leuco Indigo Liquors: white, green, black Lime Lithium Magnesium Manganese Mercaptane Mercury Metaborate Nickel Nitrate Nitrite Nitric Acid Nitrogen, Total Oleum P & M number Peracetic Acid Peroxide Persulphate Phenol Phosphate Phosphate, Total Phosphoric Acid Phthalic Acid Pickling Bath Solutions Silica Silver Sodium Sulphate Sulphide Sulphite Sulphonic Acid Sulphuric Acid Surfactant TBC Tetrafluroborate Thiocyanate Tin Titanium TMAH Urea Water, Karl Fischer Zinc www.mep.net.au TOC TOTAL ORGANIC CARBON ON-LINE Monitoring organically bound carbon in water streams ADI 7010 Reliable on-line TOC measurements The ADI 7010 TOC Analyzer measures Total Organic Carbon in liquid samples using the method of UV persulfate oxidation with carbon dioxide detection by non-dispersive infrared. The Analyzer can measure TOC in liquid samples ranging from 0-5 mg/L up to 0-50,000 mg/L and conforms to EPA, DIN, CE, ASTM, NAMUR regulations and meets European ISO/CEN guidelines. Application of Total Organic Carbon By monitoring TOC during their processes many industries are able to save costs, by confirming a process is optimised and operating efficiently. Monitoring TOC also helps ensure wastewater is treated correctly, meeting consent requirements before discharge to the environment or meeting organic load limits for discharge to municipal treatment plants. TOC monitoring is applied in many industries like: Chemicals, Pharmaceuticals, Food & beverage, Automotive, Oil & gas, Power & energy, Petrochemical, Pulp & paper, Airports and Environmental monitoring. Sample types: Waste water, Drinking water, Surface water, Process control, Boiler feed water/condensate, Cooling water, Run-off/storm water MEP Instruments Full Application Guarantee TURNKEY SOLUTIONS Economical and guaranteed Monitoring continuous sample streams maybe necessary and more economical than lab solutions. Our Metrohm – Applikon specialists have developed and implemented numerous systems worldwide covering an extensive range of applications for the determination from µg/L to g/L levels. Sample preconditioning units for liquids, solids and gases: More often than not, samples need to be preconditioned before they can be sent into the analyser. • Filtration and settling (e.g. slurry) • Extraction, stripping, distillation • Cooling and heating • Dilutions and reactors • Grinding and dissolving (powder) •Mixing Construction Materials MEP provides simple one sample preconditioning to complex turnkey solutions including shelter. Contact our engineers to discuss your needs. • Stainless steel (SS316), hastelloys, teflon, Viton, PP etc. Ingress protection • IP65 and IP66 Shelters • Cooling and/or heating • Drainage of waste to sewage • Service table, tap, sink etc. •Lighting • Power backup systems MEP Instruments • A company of Metrohm and Anton Paar 15 Process Analysis MONITOR FOR AEROSOLS AND GASES IN AMBIENT AIR Environmental surveillance Continuous Measurements of Aerosols in Sydney, NSW. MARGA for autonomous operation With MARGA, gas and aerosol composition of ambient air can be measured simultaneously and continuously. The whole MARGA system runs autonomously, generating aerosol and gas concentrations every hour, only requiring user intervention once per week to supply new solutions. The sensitivity of the ion chromatographs is sufficient to reach detection limits below 0.1 µg/m3 with an air sampling flow rate of 1 m3/h. The MARGA is available with 1 or 2 sample boxes, the latter allowing simultaneous sampling of two different aerosol sizes, for example PM 2.5 and PM 10. • Continuous monitoring with hourly results • Results on the composition of gases and aerosols • Remote access and data transfer • One week unattended operation • Smart software with security and validation levels • Quality assurance of the measurement with internal standard ion chromatography 16 www.mep.net.au Anton Paar Process PROCESS MEASUREMENT SOLUTIONS Continuous control of beverages and liquid chemicals Inline and online beverage analysers Process Density and Sound Sensors Anton Paar‘s series of density and sound sensors are used for the measurement of liquids, aggressive liquids, liquids with high temperatures or whenever the highest accuracy is needed. They continuously measure density, concentration, phase separation and product identity to optimise production processes and ensure a consistently high quality of product. • The highest accuracy • Robust measuring technology • Safe use • Small and compact Inline Viscometer This revolutionary viscometer continuously and reliably monitors the viscosity of process liquids such as suspensions, lubricants and starch adhesives. The inline viscometer is installed in a pipe or tank and shows the viscosity at process and reference temperature in 24-hour operation. First-class instruments for continuous, accurate and safe measurement of important quality parameters such as °Brix, % Diet concentration, CO2, alcohol, sugar inversion, extract, etc. during the entire production process. Inline and online beverage analyser models from Anton Paar – powerful, tried-and-tested measuring procedure and user-friendly software. Models include; • Cobrix 5 for °Brix, % Diet, CO2, alcohol, original extract, real extract, apparent extract, degree of fermentation and other optional parameters • Beer Monitor for alcohol, real and original extract and optional CO2 • Wine Monitor for alcohol, extract and CO2 content of wine • CO2 sensor: Highly accurate inline CO2 sensor for the continuous monitoring and control of CO2 content during beverage production. • Consistent product quality • Simple installation • Determination range from 1 mPa.s to 50.000 mPa.s • Not influenced by drops in pressure or flow rate • Constant results, even under adverse flow conditions MEP Instruments • A company of Metrohm and Anton Paar 17 Concentration DENSITY AND CONCENTRATION Measurements made easy: 0.001 to 0.000005 g/cm3 accuracy It all started in 1967; Anton Paar produced the first