INSTITUTE OF ELECTRON TECHNOLOGY
Transcription
INSTITUTE OF ELECTRON TECHNOLOGY
1 Ministry of Foreign Affairs Republic of Poland Catalogue of technologies developed by Polish Research Institutes Warsaw, 2012 2 This page is left intentionally blank 3 LIST OF INSTITUTES BY SECTOR BUILDING AND ARCHITECTURE Institute of Spatial Management and Housing ............................................................................... 8 Institute of Urban Development ................................................................................................... 13 Road and Bridge Research Institute.............................................................................................. 18 ELECTROTECHNICS, ELECTRONICS, AUTOMATION AND INFORMATION TECHNOLOGIES Electrotechnical Institute .............................................................................................................. 30 Industrial Research Institute for Automation and Measurements .............................................. 46 Institute of Electron Technology ................................................................................................... 62 Military Communication Institute ................................................................................................. 69 National Institute of Telecommunications (NIT) .......................................................................... 72 Tele& Radio Research Institute................................................................................................... 103 ENVIRONMENTAL PROTECTION AND ENGINEERING; ENVIRONMENTAL, AGRICULTURAL AND FOREST TECHNOLOGIES Forest Research Institute ............................................................................................................ 122 Institute of Agricultural and Food Biotechnology ....................................................................... 128 Institute for Ecology of Industrial Areas ..................................................................................... 134 Institute of Environmental Protection ........................................................................................ 140 Institute of Meteorology and Water Management .................................................................... 144 Institute of Organization and Management in Industry ORGMASZ ........................................... 148 Institute of Plant Protection ....................................................................................................... 153 Institute of Technology and Life Sciences ................................................................................... 157 Maritime Institute in Gdańsk ...................................................................................................... 159 National Marine Fisheries Research Institute ............................................................................. 166 National Research Institute of Animal Production ..................................................................... 169 National Veterinary Research Institute ...................................................................................... 173 Research Institute of Horticulture .............................................................................................. 174 The Stanisław Sakowicz Inland Fisheries Institute ...................................................................... 176 HEALTH PROTECTION AND PHYSICAL CULTURE Institute of Sport ......................................................................................................................... 180 Military Institute of Hygiene & Epidemiology............................................................................. 182 4 MATERIAL AND CHEMICAL TECHNOLOGIES, MATERIAL SCIENCE, CHEMICAL AND PROCESS ENGINEERING Fertilizer Research Institute ........................................................................................................ 204 Foundry Research Institute ......................................................................................................... 213 Industrial Chemistry Research Institute...................................................................................... 235 Institute for Chemical Processing of Coal ................................................................................... 357 Institute for Engineering of Polymer Materials and Dyes........................................................... 363 Institute for Ferrous Metallurgy ................................................................................................. 386 Institute of Biopolymers and Chemical Fibres ............................................................................ 392 Institute of Ceramics and Building Materials .............................................................................. 393 Institute of Electronic Materials Technology .............................................................................. 412 Institute of Heavy Organic Synthesis „Blachownia” ................................................................... 413 Institute of Natural Fibres and Medicinal Plants ........................................................................ 432 Institute of Non – Ferrous Metals ............................................................................................... 437 in Gliwice ..................................................................................................................................... 437 Institute of Nuclear Chemistry and Technology ......................................................................... 438 Institute of Precision Mechanics ................................................................................................. 439 Institute of Security Technologies MORATEX ............................................................................. 457 Metal Forming Institute .............................................................................................................. 462 Polish Welding Centre of Excellence........................................................................................... 480 The Research and Development Centre for Building Insulation Industry .................................. 488 Wood Technology Institute......................................................................................................... 489 MECHANICS, BUILDING AND OPERATION OF MACHINES, PRODUCTION ENGINEERING Institute for Sustainable Technologies – National Research Institute........................................ 493 Institute of Mining Technology ................................................................................................... 505 The Institute of Advanced Manufacturing Technology .............................................................. 509 MEDICAL SCIENCE Institute of Physiology and Pathology of Hearing ...................................................................... 511 Institute of Rheumatology .......................................................................................................... 519 Institute of Rural Health .............................................................................................................. 521 Institute of Sensory Organs......................................................................................................... 527 Maria Skłodowska-Curie Memorial Cancer Center and Institute of Oncology (MSCMCCIO) .... 532 National Institute of Tuberculosis and Lung Diseases ............................................................... 534 Polish Mother's Memorial Hospital - Research Institute ............................................................ 538 The Cardinal Stefan Wyszyński Institute of Cardiology .............................................................. 541 5 MINING, TECHNICAL GEOLOGY, GEODESY, POWER ENGINEERING AND TRANSPORT Automotive Industry Institute .................................................................................................... 545 Central Mining............................................................................................................................. 549 Institute of Geodesy and Cartography (IGiK) .............................................................................. 562 Institute of Innovative Technologies .......................................................................................... 564 Motor Transport Institute ........................................................................................................... 576 Oil and Gas Institute.................................................................................................................... 580 Polish Geological Institute – National Research Institute........................................................... 588 The Institute of Aviation ............................................................................................................. 591 NON-CLINICAL RESEARCH UNITS Institute of Biotechnology and Antibiotics ................................................................................. 604 PHYSICS AND ASTRONOMY Institute of Plasma Physics and Laser Microfusion, EURATOM – Association ........................... 618 National Centre for Nuclear Research ........................................................................................ 620 SAFETY AND OTHER GENERAL TECHNICAL ASPECTS Air Force Institute of Technology ................................................................................................ 628 Central Institute for Labour Protection - National Research Institute (CIOP-PIB)...................... 654 Institute of Industrial Organic Chemistry .................................................................................... 658 Military Institute of Armour and Automotive Technology ......................................................... 660 Military Institute of Engineer Technology .................................................................................. 662 Scientific and Research Centre for Fire Protection im. Józefa Tuliszkowskiego - National Research Institute ....................................................................................................................... 672 The Military Institute of Chemistry and Radiometry .................................................................. 685 SMALL RESEARCH UNITS IN TECHNICAL FIELDS Institute of Applied Optics .......................................................................................................... 687 Institute of Logistics and Warehousing....................................................................................... 691 “COBRO” Polish Packaging Institute ........................................................................................... 695 Research and Academic Computer Network (NASK) .................................................................. 696 Research and Development Centre of Electric Machines “Komel” ........................................... 701 Reaserch and Development Centre of Hosting Machinery and Mechanical Conveyiny Equipment “Detrans”..................................................................................................................................... 702 6 Catalogue of technologies developed by Polish Research Institutes BUILDING AND ARCHITECTURE © ArchMen - Fotolia.com 7 INSTITUTE OF SPATIAL MANAGEMENT AND HOUSING (Instytut Gospodarki przestrzennej i Mieszkalnictwa IGPiM) Organisation Contact Data 45, Targowa st., 03-728 Warsaw, Poland phone: + 48 22 619 13 50 fax + 48 22 619 24 84 e-mail: [email protected] http://www.igpim.pl/main-e.html Institute of Spatial Management and Housing is a research institution that carries on the tradition of the 1949-founded Research Institute of Town Planning and Architecture. The Institute deals with the issues of planning and spatial development, as well as municipal economy on all levels of administrative and functional division. With regards to the above, it offers: research work, ongoing process monitoring, changes forecasting, urban planning and design study methodology, system and detailed solution concept, legal solution proposal creation, standardization and normalization of spatial management and housing issues and current government administration consulting. It also has experience with environment protection. The Institute's staff consists mainly of architects, town-planners, geographers, biologists, economists, sociologists and lawyers. With the aid of an experienced and inter-disciplinary team, the Institute also conducts training in the field of spatial planning, real estate and municipal services management, as well as organizes international conferences, seminars and workshops. The Institute's structure consists of three departments: Spatial Planning Department The Department is specialized in preparation of studies and documents according to spatial management with the use of modern GIS technology (Geographical Information System). The Department's scope of work is handled by five teams: Technical Infrastructure; Applied Geoecology; Landscape Architecture; Architecture & Town Planning; Revitalization. 8 The Department's mission is to create modern GIS solutions for commune selfgovernments based on complete spatial information. Such information might come from: the study of land development conditions and directions, a local plan of spatial development, current aerial and satellite views, land and property register and other data. The available source of data coupled into one information system makes the information comprehensive and clear by giving it the form of maps, charts and types of action. The powers that be can make effective decisions thanks to user-friendly GIS applications. As part of creating a portfolio of complex solutions (in the form of an information system), the Department offers a broad range of works: preparation of GIS data and modification, vectorization, creating Digital Terrain Models (DTM) based on the cartographic method, 3D visualizations, creating photo maps, transforming data in various coordinate systems, spatial analyses, and preparing documents, such as: the study on the conditions and directions of the district development, local plans of district spatial development, ecophysiographic studies, the forecast of impact of a local plan of spatial development on the natural environment, local development plans, strategies of development, analyses for locations of shopping centers according to market employment, communication opportunities and influence on local shopping markets, revaluation of historical assumptions of park and palace complexes. 9 Municipal Transport Department The Municipal Transport Department was founded in 1954. Since the beginning, its domain of action has been the broad issue of municipal transport, its development and initiation of modern constructional design. The Unit is currently busy with research and consulting, as well as preparing expertizes for manufacturers and users of tramways, trolleybuses and appliances used in them. By right of the Decree of the Ministry of Infrastructure, it is authorized to conduct homologation analyses of tramways and trolleybuses with regards to their electrical parts, as well as control the conformity between the manufacturing/installation and homologation conditions. Since 2004, the Municipal Transport Department has been awarded with a PN-EN ISO 9001: 2001 (PN-EN ISO 9001:2009 since February 2010) Quality Control System Certificate with regards to: technical checkups of tramways and trolleybuses, homologation checkups of types of tramways and trolleybuses' electrical parts, checkups of tramway and trolleybuses' assemblies and appliances. Activities conducted at the Municipal Transport Department can be divided into the following groups: 1. Homologation checkups of new tramways and trolleybuses and exploitation analyses and appraisal of new technical solutions, which are to be incorporated in the currently used fleet. The checkups consist of checking the conformity between the products and requirements found in the current legal regulations and technical standards. The results of exploitation analyses are published in the form of a report or opinion. A positive result constitutes the basis for receiving a homologation certificate by the manufacturer or future user, issued by the Minister of Transport, Construction and Maritime Economy, or a permission to operate the given type of product. 2. Extended technical and start-up checkups of tramway and trolleybus carts, granting permission to operate used and modernized vehicles (applies mainly to imported fleet). The checkups are conducted according to the decrees on the scope and type of conducting technical checkups, as well as technical conditions of tramways and trolleybuses and the scope of required appliances. 3. Periodical technical checkups of tramways and periodical technical checkups of trolleybuses operated by municipal transport companies. A positive checkup result constitutes the basis for issuing a permission to operate the given vehicle. 10 4. Checkups and assessment of tramway appliances, such as: door mechanisms, couplings, current collectors, traction and voltage converters, heaters, as well as other apparatus and appliances constituting the equipment found in tramway and trolleybus fleets. Moreover, the Municipal Transport Department actively participates in the planning and consulting in the areas of: constructional design of tramway and trolleybus fleets, novelization and preparation of technical norms with regards to municipal transport, electric traction, updating the regulations regarding the municipal electric traction. The Unit is in possession of a mobile lab, equipped with modern, electronic appliances for conducting homologation checkups of vehicles, especially the measurement and registration of the movement parameters of vehicles and for checking the lighting, noise and electrical measurements, including insulation resistance and strength, protective installation measurements, etc. Landscape Architecture, Training and Real Estate Management Department The Department's scope of works circulates around the broad issue of environment, especially the municipal tree covering and greenery within the urban areas. For many years, the Department has been conducting research and implementation activities, as well as trainings on a national level, especially for the local self-governments. Besides dealing with the issues of greenery, the Unit's scope of activities includes conducting a system of trainings on the issue of real estate on an advanced (post-graduate studies) and intermediate level, as well as implementing an educational cycle as part of inservice training. 11 In the area of municipal greenery, the Institute employs a group of distinguished experts, who for years have been conducting nationwide-recognized research on determining the actual value of trees growing within the urban areas. The Department has prepared and published a new "Method of Valuation of Trees within the Urban Areas with Regards to Polish Conditions." The study constitutes the basis for works carried by the Ministry of Environment with regards to the novelization of rates for the removal of trees and bushes and rates for destroying the greenery. Since 2010, the Institute's employees have conducted both practical workshops and trainings on the use of the new method of valuation of trees within the urban areas. The team of the Department's experts collaborates with the General Directorate for Environmental Protection, which is obliged by the Minister of Environment to implement the new, abovementioned method of valuation of trees. The Department performs stock-takings, expertizes and health condition assessments, i.e. the condition and statics of individual trees, as well as tree covering complexes within the urban public areas. Since 2011, it began monitoring the changes in buffer strip and inner housing estate landscape greenery management within a select area in Warsaw. The Department plans to monitor changes in the natural landscape development for years to come. As part of the training system, trainings and conferences regarding real estate management and turnover, spatial planning and building law have been organized for more than 20 years. In collaboration with university colleges, we conduct two higher education majors in real estate management and real estate turnover agency. For the last eight years of conducting higher education studies, together with the Leon Koźmiński Academy, our studies have been graduated by more than 200 students per year (three editions within a year). After completing a six-month long internship, graduates have received their professional licenses. 12 Trainings are conducted by approx. 40 experts with a lot of experience in consulting and training activities. The Department's employees have professional real estate agent/manager licenses. The Department, in cooperation with the lecturers from the Warsaw School of Economics, prepares for launching a series of trainings for the self-government administration with regards to introducing new legal regulations on district municipal waste management. Waste dump development and waste utilization is directly connected with proper spatial planning, environment pollution and landscape architecture by creating spatial order and aesthetics in communes. 13 INSTITUTE OF URBAN DEVELOPMENT (Instytut Rozwoju Miast) IRM Organisation Contact Data 2, Cieszyńska st, 30-015 Cracow, Poland Phone: +48 12 634 29 53 (director) Phone: +48 12 634 29 53 (chief accountant) Fax: +4812 633 94 05 e-mail: [email protected] http://irm.krakow.pl/en/ Institute of Urban Development (IRM) is a scientific and research institute. The Institute's personnel is composed of 64 persons constituting an interdisciplinary team of research and technical staff representing the following areas: urban planning, spatial planning, architecture, geography, law, economy, political science, biology, civil engineering, hydroengineering, sanitary engineering, land reclamation, chemistry, transportation, computer science, organisation and management, geology and forestry. The Institute employs five Professors, twelve holders of Ph.D. The IRM team also includes experts and specialists holding authorisations of professional institutions and organisations. The Institute is member of international consortia participating in research projects of the European Union, and its intention is to increase its involvement in research projects supported by the EU, the UN and other organizations. The Institute has worked out self-developed and tested methods and techniques for resolution of specific problems. As a research and development unit carries out both: constant research and pilot projects and works on continuous quality improvement. The Institute experience comprise works on: spatial planning, municipal economy, environmental assessment, communication, regeneration, rehabilitation, strategy and housing policy at national, regional and local levels, social and economical problems of housing, management of housing resources, building market and real estate market. The main goal of the Institute is to lead researches and to transfer their results into practice, so to: support the central local governments in the realization of the state policy in the field of spatial and housing management elaborate and opinion on standards of spatial management, research on socio-economical and spatial processes of urban development research on conditions and definition of urban and urbanizing space sustainable development principles assess the employed methods, regulation policies, instruments of urban development 14 elaborate methodical, legal, organisational, planning, financial and other, conditions of urban development. The results of research works are used by the Polish Ministry of Transport, Construction and Maritime Economy and other government agencies, Parliament committees and regional and local governments. The results of current operations are published in own publications and regular scientific and professional journals. The Institute achievement include for example the works carried out as part of aid offered to municipalities (Phare Fund, British Know-How Fund, USAID). Other projects were conducted jointly with the Norwegian Institute of Urban and Regional Research (NIBR) and the University of Lille and as part of the European Union programmes. The Institute and the members of the staff are involved in cooperation with several associations and research networks such as IFHP (International Federation for Housing and Planning), ENHR (European Network for Housing Research), ENTP (European New Towns Platform) and METREX (Network of European Metropolitan Regions and Areas). SCOPE OF ACTIVITIES Spatial Economy Spatial Planning Strategies of Municipality or Regional Development Studies of the Conditions and Directions of Municipality Development Local Physical Plans Ecophysiographic Studies Environmental Impact Assessment and Strategic Environmental Assessment Forecast of the Financial Consequences of the Spatial Plans Approval Programs of Local Regeneration Environmental Protection Plans for the Protection of Nature Areas (National Parks and Landscape Parks) Environmental Protection Programmes for Municipalities, Districts and Provinces and Waste Disposal Plans Municipal Management Transportation Management Transportation Studies for Spatial Planning Purposes in Towns 15 Traffic Research and Analyses and Network Simulation Studies