Certificate of non-use for examining part

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Telecom Brick Fuse
Product #:
461xxx Series
Issue Date:
January 3, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
And it is certified by Littelfuse, Inc. that the series products listed above are compliant with
Halogen Free permissible limits (Cl≤900ppm, Br≤900ppm, Cl +Br≤1500ppm), as defined
according to IEC 61249-2-21 standard.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
< Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Telecom Brick Fuse RoHS-Compliant series products
manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
1
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
Raw Material Part Number
910-259
909-422
11-0595 (082xxx-001)
648106-001
692235
Raw Material Description
Cap
Body
Element – Cu99.9MSn
Yarn
Solder
2
Page(s)
3-10
11-18
19-24
25-32
33-37
scs
Test Report
No.:LB12-01094C
March5, 2012
Page1 of 4
LTTTELFUSE
PHtLS.,tNC.
LimaTech Center,SEZ,
Lipa,Malvar,Batangas
The followingsample(s)was/veere
submittedand identifiedbylonbehaltol the clientas:
ProductName
Cap 910-259/ Base
SGSSamplgNumber
LB12-01094.004
RecelvedDate
FebrJary21,2012
Test PerlormingDate
F€bruary
21,20121o
March5,2012
T6sl Perlormed
SGS Philippines
subcontracted
the testingot sampte(s)
setecl€dby
applicantwithfollowingresults
Test Requested
Selectedtest(s)as requested
by client.
Test llethod
Pleaserelerto nextpage(s).
Ted n6sult(5)
Pleaserefer1onextpage(s).
C,oncluslon
Basedon the perfomedtestson submittedsample(s),
the resultsof
Lead,Cadmium,Hexavalent
chromiumand l\,,lercury
complywith
lhe RoHSDnective2002/95/EC
and iis subsequeniamendments.
This reportwillbekepl on filefor six monthsfromthe dateol issue.
Signedfor and on behaltol
INC.
SGSPHILIPPINES,
I'EDEN L. PENEYHA
LaboraloryOperalions Manager
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SGS
Test Report
No.:LB12'01094C
Page2 ol4
March5.2012
: LB11-01094.004
SampleNumber
metal
of silvercolored
PhyslcalDas€ription : Basematerial
Item/ BatchNumb€r : fl/A
RoHSDlreclive2002/95/EC
Tesl ltem(s)
unit
(Cd)
Cadmium
mg/Kg
Lead(Pb)
MEKg
(Hg)
Mercury
mg/Kg
C(Vl)
Hexavalent
Chromium
Itothod
IEC62321:2008application
of modifieddigestionby
surlaceetchingand
perfomedby ICP-AES.
withreference
to lEc 62321:
2008andperfomedby
Boiling
waterextraction
Method.#
iIDL
n6sult
2
2
ND
'|19
2
ND
Negative
Nole :
1 mg/kg= ppm ; 0.1wt%= lOOOppm
2. ND = Not Detected
3. MDL = lllethodDet€ctionLimit
4. " = Oualitative
analysis(NoUnit)
5. # = a. Posilivemeansthe presenceol CrVlon the testedareas
b. Negativemeansthe.absenceof CrVlon the testedareas
solulionis equalorgrealerthan0 02 mg/kg
in boiling-water'extraction
The detecGdconcentration
with 50 cm2lesleda€as.
6. Analyseswere subcontractedto SGS Taiwan,Ltd
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sGs
TestReport
No.:LB12-01094C
March
5,2012
Page 3 of 4
ATALYSISFLOWCHARTOFHEAVYMETALS
Pb, cd, Hg
Negalive
A d d i n q1 , 5 lor
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Adding1.5the prssenceo, Cl6+.
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SGS
Test Report
No.:LB12-010S4C
March5, 2012
Page4 of 4
SamplePhoto (As Becaived):
LB12-01094.004
,
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Test Heport
No.:1812-01094A
March5, 2012
Page1 ot 4
INC.