digital density meter with an oscillating U-Tube, marking a turning point for density measurement and replacing hydrometers and pycnometers. Today the 7th generation of DMA density meters is being manufactured, while instruments of the first generation are still operating in many laboratories. DMA 4100 M, 4500 M & 5000 M The DMA Generation M series enables the connection of new Modular Extensions (ME) directly to the Master Instrument (M). Anton Paar has developed modular extensions to analyse CO2, O2, Turbidity, pH, Diet Strength and Alcohol in combination with density. • Accuracy range g/cm3: 0.0001 to 0.000005 • Automatic sample changers and built-in filling options • Automatic filling check and video in selected models • Patented reference oscillator for drift free measurement and single point adjustment • Built-in concentration tables and custom functions DMA 35 Portable density meter DMA 500 Stand-alone density meter The four models of the DMA 35 give you the density, specific gravity, %-concentration of several parameters including Baume, Brix and Plato within seconds by simply pressing the lever. The intrinsically safe Ex versions enable safe testing of fuels and battery acid in the field. The stand-alone DMA 500 density and concentration meter provides results with an accuracy of 0.001 g/cm3 at the push of a button. • Accuracy ± 0.001 g/cm3 18 • Temperature range 15˚C to 40˚C • Integrated battery for mobile use •FillingCheck™ and camera image of measuring cell www.mep.net.au Concentration BEVERAGE ALCOHOL, CARBONATION AND OXYGEN METERS Setting industry standards Beverage carbonation and oxygen meters The CarboQC, OxyQC and new combined CboxQC are suitable for lab and at-line beverage applications. With robust IP67 construction, patented CO2 measuring method and modern O2 luminescence sensors the new series is perfect for your measuring requirements. Sampling direct from beverage packages is possible with PFD device. PBA – Package Beverage Analysers Portable Alcohol Meter for Distillates: Snap 50 Alex 500: Alcohol and Extract Meter for Beer Alcolyzer® Beer, wine and spirits Quality parameters, such as Brix, Alcohol, Extract, pH, Turbidity and colour, are measured directly out of the bottle or can, without time-consuming sample preparation. The beverage analysis systems are more reliable and quicker than previous systems on the market. Beverage analysis – easy, quick, modular. The portable alcohol meter Snap 50 measures distillates in all strengths within seconds: from pure distillates to samples taken during watering down to drinkable strength and ready-to-drink spirits. The alcohol meter automatically compensates the temperature influence on the result and shows the alcohol concentration with an accuracy of 0.1 % v/v on the large display. Alex 500 is a compact instrument for the determination of alcohol and extract content, calories, and the degree of fermentation in beer. The Alcolyzer® is the standard instrument for alcohol measurement. Based on a patented method for selective alcohol analysis using NIR spectroscopy, the Alcolyzer® is easy to use and delivers results within minutes. The new Alcolyzer ME measuring module makes it possible to measure the alcohol content of spirits, wines and beers with a single alcohol meter, just by selecting the appropriate method. MEP Instruments • A company of Metrohm and Anton Paar • Alcohol accuracy 0.2 % v/v • Density accuracy 0.001 g/cm³ A small unit with great power. 19 Concentration POLARIMETRY AND REFRACTOMETRY A range of instruments suitable for quality control to research applications A refractometer for every task The new Abbemat series Anton Paar launches a new range of Abbemat refractometers, which embody four decades of technical know-how. Building on the longstanding knowledge from Dr Kernchen, Anton Paar continues the tradition of producing high-end refractometers and presents three new product lines: the Performance line, Performance Plus line and Heavy Duty line. • Accuracy to ± 0.00002 nD • Temperature range 10°C to 110°C • Up to 8 wavelengths with the MW model MCP 200/300/500 Polarimeters The MCP series is the latest generation of polarimeters with full compliance with international standards (pharmacopeias, OIML, ASTM, Australian Standard K157). Modulyzer Multiparameter measurements • Peltier temperature control As an alternative to using a number of single instruments, Anton Paar now provides a complete system for measurement: the DMA Generation M which can be combined with: • 100% ICUMSA compliance • a high precision • Resolution down to 0.0001° with the Sucromat model • Temperature range 15 to 45°C refractometer RXA • a MCP series polarimeter • a colour measuring instrument • a pH module and more. 20 www.mep.net.au Material Testing INTELLIGENCE IN RHEOLOGY AND VISCOSITY Cutting-edge technology for research and development MCRXX2 Modular Compact Rheometers LOVIS microviscometer The Lovis measures viscosity of low viscous solutions in small volumes that require accuracy and repeatability according to DIN 53015 and ISO/DIN 12058. • Peltier temperature control + 5˚C to 100˚C • Sample volume 0.1 mL to 0.8 mL (1 mL to 3 mL w. ME) • Range 0.3 to 10,000 mPa.s • Optional combination of density meter and sample changer SVM3000: Viscosity and density in one Anton Paar introduces the third generation of Modular Compact Rheometers. More versatile than ever, the new MCR series offers an open range of possibilities. This is how Anton Paar defines future-proof rheometry: Whichever new application opens up, MCR users can rely on the fact that they are always covered. Whether in routine QC lines or high-end R&D applications, the speed and precision of the systems’ dynamic EC motor and numerous features are always readily available for convenient operation and reliable results. The SVM3000, meeting ASTM D7042, opens up a whole new era in viscosity measurement. Requiring a fraction of lab space, the SVM is extremely robust, very easy to use and can