Practical Pharmaceutical Analytical Chemistry and Instrumental
Transcription
Practical Pharmaceutical Analytical Chemistry and Instrumental
Practical Pharmaceutical Analytical Chemistry and Instrumental Analysis 501266 Second Semester, 20012-2013 General Information: Instructor: Dr. Ala Y Sirhan E-mail: [email protected] Office Hours To be announced Location: Room 334 Course Objectives: The students will be oriented to the safety guidelines to be followed when practicing in the lab. The students will be instructed to follow strictly the uniform policy, attitude guidelines and the general rules for practical laboratory sessions. A course designed to provide the student with a basic understanding the theory and design of the instrumental instruments in addition o understand how the instrument actually makes the measurement. The students will be introduced to the most used techniques in pharmaceutical analysis. The students will be made familiar with Classical methods such as gravimetric analysis and titration as well as instrumental analytical methods such as spectroscopic and chromatographic methods. Required Texts: Skoog, West, Holler, and Crouch, “Fundamentals of analytical chemistry”, 8th Ed., 2004, Thomson ISBN: 0-534-41797-3. Skoog, Holler, and Crouch, “Principles of Instrumental Analysis”, 6th Ed., 2007, Thomson ISBN: 0-495-01201-7. Attendance: Attendance in all labs REQUIRED. You should inform the instructor before, or as soon as possible afterward, if you must miss a class, quiz, or exam. University policy states that students are allowed a maximum of 2 excused or unexcused absences from a 1-credit hour course. Any absence beyond this maximum will result in a student's immediate withdrawal from the course. Course Evaluation: Reports ................................................................................................................. 15 % In-Lab Quizzes ..................................................................................................... 10 % Evaluation (5% each) ............................................................................................ 10 % Midterm Exam ...................................................................................................... 25 % Final Exam ............................................................................................................. 40% Week 1 Week 2 Check In, Introduction, Safety Laboratory Rules Preparation of Standard Solutions Experiment 1: Sampling and Statistical Handling of Data Week 3 Experiment 2: Analysis of Commercial Antacid Tablets Week 4 Experiment 3: Phosphoric Acid Analysis Week 5 Experiment 4: Gravimetric Determination of Chloride Week 6 Experiment 6: UV- Visible Molecular Absorption Spectroscopy Assay of Paracetamol Experiment 7: UV- Visible Molecular Absorption Spectroscopy Determination of Chromium Concentration Experiment 9: Atomic Emission Spectroscopy Determination of Sodium using Flame Photometry Experiment 8: Atomic Absorption Spectroscopy Determination of Lead Concentration Experiment 10: Thin Layer Chromotography (TLC) Separation of Paracetamol and Metabolites by TLC Experiment 11: High Performance Liquid Chromatography (HPLC) Assay of Mefenamic Acid Experiment 11: High Performance Liquid Chromatography (HPLC) Week 7 Week 8 Week 9 Week 10 Week 11 Week 12
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