ARL 3460 Metals Analyzer
Transcription
ARL 3460 Metals Analyzer
e l e m e n t a l a n a l y s i s ARL 3460 Metals Analyzer The worldwide reference in the industry Analyze • Detect • Measure • Control™ ARL 3460 Metals Analyzer ARL 3460 Long experience has forged Thermo’s reputation For 70 years, one company has set the standard for instrumental analysis of metals – Thermo Electron Corporation. A continuous stream of innovative products using optical emission and X-ray spectroscopy has been the cornerstone around which that long and successful tradition of leadership has been built: • Regular «firsts» in spectrometry, software and automation • Tens of thousands of systems supplied • Continuous improvements in order to provide improved analytical performance and shorter analysis times • Active operating installed base > 10,000 units around the world • Ease-of-use • Easy integration to increase productivity • Unrivaled reputation for quality, stability, reliability and long lifetime • Easy to upgrade • Worldwide customer support network. The first model of the ARL 3460 Metals Analyzer was launched in 1982 and it is since then, the most widely used optical emission spectrometer in the world. Over the years the instrument has undergone continuous improvements regarding optics, electronics and software in order to provide improved analytical performance and shorter analysis times. These improvements have been achieved without decreasing its legendary stability and ease-of-use, allowing easy integration in the customer environment with the target to increase productivity. For instance, the optical emission technique has been extended into analytical tasks previously handled by combustion analyzers. The ARL 3460 has been right at the forefront of these developments, with over 1,000 systems already installed for the analysis of nitrogen in steels. Even more recently, work has been conducted to analyze oxygen in iron and copper bases and the ARL 3460 has proved equal to this challenge too. As a multi-channel optical emission spectrometer, the ARL 3460 is designed for fast, accurate metals analysis in primary plants, foundries, forges, mini-mills and casting operations. It is also eminently suited to incoming material control and as the workhorse in metals QC and R&D laboratories. The ARL 3460 is custom designed exclusively for meeting the customer specific requirements, whether it is working in a small cast iron foundry or in a large aluminum smelter. Thermo has a wealth of experience in analyzing almost every type of metal. This means that Thermo has the necessary personnel, tools and expertise to provide an exceptional product that meets or exceeds every customer’s requirements. This experience extends to the less common alloys of magnesium, titanium, nickel and cobalt. When it comes to the analyses of toxic materials, such as zinc, and lead, the ARL 3460 with a special exhaust system ensures worker safety, as well as providing unparalleled performance. Turn-key operation For the most common applications, the ARL 3460 is supplied as a turn-key system ready to use. It is configured and calibrated in the factory before delivery. Thermo is fully aware that accuracy, which depends on the calibration of the instrument, is the most important figure of merit required from a spectrometer. Our factory calibrations with CARL (a very sophisticated multi-variable regression software tool that corrects for matrix effects as well as spectral interferences), ensures the customer the highest possible accuracy. CARL provides an immediate «turn-key» instrument ready to analyze customer samples on the installation day. Designed for Today’s Metals Production The design of the ARL 3460 combines high performance with rugged construction and operational convenience with reliable operation. The productivity needed by a modern metals production is optimized by the system providing fast, accurate results, day-by-day, month-by-month and year-byyear. In addition to the technical excellence used in the manufacturing and development, the certification of the OE manufacturing facility in Ecublens, Switzerland, under ISO 9001 : 2000 gives the confidence margin necessary in the customer’s daily operation. A well proven, one meter, stabilized cast iron spectrometer is at the heart of the system, providing unrivaled precision and stability over both the short and long term. This brings the advantage that less time is spent on «re-tuning» calibration parameters and more time can be spent on the productive analysis of metals from the manufacturing process. The cabinet is also ergonomically designed to allow the sample and its identification to be rapidly input by a standing operator, thus avoiding wasted seconds and further optimizing result turnaround times. WinOE software: Simplicity itself The WinOE analytical software has been used for now more than a decade. The software has