be installed in minutes. • Extensional rheology with SER and UXF fixtures • Measures viscosity and • DMTA with fixtures for solids, films and fibres density • Displays dynamic/kinematic viscosity and density • Temp. range of –56˚C to 105˚C • TwinDriveTM Ready for Stress and Strain controlled rheology • Choice of air bearing or ball bearing models • TruRate™ and TruStrain™ • Largest range of accessories available • Temperature range from –150˚C to 1600˚C • Pressure range up to 1000 bar • Rheo-microscopy (UV, SALS, SAXS, SANS) • Starch Rheology • Interfacial Rheology • Powder Rheology •Tribology • Viscosity 0.2 to 20,000 mm2/s. • Density 0.65 to 3 g/cm3 MEP Instruments • A company of Metrohm and Anton Paar 21 Material Testing SURFACE MECHANICAL PROPERTIES Indentation, scratch and tribology testing Indentation, scratch and tribology Multiple Indentation or Scratch testers along with 3D confocal or AFM modules are installed together on the same, compact platform. All measurement and imaging modules are “synchronised” to each other, allowing complete automation and control when performing measurements in the macro, micro and nano scale. Anton Paar TriTec solutions provide configuration flexibility to grow with all customer needs. Swiss made with over 30 years of experience. • Indentation/hardness testers • Scratch testers •Tribometers • Coating thickness measurements NANOSTRUCTURE ANALYSIS ZETA POTENTIAL SAXSpace Zeta Potential analysis on solid samples The Small-Angle X-ray Scattering (SAXS) method generates information about the morphology of a huge variety of materials, ranging from proteins, nutrients and active pharmaceuticals to polymers, fibres, paints and catalysts. SAXSpace gives users both line and point collimation options, with two beam lines connected to the same X-ray source. Users can now analyse the overall nanostructure of a sample up to 200 nm, as well as their crystal lattice at the atomic level below nanometer size – by performing continuous SAXS and WAXS measurements. The SurPASS electrokinetic analyser is a state-of-the-art tool for solid surface characterisation. This instrument is the culmination of many years of experience with the streaming potential technique at Anton Paar and our close cooperation with universities and research institutes. The well-engineered electrolyte circulation, integrated electronics and the easy-to-use measuring cells provide a user-friendly platform for advanced surface analysis. The myriad of measuring cells allow a range of solid samples to be characterised, including films, fibres, powders, flat sheet and hollow-fibre membranes, ceramics, electronic wafers and textiles. Modular nanostructure analysis • TrueFocus – automatic system alignment Advanced science for material testing • Single source – multiple beam lines • Maximum efficiency – high sample throughput • Simultaneous small- and wide-angle measurements (SWAXS) 22 www.mep.net.au Material Testing FUEL AND BITUMEN TESTING High-tech test equipment for the petrochemical industry Flash-Point Pensky-Martens Method PMA 5 In 1873 Berthold Pensky founded his own company and started producing flashpoint testers, viscometers and other machinery. The Pensky-Martens flashpoint tester was born! The PMA5 covers the ASTM testing methods D93 A, B & C. PNR 12 Penetration Test • Automatically lights test flame, relights if necessary during the test, suppresses gas source at end of test • Built-in sensor for automatic barometric pressure correction • Overheating detection with automatic heat shut-off during the test • Integrated fire-extinguishing system • Suitable for standard & small sample volumes MEP Instruments • A company of Metrohm and Anton Paar The Penetrometer PNR 12 is suitable for measurements according various “Bitumen” methods such as ASTM D5. Needle-Penetration Measure the consistency of semi-solid and solid bituminous mixtures. Rod-Penetration Measure the apparent viscosity (Bitumen No.) of filler aggregates used in bituminous mixtures. Cone-Penetration Determine the consistency of hot-applied, fuel-resistant joint sealants with or without being immersed in fuel or oil. ADU 5 Automatic Distillation Unit Examine motor gasolines, aviation gasolines, aviation turbine fuels, special boiling point spirits, naphthas, white spirits, kerosenes, gas oils, distillate fuel oils, solvents and similar petroleum products. • Volume detection by solid state light barrier system • Temperature controlled swing-out receiver chamber • Integrated computer (with Windows & ADUpro software) • LIMS, impact or ink-jet printer are connectable 23 Spectroscopy SPECTROSCOPY Elemental analysis from sub ppt to percent eayr Y 0 1 rrant Wa tical p on O onents p m Co Highest performing ICP-MS Powerful, patented technology: PlasmaQuant® MS The PlasmaQuant® MS is the world’s highest performing ICP-MS with unsurpassed sensitivity of over 1.5 billion counts/second/ppm. Integrated patented technologies provide an efficient and robust plasma system, superior interference removal and extended linear dynamic range, handling any application with ease. Two models are available that serve both the routine and research industries. High-Resolution Array ICP OES contrAA® From budget AAS to the strongest Zeeman PlasmaQuant®PQ 9000 The most powerful ICP OES. PlasmaQuant® PQ 9000 combines robust high-resolution technology and a revolutionary small design. Outstanding analytical capabilities arise from synergetic interactions between its four patented key components: Unique multi-element analysis with flame, hydride and graphite furnace technology, using just one light source The contrAA® series exceeds the performance of conventional AA spectrometers in all parameters. High-Resolution Continuum Source AAS (HRCS AAS), represents previously unattained effectiveness and quality of measurement results. Following decades of experience in the development of spectrometers and graphite furnaces, a vision has become reality with the contrAA® series, which