LITTELFUSEPHII..S.,
LimaTech Center,SEz,
Lipa,Malvar,Batangas
bylonbehalfof theclientas:
andidentilied
The followingsample(s)was/were submitled
ProductName
Cap910'259/ Plaling
SGSSampleNumbel
L812,01094.002
RecelvedDate
Fehtuary21, 2012
Test PerformingDate
21, 2012to lllarch5, 2012
February
T€st Perfurmed
by
selected
lheteslingol sample(s)
subconlracted
SGSPhilippines
results
wilhfollowing
applicant
Te€t Requested
byclient.
teg(s)asrequested
Selecled
Test Method
Pleaserelerto nextPage(s)
Tqrt R.eult(s)
Pleaserefer10nextpage(s).
conclugion
theresultsof
sample(s)'
testsonsubmitted
Basedontheperlormed
complywlth
andl\rercury
Hexavalent
chromium
Lead,Cadmium,
amendments
anditssubsequent
2oo2l95/Eo
theRoHSDkective
This repodwill be kept on filelor six monthsfromthe dale of issue'
Signedlor and on behalfol
INC.
SGSPHILIPPINES,
i,EDEN L. PENEYRA
LaboratoryOperationsManager
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sGs
TestReport
No.:1812-01094A
PaOe2 ol 4
Llarch5, 2012
: LB11-01094.002
SampleNumber
PhygicalDescriplion : Platinglayerot siMercolored
metal
Itom/ BalchNumbor
RoHS Dlrectlve 2002/95/EC
Test ltem(s)
(tu)
Cadmium
Lead(Pb)
(Hg)
Mercury
Unlt
Method
MDL
Rg€ult
mgKg
m9Kg
mg/kg
IEC62321:2006application
ol modifieddigestionby
surfaceetchingand
performedby ICP-AES.
2
2
ND
18
NO
HexavalentChromiumC(Vl)
wilh reference
to lEc 62321:
2008andperformedby
Boiling
waterextraction
Method.#
Negalive
Nole :
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2. ND= NotDetected
Limit
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(NoUnit)
analysis
4. " = Qualitative
meansthepresence
ot CrVlonthetestedareas
5. # = a. Positive
b. Negativemoansthe absenceof CrVlonlhe testedareas
is equalorgreaterthan
0.02mg/kg
Thedetected
concentration
in boiling-waterexlraction
solulion
with50 cm,testedarcas.
to SGSTaiwan,Ltd
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SGS
Test Report
No.:LB12-01094A
Page3 of 4
March5,2012
OF HEAVYMETALS
ANALYSISFLOWCHART
l,leasursmenl
Sample
Pb, cd, Hg
Posilive
Negative
Heating
ro90-95'C
TotatDigestion
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SGS
Test Report
No.:LB12-01094A
March5,2012
Pege 4 ol 4
SamolePhoto (As Receiv€dl:
LB12-01094.002
,
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Test Report
Applicant:
Number : TWNC00285767
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 19, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Body
Part Number
: 909-422
Date Sample Received
: Nov 12, 2012
Date Test Started
: Nov 13, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 8
Number : TWNC00285767
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
White Plastic
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 8
Number : TWNC00285767
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
White Plastic
Test Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 12, 2012
: Nov 13, 2012 To Nov 15, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 8
Number : TWNC00285767
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 8
Number : TWNC00285767
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
PBBs/PBDEs
Weigh sample and
add organic solvent
By Soxhlet
extraction or
Solvent extraction
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Cr
6+
Substrate
Cd/Pb/Hg
Weigh sample
and add
alkaline
solution
For different
material, digest
the sample with
*1
appropriate acid
Plating
Cr
6+
By spot test
Definite temp.
extraction
Cool and filter
the extract
Confirm the tested
samples are
totally dissolved
Negative
*2
Get 50cm2 sample
Make up with
deionized water
By boiling water
extraction
Analyzed by ICP-OES
Make up with deionized
water and add
diphenyl-carbazide
solution
Analyzed by UV-VIS
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 8
Number : TWNC00285767
Test Conducted
(Ⅳ) Measurement Flowchart:
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 8
Number : TWNC00285767
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 8
Number : TWNC00285767
Test Conducted
Photo
*THJ0285767*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 8 of 8
Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth ·
Polyfil AG
Gina Gregorio
Oberallmendstrasse 20A
6300 Zug / Switzerland
Fürth, 2012-12-19
Test report No. FUHL1236932
Testing of a material sample according to the RoHS directive 2011/65/EC
Sample description: Cu99.9MSn wire; part no. 450229862; batch 1389386
Arrival in lab: 2012-012-04; Period of XRF analysis incl. sample preparation and photo documentation: 2012-12-07 – 2012-12-10
Head of Inorganic Lab: Claudia List
Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item.