for Transport Management Purposes Housing Housing Management Housing Strategies and Policies at National, Regional and Local Levels Housing Stock Economy and Management Housing Monitoring Social Problems Associated with Housing Residential House Building Organisation and Financing of Residential House Building Building Law and Public Procurement System Operation Cost Calculation in Residential House Building Real Estate Market Market Size and Real Estate Agencies Real Estate Transaction Size and Types Land Management in Municipalities Land Management Laboratory Tests Laboratory Testing of Water Quality Evaluation of Soil Pollution Evaluation of Waste Harmfulness for the Environment Noise Level Testing Dissemination of Experiences Training – short courses (Tools For Improving Urban Development and Regeneration; Local Planning And Urban Design; Planning for Sustainable Regeneration) Conferences Publications Monitoring of Housing, Building and Real Estate Markets 16 OUR OFFERINGS Research on the Urban Space Quality and the Effectiveness of Urban Development Processes Studies of the Spatial Economy Conditions and Local Physical Plans Forecast of the Financial Consequences of the Spatial Plan Approval Environmental Assessment Natural Conditions of Urban and Rural Land Development Transportation Studies for Spatial Planning Purposes Designs and Conceptions of Solutions for Technical Infrastructure Municipal Road Management Organisation Works Long-Term Programmes for Municipal Housing Management Housing, Building and Real Estate Market Monitoring Housing Development and Financing Projections and Strategies Conceptions of Solving Housing Problems of Economically Poor Population Groups Analyses of Economic Effectiveness of Public Capital Projects 17 ROAD AND BRIDGE RESEARCH INSTITUTE (Instytut Badawczy Dróg i Mostów) Organisation Contact Data 1, Instytutowa st., 03-302 Warsaw, Poland phone: +48 22 698 06 06 fax: +48 22 814 50 28 e-mail: [email protected] http://www.ibdim.edu.pl/eng/ The Road and Bridge Research Institute is a scientific institution supervised by the Minister of Transport, Construction and Maritime Economy. It is acting on the basis of the Act of 30 April 2010 on research institutes. The Institute conducts research and development work concerning the construction and maintenance of transportation structures, specifically roads and road bridges, railway bridges and underground structures. The main scope of the Institute activities and implementations is focused on the following subjects: principles of design, execution and maintenance of transportation structures, materials and products for communication engineering, technical state of roads and engineering structures, geotechnics, economic analysis, engineering and traffic safety, road network management systems, transportation issues, database of roads and engineering structures. Besides the research and development activity, the Road and Bridge Research Institute adapts R&D results to the practical needs elaborating guidelines, instructions, expert opinions and procedures. The Institute takes part in the work of numerous international organizations, such as: FEHRL - Forum of European National Highway Research Laboratories, FERSI - Forum of European Road Safety Research Institutes, IABSE - International Association of Bridge Structure Engineering, RILEM - The International Union of Testing and Research Laboratories. The Institute is a participant and coordinator of many international projects, for example: EUREKA, COST, Framework Programme of the European Union. Divisions: Bridge Department Concrete Division 18 Division of Management Systems and Telematics Economic Division Geotechnics and Foundation Division Pavement Diagnostic Division Pavement Technology Division Bridge, Concrete and Aggregate Research Center, Branch "Wrocław" Bridge Research Center, Branch "Kielce" Accredited Laboratories: Concrete Laboratory Pavement Diagnostic Laboratory Geotechnics Laboratory Pile Testing Field Laboratory Bituminous Binders Laboratory Pavement Technology Laboratory Chemistry & Environmental Protection Laboratory Bridge Structures Research Laboratory Bridge Diagnostics and Repairs Unit Bridge and Drainage Division Concrete and Aggregate Division Crash Tests & Road Meteorology Team 1. Pavement diagnostics, repairing technologies and reinforcement of pavement construction Two divisions are involved in research work on evaluation, repairing technologies and reinforcement of pavement construction. The activity of Pavement Diagnostics Division covers analysis of such pavement technical parameters like bearing capacity, longitudinal and transverse evenness, anti-skid properties and pavement condition. They issue expert appraisements and opinions based on the complex investigation of road network and road sections prepared for reconstruction. Pavement Diagnostics Division carries out research works in the following areas of road construction: materials used in pavement construction, structural design methods, road traffic safety. In their work they apply modern research, analysis methods, advanced technologies and devices like: ground penetrating radar GPR, laser deflectometer, dynamic deflectometer HWD, system of automatic evaluation of the surface condition, 3D radar system, CPX system for pavement noise measurement, 19 radar system for bridge measurements, system for research and analysis of bridge structure, profilograph ARGUS (in cooperation with private company), falling weight deflectometer FWD and skid resistance tester SRT3. Modern laboratory, team and big experience allow them to conduct several works connected with evaluation of road infrastructure i.e.: pavement structural design, complex assessment of roads and streets pavement condition, assessment of airport pavement condition, scientific supervision of measurements and data processing, evaluation of anti-skid properties of pavement, assessment of longitudinal and transverse evenness, assessment of pavement bearing capacity, semi-automatic identification of pavement surface damages etc. The Road and Bridge Research Institute lead the way in modern road infrastructure research. "SPID - System for Pavement Infrastructure Diagnosis" is a The Institute’s brand new mobile laboratory equipped with state-of-the-art devices allowing us to use non-destructible methods to examine roads and bridges. Causing no traffic interruptions, the research equipment is capable of evaluating the condition of bridges and roads, and controlling the quality of technologies and materials deployed for the building of transportation routes. This bears particular importance in countries featuring dense traffic and road networks. Contact Person Data Jacek Sudyka e-mail: [email protected] 20 Pavement Technology Division is divided into three departments dealing with bituminous binders, asphalt mixtures, asphalt emulsions, road markings and road signs. The range of the division activity covers:·flexible road and bridge pavements design,·mixtures design, tests of materials (bituminous binders, aggregates, fillers, additives, road paints, thermoplastics, cold plastics, tapes, bitumen emulsions etc.), modification of binders and bituminous mixtures, development and implementation of new technologies (high modulus asphalt concrete, coloured pavements, rubber additive, fibres additive, cold mix pavement), pavement reinforcement (meshes), utilization of waste materials and byproduct. The division is well equipped with the modern test equipment for standard and advanced research testing. EXAMPLES OF RESEARCH ACHIEVEMENTS: TOFIC® fibrous additive to bituminous mixtures TOFIC® additive contains synthetic polymer fibres, polyester fibres, para-aramide fibres and viscose fibres. It is obtained through the process of grinding rubber wastes reinforced with textile cord, mainly automobile tires. The material has very good mechanical properties, such as resistance to water, elasticity and strength. It can be used as a fibrous stabilizing, reinforcing and modifying additive to bituminous mixtures for construction of road pavement. Benefits from using TOFIC® additive: improve pavement bearing capacity, resistance to rutting, resistance to low temperature cracking, extension of road pavement exploitation period. TOFIC® additives have been implemented: - in SMA mixes and gap graded asphalt mixtures - mainly as a stabiliser of road binder and giving necessary reinforcement, - in asphalt concrete mixtures - for modification and reinforcement. The research tests of bituminous mixtures containing 0,6% of TOFIC S prove even two times slower fatigue process than the comparative mixture. Use of waste materials in bituminous mixtures is very important from ecological point of view. Waste tires are usually useless and burned causing emission of toxins. Ecological benefits results also from higher durability and less maintenance needs. TOFIC® additive has been awarded with the "2007 Innovation of the Year" title. 21 The modified bituminous mixture GUFI The modified bituminous mixture GUFI is the exceptional product having of the wide use. It can be used for the surface of roads, bicycle paths and fields and the playgrounds, because addition of granulated rubber reduces the hardness of the surface and the effect of the fall softens. The mix contains granulated rubber next to standard components: aggregates and asphalt. The rubber is coming from the processing the used car tires and polymer fibers which inflict that one gets special proprieties distinguishing this mixture from standard bituminous mixtures. The additions of gum and fibers in the connection with the use polymer modified bitumen assure obtainment of special proprieties of layer of such surface as: - the resistance to cracking and thanks to this the possibility of fulfilling the part of the anticracking layer, - very good adhesiveness to the all materials of the basis, including concrete plate and cable stone, etc., - decrease of the noise of the contact between the tyre with the surface. Effect of realization of surface from such mixture is so double: technical – as the improvement of the durability of the surface and ecological – as decrease the noisiness of the movement of vehicles (low surface) and the use of the industrial waste, that is granular rubber from car tyres. The Road and Bridge Research Institute has been awarded with a Silver Medal for the modified bituminous mixture GUFI on Brussels Eureka 2005 International Fairs of Innovation, Scientific Research and New Techniques. Contact Person Data prof. Dariusz Sybilski e-mail: [email protected] 22 2. Bridge diagnostics The Bridge Department conducts works that lead to assess the technical conditions of bridge structures. The Department also determines the applicable load capacity of exploited bridges’ structures, using the test load method and the RYM-IBDIM computational method. Sometimes the RYM-IBDIM computational method is useful for quick load capacity estimation of structures located along the route. Since 2004 the method was advised for usage on General Directorate of National Roads and Motorways road system in Poland. 3. Repairing technologies and reinforcement of bridges On the basis of a structure technical condition assessment and detailed inspection the Bridge Department prepares recommendations. Those recommendations include the way of the damage reparation (indication of a method and materials) and they can indicate the manner of the structure strengthening. The range of works, recommended methods and materials depend on the individual technical condition of the structure and should be adapted to technical abilities of the contractor. There are professional teams in the Bridge Department that specialise in following issues: repairs of concrete and steel structures, waterproofing and anticorrosion protection. Contact Person Data Tomasz Wierzbicki e-mail: [email protected] Piotr Olaszek e-mail: [email protected] 23 4. Road marking and signs, NATO Code System Pavement Technology Division (chemistry laboratory) performs tests of materials for horizontal and vertical road marking. In this scope they are test: road paints, thermoplastics, cold plastics, tapes, road studs, glass beads and retroreflective foils, road signs (substrate and supports). Properties of ready road markings are done in the scope: retroreflectivity, luminance factor, chromatic coordinates, skid resistance with using hand equipment or mobile (on the car). Road signs on site are controlled in the scope: retroreflectivity, luminance factor and chromatic coordinates. The country operation in crisis conditions needs appropriate transport infrastructure background. It is essential, in order to provide technical efficiency of the land transport net, to indicate quickly possibility of: crossing an obstacle along an existing structure, erection of a permanent bridge structure or a temporary, folding structure. The Polish MILORY method was elaborated in the Bridge Department. It is used to the quick military class MLC bridge structures determination according to the NATO standards and NATO standardisation agreement STANAG 2021. MLC bridge structures determination is a basis for structure coding, with the use of the signs in accordance to the NATO requirements, included in NATO standardisation agreement STANAG 2021. Contact Person Data Janusz Rymsza e-mail: [email protected] 24 IMPORTANT ACHIEVEMENTS OF IBDiM 1) Project „Bridge in 3 months” Modern technologies: - structures, - materials, - assembly. Aims of the project: - increase of structure durability, - costs reduction, - reduction of bridge construction time, - decrease of traffic disturbances, - less hazards to the natural environment, - worker in the safe work environment. Innovative project: 9 patents Contact Person Data Janusz Rymsza e-mail: [email protected] 2) Project and implementation of the new generation of the variable message sign The design of the Variable Message Sign (VMS) has the following advantages: innovative optical system eliminating the phantom effect developed and designed in the Institute of Applied Optics, full color front panel, - message displayed consisting of symbols and/or text, excellent visibility of the sign pattern regardless of weather conditions, easy size configuration thanks to the modular construction, new electronic setup - CZMUDA JSC. Innovative project: 3 patents Contact Person Data Leszek Kornalewski e-mail: [email protected] 25 3) ISKIP - Intelligent Comprehensive Vehicle Identification System The Intelligent Comprehensive Vehicle Identification System (ISKIP, Inteligentny System Kompleksowej Identyfikacji Pojazdów) is a universal, developmentoriented system for automatic identification of vehicles, based on parallel recognition of vehicle features such as category (car, van, truck, bus, etc.), colour, make, type and registration number. The recognition of all the above-mentioned vehicle features is made only on the basis of an analysis of the vehicle's photo, with no need for physical interference with the structure and environment of the road or other point of system operation. The proposed concept is a solution unique in Europe and globally. There is currently no other effectively operating system in place to enable vehicle make, model, type and colour to be recognised. The system is based on a complex algorithm of neural networks, analytical software and a database of about 500,000 vehicle photos. The Intelligent Comprehensive Vehicle Identification System, ISKIP, can be installed both in a fixed version (e.g. at border crossings, major road junctions) and in a mobile version (e.g. on vehicles of the Police, the Border Guard, the Road Transport Inspection Service – ITD, and special services). The system can also be integrated with other components of Intelligent Transport Systems, i.e. with weigh-in-motion systems, average speed control systems, red light violation detection systems, etc. In Poland, the results of the project are currently being implemented at the Internal Security Agency, the Police, the Central Bureau of Investigation and the Board Guard. 26 Project has been awarded: Lider ITS (Intelligent Transportation Systems) 2011 - Prize for the best research work Gold Medal - iENA 2011 - International Trade Fair - Ideas, Inventions, New Products Silver Medal, ARCA - International exhibition of novelties, new ideas, new products and technologies, Croatia 2011 Silver Medal - BRUSSELS INNOVA 2011 - International Fairs of Innovation, Scientific Research and New Techniques Special Prize, Technopol Moscow, Russia Grand Prix of the Minister of Infrastructure - 2011 Lider ITS (Intelligent Transportation Systems) 2012 - Prize for NeuroCar Red Light System Polish Promotional Emblem "Teraz Polska" 2012 Contact Person Data Michał Karkowski e-mail: [email protected] 4) AIBDiM - Active Intelligent Road and Bridge Restrain Systems The aim of the project "Active Intelligent Road and Bridge Restrain Systems" is to develop new in the world - an active, intelligent road barrier. Its use in particularly dangerous places on the roads, bridges and tunnels will highly increase the road safety. Implementation of the invention for the industry production will increase the competitiveness of Polish producers and contribute to the strengthening of cooperation between science and economy. The main research goal of the project is to develop and implement an universal, active, intelligent road barriers, intended to restrain and referral the vehicle on the right track after the collision, while maintaining safety of the vehicle occupants and other road users. This barrier, equipped with electronics and modern design 27 solutions will, in contrast to the currently used passive protection systems, in an intelligent way, actively regulate the level of impact energy absorption of different weight vehicles - car, bus, truck. Contact Person Data Michał Karkowski e-mail: [email protected] 5) Mixtures used for building the bottom and upper layers of road embankments Within the project, there has been formulated the composition of the mixture of waste materials such as phosphogypsums and ashes. The mixture has been improved by the binder and it can be applied in the layers of the improved road subgrade. Neutralization of the acidic phosphogypsum, which has a very high pH, by an alkaline material (ash), was the essence of the invention. The developed product can be used for building roads without any damage to the environment. It is squeezing resistant and frostproof. Its durability and ecological safety have been positively verified in practice. Utilization of the invention will make it possible to use 70 million tons of phosphogypsums (in Poland) which have been obtained through the production of the phosphoric acid and piled on slag heaps, threatening human health and natural environment. Inorganic Chemistry Division of the Fertilizers Research Institute in Gliwice together with the Road and Bridge Research Institute have been awarded with a Gold Medal for the collectively implemented project on the 60th anniversary edition of “BRUSSELS INNOVA 2011” International Fairs of Innovation, Scientific Research and New Techniques. Furthermore, the team of scientists received the SPECIAL PRIZE, Technopol Moscow, Russia. Contact Person Data Jadwiga Wilczek e-mail: [email protected] 28 Catalogue of technologies developed by Polish Research Institutes ELECTROTECHNICS, ELECTRONICS, AUTOMATION AND INFORMATION TECHNOLOGIES © vladgrin - Fotolia.com 29 ELECTROTECHNICAL INSTITUTE (Instytut elektrotechniki) Organisation Contact Data 28, Pożaryskiego st, 04-703, Warsaw, Poland phone: +48 22 812 20 00 fax: +48 22 615 75 35 e-mail: [email protected] http://www.iel.waw.pl/ The Electrotechnical Institute is a modern and innovative unit, which meets the European standards when it comes to the science-research potential, performing research and development works, as well as producing highly processed and technologically advanced products. At present, it is one of the largest technical research institutes in Poland. Carrying out its works, the Electrotechnical Institute operates in compliance with the sciencetechnical policy and innovative policy of the state, actively participating in the economical development of the country. It cooperates with domestic and European bodies through the usage of the European Union's Structural Funds, taking part in countless EU research programs and national projects, especially in the Innovative Economy Operational Program. By cooperating with domestic and international science centers, the Institute provides for entrepreneurs from the electrotechnical and electric power industry a strong science-research background, which is directed towards innovative technologies and obtaining energy from renewable sources. The Institute strives to improve and develop its position as the leading national research center, which operates in the united Europe, in the field of electrotechnics and related domains. It also strives to maintain and strengthen its good image among current and future customers. The Electrotechnical Institute comprises two sections in Gdańsk and Wrocław, seven scienceresearch departments, experimental plant in Międzylesie near Kłodzko and four accredited research laboratories. 30 The range of activities of the Institute includes: electrical machines, electric vehicles, electrical drives, electrical traction, -power converters, lighting technology and optical radiation, measuring-diagnostic systems, high power, power electronics Scientific research work, projects and design work are performed in the above areas and there are produced single, highly processed electrical equipments in the range of testing and certification. The Institute operates in the EU system of conformity assessment and it is a notified unit Nr 1460 for the Low Voltage Directive (LVD) and for electromagnetic compatibility (EMC). The Institute has got the authorization of the Minister of Economy for issuing opinions on quality of high and low voltage apparatus and electrical equipment installed and operated in Polish enterprises producing, transmitting and using electric energy. 31 THE OFFER OF THE ELECTROTECHNICAL INSTITUTE: BRANCHES WROCŁAW Research work on the following topics is being realized currently new technologies, materials and products aimed at energy and material saving in the process of their production and utilization (e.g. composite isolators elastic heating conductors, electroinsulating lacquers); new groups of materials, the so called advanced and smart ones; nanotechnologies and nanocomposites; new composite and ceramical materials for application in power engineering, biotechnology and medicine; inconventional sources and storages of energy: fuel cells, supercapacitos (their production technologies and application); ecological solar power plant (conversion of solar energy into mechanical, of mechanical into electrical energy with simultaneous storage of energy in the form of hydrogen produced by hydrolysis of water); utilization of strong magnetic and electrical fields in technological processes; materials for screens of electromagnetic radiation; electro-active materials. Testing Laboratory Branch in Wrocław – Accreditation nr AB 067 Testing of materials and electrotechnical products such as: isolators and electroinsulating lacquers, cables and conductors and equipment for personal protection for working at high voltage, materials and equipment used in electrotechnis, testing thermal properties of plastics, testing fire hazards and flammability of electrotechnical materials and plastics, testing resistance to corrosion of electrotechnical material lacquers and protective covers, testing soft magnetic materials. GDAŃSK Research and development work is performed in the following domains: power-electronics, automation and control systems, electromagnetic compatibility (EMC) of electrical equipment, miniature low and medium voltage fuses, complex automation of melioration pump stations. 