finally closes the gap between ICP OES and AAS. novAA: AAS for flame, hydride and direct solids analysis with D2 background correction. Nova 350: Flame. Nova 400P Flame/Graphite/Solids. • High-resolution optics • V Shuttle Torch • Dual View PLUS • High-frequency generator 24 Zeenit: 3 Field Mode for maximum sensitivity or for expansion of linear working range; Dynamic Mode for automatic adaptation to varying element concentrations without dilution. Mercur AAS/AFS Analysers Based cold vapour technique using AFS or AAS, with or without enrichment. Mercur Duo and Duo Plus tandem analysers based on AAS/ AFS with or without enrichment to sub ppt. www.mep.net.au Spectroscopy TOC/TN, AOX/TOX SUM parameter analysis for routine and research multi N/C® High performance TOC analysers AOX/TOX: Fast, flexible and cost-effective Routine and specialist tool for any application The multi N/C® series offers the optimum solution for every application. The parameters TOC, NPOC, POC, TC, TIC and TNb can be measured quickly, easily and without any conversion in liquid and solid samples. Working with multi N/C® series analysers guarantees compliance with the valid national and international standards, such as: ISO, EN, DIN, EPA, ASTM, FDA and pharmacopoeias. multi X® 2500 – A versatile system that opens up new dimensions in AOX analysis Whether fastest AOX routine analysis in vertical operation mode or reliable determination of the smallest EOX trace concentrations in horizontal operation mode, the double furnace technology of the multi X® 2500 allows you to select the best combustion mode for your application. The intelligent software multiWin®, the fast changeover between column and batch method, and the user-friendly design ensure outstanding ease of use and efficiency. Diverse automatic sampling systems offer convenient and uniquely flexible operation. The system greatly minimises idle time and increases the throughput of AOX samples – you remain flexible and cost-effective. MEP Instruments • A company of Metrohm and Anton Paar 25 Spectroscopy UV-VIS SPECTROSCOPY Spectrophotometers for all budgets The SPECORD® series covers the range from budget-priced, single-beam to high-performance real double-beam instruments with Cooled Double Detection. They also include high power diode-array systems for simultaneous high-speed measurement and spectrophotometry using Split-Beam technology. All our powerful spectrophotometers operate in the spectral range of 190–1100 nm. A versatile software provides maximum efficiency and offers specific tailor-made software packages. The extensive range of accessories enables flexible and convenient operation in various fields of application. ELEMENTAL ANALYSIS From petrochemical to environmental samples multi EA® 4000 C, S, Cl analysis in solids multi EA® 5000 Elemental Analyser Determining carbon, sulphur and chlorine from solid samples is not a problem! The multi EA® 4000 convinces with its ease of use, analysis flexibility, and particularly excellent instrument stability and precision. This universal talent determines C, N, S, Cl as well as TOC, EOX and AOX/TOX. • The parameters TS, TC, TX, TOC, TIC, EC and BOC are determined quickly and easily in organic and inorganic solids. • Determination of TOC, TIC in one simple step without sample preparation • Low operating costs • State-of-the-art NDIR detector • One analyser for liquid, paste-like, solid, gaseous and LPG samples • Multi-matrix autosampler for the fully automatic determination of solid and liquid samples • Conformity with a multitude of common international and national standards such as ASTM, EPA, DIN, ISO, EN etc. • Double furnace technology, vertical and horizontal operating mode in a single device • Flame sensor technology for matrix-optimised sample combustion • Flame sensor technology for matrix-optimised sample combustion 26 www.mep.net.au Spectroscopy RAMAN / NEAR-INFRARED SPECTROSCOPY Control at the speed of light Near-infrared spectroscopy is a simple, quick, nondestructive technique. Metrohm NIRSystems instruments can be installed in the laboratory, atline or directly into a process stream, dryer, extruder, or reactor. The measurement mode and location of the analyser depend on the optical properties of the samples, the required analyte selectivity and sensitivity, the duration of the process run and the monitoring and control requirements. A suitable analyser is available for every sample type and processing environment. Mira Metrohm Instant Raman Analyzers With the mobile Mira spectrometers you can rapidly extract a great deal of chemical information of a wide variety of unspecified samples. Within seconds, the handheld Analyzerrs offer you reliable and easy interpretable results, be it for material verification or counterfeit detection. • Reproducible results with averaging Orbital- RasterScan (ORS) mode for the most complex samples • Maximum flexibility – «open library» principle ensures Laboratory / At-Line Analysers Process Analysers A patented monochromator and modular sampling accessories make Metrohm NIRSystems instruments designed by Foss uniquely capable of analysing powders, granules, solids, slurries, gels, pastes, and turbid or clear liquids, in any order. Metrohm NIRSystems Process Analyzers are setting the standard for real-time process analysis. Designed for seamless integration into process control strategies, these NIR (nearinfrared) Analyzers provide outstanding measurement stability and performance. Users can optimize the measurement method in reflectance, transmittance or interactance mode according to sample type. Fiber optic probes permit the use of laboratory instruments for scale-up and reaction monitoring as well. Process NIR analysis requires no sample handling or reagents and no disposables; potential environmental concerns and potential health and safety risks associated with sampling are eliminated. reliable outcomes • Reduced to the max – light, compact, handy MEP Instruments • A company