This report consists of 6 page(s).
The test methods signed with * are not listed in the attachment of the accreditation certificate.
Conclusion based on tested item
Status
Test order
testing according to the RoHS directive 2011/65/EC
°
conform°
Please see overview of test results
- Test results see next pages -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
USt-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Durch die DAkkS nach DIN EN ISO/IEC
17025 akkreditiertes Prüflaboratorium
Die Akkreditierung gilt für die in der
Urkunde aufgeführten Prüfverfahren.
Page 2 of 6 page(s) of our test report No. FUHL1236932 dated 2012-12-19
Sample description: Cu99.9MSn wire; part no. 450229862; batch 1389386
nM = non Metal
M = Metal
cM = composite Material
List of component parts:
Sample No. Part No.
236932
1
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Material Description
M
Cu99.9MSn wire; part no. 450229862; batch 1389386
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 3 of 6 page(s) of our test report No. FUHL1236932 dated 2012-12-19
Sample description: Cu99.9MSn wire; part no. 450229862; batch 1389386
Comment
LOD = Limit of Detection
BL
OL
X
σ
=
=
=
=
Below Limit
Over Limit
Inconclusive, further test necessary
Standard deviation
CS
= Composite sample
Remark:
Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb),
AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration
exceeds the below warning value according to IEC 62321.
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
non - metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (300-3σ) < X
BL ≤ (700-3σ) < X
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
composite material
LOD < X < (150+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (250-3σ) < X
BL ≤ (500-3σ) < X
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
-BL ≤ (700-3σ) < X
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 4 of 6 page(s) of our test report No. FUHL1236932 dated 2012-12-19
Sample description: Cu99.9MSn wire; part no. 450229862; batch 1389386
1. XRF screening
Method:
Sample No.
236932
XRF according to IEC 62321:2008*
Part No.
1
Pb
Hg
Cd
Crtotal
Br
Status
BL
BL
BL
BL
--
conform
Comment:
Elements
Lead (Pb)
Mercury (Hg)
Cadmium (Cd)
Chromium VI (Cr VI)
Polybrominated Biphenyle (PBBs)
Polybrominated Diphenyl ether (PBDEs)
RoHS-limit value
1000 mg/kg
1000 mg/kg
100 mg/kg
1000 mg/kg
1000 mg/kg
1000 mg/kg
- Flow charts see next page(s) -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Test procedure
Page 5 of 6 page(s)
YES
non-destructive
sample
preparation
sample
uniform ?
screening
procedure
by XRF
YES
NO
samples
mechanical
sample
preparation
screening
by XRF ?
metallic
materials,
pass
meets
limits ?
YES
NO
YES
fail
further
testing ?
NO
NO
mechanical
sample
preparation
polymer
materials,
entity based
conforming
sample
chemical test
procedure (verification)
various methods
(please see verification test
procedure below)
entity based
non conforming
sample
pass
YES
electronics
(PCB / component)
entity based
conforming
sample
meets
limits ?