32 The offered services include: Consulting and expertizes concerning electric apparatus automation systems and electric drive, Services of the Testing Laboratory with a certificate of accordance with the PN-EN ISO/IEC standard 17075:2005, accredited by PCA (Polish Accreditation Centre). The Laboratory co-operates with DEKRA/KEMA Quality. Testing Laboratory Branch in Gdańsk – Accreditation nr AB 607 Tests: electrotechnical and electronic, electromagnetic compatibility (EMC), concerning environmental engineering of (environmental and climatic tests), Equipment tested: switchgear and control apparatus, laboratory equipment, automation and apparatus for measurements, common use equipment and similar, welding equipment, power electronic equipment, equipment for information science. Organisation Contact Data Contact Person Data Electrotechnical Institute , Gdansk Branch 1, Narwicka st, 80 – 557, Gdańsk, Poland phone: +48 58 343 12 91 fax: +48 58 343 12 95 e-mail: [email protected] 28, Pożaryskiego st, 04-703, Warsaw, Poland phone: +48 22 812 20 00 fax: +48 22 615 75 35 e-mail: [email protected] http://www.iel.waw.pl/ 33 MIĘDZYLESIE n. KŁODZKO – PILOT PLANT III The offer includes: composite line, screening, and stand-off isolators, reactance and bushing isolators, made of other epoxy resins, tubes and profiles made of epoxy glass, electroinsulating sleeves, tapes made of epoxy glass In 2003, in ZD III was implemented the quality management systems acc. to ISO 9001, certificated by TUV NORD and PCBC. SCIENTIFIC – RESEARCH DEPARTMENTS IN WARSAW offers Department of Electrical Drives drive systems with ac motors, modern control methods, laboratory test of electrical drive systems with ac motors, research and development work concerning energy conversion in contactless power supply systems, research and development work concerning renewable energy and its transmission into the power grid, technological consulting in the domain of design and application of drives in the industry. Department of Electrical Traction design and testing of electric and electronic equipment for tration vehicles and powerelectronic drive systems, design and testing of electrical traction machines (motors, generators, transformers, inductors), design and development work on energy storage, tests for certification, attestation and testing ace. to international standards, testing of electromagnetic compatibility and cathodic protection Department of Electrical Machins design of electrical machines: three-phase induction low voltage cage motors with different efficiency classes, synchronous generators with electromagnetic and permanent magnet excitation, magnetoelectric motors, 34 testing of electrical machines: 3-phase induction motors (voltage up to 600 V in power ranges 0.75-200 kW at frequencies of 50 and 60 Hz), synchronous generators and special motors. Department of Power Converters individual designs and execution of power-electronic systems adapted to customer’s requirements, testing and putting into operation of power-electronic equipment, warranty and ofter-warranty service, technological consultations concerning design and operation problems, testing semiconductors and power-electronic power devices, power supply for high power systems. Department of Measuring and Diagnostic Systems scientific research and development work in the range of metrology and nondestructive testing, design, monitoring control and diagnostics of electrical vehicles, infrastructure of charging electrical vehicles, impedance and optical tomography. Department of Lighting Technology abd Optical Radiation optical radiation (UV,VIS) – testing, technologies, consulting, illumination-design and execution, spectroradiometric and calorimetric testing of light sources and equipment, special lighting equipment-developing and execution, ultraviolet radiators and high pressure discharge lamps. Department of High Power work in the domain of design and execution of circuit breakers and low and medium voltage distribution equipment in a broad range of currents, design and execution of models of superconducting equipment, calculations using field programs in electric equipment Laboratories of the Electrotechnical Institute Testing of products acc. to the EU directives is performed in laboratories accredited by the Polish Accreditation Centre, notified in EU under Nr 1460. 35 Quality of the performed tests and calibrations is ensured due to: staff with suitable competences, structure based on division into specialized laboratories, suitable infrastructure and measuring and testing equipment, satisfying requirements of the Quality System acc. to the Standard – PN-EN ISO/IEC 17025-2005 and of the Quality Management System acc. to the Standard PN-EN ISO 9001-2009, the system of taking part in comparisons between laboratories. Testing Laboratory of Switchgear in Warsaw - Accreditation nr AB 074 Testing high and low voltage electric apparatus and equipment: ac and dc switchgear, container type transformer stations, ac and dc circuit breakers, disconnectors and disconnector sets, high and low voltage disconnecting, earthing and short circuiting switches, electroinsulating protection and auxiliary equipment for live operation. Testing and Calibrating Laboratory - Accreditation nr AB 022 ans AP 102 Testing equipment and products in the range of the low voltage machine, noise, toy and electromagnetic compatibility directive for: handoperated and mobile tools with electric drive, equipment and devices of common use, lighting, office and computer equipment, low and medium power electric machines, light sources for common lighting purposes and for special purposes, Calibration of measurement apparatus in the range of electric metrology, high voltage and photometry. 36 1) Flexible DSP/CPLD/FPGA-based Control System – Educational Platform for Power Electronics CPU modules Sophisticated power electronics applications, especially new R&D projects, require increasing speed and computing power of the control system. The CPU family must follow on the technological trends. Continuous development and improvement are required. Actually available are DLHF2812/R2812 CPU module and DLHF280x/280xx flexible CPU module family. New CPU concepts are focused on advanced floating-point DSPs: TMS320F2833x (150MFLOPS), DELFINO (300MFLOPS), TMS320C6x (2.1GFLOPS), SHARC (2.4GFLOPS). Additionally, high-speed FPGAs (Cyclone, Stratix, Spartan, Virtex) can be used as the main processor with parallel processing capabilities. Some of them are under development and will be available soon. Flexible baseboard family for power electronic appplications Flexible baseboard was designed to be easily used for the different power converter control system configuration: AC/DC/AC converters, advanced AC drives active filters and compensators matrix and multilevel converters UPS, specialized power supplies traction vehicles and electric car drives power conditioners Standard version of flexible baseboard is established as control system core. Extended versions can be achieved by including on a single board additional components (e.g. optical links, transducers) and connectors. Educational applications The flexible control system architecture is well suited for complex AC/DC/AC converters topology. The mains and machine inverters can be controlled by similar, but separate peripherial block and one DSP. This topology is used for precision sensorless drive with bidirectional energy flow. Incremental encoder module included in diagram is for algorithm’s performance verification only. The project is managed by research team of the Institute of Electrical Machines, Drives and Measurements (Wroclaw University of Technology, Poland). The flexible control system was also applied for standard 3-phase frequency converter structure with the SiC-based power stage. Fast switching algorithms are implemented and tested by research team of the Institute of Control and Industrial Electronics (Warsaw University of Technology, Poland). 37 R&D applications Supercap-based power conditioner Supercapacitors offer new possibilities for energy storage and power conditioning applications. Most industrial system faults were caused by short-term voltage disturbances. It is possible to replace standard battery-based UPSs by supercaps-based power conditioners with fast response and recovery time. Active filtering option can be also included and maintenance cost significantly limited. The Gdansk Branch of the Electrotechnical Institute has arranged the special R&D project of supercap-based power conditioner. Single-phase version was designed and successfully tested. The flexible controllers are used: one board for phase invertes control, second board for DC-DC conversion support. Multilevel current inverter Multilevel current inverter analysis and control algorithm development was proposed as a new Ph.D. project accepted by Scientific Board of the Electrotechnical Institute. The experimental setup includes flexible control system. Industrial applications Electric Traction Dept. of the Electrotechnical Institute is specialized in development and applications of electric and electronic solutions dedicated for electric traction vehicles (electric locomotives, integrated electric trains, trams, trolleybuses). The flexible control system was adapted and successfully applied as DC drives upgrade to replace traditional motion controller by high-voltage (6.5kV) IGBT chopper – based controller. Four metropolitan trains EN-57 was equipped with upgraded DC drives and general control/monitoring solutions in 2007. Current developments are focused on new design of motion control, diagnostics and power supply systems dedicated for heavy electric locomotive (6ACT) prototype. It features 6-axis motion system with asynchronous motors of 5MW total power. The flexible control system was also used in this project and high-voltage DC-DC supplies for traction vehicles power supply systems. The presented flexible DSP/CPLD/FPGA-based control system was set as a standard development platform for all branches of the Electrotechnical Institute (Poland) involved in power electronics applications: Electric Traction and High Power Converters Dept., Electric Drives Dept. and the Gdansk Branch. Contact Person Data Electrotechnical Institute , Division of Electrotechnology and Material Science 55/61, M. Curie Skłodowskiej st, 50 - 369 , Wrocław, Poland phone: +48 71 328 30 61 fax: +48 71 328 25 51 e-mail: [email protected] 38 2) Anisotropic Nd–Fe–B magnets aligned by hot deformation The subject of the invention was the method of fabrication of anisotropic high energetic Nd– Fe–B magnets. In the result of the invention, optimal technological parameters of production process had been established and device to realize the process had been build. The method of the fabrication contains hot densification of Nd–Fe–B powder followed by hot deformation. The hot densification process yields isotropic magnet (soft–product, precursor) while hot deformation generates texture in the processed material and anisotropic properties of the magnet. The invention allowed to produce anisotropic Nd–Fe–B magnets with the following properties: remanence Jr = 1,41 T, coercivity JHc = 780 kA/m, energy product (BH)max = 395 kJ/m3. Such result, for standard raw material: MQP–A powder, applied in the experiment, had never been received before. Contact Person Data Electrotechnical Institute , Department of Electric Machines 28, Pożaryskiego st, 04-703, Warsaw, Poland phone: +48 22 812 30 20 fax: +48 22 812 12 46 39 3) Synchronous Eco-Generator for Devices Cooperated with Renewable Energy Sources Synchronous Eco-Generator with permanent magnets is developed in Electrotechnical Institute in Warsaw (Poland). It has rated power 1 kW, rated voltage 3x53 V, rated speed 100 RPM and weight 50 kg. This generator is designed for devices that cooperate with renewable energy sources such as wind and water. Because of low rated speed it perfectly suits for direct drive (without mechanical gear) by winter or water turbine. Additionally, low voltage gets up the operational safety. Because of using innovative construction solutions the generator stands out from similar devices on the market of lower weight (about 50 %) with the same energetic parameters. Lower weight has a big significance when the generator has to be placed on the top of mast (in case of wind turbine) or on the swimming platform (in case of swimming water turbine). Contact Person Data Electrotechnical Institute , Gdansk Branch 1, Narwicka st, 80 – 557, Gdańsk, Poland phone: +48 58 343 12 91 fax: +48 58 343 12 95 e-mail: [email protected] 40 4) Compensator of voltage sags and short time interruptions of voltage at power grid with an energy storage implemented as battery of high-voltage stacked supercapacitors. A purpose of the compensator is riding through short time voltage sags and interruptions at public power grid. It is estimated that 90 % of grid disturbances are provoked by voltage sags and interruptions of duration less than one second. Even such interruptions of power supply cause significant losses of manufacturing process and disturb operations of information systems. The compensator is continuously monitoring the voltage of the grid. After detecting a voltage sag or interruption a load is disconnected from grid power supply. At the same time a sinusoidal voltage generator (implemented as cascade DC/AC converter) is started. The converter generates supplying voltage using electric energy stored in supercapacitors. The compensator assures the required level of nominal amplitude and phase which are in conformity with parameters of the grid. When the nominal voltage occurs again at the grid, the load is back connected to the grid and the sinusoidal voltage generator is switched off. The time when the compensator is on stand-by is used to charge the supercapacitors. Specific features: the energy storage is implemented as a high-voltage device built of stacked supercapacitors, which do not contain toxic electrolyte, the compensator includes DC/AC converters based on a novel structure of cascade inverters, the device enables synchronous compensation in one-phase and 3-phase system with independent compensation of each phase, the control is performed by three independent microprocessor-boards based on DSP (Digital Signal Processors). Contact Person Data Electrotechnical Institute , Division of Electrotechnology and Material Science 55/61, M. Curie Skłodowskiej st, 50 - 369 , Wrocław, Poland phone: +48 71 328 30 61 fax: +48 71 328 25 51 e-mail: [email protected] 41 5) Novel design and technological process of surge arrester The invention relates to new construction and technology of surge arrester, allowing for lower production costs to a level that guarantees a competitive price. Medium voltage surge arresters are designed primarily to protect the insulation, responsible substation power equipment such as transformers with rated voltage of several to tens of kilovolts. Overhead surge arresters for voltages above 1 kV consist of a few to several varistors stacked in piles, which require special housings. They are used mostly internal housing made in the form of pipes, loops and glass-epoxy rods or varistor stacks directly wrapped with tissue or fiberglass impregnated with epoxy resin. These internal housing of varistor stacks determine a good electrical contact between the varistors and the mechanical strength of the surge arresters. Active element - varistors stack with internal housing is placed in a sealed external housing that protects it from the effects of weathering. Overhead surge arresters performed most often in the porcelain or polymer external housings. So far, structural solution used productively surge arresters involves the use of glass-epoxy pipe, which are placed in varistors and elements attached to the pipe by dowelling. Electrical contact is accomplished by pressure springs tows and flexible cables with copper links. This solution is labor-intensive assembly and construction requires the use of multiple components, which adversely affects the cost of materials and labor. The Electrotechnical Institute Division of Electrotechnology and Materials Science in Wroclaw, together with APATOR SA enterprise from Torun, preliminary developed the technology of the internal housing of surge arrester, which ensures lower production costs. From the technological point of view, developed the concept based on a common processing thermoplastics technological phenomenon of shrinkage. The thermoplastic material is directly injected onto the stack and shrinkage of the material ensures good electrical contact between the varistors and adequate strength of surge arrester. Patent application nr P-387216 “Over–voltage limiter and a method of producing the overvoltage limiter” Contact Person Data Electrotechnical Institute , Department of Electronic Traction 28, Pożaryskiego st, 04-703, Warsaw, Poland phone: +48 22 812 33 00 fax: +48 22 615 68 70 e-mail: [email protected] 42 6) The stationary supercapacitor storage system 2MJ, 0.15MW Supercapacitor energy storages which booster traction power supply system can be installed on traction substations or at long no-load run routes in special containers. Energy storages installed on substations should comply with the requirements specified below: Decreased value of the peak current input to traction vehicles from substations; Capture of a considerable (40 – 50%) part of energy to be returned to the contact line for the period of braking; Reduction in line voltage fluctuations. Energy storages installed on long no-load run routes must: Reduce the values of line voltage drop for the period of intensive current consumption by the vehicles for the start-up phase; Capture the entire vehicle braking energy; Reduce the load on power units and traction sub-stations. Installation of supercapacitor energy storages featuring useful energy of ~2MJ (10F, 800V) ensures the economies of about 50KWh electric energy per one hour. Electrotechnical Institute has designed a supercapacitor energy storage system to be mounted in a container and is testing the model on a selected tramway line in Elbląg. In the case of sub-stations, the energy storage may be designed as a modular model with its units adapted to the sub-station power capacity. Production of a double-module (2x10F, 800V) system for Gdynia-based sub-station is in progress. Contact Person Data Electrotechnical Institute , Division of Electrotechnology and Material Science 55/61, M. Curie Skłodowskiej st, 50 - 369 , Wrocław, Poland phone: +48 71 328 30 61 fax: +48 71 328 25 51 e-mail: [email protected] ] 43 7) A device for magnetic properties measurements of soft magnetic materials by means of a non-destructive method This invention relates to a device for measuring the magnetic properties of punched parts magnetic materials by means of a non-destructive method. The device is based on on the tangent component continuity of the magnetic field strength on the border of ferromagnetic material-air as well as on the magnetic flux continuity on the contact of the magnetizing circuitexamined object. The values of magnetic parameters of electrical steel sheets, which are obtained by means of measurements carried out in the standard yokes (i.e. Epstein apparatus or SST as well as a ring sample), differ significantly from values of the obtained parameters for ready magnetic cores of machines and devices. They do not take into consideration the processes which take place during the steel processing method and the shape used, for example, in the rotating machine. During the production of the final product, magnetic cores undergo various technological processes such as punching, stacking, riveting, etc. This influence can be different depending on the method of processing and the steel type as well as on the efficient cross-section of the magnetic core. Using a specially designed measuring yoke allows to control the quality of magnetic materials such as blanks electrical sheets at each stage of production of electric machines or electromagnetic devices, without the need for special sample preparation of tested material, which saves time and material. Contact Person Data Electrotechnical Institute , Division of Electrotechnology and Material Science 55/61, M. Curie Skłodowskiej st, 50 - 369 , Wrocław, Poland phone: +48 71 328 30 61 fax: +48 71 328 25 51 e-mail: [email protected] 44 8) Ecological Solar Power Station The aim of the European energy strategy is to help create a unified energy policy, guaranteeing the security of energy supplies. Brussels pays attention to climate change. It proposes that by 2020, one-fifth of the consumed energy will be from renewable sources - water, wind and sun. The European Commission aims to reduce greenhouse gas emissions and thus protect the environment. In 2007 EC published a special report in which it has proposed to reduce carbon dioxide production in Europe by at least 20 percent by 2020. The solution requires the increase of clean energy production - at the end of the second decade of our century, wind, solar and water should be utilized in production a one-fifth of EU electrical energy. Electrotechnical Institute has started realization of this assumptions, it designed and built a prototype organic solar power station (several kW) enough for a supply house or a small public building. Processing of the usable solar energy takes place in the solar thermal and photovoltaic panels. The heat generated in the collectors can be converted into electricity. One way to convert low and medium temperature heat to electricity is the use of organic Rankine cycles (ORC). Surplus of heat energy, obtained in solar collectors and heat at a temperature too low to power the ORC system can be used, for example, to prepare hot water for municipal and economic. In the model system, powered by heat from the vacuum solar collectors, supplying approximately 20 kW of heat (the temperature in the evaporator circuit about 100 °C), operates a power generator 1.5 kWel. Electricity for supply own system elements: power control system, pumps, fans, etc. - is obtained from photovoltaic cells. Excess electricity from photovoltaic cells and ORC can be used to produce hydrogen in the electrolyser. Hydrogen stored in the composite, pressure vessels (designed and performed at the Institute) allows for storage of energy for a long time and can be used to produce electricity in fuel cells (our design). An alternative way of electricity storage is hybrid systems: chemical battery - supercapacitor, which is currently being developed in Wroclaw. 45 INDUSTRIAL RESEARCH INSTITUTE FOR AUTOMATION AND MEASUREMENTS (Przemysłowy Instytut Automatyki i Pomiarów) Organisation Contact Data 202, Jerozolimskie st, 02 – 488 Warsaw, Poland phone: (+48) 22 8740 164 fax: +48 22 8740 221 e – mail: [email protected] http://www.piap.pl/en/ Industrial Research Institute for Automation and Measurements - PIAP is a leading Polish research institute, active in the fields of robotics, automation and measurements systems. PIAP was established as a government-owned research institute in 1965. Products PIAP offers research and development works in systems integration and special products, covering design, realisation, start-up, implementation, maintenance and training activities. For many years we design and develop technologically advanced electronic and mechanical systems, dedicated to military and police applications as well as for industry. Our mobile robots and specialised devices are successfully used by various forces responsible for safety and security (Police, Polish Army, Border Guards). As a reliable partner, PIAP delivers applications bases on industrial robots and as a specialist in measurement area, offers the electronic tachograph for rail vehicles. Projects The Institute is very active in realisation and coordination of international and national multipartner projects. Currently, we execute and coordinate about 20 international research projects. We have a well established European cooperation also within NATO, EDA and ESA research programmes, as well as with US and Israeli partners. Certificates ISO 9001:2009, AQAP 2110:2009. The Institute is certified with Industrial Security Clearance of First Class, and it is prepared to handle EU SECRET and NATO SECRET classified materials. Fields of activity and applications Specialised internal unit - Intelligent Defence and Security Systems Department - is focused on creation of a wide spectrum of devices and systems dedicated to various applications, including: C-IED and EOD operations, border and infrastructure protection, convoys and patrols escort, 46 reconnaissance and remote observation, surveillance and patrolling, crisis management, SAR operations. As a automation institute we cooperate with companies on the field of automation and robotization. Technologies Many years of work over the research projects and specialised products development allowed us to build a wide range of competencies, supported by vast experience, which cover: robots constructions of a high mobility, HMI and MMI, data transmission, including satellite communications, tele-operation and control systems, environment recognition, manipulation and gripping, autonomy, data processing and analysis. Our long-term experience and vast network of partners allows us to create and implement complex system solutions in the security area. We are one of the main suppliers for: army, police, fire brigades, other forces responsible for public security, crisis management and civil protection. DESCRIPTION OF PIAP’S PROJECTS PIAP carries out many international projects Crisis Management PROTEUS „ Integrated Mobile System for Crisis Management and Counterterrorism Support”, structural funds IED/EOD UGTV - „Unmanned Ground Tactical Vehicle”, EDA (national consortium’s coordinator) E-STAR – “Explosive detection-Spectroscopy, Terahertz technology And Radar”, EDA Autonomous detection system for neutralisation of non-metal landmines, national funds SAR SARBACAN – “SAR BeAcon with CANada”, FP7 GSA VIEW FINDER - “Vision and Chemiresistor Equipped Web-connected Finding Robots”, FP6 Dedicated data processing and analysis systems MICIE – “Tool for systemic risk analysis and secure mediation of data ex-changed across linked CI information infrastructures”, FP7 HEMOLIA – “Hybrid Enhanced Money Laundering Intelligence, Investigation, Incrimination and Alerts”, FP7 Satellite applications SAFETRIP – “Satellite Applications For Emergency handling, Traffic alerts, Road safety and Incident Prevention”, FP7 IEGLO – “Infrastructure-Augmented EGNOS/Galileo Receiver for personal mobility”, FP7 GSA 47 PACIFIC – “Public Regulated Services Application Concept Involving Future Interested Customers”, FP6 GJU Soldier protection MUSAS – “Multi Sensor Anti-Sniper System”, EDA AHEAD – “Advanced HElmet And Devices for Individual Force Protection”, EDA CARDINAL – “CApability study to investigate the essential man-machine Relationship for improved Decision making IN urbAn miLitary operations”, EDA Border and critical infrastructure protection TALOS - „Transportable Autonomous patrol for Land bOrder Surveillance”, FP7 (koordynator) STABORSEC - “Standards for Border Security