of Metrohm and Anton Paar 27 Particle Characteristics SIEVE ANALYSIS Taking a close look at quality SIEVE with the highest precision for accurate results RETSCH sieve shakers and test sieves are the key to easy, rapid, reproducible and, above all, accurate analyses. • Manufactured in accordance with ISO 3310-1 or ASTM E11 • One piece construction • Unique, fully automatic production process and optical inspection • Superior product quality • Full traceability ensured with clear and precise laser-engraved labelling RETSCH’s test sieves are available in a range of frame sizes: 200 mm, 203 mm (8”), as well as smaller (100 mm and 150 mm) and larger (305 mm, 400 mm and 450 mm) sizes. Stocked in Australia: The most commonly requested sieves are held on stock in Australia for your convenience. AS 200 Jet for powders Sieving with a 3-D effect Air-jet sieving for fine powders that tend to agglomerate is considerably faster than vibration sieving, yet gentle on the material by air dispersion of the powder. The patented electromagnetic drive of the AS 200, 300 and 450 produces a 3-D throwing motion for optimal use of the open sieve area. • For dry and wet sieving • Control, evaluation and documentation with EasySieve® software 28 www.mep.net.au Particle Characteristics PARTICLE SIZE AND SHAPE ANALYSIS Because size does matter Patented Camsizer Measurement Principle Digital dynamic image processing with the CAMSIZER P4 and the CAMSIZER XT Measuring principle The CAMSIZER family of dynamic image analysis instruments are based on the proven, patented two-camera system. Depending on the particle size and the degree of agglomeration, either the CAMSIZER P4 or alternatively the CAMSIZER XT represent the optimum solution for your particular sample and your analytical requirements. Camsizer P4 Camsizer XT • 20 µm to 30 mm • 1 µm to 3 mm Typical examples of applications: • Pourable bulk materials • Gravity dispersion • Permanent quality assurance during production • Unattended operation with • Air pressure dispersion • Immediate checks on incoming and outgoing goods • Meaningful laboratory measurements with a wide range Auto Sampler option • On-Line version available • Fine and agglomerated particles • Wet dispersion of different sample materials • Roundness of sand and sediments for geologists e.g. proppants and frac sands MEP Instruments • A company of Metrohm and Anton Paar 29 Sample Preparation PERFECT SAMPLE PREPARATION Essential for reproducible analysis Solutions for size reduction and homogenisation: milling, grinding and cutting Reliable and accurate analysis can only be guaranteed after reproducible sample preparation. The aim of sample preparation being to turning a laboratory sample into a representative part sample with homogeneous analytical fineness. Cutting Mills Jaw Crushers RETSCH offers a comprehensive range of the most modern mills and crushers for coarse, fine and ultra-fine size reduction of almost any material. The choice of grinding tools and accessories not only ensures contamination-free preparation of a wide range of materials but also the adaptation to the individual requirements of different applications. The Cutting Mills SM 100, 200 & 300 are used for preliminary size reduction by cutting and shearing of soft, mediumhard, elastic and fibrous materials. They are suitable for temperature-sensitive samples. The powerful RETSCH Jaw Crushers (BB 50, 100, 200, 300) are designed for the rapid, gentle, coarse and primary crushing of hard, brittle and tough materials. The breaking jaws are available in a variety of materials. Selection guide RM 200 PM 100 PM 200 PM 400 MM 200 MM 400 CryoMill 10 10 15 15 15 10-40 130 80*60 2 5 0.04 0.5 0.1 Ball/ Mixer Mills DM 200 130 4 Mortar Grinders RS 200 90 SM 300 50 SM 200 0.01 SM 100 0.1 GM 300 0.04 GM 200 8 SR 300 8 SR 200 6 SK 100 10 Twister 4 ZM 200 10 BB 300 8 BB 200 20 BB 100 15 0.2520 35 0.5 Disc Mills Knife/ Cutting mills Rotor Mills Jaw Crushers Final fineness* approx.(mm) BB 50 Feed size* approx.(mm) 0.08 0.05 0.3 0.3 O ✓ ✓ O O O O O O O ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ O O O O ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ Chemicals products O O O O ✓ Coal, coke ✓ ✓ ✓ ✓ ✓ Construction materials ✓ ✓ ✓ ✓ O 0.001 0.001 0.001 0.01 0.005 0.005 Electronic scrap, circuit boards ✓ O O ✓ ✓ O ✓ ✓ ✓ ✓ ✓ ✓ Feed ✓ ✓ O ✓ ✓ ✓ ✓ ✓ ✓ ✓ O O O O ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ O O O O ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ Food ✓ ✓ Glass, ceramics ✓ ✓ ✓ ✓ O Leather, textiles O O O Minerals, ores, stones ✓ ✓ ✓ ✓ O O O O O O ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ Pharmaceutical products ✓ O O ✓ ✓ ✓ ✓ O O O O ✓ ✓ ✓ ✓ O ✓ ✓ Plants, hay, straw ✓ ✓ O O O O ✓ ✓ ✓ ✓ O ✓ ✓ ✓ ✓ ✓ ✓ Plastics, cables, rubber ✓ O ✓ ✓ O Secondary fuels ✓ O ✓ ✓ ✓ ✓ ✓ O O O O ✓ ✓ Soils, sewage sludge O O O O O O Wood, bones, paper ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ O ✓ O O ✓ ✓ ✓ ✓ ✓ ✓ ✓ O ✓ ✓ ✓ ✓ ✓ Suitable O Suitable to a limited extent *depending on sample and grinding time. This chart serves only for orientation purposes. The selection of the appropriate mill depends on a variety of parameters of the actual application. Please contact us to discuss the best solution. 