fail
NO
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
entity based
non conforming
sample
Verification test procedure
Page 6 of 6 page(s)
Sample Preparation
Sample Measurement
Acid digestion with
microwave / hotplate
Sample solvent
extraction
Filtration
Concentration/
Dilution of extraction
solution
Solution
Cr6+
PBBs/PBDEs
Pb/Cd/Hg
Residue
Filtration
Total digestion
GC/MS
DATA
Non-metallic
material
Alkaline extraction
Adding extraction
solution
Metallic
material
Positive
Negative
Boiling water
extraction
Alkaline extraction
Heating to 90~95°C
for extraction
Adding 1,5diphenylcarbazide
for color development
Filtration and pH
adjustment
ICP-OES/AAS
A red color indicates
the presence of Cr6+
If necessary, confirm
with UV-VIS or
IC-UV/VIS
Adding 1,5diphenylcarbazide
for color development
DATA
DATA
UV-VIS or
IC-UV/VIS
DATA
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Spot test
Geschäftsführer
Kay Grönhardt
Rainer Mast
Test Report
Applicant:
Number : TWNC00285760
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 19, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Yarn
Part Number
: 648106-001
Date Sample Received
: Nov 12, 2012
Date Test Started
: Nov 13, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 8
Number : TWNC00285760
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
White Yarn
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 8
Number : TWNC00285760
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
White Yarn
Test Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 12, 2012
: Nov 13, 2012 To Nov 15, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 8
Number : TWNC00285760
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 8
Number : TWNC00285760
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
PBBs/PBDEs
Weigh sample and
add organic solvent
By Soxhlet
extraction or
Solvent extraction
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Cr
6+
Substrate
Cd/Pb/Hg
Weigh sample
and add
alkaline
solution
For different
material, digest
the sample with
*1
appropriate acid
Plating
Cr
6+
By spot test
Definite temp.
extraction
Cool and filter
the extract
Confirm the tested
samples are
totally dissolved
Negative
*2
Get 50cm2 sample
Make up with
deionized water
By boiling water
extraction
Analyzed by ICP-OES
Make up with deionized
water and add
diphenyl-carbazide
solution
Analyzed by UV-VIS
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 8
Number : TWNC00285760
Test Conducted
(Ⅳ) Measurement Flowchart:
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 8
Number : TWNC00285760
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 8
Number : TWNC00285760
Test Conducted
Photo
*THJ0285760*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 8 of 8
!!eat
ApplicanE
c:rnlo
RoDort
t
naa^,i
TWNC00240907
Litstselfuse Philippines
Inc.
LIMA Technology Center, Lipa City,
Malvar,
Batangas
^Fi
:
Parts Nuniber
Date Sample Received
Date Tests Started
Test. Conducled :
As requesled
by the
Authorized By:
On Behalf Of Inler.tek
Taiwan T,imited
Y.
llang
Drrector
20L2
^-.
One (1) group of submitted
K.
Jatf, 19,
I
.
samples
Solder
to
be
:
Jarl 76, 201,2
Jan 1,6, 2072
applicanL,
Testing
said
for
details
please
refer
tso attached
pages
Services
This report shall noL be repr.oduced
except in fu11, withouts the writsten
approval of tshe laboratory.
Intenek T63tingSedice Talu,anLtd.
gF.,No.423.Ruisuans
Rd.,NeihuDisrrict,
Taipei114,Taiwan.R.o c.
+EAEiiN&6€FAFI
114elLfiteflE*)E$423S8l
. 279ru885 Fax (+886-2)
Tsl (+83d2)6602-2888
6602-2,|006602-2401
Nunlcer : TWNCO0240907
Test Conducted
(I)
Test. Result
Test
E.avtr
ILem
Result
(ppm)
Silvery
Metal
U€ta1
Cadmium (Cd) cont.ent
Lead (Pb) content
Mercury (Hq) conlent.
chiorium vr
ND
908571
(cr6') concent Img,Fs r,'r'tt- 5bE;rl
ND
Negrative {< 0.02)
Reinarks. ppm = Parts per million
based on weighL of resred sampte = ms/kg
ND = Nots detectsed
= Less than
<
mg/kg witsh socm'] = milligram
per kilogram with 50 square centimetre
Negatsive = A negative test resu1ts indicaLed posirive
observat.ion
was not found ats tshe tift\e of Test.