Enhancement”, FP6 PASR TRIPS - “Transport Infrastructures Protection System”, FP6 Reconnaissance „Secret audiovisual observation vehicle”– DALILA”, national funds „UAV management in uncontrolled aerial space – technical, organisational and legal aspects”, national funds DESCRIPTION OF PIAP’S MEASUREMENT DEVICES PIAP is a producer one of the best known electronic tachograph for rail-vehicles in the eastern Europe The electronic tachograph T-130P measures and registers speed of a rail vehicle, current time and the distance covered by the vehicle and registers two-state signals sent from the vehicle devices and mechanisms (e.g. dead-man.s handle, SHP, door closing and others). Moreover, the tachograph can generate signals of exceeding de-fined speeds. The T-130P tachograph consists of a central processing unit, a speed converter that is mounted on the wheel hub and cab speed indicators installed in the driver field of vision. All information is registered in a continuous way in an electronic memory card (EMC). SYSTEM ELEMENTS The tachograph central processing unit receives all information from the vehicle, i.e. a speed signal, two-state signals and information from the keyboard and produces a digital signal for control of the cab speed indicators, and two-state signals, e.g. signalling of exceeding established threshold speeds for systems control. Some functions e.g. change of the wheel coefficient, change of threshold speeds, clearing of the distance meter are reserved only for service personnel and are not accessible for driver. Each switching off of the EMC card or switching off of the tachograph supply is marked on the graph after reading out of the record. The EMC card makes it possible to record of 75 hours of operation. The speed converter that is mounted to the vehicle hub produces pulses for control of the distance speed measurement. The converter is adapted to cooperation with central dog and 48 eccentric one to couple with the wheel axle. The way of mounting and coupling with the axle can be adapted to the buyers needs and is adapted to rugged operating conditions that are in the place of its installation (heavy vibrations and impacts, weather conditions). The cab speed indicator shows the vehicle current speed and is installed in the con-sole, in the drivers field of view. It is equipped with a legible scale of readout range adapted to the vehicle type. Information recorded in the EMC memory can be read out by means of PC equipped with program and interface for connecting to the EMC. Speed measuring range 0 ÷ 130 [km/h] Nominal supply voltage 24V; 110 DC or other agreed Admissible range of supply voltages 16 ÷ 36V (for voltage 60 ÷ 160V (for voltage of 110V) Vehicle wheels nominal diameter Adjusted in service mode Distance meter indication range 4 000 000km Number of registered signals 8 Number of output signals maximum 7 of 24V) Signal for control of station announcement Pulse, 2 pulses/wheel rotation device EMC card capacity Registration of 75h of operation Full card signalling Full card signalled by electric contact > 65 hours. Record registration resolution in function of time 1s Record registration resolution in function of 1m distance Speed registration error ± 1km/h 49 DESCRIPTION OF PIAP’S AUTOMATION AND INDUSTRIAL ROBOTS PIAP as a reliable and professional partner for every kind of companies which needs automation and robotics into their production activity Industrial robots – safety and precision for processes, rise in efficiency and quality stabilization. PIAP gives more than 30 years of experience in robotics area to the partners. We are specialist and we can be helpful for upgrading every kind of producers. Robotization and automation including: - analyzing abilities for robotization and automation, - selection the best products for implementation, - project and implementation robotics cells, - training for robot operators. Industrial robots for welding – it doesn’t matter, whether it is steel, or aluminum, or any other type of material (possible to weld), we are able to create a cell for welding them. There are only two conditions: a high quality details and their quite big number. We can deliver cell for welding that products. Industrial robots for palletizing – almost every kind of product, into every kind of production field, into a vast variety of conditions can be transporter by robots. Dust, high or very low temperatures, humidity could create difficult environment for working people. Robotics cells from PIAP are for helping into actions like that. The highest quality of the process gives the company advantage into delivering its products on the demanding market. Others – any kind of activities, where people are doing repeatable moves are perfect for automation, or for using robots. Dust, humidity, temperatures, gases, fumes etc. are danger for workers, but after preparation, are neutral for robots and other types of automation. 50 DESCRIPTION OF PIAP’S MOBILE ROBOTS 1) PIAP INSPECTOR ROBOT Inspector is a big and strong robot designed for urban operations. Unique features of INSPECTOR robot The INSPECTOR can tow vehicles left in any gear of a mass of up to 1500 kg. Front tracks (remote control of tilt angle) increase traction abilities, longitudinal stability and enable smooth motion on stairs, as well as highly uneven terrain. The manipulator is able to lift 30 kg on extended arms and 60 kg on folded arms. The turn of the manipulator’s base amounts as much as 400º. Constant spatial orientation of the object placed in the gripper, irrespective of the movement of other manipulator arms, enables precision manipulation of hazardous devices. Control system of the robot enables to control all of its drives at the same time. A program for automatic folding of the manipulator down to a transport position speeds up and makes easier preparing the robot for transport Basic features of INSPECTOR robot Width of the mobile base enables to drive through standard doors (70 cm) and to move around the interiors of residential and office buildings. The robot is powered by batteries installed inside the mobile platform or through a cable plugged into the 230V power network. The maximum operation time when powered by batteries is 2 to 8 hours (depending on the operations). During the external power supply (by cable) the batteries are automatically recharged. INSPECTOR is equipped with 4 cameras: on the gripper, in back and front of the robot and on the manipulator (the main camera which may be turned completely around by 360° and 90° up and down). Special driving system reduces recoil effect when firing the pyrotechnical disrupter or in case of explosion of the load placed in the gripping device or its vicinity. The manipulator is equipped with: manipulator arms extreme position sensors, position sensors in main manipulator’s degrees of freedom, gripping force sensor, sockets for fixing of so-called ‘whiskers’ on the gripper’s master jaw (for visual estimation of distance), an omni directional microphone. 51 The operator’s post is equipped with three LCD monitors, which show, apart from the view from chosen camera, a graphic interpretation of the manipulator arm and front tracks configuration. Robot can be controlled by radio or by cable. 52 2) PIAP EXPERT ROBOT Expert- robot designed for missions inside the means of transportation. Unique features of EXPERT robot EXPERT’s construction combines two unique features: manoeuvrability in tight places achieved thanks to the mobile platform’s small size as well as broad range and high load capacity of the manipulator. Front tracks (with remote controlled tilt angle) ensure stability of the structure when negotiating obstacles and climbing stairs. Unfoldable lateral stabilizers enable secure fixing of the mobile platform, which allows safe lifting of considerable loads and precise operation of the manipulator even during maximum lateral reach of its arm. Stabilizers can be dismounted to reduce the robot’s by 8 cm. Maximum reach is 3 meters (including the gripping device). Exceptional length of the upper arm allows inspection of spaces both at the level of hand luggage overhead lockers and under passenger seats. EXPERT is equipped with 6 cameras. Four colour cameras are placed respectively on the gripper, at the back and front of the robot and on the manipulator (main camera which can make a 360° turn and move 90° up and down). Additionally, two colour cameras are placed on the sides of the front tracks, these enable inspection of areas such as places under seats. Control system of the robot enables to control all of its drives at the same time. Self-diagnostic system constantly scans for potential faults and shows special warnings on the supplementary LCD screen. Most cables are led inside the robot’s manipulator, which reduces the risk of damage. Basic features of EXPERT robot - The mobile platform’s maximum velocity of 2 km/h allows quick displacement in areas such as an extensive safety zone around an aircraft. Fluent control of all drives, from 0 to maximum speed, ensures high precision of operation. It is possible to reduce maximum velocity thus allowing greater precision of operation (after pressing the appropriate button, maximum velocity is reduced to 20%). Special manipulating driving system reduces recoil effect during firing from the pyrotechnical disrupter or upon explosion of a load carried in the gripping device or its vicinity. The manipulator is equipped with: manipulator arm’s extreme position sensors, 53 - manipulator’s main degrees of freedom position sensors, gripping force sensor, sockets to fix the so-called ‘whiskers’ on the gripper’s master jaw (for visual estimation of distance), an omnidirectional microphone. 54 3) PIAP SCOUT ROBOT PIAP SCOUT is a robot designed for quick reconnaissance of field and hard-to-access spots, i.e. vehicles’ chassis, places under seats in means of transportation, narrow rooms or ventilation ducts. The PIAP SCOUT robot’s basic moving assembly consists of a hybrid system (tracks-wheels), but if necessary, moving wheels can be dismantled. Solid construction combined with small dimensions and light weight as well as a dynamic driving system ensure remarkable manoeuvrability and high speed of the robot (7 km/hr). By mounting additional devices to the robot’s mobile base, its scope of application is significantly broadened. Unique features of PIAP SCOUT robot Small dimensions of the robot enable swift inspections of hard to reach areas and rooms; The robot’s wheels are easy to dismantle. This allows for a reduction of the robot’s overall dimensions and enables operation in spaces that are hard to reach; Very small weight enables transportation of the robot in a typical military backpack; Thanks to its specific drives, the robot efficiently travels across uneven areas and obstacles of inclination angle up to 45º; The robot’s module structure enables easy and swift replacement of any additional equipment; The robot is able to carry loads from 2 up to 5 kg with its manipulator; Both the robot and the manipulator can be controlled from the operator’s station (in a form of a small and light-weight suitcase); Optional use of fibre-optic transmission enables the robot to operate at significant distances, even in an environment of high electromagnetic noise level; PIAP SCOUT robot can be adapted to various applications: - use by special squads: neutralization of explosives, negotiations with terrorists, recording of operation course, taking X-ray images, - use by commercial firms: inspection of ventilation ducts, inspection of areas exposed to chemical and biological pollution, location of defects in places difficult to access by a man. 55 4) PIAP IBIS ROBOT IBIS is a robot for pyrotechnic and combat missions. It is designed especially for operations in difficult and diverse terrain (including sand, rocks). High speed of the robot enables taking dynamic actions. Robot’s manipulator provide big range of activities and applications. Precision drive system gives fluidity of the movement of every part of the robot, even during fast ride. Unique features of IBIS robot High speed of the robot (10 km/h), Mobile platform with six-wheel drive, Each wheel is powered with independent drive, Longitudinal axis of front wheels is able to turn in wide range, Wheel arms used in robot’s suspension, provide very good grip to the ground, High load capacity of the robot’s arm (15 kg – unfolded arm, 50 kg - folded arm), The range of manipulator with gripper is over 3 m. Possibility of robot control by fibre optic cable. Robot’s control system enables independent and simultaneous steering of its every drive. Auto diagnostic system detects all faults and projects text announcements on the LCD monitor. The robot is compatible with different additional equipment: pyrotechnical disrupters, chemical and radioactive contamination sensors, bus bar for remote detonation of explosives, barbed wire cutters, drills, recording devices and many others. Basic features of IBIS robot The manipulator can be controlled in two modes: independent control of each segment, direct control of the gripper (the speed of movement of the manipulator’s remaining segments is controlled automatically). The manipulator is protected from damage by 3 independent systems: mechanic clutches, electronic protection, dynamic analysis of allowed movement range. The robot is equipped with 4 cameras: front camera: colour/infrared; powerful LED lamps, rear camera: colour/infrared; powerful LED lamps, gripper camera: colour; LED lamp, main camera: colour or thermo vision; powerful LED lamps; vertical and horizontal rotation. Fluid control of each driver speed (from 0 to maximum) provides precisions of the operation. There is also a possibility of reduction maximum speed of all drives 56 movements, which gives more precision to all activities (after pressing appropriate button maximum movements speed can be reduced to 20 %). Special manipulator’s drive system is minimizing the result of recoil, during shooting from pyrotechnical disrupter or explosion of item carried in the gripper The manipulator is equipped with: Manipulator’s arms extreme position sensors, position sensors in main manipulator’s degrees of freedom, gripping force sensor, sockets for fixing of so-called ‘whiskers’ on the gripper’s master jaw (for visual estimation of distance), an omni-directional microphone. The robot is powered by the batteries inside the mobile base. Time of the operation when powered by batteries is up to 8 hours (it depends on the kind of carried out activities). Convertible, suitcase-like shape operator’s post is mechanical damages resistant. The operator’s post is equipped with colour LCD monitor, which shows the view from one chosen camera or 4 cameras at the same time; additional LCD monitor shows graphic interpretation of the manipulator’s arm and data from robot’s sensors. Fibre optic cable with rolling device, using interchangeably with radio control, is very light and tough. Advanced negotiation system (an option). The robot is easily adaptable for cooperation with wide range of additional devices, offered by PIAP or adapted to the Client’s needs. 57 5) PIAP GRYF ROBOT PIAP GRYF is a robot designed for quick reconnaissance of field and places difficult to access. PIAP GRYF robot’s basic moving assembly consists of a hybrid caterpillars-wheels running gear. However, moving wheels can be dismantled when necessary. Solid construction combined with small dimensions and light weight as well as a dynamic driving system ensure very good manoeuvrability and high speed of the robot (3.6 km/h). Unique features of PIAP GRYF robot Small dimensions of the robot enable swift inspections of hard to reach areas and rooms; The manipulator has seven degrees of freedom (including one manual telescopic part of the arm); The robot’s wheels are easy to dismantle. This allows for a reduction of the robot’s overall dimensions and enables operation in spaces that are hard to reach; Thanks to its specific drives, the robot efficiently travels across uneven areas and obstacles of inclination angle up to 40º; The robot’s module structure enables easy and swift replacement of any additional equipment; The robot is able to carry loads from 5 up to 15 kg with its manipulator; Both the robot and the manipulator can be controlled from the operator’s station (in a form of a small and light-weight suitcase); Optional use of fibre-optic transmission enables the robot to operate at significant distances, even in an environment of high electromagnetic noise level; 58 6) PIAP TRM® (Tactical Throwable Robot) TRM® is a small, robotic device designed to deliver support in antiterrorist operations. TRM® has been designed in response to the threats faced by special forces units during area reconnaissance. TRM® has a pipe-shaped body which contains a camera and a microphone. The drive function is operated by two elastic rubber wheels located on each side of the robot. The TRM® can be thrown into a building or to an open area and steered by remote control in order to perform an inspection. TRM®’s construction is designed to withstand the impact produced by a fall from a high altitude. TRM® applies to: open area or interior inspection and reconnaissance before an operation, tele-observation possibility to transmit sounds produced in the robot’s immediate area, possibility to work in different light conditions, possibility to cast light on targets and dangerous objects, support in locating defects of objects placed in hard-to-reach spaces. Unique features of TRM® Intended application of TRM® significantly reduces the risk of threat to the life and health of its users; Owing to its durable construction (fall from significant height, journey in rough area), high manoeuvrability and fast speed (3.3 km/h), TRM® is a reliable device supporting even the most difficult operations; The camera placed in the body of TRM® enables to carry out area reconnaissance with precision; The microphone placed in TRM®‘s body enables to carry out remote eavesdropping; Its small size, light weight, handiness and capaciousness facilitate transportation of the unit to the operation site; Control panel enables to steer a set of up to 3 robots and operate their additional equipment; The user can operate between 1 and 3 devices simultaneously. This way it is possible to obtain several vantage points and carry out reconnaissance of a vaster area or of a higher number of rooms. 59 7) PIAP EXPLORER DEVICE EXPLORER device. Remote viewing system especially designed for visual inspection of difficult to reach and high risk, tight spaces, vehicles and suspicious packages. Explorer is a camera with set of different length telescope extension arms, which makes an inspection of difficult to reach and tight spaces extremely easy. This device have a wide range of use: an inspection of difficult to reach and high risk tight spaces, vehicles and suspicious packages, protection and object inspection and support of counter-terrorist operations. Thanks to set of different length telescopic booms, the device is also limiting a danger of health and live loss. The view from camera is sending to monitor in module of visualization, which is placed in special waistcoat. This solution gives an opportunity to operator easily move during the time of action. An operation after dusk can be easily leaded with using a LED or IR lights. Explorer device gives a possibility of connecting a digital video recorder, which is sending view to other receivers. After separating an inspection camera, a monitor of visualisation module can be use to perform view that has been recorded before. Explorer is powered by service-free Li-Ion rechargeable battery, integrated with module of visualization. Special joint in module of visualization makes easy changing of batteries. Unit standard equipment Telescopic booms: 1. Telescope extension arm, continuously adjustable from 0.70 m to 1.70 m. 2. Long, straight telescope extension arm – 4 m. 3. Folding telescope extension arm continuously adjustable to 4,10 m. 4. Light telescope extension arm, continuously adjustable from 0,40 to 1,65 m. Cameras: 1. Remote controlled inspection color camera rotating by at least 250° with powerful LED illuminators. An incorporated socket in the camera to quickly connect the camera to the telescope extension arm. Camera with standard lens makes possible an object observation for very far distances. 60 2. Waterproof black and white or color camera with IR illuminators (according to intensity of light camera is switching on automatically). The camera is integrated with chosen telescope extension arm. Visualization module: 1.LCD panel, 2.Sunscreen, 3.Power switch, 4.Camera illuminator switch, 5.Monitor brightness knob, 6.Camera motion control knob, 7.LED signaling the camera ON, 8.LED bar graph array to indicate battery charge level. Additional accessories: 1. A mobile wheel support, which guarantees telescopic arm’s stability and make easy difficult to reach spaces (especially car chassis), 2. A digital video camera for recording view from eXplorer, 3. Additional lenses (f=2,5; 2,9; 3,6; 4,0; 4,3; 6,0; 8,0) 61 INSTITUTE OF ELECTRON TECHNOLOGY (Instytut Technologii Elektronowej) Organisation Contact Data Contact Person Data 32/46, Lotników st, 02 – 668, Warsaw, Poland Director of the Institute: Zbigniew Poznański, M.Sc. phone: +48 22 5487700 http://www.ite.waw.pl/en/index.php phone: +48 22 5487700/01 e – mail: [email protected] The Institute of Electron Technology was established in 1966 and is now overseen by the Ministry of Economy. It is the leading Polish institute in the fields of micro- and nanoelectronics and photonics. The mission of the Institute is to conduct basic and applied research in the fields of semiconductor electronics and physics in order to develop and commercialise innovative microand nanotechnologies and their applications in semiconductor microelectronics, optoelectronics, photonics and micromechanics. The Institute of Electron Technology is located in Warsaw. It comprises divisions in Piaseczno and Kraków, and Division PREDOM in Warsaw. The research part of the Institute consists of 8 departments. The Institute employs over 330 people, including 7 Professors, 12 Doctors of Science, and 48 Doctors of Philosophy specialising in electronics, physics, chemistry and material engineering. ITE cooperates with higher education institutions and the Polish Academy of Sciences, and industrial enterprises both in Poland and abroad. The leading position of ITE in the area of advanced micro- and nanotechnology is the result of innovative research activities and their application in the following areas: optoelectronic detectors and sources of radiation, nuclear radiation detectors, silicon sensors of physical, chemical and biochemical quantities for interdisciplinary applications, semiconductor lasers, advanced lasers with resonant cavity type VCSEL, micro- and nanoprobes for measurements of short- range interactions, analog and digital specific integrated circuits type ASIC. The Institute is continuously strengthening its position in the European Research Area by participating in numerous EU research programmes. So far it has participated in almost 40 projects, facing strong international competition, (5th, 6th and 7th Framework Programme, JU 62 ENIAC, Eureka, including three prestigious Integrated Projects).In the past five years, nearly 600 articles authored or co-authored by the researchers of the Institute have been published, and over 70 patents have been granted. One of the important development activities of the Institute is to create favourable conditions for research and development focused on industrial implementation in cooperation with domestic academic community, including higher education institutions. In order to achieve these goals, the following research centres were established: the Centre of Microsystems and Electronic Nanotechonologies, the Centre of Nanophotonics and the Laboratory of Multilayered and Ceramic Technologies. These research centres will enable academic institutions (i.e. students and doctoral students) to conduct research, do a traineeship, produce models together with their characterisation, and develop technology and devices in cooperation with and for the needs of industry. 63 RESEARCH ACTIVITY 1. New materials and technologies 1.1. Silicon technologies, microsystems and nanostructures development of ASIC technologies for niche applications (FD-SOI, fin-FET and other); silicon sensors and nano- and micro-mechanical systems MEMS/NEMSI and bio-MEMS to be used in interdisciplinary areas; specialised silicon detectors of ionising and x-ray radiation as well as detector systems for radiochemistry and other applications. 1.2. Circuit and system design methodology of designing integrated circuits and single-chip systems; designing of reusable digital blocks (reusable IP blocks ); designing of specialised IC - digital, analogue and mixed, i.a. high-voltage specialised circuits; integration of heterogeneous systems of a cubic architecture. 1.3. Photonics new radiation sources in the area of near- and middle infrared based on III-V compounds: high power semiconductor lasers; optically pumped vertical cavity lasers (VECSELs); quantum cascade lasers (QCLs); infrared detectors based on II-V compounds: p-i-n diodes; avalanche photodiodes; type II superlattice antimonide detectors. 1.4. Semiconductor technologies of III-V, II-VI and IV-IV compounds development of MBE technology for epitaxial growth of III-V semiconductor heterostructures; processing of III-V, II-VI and IV-IV semiconductor structures for IR, VIS and near-UV optoelectronics and high-frequency high-power, and high-temperature microelectronics. 