30 www.mep.net.au Sample Preparation PERFECT SAMPLE PREPARATION Essential for perfect analysis Rotor Mills Mixer Mills Knife Mills The Rotor Mill series includes ultra-centrifugal mills (ZM 200 and Cyclone TWISTER), rotor beater mills (SR 200 & 300) and cross beater mills (SK 100). Suitable for the preliminary and fine size reduction of soft, fibrous and also hard materials. The RETSCH Mixer Mills, MM 200 & 400, are used for size reduction and pulverisation of hard, medium-hard and brittle samples as well as for soft, elastic or fibrous materials. In food or nutritional laboratories, in chemical or biological research institutes – GRINDOMIX Knife Mills, GM 200 & 300, provide size reduction and homogenisation of food and feed materials, meeting and exceeding all special laboratory and analytical requirements. They process substances with a high water, oil or fat content just as quickly and reliably as dry, fibrous, soft, elastic or medium-hard products. • Wet and low temperature grinding (MM 400) • Ideal for cell and DNA-RNA extraction ASSISTING Dividing, feeding, drying and pelletising samples Retsch Assisting RETSCH asssisting instruments optimise and support sample preparation. They provide reproducible processes with greater efficiency and are characterised by their ease of handling. • Sample Dividers: essential for the exact and representative division of pourable bulk goods in the laboratory • Vibratory Feeders for uniform and continuous feeding • Pellet Presses for preparation for XRF analysis • Fluid Bed Dryer for gentle drying and dispensing • Ultrasonic Baths for cleaning (test sieves, grinding tools) and degassing MEP Instruments • A company of Metrohm and Anton Paar 31 Microwave Chemistry MICROWAVE CHEMISTRY Sample decomposition Microwave sample preparation Clear solutions for great results The Anton Paar Multiwave range of microwave sample preparation systems provide the ultimate in flexibility and power to handle a huge range of applications, bridging the gap between sampling and analysis. They are capable of: Acid digestion: achieving safe and complete digestion in a fraction of the time required by conventional techniques Leaching: US-EPA and ASTM methods available as standard with continuous control and documentation Solvent extraction: performing Microwave-Assisted Extractions (MAE), with dramatically shorter reaction times compared with conventional methods such as Soxhlet Evaporation: evaporating acids and pre-concentrating aqueous solutions directly from reaction vessels Drying: perform gentle drying without carbonisation or contamination of samples, in a fraction of the time Special applications: oxygen combustion for the determination of halogens, UV digestion of liquid samples or acid hydrolysis of proteins 32 Routine digestions Simple and quick The High Pressure Asher HPA-S Multiwave Go and PRO are quick and convenient microwave digestion systems for the routine handling of environmental, food and many other samples. With a typical process time of just 30 minutes, including heating, holding and cooling, Multiwave simplifies sample preparation tasks and provides solutions ready for analysis in the shortest time. This is the reference instrument for wet chemical decomposition under high pressures. The instrument is TÜV certified and can prepare even the most difficult samples for reliable AAS, ICP-OES, ICP-MS and voltammetric analysis. www.mep.net.au Microwave Chemistry MICROWAVE CHEMISTRY Synthesis solutions Microwave synthesis From R&D to kilo-scale production The new generation of Anton Paar Microwave Synthesis systems has been developed in response to the increasing demand for straightforward solutions from initial R&D to kilogram scale up production. Getting started with Monowave 300 for Research & Development Method development with the Monowave 300 opens up pathways to new reaction routes for a broad variety of applications. Sequential method optimisation employing the 24 position autosampler MAS 24 with a Monowave 300 or parallel optimisation with the silicon carbide rotors of a Multiwave PRO considerably facilitates chemists’ everyday work. MEP Instruments • A company of Metrohm and Anton Paar Want more? Scale up with Multiwave PRO Masterwave BTR The big deal! For parallel scale-up to the multi-gram range, use the Multiwave PRO. Direct scalability of your optimised methods allows for library generation in significant gram amounts. A wide choice of rotor configurations provides the ideal solution whatever the task. Batch-type processing in the litre scale with Masterwave BTR leads to as much as 250 g product in a single run. The user interface for the software is identical, allowing direct method transfer from the Monowave 300. Simply multiply the amounts of your mixture and follow your optimised protocols. 33 MEP Quality Service MEP SERVICE – EXPERTS BY YOUR SIDE Our engineers are qualified to maintain your instruments Instruments that are serviced on a regular basis fail less frequently, provide more accurate results and, put simply, perform better. Our Service Engineers have received extensive factory training and are authorised to service, diagnose and repair your systems. The tools they use are specially designed to pinpoint even the slightest deviance from manufacturer specifications, so they can return it to factorynew operation. 34 MEP Remote Support Analytical Instrument Qualification Calibration of Metrohm dosing & exchange units Metrohm Software Care The advantages of MEP Remote Support are obvious. With our remote service, you will get help directly and precisely when you need it. You can use your valuable time more efficiently and reduce downtime on your analysis system to a minimum. MEP Remote Support is available for all systems that are controlled by PC-software. All you need to benefit from our new service is an internet connection. Play it safe with professional and certified IQ/OQ. Stay on the safe side. An investment that pays off As QA manager in a regulated industry you face strict requirements regarding Analytical Instrument Qualification (AIQ). However, complying with the very latest regulations from the USP, FDA, GAMP, PIC/S, and other regulative authorities at all times is a challenge that takes time and effort. With this in mind, MEP have developed services exactly tailored to your needs. You protect yourself against liability while saving valuable time and money that you can spend on other work in your lab. The Dosing Test gives you certainty that your Metrohm buretet is dispensing the displayed value. This in turn gives you assurance that you really can rely on your results, and that this will not cause problems during auditing. You will receive the corresponding certificate confirming that your burette continues to comply with the requirements as verified by the test. You know that you can rely 100 percent on the accuracy of your Metrohm burette.  