evolved through regular updates, into the most powerful, reliable and easy-to-use software available today for metals analysis by optical emission spectroscopy. For instance, WinOE is first to integrate latest HTML/Internet technologies to simplify work with the spectrometer and to significantly reduce the learning curve. With large user-friendly icons, all functions are easily accessible. Shortcuts make it possible to start analysis with just one click or keystroke. Many other features contribute to help operators performing routine analysis and all other tasks quickly and easily. ‘Push-button’ automation functions and «black box» intelligent modules run in the background minimizing user intervention to assist operators in the daily instrument operation. This kind of intelligence built into the WinOE software is key to not only easing the operator’s work, but also to reducing errors, thereby maximizing the productivity of the customer operation. Reliability, stability, potential for evolution The ARL 3460 has an enviable reputation for its proven reliability and stability. The technical excellence used in the manufacturing and development gives the confidence margin necessary in the customer’s daily operation. Working 24 hours a day, 7 days a week and 365 days a year, the ARL 3460 provides dependable performance at the lowest analysis costs over what can be a very long lifetime. Even more, continuous upgrade possibilities allow customers optimizing performance and productivity. Specifications Spectrometer Spectrometer: Focal length: Primary slit width: Secondary slit width: Type of detector: Grating type: Resolution: Sample stand: Electronics Spectrometer control: Paschen-Runge vacuum polychromator made of special cast iron and temperature controlled to ± 0.1° at 38° C. Maximum 60 channels. 1m 20 µm 20, 25, 37.5, 50, 75, 100, 150 µm Photomultiplier tube 28 mm, 10-stage side window tubes, fused quartz, glass or MgF2 envelope 1080, 1667 or 2160 gr/mm, selected by analytical task Dependent on grating, secondary slit and spectral order Argon flushed, water-cooled table with self-contained, closed loop coolant system Programmable attenuators: Dynamic range: Software: Enclosure: ARL MMB 386 Microprocessor utilizing CMOS technology with Status Measuring Card. A/D converters and attenuators included for each channel. Up to 24, available as an option 106:1 WinOE software running on Windows® XP Professional Built-in dust protection with high capacity cooling fans Requirements Ambient temperature: 16-30°C (62-86°F); maximum rate of change 5° C/hour Relative humidity: Voltage: Current: Frequency: Grounding: Argon: Consumption Electrical power: Argon: Compliance to norms: Dimensions and weight Overall dimensions: Weight: Accessories and options: 20-80% 230 V (+10%/-15%), single-phase with protective ground (5kVA regulator required if fluctuations exceed ±10%) 12 A, including PC, screen and printer 50 or 60 Hz <1Ω > 99.996% maximum 5 ppm oxygen (maximum 2 ppm oxygen for samples with high Si content). Optional argon purifier available and recommended for ultra low carbon analysis. For VUV lines (nitrogen, oxygen, chlorine), argon purifier included Max 3.5 kVA 3.5 l/min during analysis, 0.35 l/min stand-by 98/37/EEC Machinery 73/23/EEC Low voltage material 89/336/EEC Electromagnetic compatibility In addition to these offices, Thermo Electron Corporation maintains a network of representative organizations throughout the world. Australia +61 2 9898 1244 • [email protected] Austria +43 1 333 50340 • [email protected] Belgium +32 2 482 30 30 • [email protected] Canada +1 800 532 4752 • [email protected] China +86 10 5850 3588 • [email protected] France +33 1 60 92 48 00 • [email protected] Germany +49 6103 4080 • [email protected] Italy +39 02 950 591 • [email protected] Japan +81 45 453 9100 • [email protected] Netherlands +31 76 587 98 88 • [email protected] Nordic +46 8 556 468 00 • [email protected] South Africa +27 11 570 1840 • [email protected] Spain +34 91 657 4930 • [email protected] Switzerland +41 21 694 71 11 • [email protected] UK +44 1442 233555 • [email protected] USA +1 800 532 4752 • [email protected] www.thermo.com 166.5 x 91 x 119 cm or 65 x 47 x 36 inches, including excitation stand 450 kg. or 992 lb approximately Small samples analysis kit Argon purification systems Voltage stabilization systems Uninterruptible Power Supply (UPS) Suction device accessory to exhaust toxic fumes Stand upgrade for semi-automatic operation Data communication software options Analytical results processing software options Thermo Electron SA, Ecublens, Switzerland is ISO certified. ©2004 Thermo Electron Corporation. All rights reserved. Windows® is a registered trademark of Microsoft corp. All other trademarks are the property of Thermo Electron Corporation and its subsidiaries. Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details. BR41121_E 06/04C