1.5. Hybrid microelectronics study and development of technological processes for forming thick film hybrid microcircuits, multi-layered microcircuits LTCC, ceramic and polymer-carbon-metallic composites; 64 synthesis, characterisation and verification of the usability of selected materials, such as perovskites, multiferroics, ceramic composites for forming capacitors, fuel cell electrodes, resistors, gas and humidity sensors; design of hybrid microcircuits (including LTCC), specialised passive elements, electronic modules for photovoltaic systems. 2. Advanced methods of material and structure characterisation scanning and transmission electron microscopy of materials and structures; spectroscopic ellipsometry of materials and structures; photonic spectra of solids by means of Raman microspectroscopy; photoelectrical methods of studying the nanoelectronic structure properties in UV region; three-dimensional parametric visualisation of bandgap in the interface areas between dielectric and semi-conductor; advanced electro-optical and electrical methods - characterisation of energy quantised states and defects in low-dimensional structure.__________ 65 RESEARCH CENTRES FOR INDUSTRY AND ACADEMIA Centre of Nanophotonics The Centre unites institutions which are national leaders in the field of nanotechnology as well as semiconductor physics and electronics. Thanks to a consequent research policy, nanophotonics may become a Polish speciality and secure a strong position of Poland in the European hi-tech research and industry market. The establishment of the Centre of Nanophotonics enabled R&D activities in the following areas: lasers (VCSEL and QWL) and infrared detectors; visible and ultraviolet radiation sources based on wide band-gap semiconductors; photonic structures, including lasers with photonic crystals; antimony based structures for infrared optoelectronics; measurement systems and devices working with mid- and far infrared; biophotonics and medical applications. The Nanophotonics Laboratory, located in the Institute of Electron Technology, is the core of the Centre. It is based on the European Excellence Centre "Physics and Nanostructure Technology for Photonics" CEPHONA. The activity of the Centre of Nanophotonics is focused on applications, and it should lead to the development of advanced fabrication technologies for sub-assemblies used in devices and systems applied in industry, environmental protection, medicine and military technology. A natural continuation of research conducted in the Centre will concern target projects serving as an initial phase for the production of developed sub-assemblies and devices. In order to achieve the goals of the Centre of Nanophotonics, it was decided to establish a consortium consisting of the following entities actively participating in the optoelectronic sector: Institute of Electron Technology, Warsaw; Institute of Physics of the Polish Academy of Science, Warsaw; Insitute of Microelectronics and Optoelectronics at Warsaw University of Technology; Institute of Physics - Lodz University of Technology; Vigo System. 66 Centre of Microsystems and Electronic Nanotechnologies The Centre provides industry and R&D institutions with access to its potential related to technology, construction and measurement. The offer concerns micro- and nanoelectronic technologies including: micro- and nanoelectronic circuits and systems; specialised photodiodes, photodetectors and radiation detectors; heterogenic microsystems for interdisciplinary applications; modelling and simulations of technological processes. The Centre is ready to present the available technologies in a form of lectures. Within research programmes undertaken together with domestic and European academic teams, it is possible to carry out thesis-related work (for Master and Doctoral degrees). The Centre applies a principle of equal access; however, projects with a future possibility of implementing their results in industry, economy or science are preferred. On account of work safety requirements and the stability of technology, all technological activities to the benefit of partners are performed by the staff of the Centre. The material scope of work is agreed with the applying R&D unit, based on the catalogue of available process modules and process package of multiproject wafer service developed by the Centre. If the work scope defined by partners is beyond the potential offered by the Centre, access to the best European centres cooperating with ITE shall be offered. In such cases, the Centre will provide necessary organisational support and assistance in the areas of design, modelling, simulation and, in some cases, micro-assembly. The cost related to the undertaken work shall be covered by partners, depending on the scope of their research. In the case of higher education institutions and R&D units, a non-profit principle is applied to cost setting. At present, the key project MNS-DIAG "Micro - and nanosystems in chemistry and biomedical diagnostics" is carried out in the Centre and coordinated by ITE. The project is aimed at integrating academic circles and directing the work to interdisciplinary applicative research. Laboratory of Multi-layered and Ceramic Technologies The Laboratory is involved in conducting research and developing technologies as well as constructing multilayer ceramic microcircuits and microstructures. The Laboratory enables certain academic institutions and students to conduct research, do a traineeship, produce models together with their characterisation. State-of-the-art multilayer ceramic micromodule fabrication facilities are available to the research community. LTCC (Low-temperature Cofired Ceramics) is a fabrication technology for multilayered electronic circuit structures with integrated interconnects and passive components. It also enables the fabrication of integrated micro electromechanical systems (MEMS), such as sensors and actuators. Fabricated LTCC substrates can be integrated with active devices using surface mount technology or wire bonding. 67 LTCC process starts with sheets of ceramic tape. Sheets, with thickness between 50 and 250 µm are fabricated out of a mixture of ceramics, glass and organic vehicle. First, sheets are cut into desired shape. Subsequently, via holes (providing inter-layer connectivity) are drilled and filled with conductor. Then, conductive, resistive or functional layers are printed on each sheet. Next, individual foils are put together into multi-layer stack, laminated under pressure and fired. The Institute of Electron Technology - Division in Cracow has state-of-the-art technological equipment for fabricating LTCC micromodules. OFFER The Institute provides its expertise and know-how for: enterprises to foster their development by offering access to technologies as well as devices, systems, sensors, detectors, lasers, integrated circuits and more (services can be provided in small scale production mode at the Institute or ordered from specialist suppliers based on projects prepared by ITE); research centres which seek partners to carry out international programmes; higher education institutions which seek support for their educational activities (laboratories, traineeship, practical training, theses). For more information on services provided by ITE, check our website http://www.ite.waw.pl 68 MILITARY COMMUNICATION INSTITUTE WIŁ (Wojskowy Instytut Łączności) Organisation Contact Data 22A, Warszawska st, 05 – 130 Zegrze, Poland phone: +48 22 688 55 55 fax: +48 22 688 55 89 e-mail: [email protected] www.wil.waw.pl Military Communication Institute (MCI) is modern and innovative research and development unit. The area of activity of MCI focus on the field of command systems, communications and computer science for defense and national security, especially activities dealing with Ministry of National Defense, as well as their implementation in practice. In the process of assessment of scientific units conducted by Ministry of Science and Higher Education the Institute gained first category - the highest. The conduct of technologically advanced wideranging works of high quality has been confirmed by the following documents: - concession MSWiA no. B-322/2003, - certificate of management PN-EN ISO 9001:2009 no. 206/S/2009, - certificate of management AQAP 2110:2009, - management certificate WSK no. W-93/3/2011, - certificate of NCAGE - 0469H, - 1st degree certificate of industrial safety SECRET, - 2nd degree certificate of industrial safety TOP SECRET, - 1st degree certificate of industrial safety NATO SECRET, - 1st degree certificate of industrial safety UE SECRET. Military Communication Institute comprises scientific research & development divisions, laboratories and implementation & production division. The offer of scientific divisions is presented below. Communication Systems Division Designing networks: modeling, simulations, analysis. Designing elements of modern communication systems. Testing networks, objects and communication elements. Implementation of the newest technologies and services. Analyses of developing possibilities of networks, mechanisms, protocols and services. Assuring interoperability of communication systems – NATO standards. 69 Radiocommunications & Electronic Warfare Division Integration of radio communication systems and informatics platform. Designing modern electronic surveillance systems and enabling their automatic cooperation with national and NATO command systems. Radio communications planning – radio networks planning, frequency and keys generation and distribution. Designing RF installations. Quality assessment of military objects (armored vehicles, command vehicles) in the area of communications and jamming devices installation. Usefulness assessment of individual communications devices. Testing of radio devices compliance with user requirements and military standards. Electromagnetic Compatibility Division Modeling and testing phenomena of electromagnetic information leakage. Modeling and testing channels of electromagnetic information leakage. Modeling and testing compromising emanations. Designing equipments in accordance with the EMC standards. Testing equipment in the field of: - electromagnetic emissions, - immunity to electromagnetic disturbances, - information protection, - protection against the influence of environmental hazard. C4I Systems Division Designing and implementation of communication and information infrastructure in command and control systems. Working out methods and rules of sharing information in a network-centric environment according to NEC/NCW conception. Modeling, implementation and testing of services in tactical systems which are based on the latest techniques, technologies as well as communication and information conceptions. Working out, development as well as implementation of methods and techniques of management and information security assurance in systems of information command support. Participation in domestic and international research works and experiments (structural funds, NATO RTO, EDA etc.) in respect to implementation and development of information techniques in command systems. 70 Cryptology Division Scientific research and development works in the scope of cryptography and cryptanalysis. Designing, analysis, assessment and implementation of systems for cryptographic security of information. Designing, modeling, prototyping and testing cryptographic applications and hardware equipment as well as station of generation and distribution of cryptographic data for a special needs. Participation in implementation and supervision of production of cryptographic applications and hardware equipment. Test Laboratory Group (Accreditation no. AB 149) Environmental Test Laboratory Electromagnetic Compatibility Laboratory RANDOM SEQUENCE HARDWARE GENERATOR SGCL-1MB The unit is designed for random binary sequence generation (random numbers) to be used in cryptographic devices and applications for instance: cryptographic data (keys) generation stations, ciphering devices, cryptographic systems of information protection, legally processing classified information up to Top Secret clearance level. Main features and parameters: mathematical proof of truly random binary sequence generation, random sequence generation with the speed of 8 Mbit/s, easy to use – ability to connect to PC or other similar device via USB 2.0 FS interface and collecting of random sequences under Windows, Linux or other OS, small dimensions: 75 mm x 40 mm x 25 mm, small weight < 0.1 kg, powered from USB interface < 0.5 W, auto-testing generated sequences and raising an alarm in case when the sequence does not fulfill requirements (statistical tests), the Polish Home Security Authority certificate according to the Classified Information Protection Act within the scope of cryptographic security and information protection against electromagnetic penetration (Certificate no. 300/2011/JC SKW) Applications of the generator: cryptographic systems of information protection (cryptographic keys and passwords generation, key exchange protocols), scientific applications (statistics, simulations, etc.). 71 NATIONAL INSTITUTE OF TELECOMMUNICATIONS (NIT) (Instytut Łączności) Organisation Contact Data Contact Person Data 1, Szachowa st, 04 – 894 Warsaw, Poland Director of the Institute: Wojciech Hałka, BSc phone: +48 22 51 28 100 fax: +48 22 51 28 625 phone: + 48 22 51 28 448; +48 22 51 28 fax: +48 22 51 28 726 e-mail: [email protected] Deputy Director for Research: Full Professor Wojciech Burakowski, PhD, DSc phone: +48 22 51 28 308; +48 22 51 28 239 fax: (+48) 22 51 28 625 http://www.nit.eu/ National Institute of Telecommunication (NIT) was established in 1951. NIT is a modern research & development institution operating in the area of telecommunications and information technology. It conducts development works in the scope of telecommunications networks and standardization of telecommunication systems and devices. NIT has the highest class (A) of research organization. The general mission of the NIT is to serve to the purposes of the development of information society and knowledge-based economy, to provide a scientific, research and technical support to any institutions of the state, and to perform works used in practice by entities operating in the market. In 2005, NIT obtained the status of the National Research Institute, granted to research units, which have the capacity for performing duties, especially important for planning and executing of the State policy. Since the end of the 2011 , Institute is supervised by a Minister of Administration and Digitization. NIT is located in Warsaw. It has two divisions- in Wroclaw and Gdansk. Minister of Administration and Digitization Office of Electronic Communications . Ministry of Science and Higher Education National Institute of Telecommunications Commercial Partners Other Research Institutions Telecom Operators Figure 1. NIT’s supervising and cooperating organizations 72 AREAS OF ACTIVITY The main activities of NIT are: Wired and wireless telecommunication infrastructure (access and core) Future networks and architectures, internet services Pilot and research networks Network management and data bases Cognitive radio Optical and photonic transmission systems Information, knowledge and decision support systems Spectrum management and electromagnetic compatibility Radio and TV transmission Regulation and economic aspects in telecommunications, postal services and market Metrology The key purposes of NIT are: research activities focused on development of science and practical application of research results; autonomy in the research strategy. That strategy is consistent with assumptions of the national and European economic and research policy; application knowledge and the quality of any researches to achieve and maintain a leading position in the domestic and European market; perfection in scientific activities and application of good practices, as an independent organization holding a neutral position in relation to any stakeholders; taking care of proper utilization of public funding; customer satisfaction - any information obtained from customers and results of any works performed for them are treated as strictly confidential; cooperation with research organizations and institutions thus contributing to integration of the scientific environment; active participation in creation of the European Research Area; an active part in a dialogue between the scientific environment and the general public participation in debates referring to areas of research; taking care of scientific, professional and personal development. Research problems are adjusted to the world and European trends; in particular, it is connected with the participation of the NIT in the EU Frame Programs and other European undertakings. Now, NIT employs about 250 persons, among them there is the team of scientists and experts with high competences in the field of telecommunications and information technology. NIT has a good experience, highly qualified scientific and engineering staff and tangible resources. The Institute is equipped with modern research equipment. 73 An important area of the Institute’s activity is the implementations which are often a natural continuation of research work. Implementations usually have a complex information part, which may be developed due to advanced tools and properly qualified employees of the Institute. THE ACTIVITY OF SCIENTIFIC AND RESEARCH DEPARTMENTS The Equipment and Systems Research Department conducts research in the area of telecommunications equipment and systems, particularly concerning: mobile land radio communication; radio access systems and radio local networks; point-to-multipoint and point-to-point microwave networks; satellite and radio broadcasting systems; research methods of radio equipment and systems; radio wave propagation; The Department offers services in: co-operation in research programs dealing with radio equipment and systems; expert opinions concerning radio equipment and systems, and consultancy in radio communication requirements and standards; tests of radio equipment and systems within the frequency range from 9 kHz to 40 GHz; preparation of the test plans for conformance assessment with special requirements of Directive 1999/5/EC; planning of point-to-multipoint and point-to-point microwave networks; preparation of the Notified Body Expert Opinion regarding conformity to essential requirements of Directive 1999/5/EC; preparation of technical requirements and test methodology for network equipment. The Networks and Information Society Services Department focuses on research and development in the area of infrastructure of telecommunication networks and information society services, mainly related to: planning and organizing of deployment of telecommunication network infrastructure supporting deployment of broadband platforms; implementation of European Digital Agenda in Poland; operations, administration and maintenance of telecommunication networks and systems; deployment of Next Generation Access (NGA) networks; security of telecommunication networks and services; network addressing and numbering; 74 requirements on parameters of quality of service and methods of assurance; multimedia services; integration of telecommunication and information services in corporation networks transmission and signaling protocols implementation; convergence of networks and services; co-operation with Public Administration in the areas of regulation and deployment of infrastructure for broadband access and information society in Poland; The department conducts the research on shaping the telecommunications and postal policy and regulations in Poland in the context of international experiences, with particular focus on the policies of the European Union, as well on information society and its impact on socioeconomic processes in the European Union, including Poland. The Internet Architectures and Applications Department leads investigation related to the current and future packet switched networks. The Department is conducting R&D concerning new architectures of telecommunication networks (DiffServ, Next Generation Networks, IPv6based networks and Future Internet), their protocols and applications, network services, as well as IP-level mechanisms. The Department is able to realize different scientific and commercial tasks concerning IP and post IP telecommunication networks, among others are: technical consultation concerning migration of IPv4 networks towards IPv6, including implementation and tests; research on new architectures for the Internet, including DiffServ and Next Generation Networks; planning, dimensioning and implementation of IP QoS networks directed to ensure end-to-end Quality of Service; research issues on Content Aware Networks and P2P networks; analysis of the effectiveness of new network solutions and research on scalability issues; design, implementation and tests of Future Internet networks based on virtualization of network resources; implementation and programming of hardware platforms with virtualization features; technical expertise concerning network services, protocols and technologies. The Advanced Information Technologies Department activities aim at investigating the decision support technologies for the analysis, management and design of the telecommunication networks, as well as advising in operators business plans. Researchers have performed several application-oriented projects for network operators related to data mining and planning and the optimization of telecommunication networks. Development of advanced information systems integrating telecommunication and information technologies, in particular referring to the following areas: distributed data communication systems; 75 theory of design, control and analysis of data (data mining, data warehouses) in communication networks; decision support systems, intelligent systems and knowledge management; fundamentals of telecommunication and information technologies, including mathematics application. The Wireless Systems and Networks Department - the areas of scientific activities include: digital radio communication systems including marine communications; satellite communications and systems; wireless sensor networks; modern transmission techniques; security of wireless transmission; propagation aspects of terrestrial and maritime radio communication; designing and software simulation of radio networks; utilization of wireless transmission techniques in purpose to ensure safety on land and at sea, including eCall and e-Navigation systems; measurements of quality and transmission parameters in radio networks; Department takes part in meetings of national section concerning radio communication and saving (COMSAR) of International Maritime Organization (IMO). Electronic Communications Technologies Applications and Power Systems mainly performs works related to applications of electronic communication technologies, including special purpose electronic communication systems, for the needs of state administration, public safety and rescue services. The detailed fields of interest, among others, include the following: operation of electronic communication systems and networks; characteristics and quality of telecommunication and postal services; cooperation of public and special purpose electronic communication networks; security of information, systems and communication networks, including special purpose networks; unique systems and devices for electronic communication and power supply systems. studies on application of renewable energy sources in power systems – PEM fuel cells, photovoltaic generators; studies on new electrochemical energy sources and energy storage systems for telecommunication power systems; design and testing of monitoring systems for technical infrastructure of network operators; elaboration of proprietary solutions of methodologies and procedures for the investigation of telecommunication services characteristics and quality; 76 design and implementation of computer systems and tools for analysis and testing of communication systems; design of measurement devices and special equipment applicable in operation and testing of communication systems; execution of telecommunication services quality inspection, among others using own solutions of control and measurement systems and devices; functional tests and diagnostics of failure sources of power systems, rectifiers, inverters, VRLA batteries; The Central Chamber for Telecommunications Metrology (CCTM) - the main aims are to provide measurement traceability and to conduct research on new and more accurate measurement and calibration methods. CCTM consists of the following teams: Basic Parameter Metrology Team which works on the metrology of basic parameters, such as DC & AC, LF voltage and current, resistance, capacitance, inductance and impedance and automation of measurement systems; Telecommunication Parameters Metrology Team which works on the metrology of RF and microwave signals and also transmission parameters of telecommunication networks (PDH/SDH, Ethernet, SONET etc.); Optoelectronic Metrology Team which works on optoelectronic metrology of such parameters as optical power, wavelength, chromatic and polarization dispersion, optical attenuation and optical fiber length; Time and Frequency Metrology Team which conducts works in the scope of time and frequency metrology, especially in the implementation of atomic