Software maintenance for safer and more productive work Metrohm Software Care is the perfect supplement to your MEP Care Contract. A system that does not get regular maintenance can become a safety risk and negatively affect both quality and productivity. Regular maintenance guarantees optimal system availability and maximum performance. With Metrohm Software Care you benefit from peak performance of your analysis system, minimise down-time and can all but remove the risk of losing any data. www.mep.net.au MEPCare™ MEPCare™ CONTRACTS Service, certainty and so much more No matter whether you work for a private company or for a public institution, as a laboratory manager you are required to use your resources as efficiently as possible. Failing equipment is a risk you simply cannot afford. A MEPCare™ Contract is your operational insurance card: safeguarding your instrument from failure and giving you peace of mind – from day one and for as long as you have it. Cost certainty With a MEPCare™ Contract costs for maintenance and servicing are fixed and, more importantly, known to you – so you can keep in line with your budget. Reliable measurement results A MEPCare™ Contract means instruments are installed, calibrated and adjusted by trained and authorised MEP service professionals to ensure their operational efficiency. Less risk of failure Instruments that are serviced regularly fail less frequently and have a longer lifetime than instruments that do not get this care. Fast repairs With a MEPCare™ Contract professional help is just a phone call away. Repairs are always performed by trained and authorised service professionals on a priority basis. Original manufacturer spare parts Original spare parts provide the best fit for your instrument and ensure its long lifetime. The services offered by MEP are geared to your requirements. You can choose from a clearly defined range of MEPCare™ Contracts, which build on each other in terms of scope and provision. Preventative maintenance for a long service life Regular maintenance is key to long-lasting, trouble-free operation of your analytical instruments and accurate measurement results. That is why all MEPCare™ Contracts include at least one preventative maintenance check every year. This is carried out by a trained and authorised MEP service specialist. They know the hardware and software of your analyser by heart and can advise you on best practices to get the most out of your system. MEP Instruments Quality Service Discounted spare parts With a MEPCare™ Contract you benefit from discounts on spare parts as specified in your Contract. Maintain the value of your investment Regular maintenance increases the service life of your instruments, so you retain the value of your investment. Repair Protection Repair Protection On-Site Service On-Site Service Priority Response Priority Response Priority Response Priority Response Preventative Maintenance Preventative Maintenance Preventative Maintenance Preventative Maintenance Standard Care Eco Standard Care Extended Care Eco Extended Care MEP Instruments • A company of Metrohm and Anton Paar 35 Partnerships LASTING PARTNERSHIP At MEP, we do not outsource customer service In Australia and New Zealand you can tap into the vast knowledge and experience of the world’s leading network of scientists using MEP Instruments’ on location support and service. You benefit from a wide range of support options and services of which many are complimentary. ONE/14 Whilst you concentrate on optimising your operations MEP is at your side to assist with an efficient transfer of know-how. Our commitment helps you to improve and maintain high analytical standards and develop new solutions in the lab and in the field. INFORMATION Tea Time On request, a free Morning Tea session can be held at your production facility, university or research centre. At Morning Tea sessions, you will enjoy direct contact with our experts in specific fields and have your questions answered, whilst having the opportunity to attend demonstrations and presentations of the latest developments specific to your industry or research field. Just call us to arrange for a Morning Tea session. We will bring the cake. News New instruments and software for ion chromatography and CVS Customer application A report from a research vessel Application report Round robin test – voltammetric trace analysis Application Bulletins Application Notes A vast number of application reports, notes and bulletins are available to our customers 24/7 online. They contain concise but precise descriptions of steps and configurations to perform specific analyses to get you started in a flash. You can also request them at any time by phone or by email. Can’t find what you are looking for? Call our experts. They will be happy to suggest a solution for you. 36 Newsletters & Magazines Many of our newsletters are published online only as our small contribution to a greener environment. Often on a monthly schedule, they cover applications and news related to specific industries. We currently offer the following titles: BeerPops&more, WineLab, FoodLab, Mines&Minerals, Air Water Soil, Teaching+Research, Process Analytics, PetroChemist and the Analyst Express. Subscription is free. Visit our website to register. Printed versions of Analyst Express, Metrohm Information and Retsch – The Sample are distributed free of charge to our customers. Workshops & Seminars MEP regularly offers seminars covering selected topics in advanced analytical chemistry. These seminars are held by leading national and international authorities at a venue near you. The seminars are free, but registration is required. Invitations are published in our newsletters and our website. Workshops offer a more hands-on approach to new solutions. In these