Responsibility
of Chemist
Date Sample Received
Test Period
{[)
: Irene
Chiou / Kevin Liu
: Jar\ 76, 20L2
| ,Jan 76, 201-2 Ia
Jan L9, 2012
](oHs RequatemenE:
RestricEed Substances
Cadndum (Cd) contents
read (Pb) Contents
Mercury (Hq) Contsent
Chromium VI (Cro') Content.
Limits
0 . 0 1 * (1 0 0 p p m )
0 1t (100oppm)
0 18 ( 100oppm)
0 1t ( 100oppm)
The above fimits
were quoced fr.om 2OO2/95/EC and amendments2AA5/6IA/EC for
homogeneous material.
Pase 2 of
Inlertek Testingservic$ Taiw.n Ltd.
Taiwan,
R.O.C
Ruiguang
Rd.,NeihuDistrict.
Taip€i114,
8F.,No.423,
€EAEI&I&6€EAE
114*lbfi^*n**9423s81
. 6@2-2401
Tel:(+8A6,2)
6602-288a
2797,88I5Fd: (+8l6-2)e6o2-2440
5
Numlcer : fiINCo 0240907
Test ConducEed
(m)
Tests MeEhod:
Test rtem
Cadmium (cd)
Lead
(Pb)
l4ercuiy
contenc
iHs)
:hromium VI
(Cr6')
(mg/kg witsh 5ocm')
Remark:
ReporLing
Test Method
l{itsh reference t.o IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digest.ion until
the lested
samples ar.e totally
dissolved and
deLermined by ICP-OES.
With reference to IEC 62321 edlLion
1.0:2008 in clause 8/9/10, by
microwave digestion unril
the tesred
samples are totally
dissolved and
detennined by ICP OES.
with reference to rEc 62321 edition
1.0:2008 in clause 7, by nicrowave
digestion until
tshe tested samples are
totally
dissolved and determined by
lCP-OES.
With reference ro rEC 62321 editsion
1.012008 in annex B, by boiling water
exEractsion and detsermined by lry-Vis
Spectsrophotometser .
linit
= Quant.itsatsion limit.
of analyte
Reporting
Limits
2 ppm
2 ppm
2 ppm
a. 0 2
mg/kg with 5ocm'?
in sample
Page 3 of
lfttertek T*tlng servlces laiwan Ltd.
Tsiwan,R.O.C
8F.,No.423,Ruiguang
Rd.,NeihuDisvict.Taipei114,
TEAE&N&6E.FAE
114ajhrfi^fl E*)tg423s8l
Tel:(+88e2)6602-2884
2797'8845Fd:{[email protected],()1
5
Nurobei : TUNCo0240907
Test
Conductsed
iM
Measurenlent Ffowchart:
Test For Cd/PblHqlchromium (VI)
Reference Standald: IEC 62321 edition
sanplang/grindins
app!op!iate
1,0r2008
or
culting
acid'r
halyzedbylc"oEs
solution
carbazade
by r'V vls
AElyzed
*1:
Lisl
Of Appropriate
acid
Added
For
pigestion
:tNol.ltcl , HF , Ilror , It3Bor
r l l o r . H C 1 ,H F
HNOI HC1 , ll2o,.llBF4
*2:
If
tbe
result
of
spo!
test
is
positiwe,
Chronium
VI
dould
be detemined
as
End of
detecEed'
ReporL
Page 4 ot 5
Inle.lek Testing SeTvlcs. Ttiwan Lld.
Taiwan,R O C
Taip€i114,
Rd.,NeihuDislrlct,
8F.,No,.r23,Ruiguang
AEAE&N&6€EAA
114Altfifi#F*)E*423li8t
. 2797€885 Far:(+88&2)6602-2'|006602-2401
Tsl (+s8d2)6602-2888
Nunicer : TWNC00240907
Test Conducled
Photo
Page 5 of
IntertekTe6iing S€rvic€ Taiwan Ltd.
8F..No 423,RuquangRd . NerhuD6lnct TaiperI14 TaNan R o c
EEAE*&&6EFAA
1 1 4 e l b f id f l E * ) E * 4 2 3 t i I I
6602_2401
T€l:(+s842)6602-28582?9?4885 Fd: (+88G2)6602_2'100
5