clocks comparison algorithms, and determines timescales, accurate measurements of frequency, time, phase time, interval, TIE. Another area of interest is the diffractive optical elements for photonic purposes. In particular, the new kind of diffractive optical elements (DOE) were simulated and designed for fiber Bragg gratings (FBG) inscription. In collaboration with other research units, the new technologies of phase masks with variable diffraction efficiency fabrication for apodized Bragg gratings (AFBG) manufacturing were developed. AFBG is used in telecom (for example as optical filters or for chromatic dispersion compensation) and for sensing (discriminators) applications. An important research area is the participation in International Atomic Time – TAI and Polish Atomic Timescale – TA(PL) and implementation of new algorithms for TA(PL). The Transmission and Optical Technologies Department conducts research and implementation work on advanced optical communications. This includes research on ultra-fast transmission in optical transparent networks, wavelength multiplexing (DWDM and CWDM), optical fiber access (FTTH), non-linear optical effects, application of innovative photonic crystal 77 technologies, micro structured fibers, characterization of polarization mode dispersion (PMD), reliability of optical components and networks, design, modeling, and optimization of optical networks, implementation of optical IP networks, research on elastic optical networks, energy efficiency, and assurance of Quality of Service (QoS). The main competence is : modeling of physical constrains in optical communication systems, fiber access networks (FTTH-PON), DWDM and ultra-fast terabyte transmission with self-developed Fiber Optic Communication System Simulator; modeling, design, and optimization of modern optical communication networks taking into account the quality of service (QoS), physical layer impairments (PLI), energy efficiency (EE), and elastic spectrum assignment (SA); expertise in photonic crystal technologies, micro structured fibers (PCF) and subwavelength photonics; characterization of transmission, mechanical and thermal properties of standard and specialty optical fibers, also when subject to external factors, like temperature, aging, strain, twist etc.; consultancy and training services for operators and installers of fiber networks; this includes DWDM, CWDM, FTTH and high capacity core/metro networks, fiber optic cabling technologies for telecommunications, LANs and power networks, as well as troubleshooting and characterization of optical fiber networks and their components; conformance and certification testing of optical fiber cables and passive components, in particular connectors and patch cords to Polish and international standards; measurements of: attenuation, return loss, PMD, OTDR, environmental tests, etc.; The Electromagnetic Compatibility Department carries out research and practical expertise in the field of electromagnetic compatibility (EMC) of systems and devices, and of spectrum engineering and management based on their electromagnetic compatibility. In particular, the activities of the Department are focused on: radio network planning and optimization for radio, television, and radio communication; systems, Point-to-Point and Point-to-Multipoint systems (DVB-T, DAB+, DRM, DVB-H, UKF FM, TETRA, PMR, cellular, WiMAX, CDMA, LTE and others); radio wave propagation measurement and analysis, prediction of coverage in real interference conditions, network CAPEX and coverage optimization; digital broadcasting systems and networks development and standardization: DVB-T, DVB-T2, DAB+, DVB-H; development and standardization of new digital radio technology: LTE, Cognitive Radio, White Space Radio Systems etc.; research methods and practical analysis of electromagnetic compatibility and probability of interference between various radio systems; analysis of the availability of the radio spectrum resources, searching for new radio frequency resources destined for new radio services; 78 developing new methods of radio spectrum and interference management, spectrum engineering; evaluation of efficiency of radio technologies and possibility of their implementation; technical support for radio analyses and license assistance for radio procedures given by UKE; development of the computer system for radio networks planning, their optimization and interference/compatibility analysis; international co-operation and standardization within CEPT, ITU, ECC, ERO, IEEE; electromagnetic compatibility of electric and electronic equipment, including medical, military and industrial equipment, as well as the equipment used in mining; electromagnetic environment research, especially of special industrial environments; electromagnetic fields and their influence on people’s safety and environment protection; new electromagnetic compatibility measurement techniques; electromagnetic compatibility standardization – working for IEC CISPR and for Polish Committee for Standardization (PKN); intermodulation characteristics of radio equipment for different radio communication systems; development of specialized measuring equipment. 79 LABORATORIES 1) Testing laboratories There are two testing laboratories: Telecommunications Equipment Testing Laboratory (LBUT), working under accreditation (AB 121) granted in 1997 by the Polish Centre for Accreditation (PCA). The Laboratories perform all the necessary tests required for CE marking of telecommunications and electrical equipment. LBUT performs: testing of cable TV systems and equipment, TV transmitters and converters, digital TV equipment; conformity assessment in the area of conducted and emitted disturbances and immunity to electromagnetic field radiations, magnetic fields, electrostatic discharges, conducted disturbances, and other kinds of disturbances; conformity assessment of the equipment connected to public switched telephone network; techno-climatic tests of telecommunication equipment using climatic chambers and shaking machines (vibrating and shocking); tests of transmission parameters of single-mode and multimode optical fibers, cables and passive components. EMC Testing Laboratory in Wroclaw, accredited by the Polish Centre for Accreditation (AB 666), performs tests in four main areas: EMC measurements of equipment covered in EMC Directive, according to the standards of PN-EN series, and military equipment according to the NO standards; antennas according to the standards of PN-T series; coaxial cables according to IEC 1196-1 standard; electromagnetic field sources for safety and environment protection, according to Polish government regulations. Additionally, the Laboratory performs the following measurements: shielding effectiveness of structures, according to military NO standard; NSA measurements of open area test sites and anechoic chambers, according to PN-EN 55016-1-1 standard. The Laboratory is specialized in measurements of industrial equipment, performed on its installation site or in place of manufacturing, including equipment for use in special environments. 80 81 2) Calibration laboratories Laboratory of Electrical, Electronic & Photonic Metrology(LMEEiO) LMEEiO has accreditation certificate issued by the Polish Centre for Accreditation (AP 015). It grants claims of PN-EN ISO/IEC 17025:2005 in the following calibration areas: Basic Parameter Metrology such as DC & AC, LF voltage and current, resistance, capacitance, inductance, impedance and power and automation of measurement systems; Telecommunication Parameters Metrology – RF and microwave signals, and also transmission parameters of telecommunication networks (PDH/SDH, Ethernet, SONET etc.); Optoelectronic Metrology of such parameters as optical power, wavelength, chromatic and polarization dispersion, optical attenuation and optical fiber length; Time and Frequency Metrology - accurate measurements of frequency, time, phase time, interval, TIE. 82 The main activity of LMEEiO is the calibration of measurement equipment for telecommunication and electronic companies. The out-of-LMEEiO premises calibration service is also offered. LMEEiO extends the scope of accreditation, especially in optoelectronic, parameters of quality power and telecommunication testers and analyzers. LMEEiO using NTP server (Stratum 1), distributes precise time directly connected to atomic time standards. In 2011, LMEEiO received the following awards: Leader of Polish Market 2011 for the best specialized calibration services of measurement equipment; Euro Leader 2011 for the best specialized calibration services of measurement equipment and Europroduct 2011 for research project “Specialized calibration services of measurement equipment for a wide range of businesses” awarded by Polish Trading Society Ltd. Laboratory of EMC Measuring Apparatus in Wrocław The Laboratory has unique capability to check equipment in EMC field according to EMC Directive requirements. It is the only laboratory in Poland of that kind and to some extend in Europe, which is completely independent from producers of equipment. The Laboratory, basing on its modern calibration equipment and highly qualified personnel, is authorized to check and calibrate (also according to standard EN 55016 –x-x series) the correctness of the following measuring apparatus used in the measurements of the disturbance emission levels: radio interference meters, power meters; artificial mains networks (AMN); MDS clamps, antennas; test signal generators used to check the radio interference meters and click analyzers, voltage and current hf probes; coupling/decoupling networks (CDN; ESD generators according to EN 61000-4-2, EFT/B generators according to EN 61000-44, surge generators according to EN 61000-4-5. 83 3) Unit for Inter laboratory Comparisons (JPM) The JPM holds accreditation issued by the Polish Centre for Accreditation (PT 001). JPM grants claims of PN-EN ISO/IEC 17043:2011. The Unit organizes Proficiency Testing and Inter laboratory Comparisons programs for laboratories in the area of LF electrical DC & AC parameters. The Unit meets the requirements for the competence of providers of proficiency testing schemes and for the development, and operation of proficiency testing schemes. 4) Within the Institute operates Notified Body No 1471 under Directive 1999/5/EC (R&TTE Directive) and offers consultancy services concerning technical requirements and standards. 84 RESEARCH PROJECTS 1) Projects supported with the European Regional Development Fund: Innovative Economy Operational Program 2007-2013 Within the scope of this program several projects have been done in last years: Information system concerning broadband infrastructure and the “Broadband Poland” portal –SIPS (2009-2013). The aim of this project is to create countrywide data communication infrastructure which will support state and local authorities in the management and coordination of projects related to building regional broadband networks, both core and access, in the area where intervention is necessary. New generation of equipment for VRLA battery inspection in telecommunication power supply systems (2009-2011). The goal of this project was to build a prototype of new generation equipment – TBA160-IŁ. The purpose of this equipment is an effective checking of batteries sets, which should result in the improvement of energetic safety in telecommunication sector. Computer platform for propagation analysis, electromagnetic compatibility and optimization of wireless networks in telecommunication and data communication systems – PIAST (2010-2013). The aim of the project is to develop and establish the full computerized software system (including hardware clients - server architecture) which can be used by NIT experts for research and business activities, academic institution for educational purposes, and other companies or individuals accessing to the project Web page for tutorial and other commercial reasons. In 2011, the project received Award of the Ministry of Science and Higher Education . Future Internet Engineering (2010-2012). The aim of the project is to develop and test a proposal for a new architecture based on resource virtualization with new mechanisms and algorithms for achieving different packet transmission techniques (packet switched, circuit switched, content-oriented) over one common platform. The project also sets itself the goal of promoting IPv6 start in Poland by creating a national network of environmental testing for the IPv6 Internet and extending the so-called “good practices” in IPv6 implementation. Human Capital Operational Program 2007-2013 Improvement of competitiveness of electronic trade enterprises (2009-2010). The project was realized in consortium with Polish Chamber of Commerce for Electronics and Telecommunications. 85 2) National projects funded by Ministry of Science and Higher Education: Next generation data communication services and networks – technical, application and market aspects (2008-2010). The goal of this project was to prepare tools and procedures enabling the implementation of solutions which are necessary for the state and selfgovernment development and being competitive on the market. NIT has played an important role in several subjects: decision support systems, electromagnetic compatibility, traffic management in IP nets, metrology and monitoring, digital radio networks, design tools and methods. Differential modeling for use in marketing and biomedical investigations (2010-2012) The aim of this project is to develop methods of differential modeling, which means modeling of differences between objects belonging to two groups: experimental and of reference one. Interdisciplinary system of interactive scientific and technical information – SYNAT (2010- 2013) is realized in the framework of Strategic Research Program. The aim of the project is to develop integrated computer platform of the national system of scientific and scientifictechnical information. The platform will enable realization of infrastructure development programs of scientific information resources, scientific and academic communication systems, and simultaneously it will become the development base of integral structure of collecting, making available and developing national scientific and educational contents, and documentation of cultural heritage. PaCal – a library for arithmetic calculations on random variables (2009-2011) The PaCAL project (ProbAbilistic CALculator) aims to develop a library for arithmetic with random variables. The library hides all implementation details such as interpolation of probability densities and numerical integration needed to perform the arithmetic. It is easy to obtain moments, quantiles, confidence intervals, etc. from the resulting distributions. A prototype of perimetric protection system of telecommunication critical infrastructure – SPOT (2010-2012). The aim of this project is to provide operators of telecommunication networks with a versatile system enabling effective protection and security management of their infrastructure, in particular copper and fiber cable networks. Prime issues are: protection against theft of copper cables and related damage to network facilities (cable cuts, destruction of manholes, etc.) resulting in service disruption and costly repairs, and effective, centralized real-time monitoring of cable infrastructure to improve network security and quality of service. Mobile laboratory for functions and quality testing of electronic communication services to be used by command and communication teams (2010-2012). The general aim of the project realized with Military Communications Works is the improvement of telecommunication networks efficiency, especially the networks that are important for public security. Final product of the project will be a prototype of mobile laboratory designed for operation in real environment in which the services are utilized. Methodology development for evaluation of the in-vehicle emergency call system (eCall) (2009-2011). The aim of this project is to develop a simulator of eCall device, and to test the 86 correctness of eCall messages (MSD/FSD) transmission via cellular networks to alarm 112 number centers, with respect to conformity with proper standards and specifications. Research and development of timescale ensembles in Database for TA(PL) – RATAPL (2011-2013). The aim of this project is to develop and implement a new timescale algorithm based on NIST AT2 algorithm. The project requires analysis of algorithm theorem to adjust it to small remote group of time standards. After the set of tests, the best solution should be chosen for normal operation. Development of method of automatic acquirement and real time presentation of content destined for local service suppliers operating in networks of interactive digital television (2011– 2013. The aim of the project is development of new methods, which enable wide introduction of interactive services for use by medium, small and micro enterprises, and in this way by significant groups of citizens. Modelling and optimization of elastic optical networks for 100+ Gbit/s – ESO (2011– 2014). The project concerns the design of elastic optical (fiber) communication networks that are a successor of the current DWDM networks and they are able to support efficiently the multi-rate and huge-bandwidth (100+ Gbit/s) connection provisioning in current, and next generation Internet networks. 87 3) European projects realized within the scope of COST Actions NIT participates in the following COST Actions (European Cooperation in Science and Technology Actions): COST Action MP0702 – Towards Functional Sub-Wavelength Photonic Structures (2008-2012) The main objective of the Action is to establish active links between European laboratories working in the field of artificial materials for photonics applications where the structural dimensions are at or below the wavelength of light. COST Action IC 0804 – Energy Efficiency in Large Scale Distributed Systems (2009– 2013) The main objective of the Action is to foster original research initiatives addressing energy awareness/saving and to increase the overall impact of European research in the field of energy efficiency in distributed systems. COST Action IC 0905 – Techno-Economic Regulatory Framework for Radio Spectrum Access for Cognitive Radio/Software Defined Radio – TERRA (2010–2014). The main objective to bring together regulatory, technical and economic experts for spearheading a regulatory break-through for European development of Cognitive Radio and Software Defined Radio (CR/SDR) technologies. COST Action TD 1001 – Novel and Reliable Optical Fibre Sensor Systems for Future Security and Safety Application – OFSeSa (2010–2014). The advantages of such sensors are well known, but there is a number of identified technical problems to be resolved. By supporting collaboration of experts from multidisciplinary fields to share their knowledge in sensor development and system design, together with developing characterization and validation procedures, these problems may be addressed and new generation of optical fiber sensor systems can be realized. 88 4) Other international projects EfficienSea – Efficient, Safe and Sustainable Traffic at Sea (2009-2012). The project financed by European Regional Development Fund is realized in a consortium gathering 16 partners from six countries around the Baltic Sea. EfficienSea is an Interreg project aiming at improving the Baltic Sea with focus on the environment and the safety of navigation. Functional state evaluation system with distributed intellect for elderly and disabled population–EDFAS (2009-2012). Project realized within EUREKA in a consortium of 6 institutions from Lithuania, Germany and Poland led by the Institute of Cardiology of Kaunas University of Medicine. The goal of EDFAS project is to develop a system for monitoring and multilevel complex evaluation of heart function and motion abilities for the elderly and the disabled. Collaborative Project ALICANTE– Enlarge MediA Ecosystem Deployment through Ubiquitous Content-Aware Network Environments– Enlarged EU (FP 7)(2011-2013). The aim of the project is to provide content-awareness to the network environment, network and user context – awareness to the service environment, and adapted services/content to the end user for one’s best service experience possible. INTERNATIONAL BILATERAL COOPERATION Apart from the participation in the projects listed above, the Institute’s experts have cooperated with a number of foreign research organizations, as follows: University of Stellenbosch, Republic of South Africa, joint book in preparation; Brock University, St. Catharines, Ontario, Canada, joint publications; University of Catania, Italy, joint publications; Abdus Salam International Centre for Theoretical Physics (ITCP), Trieste, Italy, research co-operation; International Institute for Applied Systems Analysis (IIASA), Austria, knowledge engineering, knowledge management, joint publications; Instituto Superior Técnico, Lisbon, Portugal, joint research and publications; Universitat Politècnica de Catalunya (UPC), Barcelona, Spain, joint research and publications; University of Nottingham, George Green Institute for Electromagnetics Research, UK, Honorary International Advisor, joint research in sub-wavelength photonics; Royal Institute of Technology KTH, Stockholm, joint organization of ICTON 2011; School of Engineering, University of Warwick, preparations to ICTON 2012; Université d’Angers, France, joint research in sub-wavelength photonics; Institute of Command Engineers, Minsk, Belarus, joint research in microstructured fibres; State Engineering University of Armenia, Erevan, joint research in nanoplasmonics; Universitat Politècnica de Cartagena (UPCT), Spain, joint research and publications; Centre Tecnològic de Telecomunicacions de Catalunya (CTTC), Castelldefels, Spain, joint publications; 89 The International Union of Radio Science (URSI) - activities of URSI Commission D: Electronics and Photonics; NIT cooperates with some partners from Asia Region: 1. Scientific cooperation with Japanese Research Institutions started when professor Andrzej P. Wierzbicki worked during the years 2004-2007 as a research professor at the School of Knowledge Science of Japan Advanced Institute of Science and Technology (JAIST) in Nomi, Ishikawa This joint research concerned creative processes in science and technology, computerized support of decision making and creativity, impacts of informational revolution on science and technology. It resulted in many publications (books 2, chapters in books 4, papers in scientific journals 14, papers at international conferences 39) but also in the official bilateral agreement on research cooperation between NIT and JAIST. Within this cooperation, many bilateral research visits were made and further collaborative research output was produced (chapters in books, scientific journal papers, conference papers etc.). The cooperation of NIT with Japan focuses mostly on joint work with JAIST, but there are also many other Japanese research institutions - such as Kyoto University, Tsukuba University, Hiroshima University, etc., to which this cooperation is extended. 2. In 2011, Bilateral Co-operation Memorandum of Understanding between Korea Electronics Technology Institute located at #68 Yatap-dong, Bundang-gu, Seongnam-si, Gyeoggi-do and National Institute of Telecommunications was signed. The parties have identified the following cooperative areas in Research and Business Development Activities: Electronic Communications Technologies, Wireless Network Research, Transmission and Optical Technologies. Signing Ceremony of NIT – KETI Co-operation MoU, President of KETI Mr. Pyeing Rak Choi and Director of NIT Mr. Wojciech Hałka, Warsaw, March, 2011 90 MAIN PRODUCTS 1) Information System for Broadband Infrastructure Inventory (SIIS). The practical implementation of the SIIS is developed in the NIT. Production phase of this system started in March 2011, and it was used by more than 9000 telecommunication companies and other entities for telecommunication infrastructure inventory designated for the Electronic Communication Office (UKE). The official report announced by the President of UKE in June 2011 noted that more than 350 thousands of telecommunication objects registered in SIIS system (lines, cables, fibers, buildings, cabinets, radio stations and masts, collocation places, etc). The aim of this project is to develop an useful IT tool for telecommunication investments planning and its optimal realization. The project is still on-going and will be continued in 2012, with the aim to develop next user friendly interfaces, for all parties involved in the inventory process and investments projects, based on infrastructure visualization on digital maps, and with some GIS applications. Awards: Distinction as the Product of the Year 2011 - Solution for Operators, XIV Grand Gala of Gold Antennas in Warsaw. 