workshops you will often have the opportunity to perform certain analyses yourself or within your workgroup. www.mep.net.au Application Testing TEST BEFORE YOU INVEST Application development and testing Application testing and development laboratory – Sydney & Melbourne MEP customers can always be certain that the acquired equipment will perform as expected. Analytical results will be accurate, precise and repeatable. We have installed a modern, efficient 120 m2 application lab at our headquarters in Gladesville, Sydney and at our Melbourne premises to best serve our customers. Unsure if your chosen method will produce the results you anticipate? Test before you buy. At MEP’s state-of-the art application lab we provide certainty before you make your final purchase decision. We test for you the desired method for viability and accuracy, develop alternatives and optimise automation projects before you buy. Fluctuating parameters? Did some possibly undefined parameters change during operation? Don’t let your people tinker too long. Save time and money. Our experts will work it out for you, right here, at our headquarters. Training Our application lab is available for expert instruction and training. Contact us for more details and for advance bookings. MEP Instruments • A company of Metrohm and Anton Paar 37 Applications Chart APPLICATIONS, METHODS AND SERVICES BY INDUSTRIES 25 Assisting (Sample Prep) 31 Atomic Absorption Spectroscopy 24 ● Baume 17/19 ● Brix 17/19 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Chloride 4 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● CO2 19 ● Combustion IC 11 ● ● ● ● ● ● Conductivity 9 ● ● ● ● ● ● Crushing 30 Cutting 30 Density (Lab, Field) 18 ● ● ● Density (Process) 17 ● ● ● ● ● Density 17 ● ● ● ● ● ● ● ● ● Differential Absorbance Colorimetry (Process) 14 ● ● ● ● ● ● ● ● ● Direct Solids by AAS 24 ● ● ● ● ● ● ● ● ● Distillation 23 ● ● 30 High Resolution CS AAS 24 ICP MS 24 ICP OES 24 Indentation/Hardness 22 Ion Chromatography ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 10 ● ● ● ● ● ● ● ● ● ● ● ● ● ● 9/14 ● ● ● ● 32 ● ● ● ● Microwave Sample Decomposition 32 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 33 Milling 30 ● ● ● Mixer Mills 31 ● ● ● NIR 27 ● ● O2 19 Particle Size and Shape (digital) 29 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Microwave Synthesis ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Microwave Digestion ● ● ● ● ● ● ● ● ● ● ● Grinding ● ● 10 12 ● ● 26 23 ● ● Cations / Metals ● ● ● C, S, Cl, N ● Wine AOX/TOX ● Water 10 Flash Point Testing Power ● ● Anions University ● 4 Electrochemistry Plastics Pharmaceuticals Petroleum Paints Mining Metal Life/Sciences Food Hospitals Fertilizer Explosives 17/19 Energy Environment 16 Alkalinity ISE Ion-Selective Electrodes (Process) 38 Detergents Alcohol Chemicals Aerosols and Gases Cement Beverage Applications and Methods Electroplating Industries ● ● ● ● ● ● ● ● ● ● ● www.mep.net.au Applications Chart APPLICATIONS, METHODS AND SERVICES BY INDUSTRIES 22 Scratch test 22 ● ● Sieving 28 ● ● Sugar purity 20 TAN/TBN 4 Titration ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Wine 28 SAXS – Nanostructure Analysis ● ● ● ● ● ● Water Sample Preparation Power ● ● University ● 21 Plastics 20 Rheology ● ● ● ● ● ● ● ● Pharmaceuticals Refractometry ● ● Petroleum 12 ● ● Paints Rancidity ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 4/14 ● TOC online 15 ● Total acidity 4 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Trace metal analysis 12 ● ● Tribology 22 ● ● ● ● ● Voltammetric Heavy Metal ● Mining 13 27 Metal ● ● Raman Spectroscopy Viscosity ● ● ● ● Life/Sciences ● Food ● Potentiostats UV-Vis ● ● ● Hospitals 20 ● Fertilizer Polarimetry (Lab) ● Explosives 8 Energy 4 pH ● Environment Peroxide number Chemicals 23 Detergents Penetration Cement Beverage Applications and Methods Electroplating Industries 26 ● ● ● ● 17/21 ● ● ● ● 14 ● Water (Karl Fischer) 7 ● ● ● Wet Process Analysis 14 ● ● ● Zeta Potential 22 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Service and Support Overview Application Notes 36 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Application Testing + Development NSW/VIC 37 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Calibration 34 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● IQ/OQ 34 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● MEP Care Contracts 35 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Newsletters 36 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Service Remote Support 34 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Software Service 34 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Training Courses 36 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● Workshops 36 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● MEP Instruments • A company of Metrohm and Anton Paar 39 MEP INSTRUMENTS IS YOUR EXPERT PARTNER TO ASSIST YOU IN RESOLVING YOUR ANALYTICAL CHALLENGES. Victoria & Tasmania 17/25 Cook Rd, Mitcham VIC 3132 PO Box 107 Mitcham VIC 3132 Tel (+61) 03 8872 7000 Fax (+61) 03 9873 4867 Western Australia Unit 6, 27 Tamara Drive, Cockburn Central WA 6164 Tel (+61) 1300 720 485 Fax (+61) 08 9381 5518 www.mep.net.au South Australia & Northern Territories 34 Grove Avenue, Marleston SA 5033 Tel (+61) 1300 720 485 Fax (+61) 08 8351 5398 Queensland Unit 9a, 253 Leitchs Rd, Brendale QLD 4500 PO Box 7280 Brendale QLD 4500 Tel (+61) 1300 720 485 Fax (+61) 07 3205 8894 New Zealand North MEP Instruments Ltd Unit E2, 14-22 Triton Drive Rosedale, Auckland 0632 PO Box 305161 Triton Plaza Auckland 0757 Tel (+64) 09 477 0620 Fax (+64) 09 476 0631 New Zealand South 352 Manchester Street, Christchurch 8141 PO Box 13 990 Christchurch 8141 Tel(+64) 03 365 9954 Fax (+64) 03 365 9958 SKA-CSSEA - M93520150127-1 New South Wales (Head Office) MEP Instruments Pty Ltd Unit 11, 56 Buffalo Rd, Gladesville NSW 2111 PO Box 2173 Boronia Park NSW 2111 Tel (+61) 02 8899 5200 Fax (+61) 02 8899 5299