91 2) TBA160-IŁ – Device to Control Telecommunication Power Systems VRLA Battery of the Designations: S – power system; Od – load; B1 – controlled battery; B2 – second battery; b1, b2 – battery fuses/disconnectors; TP – optional intermediate board; E – energy from discharged battery (5% in form of heat, 95% to the load of power system); GSM – communication by means of SMS; LAN – communication by Internet. TBA160-IŁ is designed to controlled discharging and charging the lead-acid batteries, especially of VRLA type – Valve Regulated Lead Acid, in telecommunication sites. During the work in such sites, a telecommunication equipment is supplied by power system, and the energy taken from discharged battery is fed to the supplied equipment, decreasing temporally the current drawn from rectifiers of power system. TBA160-IŁ makes possible programming test cycle, namely equalizing charging, controlled discharging, as well as return charging of batteries in telecommunication site. The connection of the device to controlled battery (separated from power system), programming tests, and after the tests sending results (LAN, memory SD) to PC and the restoration the previous arrangement of power system is the operator's task. TBA160IŁ offers (for the 24 V, 36 V, 46 V, 48 V or 50 V battery disconnected from power system during test): - discharging of single battery with set current (up to 160 A) on loads of power system, while at the same time the second (or remaining) battery is in float operation in DC power system; - discharging of battery with use of internal resistors; - return charging of previously discharged battery with set current (up to 160 A); - periodic equalizing charging of the battery, with set boost voltage; 92 - the realization of test sequence composed of the discharging – charging, alternatively preceded by equalizing charging, without part of the operator as well as the remote notifying (Internet, GSM network) the operator of the end or break of process. Patent: PL 204773 – “The measuring system for two batteries in telecommunications DC power systems” and four solutions submitted (under procedure). Awards: 1. Polish Market Leader 2012 and Distinction of Euro Leader 2012 93 2. Gold Medal at International Electronic Communication Fairs in Łódź 2011. 3. Silver Medal at 39 Salon International des Inventions in Geneva and Medal of Russian House for International Scientific and Technology Cooperation, (2011). 94 4. Gold Medal on 22nd International Invention, Innovation & Technology Exhibition, ITEX 2011, Kuala Lumpur, and Iran Special Distinction. 5. Gold Medal on Korea Invention Promotion Associaton in Seul (2010). 95 3) PM356 Test Probe for Measurement of Communication Services Parameters Interfaces PSTN - 3 ports Ethernet 10OBASE-TX - 2 ports The measured parameters Call setup time Unsuccessful call ratio Speech connection quality Fax connection quality GSM/UMTS - 2 ports, 7 switched SIM card Data transmission speed achieved Unsuccessful data transmission ratio Outages rate for SMTP and POP servers Outage rate to a set of designated sites PM356 is designated for automatic measurement of communication services parameters. It is a part of quality testing system for public communication services (AWP-IŁ). It performs the measurements according to an ordered plan, collects the results and transfers them to test center. PM356 is equipped with interfaces allowing the measurements of broadband Internet, PSTN and GSM/UMTS networks. Communication with test center is supported via Ethernet VPN or GSM/UMTS control links. In broadband Internet the test probe can perform the measurements of accessibility and throughput of downlink and uplink, packet latency, voice quality (VoIP), accessibility of selected servers. In PSTN and GSM/UMTS the test probe measures an effectiveness and time of call set up, voice quality, fax transmission quality. There is a possibility to measure call set up parameters and voice quality in different network connections, like PSTN↔GSM/UMTS, GSM/UMTS↔VoIP. Test plan is prepared by system administrator and the plan could include different test cases according to the needs. Test planning software excludes interferences between the test probes during their activity. 96 PM356 and the whole public service quality testing system (AWP-IŁ) are dedicated for telecom network operators and telecom regulators. AWP-IŁ is used by Electronic Communication Office since several years. Awards: 1. Silver Medal at 40. Salon International des Inventions, 2012, in Geneva. 2. Distinction at XXIII International Electronic Communication Fairs in Łódź 2012. 97 4) Tool for Technical Quality Assessment of Telecommunications Network (AWP-IŁ System). The system created and developed in NIT is a countrywide system for telephone calls quality measurement (voice, facsimile and data), used by Office of Electronic Communications (UKE) for monitoring of the quality of operators services. The system, continuously extended and improved since 2000, consists of ca. 800 measurement units connected as PSTN and GSM subscribers in more than 500 access points. It monitors the networks of all major operators (mobile and fixed) in Poland. The system measures the quality indicators of circuit switched network now, and will cover IP networks in the future. In 2011, a new universal test probe, covering IP networks was developed. The system is scalable and may cover up to 50000 probes. Awards: Bronze Medal 2010 at International Warsaw Invention Show 98 5) Mobile Testing Laboratory of Electronic Communication Services Functionalities and Quality for Command and Communications Teams (MLB) MLB is a set of test equipment placed in special car consisting of radio scanner, set of user terminals (telephones, modems), spectrum analyzer and radio communication device tester. MLB executes test suites while driving or at short stops. It allows making radio communication services testing in the field or in the user specific location, and in the conditions similar to these where the services are really used. It should support in provisioning of sufficient quality level of communications, especially for the crisis management services, rescue services, dispatchers and other services in public safety area. The aim of MLB is to evaluate functioning and quality of professional mobile radio communication services, especially provided by TETRA standard networks and other networks used in professional radio communication. Its functions include preparation and execution of test and measurement process, collection processing and reporting of test and measurement results, assurance of ability to standalone activity in the field, during move and at stop. Testing of service functionality and quality in networks: TETRA, DMR, GSM, UMTS, as well as execution of radio measurements needed for service evaluation. 99 6) Cable Monitoring and Protection System (SMOK-2U System), SMOK-2U fulfills the tasks related to monitoring, anti-theft protection and supervision of copper cable network. The equipment provides an effective protection against theft of communication cables within 10 km radius. Automatic alert to security personnel is able in 2 seconds. Installation of additional cabling along protected telecommunication line is not necessary. It can be quickly installed and set up. The system provides an easy integration with existing security systems. The system was developed and deployed in operators networks since 2007. Awards: 1. 2. Polish Market Lider 2008 in category: Product Silver Medal 2010 at International Warsaw Invention Show 100 7) Click Analyzer ACA-4c. DESCRIPTION Click Analyser ACA-4c enables the analysis of the time and amplitude parameters of discontinuous disturbances (clicks), according to CISPR 14-1 and CISPR 16-1-1 ( EN 55016-1-1 and EN 55014-1). QP values of disturbance (dynamic range up to 44 dB), number of clicks, their duration, duration of pauses between them, grouping of clicks in specified time intervals, and the mean value of the frequency of their appearance, are analysed. Click Analyser ACA-4c has four complete, independent measurement channels tuned to frequencies determined by standard (or by user – option). Each of them consists of an RF attenuator, a mixer, an IF filter with 9 kHz pass-band, an IF envelope detector, and a quasi-peak (QP) detector. It can, therefore, conduct the measurements simultaneously on four different frequencies. SPECIFICATIONS Parameters: according to the newest version of CISPR Publ. 16-1-1, Disturbance evaluation: the quasi-peak value according to CISPR Publ. 14-1 Number of measurement channels: four acting simultaneously tuned to frequencies: 150 kHz, 500 kHz, 1400 kHz, and 30 MHz (predetermined by newest version of CISPR Publication and appropriate EN standard) or on other frequencies according to customer specification (option) Level of analysis: any level from the range of 40 dB/V to 100 dB/V, with 1 dB increment Input impedance: 50 Recorded events: QP value, time of appearance, duration and QP values of disturbance which exceed the level of analysis Memory capacity: up to 4000 events (for four channel) Registered results of analysis: - number of clicks t 10 ms, - number of clicks 10 ms < t 20 ms, 101 Measurement channels are equipped with their own RF attenuators what allows to set the analysis level independently (individually) for each frequency channel. The measurement results are recorded in the internal memory of the instrument. They may be: reviewed directly on the own display, printed out in the form of a report, on a printer connected through the parallel connector, - number of clicks 20 ms < t 200 ms, - number of clicks 200 ms < t 600 ms, - time of measurement, - number of switching operations, Presentation of results: - on alphanumerical LCD - on printer - on external PC by serial fiberoptic interface (option) Dimensions: 350 x 150 x 350 mm Weight: 9 kg transmitted through the serial fiberoptic interface to the external PC for further processing (option). Institute so far has sold Click Analyzer to laboratories in Poland, Germany and Japan. More information about NIT’s products at http://www.nit.eu/offer 102 TELE& RADIO RESEARCH INSTITUTE (Instytut Tele – i Radiotechniczny) Organisation Contact Data 1, Ratuszowa st, 03 – 450 Warsaw, Poland phone: +48 22 619 22 41 fax: +48 22 619 29 47 http://www.itr.org.pl/en/welcome/ The Tele & Radio Research Institute continues the scientific traditions of two institutes of long history, leading in the field of electronics and power engineering: the Radio Research Institute – the first in the country scientific-research centre with electronic profile, established in 1929 by eminent Polish radio-electronic engineer, professor Janusz Groszkowski and the Industrial Institute of Electronics – established in 1956 by Prof. Wiesław Barwicz from the Central Laboratory for Electronics. The basic objective of the Institute is to create new solutions in the field of electronics and to transform them in to innovations for partners interested in manufacturing modern and competitive products. More than 70% of Institute annual turnover is acquired directly from the commercialisation of the research results. The object of Institute activities consists of carrying out scientific research and development work as well as adapting their results to practical applications. The research work is carried out in specialized centres, subordinated to priority directions of Institute activities in the field of: advanced electronic materials and technologies, ICT systems and hardware applications, systems for technological processes automation, thermo-chemical processes, vacuum technology. 103 The research projects followed by the ITR are inscribed in the objectives set by the European Union and the strategic areas specified by the National Framework Programme. The Institute’s R&D strategy is concentrated on: carrying out the key projects in the domestic and European innovation system through comprehensive, multidisciplinary research and development works, creating new solutions in the field of electronics and converting them into innovations for business entities, putting into life research projects and research and development projects of technological and IT nature playing a key role in satisfying the needs of the modern economy. The research has been channelled into the two priority directions: intelligent ICT systems supporting decision-making for the controlneeds of complex industrial infrastructure systems, integration of advanced electronic technologies for industrial applications. The Tele & Radio Research Institute carries out research within the European Research Area, implementing a number of scientific-research and development projects, including: Independent intelligent ICT network for e-diagnosing of power distribution grids IT platform of databases for effective use of research work results A new generation of switching devices for medium voltage electricity distribution Large laboratory plasma chemical reactor as an integral part of the plant for waste disposal using a pyrolytic-plasma method GDMS profile analyser Microrobot for point soldering with a visual system for positioning and soldering quality control, for applications in automated lines for electronic components assembling Experimental technology for resistive and capacity elements instalation within a printed circuit board Technology of new generation sensor of hydrogen and its compoundsfor applications in supra-standard conditions Forming soldered joints of QFP, PBGA and CSP components in fields with microholes A new generation of lead-free soldering pastes with the addition of metal nanopowders and carbon nanotubes A new generation of energy saving electric drives for pumps and fans for the mining industry Powder magnetic circuits in universal electric drives 104 1. New materials and electronic Technologies One of priority directions of the researeh carried out now comprises issues related to manufacturing of electronic components by means of printing technologies using polymer materials and nanocomposites (printed, flexible organic electronics) The research concentrates, inter alia, on: using organic LED technologies to build alternative light sources, developing a technology for an organic photovoltaic cell manufacturing, manufacturing and using printed RFID antennas for broadly understood identification purposes. Main directions of our research in the field of nanotechnology are related to the synthesis and characterisation of carbon nanomaterials (carbon nanostructures, doped with metals) for applications in micro- and optoelectronics and in sensorics. The work carried out is related to: technology of carbon-palladium layers for applications in hydrogen and hydrogencontaining gases sensors (deteH project – IEOP), technology of carbon-nickel layers (including also containing carbon nanotubes) for applications in field emitters (NanoCafe project – MNT ERA Net), technology of metamaterials based on carbon nanostructures for optoelectronic applications (project in the COST action). We have first-class specialised testing equipment enabling performance of materials characterisation. We perform tests of a wide range of materials used in electronic components assembling, including substrate materials and technologies of very high integration level. In cooperation with domestic and foreign research centres we have been developing a new generation of leadfree. soldering pastes with the addition of metal nanopowders and carbon nanotubes for soldered joints of improved mechanical and electronic properties. 105 Our long standing research experience is used in: innovative technologies of printed circuit boards manufacturing multilayer with internal and blind holes, microwave, rigid, flexible, rigid-flexible, applied in the equipment used in space research, electronic assembling on rigid and flexible substrates, highly advanced components containing miniature flip-chip type components with 0.5 mm terminals arrangement raster and R/C 0201 components, technologies of electrochemically coated wires: highly-solderable tinned copper, nickelplated steel, from nickel-plated copper alloys (brass and others), of special properties. The research work in the field of magnetic materials is related to: magnetic elements manufacturing technology using the method of binding magnetically hard or soft powders by means of a plastic, magnetising technology for bi- and multi-pole permanent magnets with diversified configuration of magnetic poles, spatial and time simulation and analysis of electrical machines and equipment electromagnetic fields, distribution of magnetic induction in an electric machines air gap, applications of powder magnetic components in electrical machines, sensors, bearings, magnetic clutches and holders, studies on operating parameters of small electrical machines. Offer concerning collaboration with institutions from the far east countries: We manufactured : cylinder, ring, cuboid-shaped and segmented permanent magnets in Nd-Fe-B alloys. We perform bipolar and multipolar magnetization of magnets, offering a diversified configuration of magnetic poles. We also manufacture magnetically sof components of magnetic circuits in iron powders , in customer – specified shapes and sizes, for application in stable and variable magnetic field, up to a few kHz. 106 We offer mounting of electronic components in following procceses: single –sided and double-sided surface mounting , mounting of threaded components. We also offer comprehensive services covering: design of electronic packages, execution of PCBs at the Center for PCB Process Innovation, testing of PCBs as er the requirements by the Principal, purchase of components (assemblies) for mounting , mounting (SMT, THT), Templates for paste application. We offer a new generation of the hydrogen and hydrogen compounds sensors for applications in above normative conditions and LPG, ammonia sensors. 107 2. Information technology The work in the field of ICT technologies and systems comprises: designing and testing specialised microprocessor equipment, testing and analysing digital and analogue measuring systems, measuring techniques using digital processing of signals, methods for monitored objects control, protection and diagnostics, comprehensive implementation of algorithms for manufacturing processes supervision and control, technology of logic functions flexible programming by the user, automated stands for ICT systems testing, comprehensive systems for scattered objects monitoring and remote control, fibre optics technology, transmission protocols, computer networks, ICT networks for remote diagnosing of power facilities of distributing grids. The Institute is performing research work aimed at development of Smart Power Grids, improving efficiency, reliability and safety of the chain of power supply. Components of Smart Grids developed at the Institute shall find application in following areas: IT systems integrating suppliers and recipients of energy, monitoring and analysis of energy quality, control and protection systems, integrating accumulators and dispersed sources of renewable electric energy, e- diagnostics of power grids, automatic redundancy switching in uninterrupted power supply systems, methods for time synchronization of facilities and remote control of stations, advanced sensors and unconventional transducers. Long-standing research experience provides the Institute with a competitive position in the field of systems and equipment implementation in niche areas of the power industry. In the last decade this allowed developing and implementing: 108 a few thousand universal protecting devices in medium and low voltage networks, computer monitoring and supervision systems, signal converters and concentrators for communication systems needs. Our studies applied in energy switchgears substantially increased the reliability of industrial power systems operation (in Siberia oil fields, in power plants, mines, steelworks, sugar factories, CHPs and others). Offer concerning collaboration with institutions from the far east countries: We offer: components for smart power grids bay controllers for SV, MV switch gears comprehensive monitoring and remote control software systems targeted at distributed facilities. SCADA type software, communication software. Embedded software for process automation and measurement systems. Communication system diagnosis. Power protection relays. 109 3. Advanced technologies and electronic devices The work in the field of excitation and propagation theory of volumetric and surface acoustic waves in piezoelectric materials carried out for a few decades determine the Institute’s leading position in Poland in the research on: high-stability quartz generators for special and space applications, piezoelectric components, inter alia resonators, reference time and frequency sources synchronised with signals from GPS and Galileo systems, measurements of long-term stability of frequency sources and phase noises, measurements of quartz generators thermal characteristics. As the only in Poland research centre, the Institute develops and manufactures quartz generators of the highest stability, used in time and frequency standards. The research carried out for many years on ultrasonic phenomena and the experience possessed allow developing and implementing. Ultrasonic generators and converters and also advanced technologies and devices based on the ultrasonic technology: for welding plastics, non-ferrous metals foils, unwoven filtration fabrics, for mixtures emulsification and disintegration. The ultrasonic bonding technologies developed at the Institute have a huge impact on the innovation of technological and manufacturing processes in various industry sectors because of elimination of solvents, reduction of energy consumption and of operation time 110 One of the Institute’s top priorities is activity in the field of medical diagnostics pursued in collaboration with medical research centres. The works include: biomedical signals testing and analysis, image analysis and recognition methods for medical diagnostics, notably acquisition and digital analysis of radiographic bone images, research on application of ultrasound technologies for dispersing remedies and aerosol generation, method of piezoceramic transducers excitation used in ultrasound dispersing devices, designing the diagnostic and specialised medical apparatus, testing of particulate mater in urban environment and in working place environment using cascade impactors, spectrometric analysis of elemental composition of particles. In the consequence of the works in ITR was developed specilized apparatus for: inhalation with dosing and visalisation, assessing the visual acuity of retina of persons suffering from cataract, diagnosing breathing disorders in sleep, automated evaluation of bone age and degree of osteoporosis’ advancement, acquisition and analysis of tremometric signals distinctive for Parkinson’s disease. Offer concerning collaboration with institutions from the far east countries: ultrasound generators and transducers ultrasound technologies and equipment for surgical tools and filters cleaning plastic laminate sealing technology and equipment ultrasound washing devices featuring different capacities and frequencies ultrasound kits for sealing parts in the kinescope production line concentrates for preparing wash baths other ultrasound cleaning and sealing devices 4. Industrial process automation systems Research and development of process automatization in industry and personal health diagnosis activities, with application of ICT and measurement technologies. The Centre activities have been concentrated on Automatic Optical Inspection and other vision systems development, medical personal diagnostic systems for personal applications in clinic and home environment, signal and image processing, methods and tools for characterization of electric, electronic and optoelectronic components and systems, design and development of complex mechatronic systems and equipment for industrial processes automatizationon, development of software systems for process control, monitoring anddiagnosis, development of auto-calibration and diagnostic methods and tools. 111 Offer concerning collaboration with institutions from the far east countries: The leading subject matter of scientific-research and development work of the Institute in the field of technological processes automation comprises: measuring-IT methods and systems for research, industrial and medical diagnostics applications, wireless distributed measuring systems, automated mechatronic systems for technological processes monitoring and controlling, equipment for products batching, packaging and labelling, optical automated inspection systems, methods and systems for non-electric quantities measurement and control. 5. Thermal and Chemical Processes For a few decades the Institute has been carrying out R&D work in the field of thermo-chemical equipment for research, manufacturing and measurement purposes. In particular, for semiconductor, materials engineering, cokemaking and metallurgical sectors. The unique apparatus developed recently at the ITR is designed inter alia for: monocrystallisation of silicon carbide, which is a semiconductor material of the future, high-temperature uniaxial pressing, for new ceramics testing and manufacturing, determination of solid fuels parameters, especially: sulphur and carbon content in solid fuels, determination of ash and volatiles content in coal, determination of coal self-ignition factor, determination of blast furnace coke parameters, 112 testing coal blends in the process of coking, testing iron ores parameters, temperature sensors calibration. The equipment developed has been applied in Polish leading research laboratories and enterprises as well as in companies of many European (Bosnia and Herzegovina, Czech Republic, Romania, Serbia, Slovakia, Hungary, United Kingdom), Asian (Kazakhstan) and African (Algeria) countries. Recently the largest customers for ITR thermo-chemical equipment include global metallurgical corporations ArcelorMittal, US Steel, Corus and Donbas Industrial Union. Offer concerning collaboration with institutions from the far east countries: Design of the thermal systems for solid fuels parameters measurements for combustion optimatization purpose. 113 6. Vacuum Technology TRRI research on vacuum technologies is the continuation of research by Industrial institute of Electronics, which used to be among the major research and development institutions in the country, developing and manufacturing modern components and high-vacuum devices. Interdisciplinary research by the Institute in the area vacuum technologies is presently focused on research of vacuum chambers, EB technology, mass spectrometers and composite layers technology. Major areas of the research in vacuum technologies, based on long-term research programme, are development and implementation of: vacuum components, such as extinguishing chambers, insulators and ceramic and metallic bushings; very high vacuum components, such as process manipulators, vacuum locks, slider valves of getter pumps; high and ultra-high vacuum instruments, such as EB welders, EB furnaces, quadrupole mass spectrometers, MBE devices. interdisciplinary research by the Institute in the area vacuum technologies is presently focused on research of vacuum chambers, EB technology, mass spectrometers and composite layers technology. Utilization of vacuum as an internal insulator with high voltage strength is the most important feature of vacuum extinguishing chambers. Vacuum technology developed by the Institute and adopted in extinguishing chambers guarantee full separation of electrical arc from the environment, and the absence of waste products of arc extinguishing medium. The Institute has vast experience in researching electron beam (EB) technologies, both with regard to construction of instruments and development of technologies related 114 mostly to EB welding in vacuum. Research is in progress on the new method of deflecting electron beam, which shall ensure high range of frequencies and amplitude of deflection, and methods allowing to obtain identical conditions for electron emission throughout the whole lifecycle of the cathode. Innovative solutions in mass spectrometry also vouch for development of vacuum technologies by the Institute. The Institute is also developing and building mass spectrometers for analyses of elemental composition of rarefied gases, solid surface analyses, and profile analyses of multilayer structures with depth resolution less than 1 nanometer. Offer Concerning collaboration with institutions from the far east countries: vacuum components, such as extinguishing chambers, insulators and ceramic and metallic bushings; very high vacuum components, such as process manipulators, vacuum locks, slider valves of getter pumps; high and ultra-high vacuum instruments, such as EB welders, EB furnaces, quadrupole mass spectrometers, MBE devices. 115 7. Laboratory for Quality Testing and Calibration of Electronic Products Laboratory for Quality Testing and Calibration of Electronic Products has been awarded Accreditation Certificate by Polish Accreditation Center (PCA), in confirmation of competence, independence and reliability as research laboratory. The basic area of Laboratory business is functional, ambience exposure, mechanical exposure, and electromagnetic compatibility tests as well as user safety tests of selected electronic devices, such as components of alarm systems, e.g. sensors, central units, signallers, data transmission systems, access control systems, power supply units; measuring instruments and laboratory equipment; computer systems and ETO equipment; organisational and engineering machinery and equipment for office work; consumer electronics equipment. The area of scientific research covers problems of metrology, diagnostics and reliability of electronic devices, as well as electromagnetic compatibility of electronic and electric devices. The area of R&D work covers developing methods for testing and measurements, guaranteeing their repeatability and/or reproducibility, developing functionalities of laboratory control and measurement systems, with regard to both hardware and software, and developing computer 116 assisted diagnostic systems for control and measurement systems, and controlling the quality of production process. Laboratory activities combine theoretical and empirical research with practical implementation of research results, by offering services in following areas: quality testing of electronic equipment; automating measurements and tests in production process; designing computerized electronic systems and dedicated software; 117 8. Scientific Achievements The Institute’s performance proves that the actions taken are efficient and contribute to the effective use of the resources possessed in order to pursue the subjects and tasks in consistency with the needs of economy and to maintain the Institute’s eminent position among scientific units with recognised competences in the field of advanced electronic technologies and ICT systems. A tangible and effective outcome of such actions are several dozens of projects undertaken each year by the Tele and Radio Research Institute under its statutory activity, internal research projects, development projects, EU and international projects, earmarked and development projects and grants. The activity and the efficiency of the actions taken is signified in particular through the funds granted to the Institute for implementing EU structural projects financed under operational programmes: The experimental technology of constructing resistive and capacitive parts inside printed boards, Developing a technology for a new generation of hydrogen sensors and its compounds for use in non-standard conditions, An intelligent automatic ICT network for the e-diagnosing of power distribution systems, Developing a new generation of MV electricity distribution switches. In the field of practical applications, the Institute is handling a number of large innovative contracts every year for retail customers concerning the development and supply of prototypes for process lines, equipment and components. A measure of the Institute’s scientific achievements are publications in reviewed domestic and foreign magazines, monographs, conferences held and multiple patents, placing the Institute amongst the leaders of all the domestic scientific institutions. The results of the Institute’s works are highly esteemed in the international arena, as exemplified by, in particular, numerous awards, honourable mentions and medals at prestigious invention exhibitions (Concours-Lepine, Brussels Innova, SIFF Seoul, Archimedes). 118 The Institute was highly assessed by the Ministry of Science and Higher Education for its achievements in 2005 – 2009 and was awarded the 1st category. 119 10.Cooperation in international research Project In the field of international cooperation a common implementation of projects within EU Framework Programmes is especially important. The following projects were implemented in FP 6: Printed Circuit Boards with High Solderability Tin Coating for Lead Free Soldering” – PRINT, Removal of Hazardous Substances in Electronics – GreenRoSE, Promoting Eco-design Activities in the SMEs of the Electrical/Electronics Sector ECODESIGN, EU-China co-operation in Green Electronics Production Research–ECGEPRO,Nanocrystalline carbon layers – ERA, Europe-China Cooperation in Green Electronics Production Research, Developing metamaterials technologies based on carbon nano structures foroptoelectronic applications (COST). Under the 7th Framework Programme of the European Community, in the field of research, technological development and demonstration the Institute has been implementing an international project in the ‘Environment’ thematic area of the detailed programme ‘Cooperation’ of FP 7 (LCA to go) – ‘Boosting Life Cycle Assessment Use in European Small and Medium-sized Enterprises: Serving Needs of Innovative Key Sectors with Smart Methods and Tools”. In particular, the Institute participates in the MNT ERA-NET (Micro- and Nanotechnology European Research Area Network), COST (European Cooperation in the Field of Scientific and Technical Research) projects. Eight research projects are implemented under the Innovative Economy Operational Programme for the years 2007-2013, Priority 1, Research and Development of Modern Technologies. A short description of the Institute is included in the appendix and more detailed information concerning the Tele & Radio Research Institute can be found on our webpage. http://www.itr.org.pl We hope this information help us to establish future cooperation 120 Catalogue of technologies developed by Polish Research Institutes ENVIRONMENTAL PROTECTION AND ENGINEERING; ENVIRONMENTAL, AGRICULTURAL AND FOREST TECHNOLOGIES 121 FOREST RESEARCH INSTITUTE (Instytut Badawczy Leśnictwa) Organisation Contact Data 1, Ratuszowa st, 03 – 450 Warsaw, Poland phone: +48 22 619 22 41 fax: +48 22 619 29 47 http://www.ibles.pl/?set_language=en CO-OPERATION AND ADVISORY OFFERS Forest ecology and game management Expert opinions on valorisation of selected natural forest areas, nature reserves as well as urban forests (paying particular attention to Natura 2000 areas). Environmental impact assessment (for the obtainment of integrated or ministerial permits) of new investments or investments specially adapted to forest ecosystems. Evaluation of animal population size (for ungulates, bats, rodents) and also training for such activity. Evaluation of animal damages to forest environment. Training and expert opinions on young plantation and young tree stands protection from animal damage. Trainings and workshops for educators and consultants on environmental education within integrated systems using interactive forms of schooling. Forest sites Evaluation of site productivity. Identification of physical and chemical soil properties, air pollution, and chemical water composition, chemical analysis of organic material towards nutrient and heavy metal content. Trainings on good laboratory practices. Expert opinions on the utility value of fertilizers, materials improving soil properties and materials used for plantation improvement for the utilization in forests according to law in force. Expert opinions on the fulfilment of the requirements on quality and allowable quantities of pollution from fertilizers, materials improving soil properties and materials used for plantation improvement for the utilization in forests according to law in force. 122 Programs of forest soil restoration, diagnostics of soils in forest nurseries and fertilizing recommendations, programs of management and recultivation of waste lands and of afforestation of agricultural lands. Environmental impact assessment of water facilities and anthropogenic activity on forest environment. Projects of water retention and irrigation systems in forests. Expert opinions on water retention enhancement and water management in forests. Development of protection plans for Natura 2000 areas. Development of plans of protective tasks for Natura 2000 areas. Environmental impact assessment of forest management plans. Evaluation of forest sites survey reports. Impact assessment of investments on forest sites condition and water management (for example: sand mines, water retention reservoirs). Counselling in typological diagnostics of forest sites and phytosociological diagnostics. Counselling in implementation of projects of restitution and protection of hydrogenic sites. Counselling in forest nurseries irrigation systems. Management of degraded lands, for example burned areas, drained lands etc. Support in applying of hydrogels on forest sites. Support in operating water melioration systems in forests. Development of methods of erosion preventing in forest areas. Soil pH regulation and soil salinity neutralization and determination of nutritional status and needs of different tree species in urban areas. Forest genetics and tree physiology DNA analyses of forest trees, fungal pathogens and animals in order to: determine a genotype, compare DNA of logs and stumps samples of stolen wood (for judicial proceeding purposes), identify genetic hybrids of forest tree species, molecular diagnostics of pathogens. Laboratory equipment of the Laboratory of Molecular Biology at the Forest Research Institute: DNA analyses: laboratory balances (Radwag and Ohaus), vortex mixers (Rietsch®), water purification systems (Elix 3 and Milli-Q Millipore®), centrifuges (Eppendorf, Genofuge and Rietch), laminar flow closets (samples and PCR preparation), ultra-low temperature laboratory freezers, incubators, ice maker, autoclaves, mixers, pH-meters. molecular diagnostics of organisms: ALFexpress™ II DNA Analysis System and Beckman CEQ 8000® DNA Sequencer, NanoDrop® ND-1000 Spectrophotometer, BioRad® 123 Electrophoresis equipment, thermocyclers (MJResearch® and Biometra®), analytical software (Gene-Scan®, Gel-Doc®, BIO-PROFIL®). Evaluation of forest trees and shrubs seeds quality Silviculture Expert opinions and advising on: use of herbicides in forestry (nurseries, young plantations, tree stands and surrounding areas), use of biological methods of protection from weeds in nurseries and on forest plantations, establishing forest plantations, afforestation of agricultural lands, wastelands and degraded forest and non-forest areas (species selection, planting densities, mixing patterns), tree tending techniques in forest stands and on wooded sites (also in urban areas) considering their conditions and vitality of trees. Additionally: organization and assistance in trainings of forestry staff in the areas of forest management with special consideration of natural regeneration, stand tending, management of protective stands, selection of appropriate methods of stand conversion, management of declining and damaged tree stands (by wind or snow), organization of trainings for private forest owners in the above-mentioned areas, preparation and conduct classes for children, youngsters and teachers on the topics of forest management. Forest protection Identification of insects: Lepidoptera (butterflies and moths), Odonata (dragonflies and damselflies), Orthoptera, Diptera (flies) and those causing damages to forest trees and shrubs Registration tests of pesticides, advising in application of insecticides and evaluating their efficiency Protective procedures – advising in: coniferous and broadleaved tree stands threatened by folivorous insects, spruce and pine tree stands threatened by secondary pests. Advising in application and production of pheromones, kairomones, and pheromone insect traps in forestry Protective procedures in coniferous and broadleaved tree stands damaged by abiotic factors (wind, snow, flood, fire etc.) Development of an optimal strategy for silvicultural and protective actions in areas permanently settled by grubs 124 Assessing tree stands health and sanitary conditions and forecasting insect pests occurrence Protective measures (pest insects control) of decorative plants, trees and shrubs in gardens, parks as well as private and communal forests Forest phytopathology Advising in seed-, seedling- and plant diseases in forest nurseries, tree stands and gardens. Identification of pathogens using techniques of molecular genetics (PCR, Real Time PCR, DNA sequencing). Inventory and expert opinions concerning health conditions of park and urban trees. Identification of biotic and abiotic pathogenic factors and developing methods of reducing damages caused by pathogens. Estimating state of forest trees mycorrhizae. Advising in fungal pathogens control. Courses and trainings in the field of phytopathology of trees and shrubs, concerning in particular: conservation of trees - natural monuments and control of pathogenic fungi development, biological methods of root pathogens control, biological decomposition of stumps after tree cutting in urban areas, methods of improving effectiveness of pesticides in use. Trainings and advisory activity: Faunistical surveys of nature reserves and other natural objects. Qualitative and quantitative assessment of rare, endangered and protected insect species in national parks, nature reserves and Natura 2000 areas, and developing protection plans for national parks and Natura 2000 areas in the field of enthomology. Trainings for the State Forests administration employees, universities, schools, national and landscape parks employees as well as forming collections of insects and their conservation. Forest economics and policy Expert opinions and professional advising in valuing forest real estates and estimating value of tree stand damages. Expert opinions in analyzing timber markets situation in Poland and Europe. Trainings for private forest owners and supervisors of private forests. 125 Forest management planning and forest monitoring Environmental impact assessment for forest management plans in Natura 2000 areas (after detailed regulations are published). Developing simplified forest management plans. Developing protection plans for national parks (co-operation), landscape parks, nature reserves as well as protection plans and plans of protective tasks for Natura 2000 areas. Expert opinions in selected aspects of forest condition assessment in forests of varying ownership using geomatics techniques. Inventory of forest resources. Developing reports on state of forest resources and their changes. Measurement of an annual growth of tree thickness in collected samples. Spatial analyses with the use of digital terrain model. Analyzing, developing and implementation of software for analyzing descriptive and geometric data gathered in the Information System of the State Forests. Developing business analyses of information projects (analitical documentation in UML notation) with the use of descriptive and geometric data gathered in the Information System of the State Forests. Untypical queries concerning data gathered in the Information System of the State Forests databases. Designing and implementation of websites and content management systems (ZOPE/PLONE technologies). Forest utilization Measuring and estimating noise and vibrations characteristics in work environment. Occupational risk assessment related to noise and vibration according to the European Union regulations (Directive 98/37/EC), physiological tests for timber harvesting operators (estimating energy expenditure and physiological cost of work). Trainings in operating timber harvesters. Monitoring of forest fire danger and occurrence of forest fires Co-operation with media and preparing notices on fire danger in forests. Establishing usefulness of new technical solutions in forest fire protection. Development of technologies utilizing instruments and equipment for detection and extinguishing forest fires. Preparing characteristics of meteorological and hydrological conditions of forest sites. Forest fire forecasting in army ranges. Development of forest fire protection programs. Advising in development of tactics in case of forest fires. 126 Consulting on interpretation of rules related to forest fire protection. Counselling in the functioning of the National Forest Fire Information System. Trainings in forest fire protection. Trainings in servicing forest fire forecasting stations in army ranges. 127 INSTITUTE OF AGRICULTURAL AND FOOD BIOTECHNOLOGY (Instytut Biotechnologii Przemysłu Rolno-Spożywczego) Organisation Contact Data 36, Rakowiecka st, 02- 532 Warsaw, Poland phone: +48 22 606 36 00 fax: + 48 22 849 04 26 ; +48 22 849 04 28 e-mail: [email protected] http://www.ibprs.pl/html/english.html Department of Fermentation Technology The Department of Fermentation Technology Institute of Agricultural and Food Biotechnology was established in 1954 and from its origin intensively collaborates with spirit and yeast industry. Generally, the activity of Department focus on the issues arising form needs of modern spirit and yeast industry as well as agriculture. On the basis of its own studies on biotechnological utility of microorganisms, yeast and lactic bacteria, Department systematically extends area of activity and nowadays offers probiotic-type bacterial preparations for livestock and mixed bacterial-enzymatic preparations for fodder ensile. The main scope of research and scientific activity involves: examination and improvement of microbial strains, bakery and distillery yeasts selection, study on the metabolisms and physiology of the lactic acid bacteria technological improvement in spirit, yeast industries for better usage of raw materials and enhance of product quality, with particular regard to the energy saving and environmental protection modifications of technological process in yeast factories including improving their economics and increase in activity of fermenting yeast biomass improving technology of yeast products obtained from baker’s, post-fermentation brewer’s yeast and sedimentary wine yeast monitoring of the state of emergency of the environmental by distillery, spirit and yeast industry elaboration of the proper criteria for estimation of the authenticity of the alcoholic beverages on the basis of studies on their isotopic composition 128 development of the chromatographic and sensory methods for analysis of taste and flavor components of alcoholic beverages (including wines, cider) studies on the identification of microorganisms by means of molecular biology methods, including PCR technique development of the procedures for identification of genetic modifications in food development of multi-componential bakery starter cultures of a new generation for application in rye and wheat-rye dough The Department carries out complex and interdisciplinary research works, provides technological solutions, licenses, know-how, expertise and analytical services to industrial companies, small business, agricultural productions enterprises, institutions and state administration offices, including: technology and technique of obtainment and application of probiotic preparations and biopreparations for fodder ensile (production on order of probiotic preparations, belonging to product series Probiomix and Probiosacc: production on order of preparations for fodder ensile: Lactosil, Lactamyl, Lactacel, Laktozym) evaluation of spirit and alcoholic beverages quality on the basis of chemical and chromatographic analyses evaluation of usefulness and effectiveness of use of enzymatic preparations in distilleries microbiological purity determination of microbial culture as well as raw materials, intermediate products and final products of yeast and spirit industry sensory analysis, analysis of the physico-chemical quality factors of raw materials, intermediate products and final products of spirit, yeast industry technology of obtainment of bakery starter cultures technology of obtainment of starter culture for vegetable ensile technology of obtainment of yeast products for food, pharmaceutical industry and for animal feeding Highly qualified staff and modern technical equipment allows professional approach to realized research. Our department is accredited testing laboratory according to ISO 17025. Our analytical competences are confirmed by Polish Centre for Accreditation (Number of accreditation AB 452). Contact Person Data Director of Department of Fermentation Technology: Assoc. Prof. Krystyna M. Stecka Ph. D. Eng 36, Rakowiecka st, 02- 532 Warsaw, Poland phone: + 48 22 606 36 49 fax + 48 22 849 04 26 e-mail: [email protected] 129 Yeast Derivated Products as Natural Food and Feed Additives We offer the technology of producing yeast products. The subject of the invention is optimization of process to obtain natural food additives from baker’s, post-fermentation brewer’s yeast and sedimentary wine yeast towards entire utilization of cell wall constituents. Due to growing demand for food additives their new, natural sources are searched for. One of them are baker’s yeasts. Yeast derivated products such as yeast autolysates and yeast extracts are obtained as a result of controlled autolysis (temp. 50 0C; pH 5,5; 24 h) with different types of inductors such as: glucose, ethanol, NaCL, organic acids. Such obtained yeast autolysate is spray-drying or cell wall are separated by centrifugation in order to obtain yeast extract. Yeast extract is preserved in form of yeast spread or spray drying. Cell walls resulting after yeast extract production are then forwarded to glucan production. It is done by alkaline extraction and acid purification. Production of yeast derivated natural food additives is illustrated by the chart below: Yeast derivated natural food additives are carriers of functional, sensory and nutritional properties. Yeast autolysates bind fats and water, are good sensory additives, have beneficial aminoacids composition. They are used as components of nutrient media in microbiology, additive to baker’s products, meat and mushroom stuffing. Yeast extracts are well soluble in all pH spectrum, bind fats, color food. Due to presence of natural flavour enhancers: MSG, 5’ IMP, 5’ GMP and products of Maillard reaction they are good sensory additives. Yeast extracts have high nutritional value of proteins and high content of vitamins. Yeast extracts are used in production of prepared meals, concentrates of soups and sauces, species blends and meat products. Yeast spreads are valuable component of vegetarian diet. Yeast glucan binds fat and water, stimulate immunology body system against bacterial and virus infections as well as cancer. Glucan obtained from yeast can be used in food products as a thickening, water-holding or fat-binding agent. Due to parapharmaceutical properties of glucan it could be utilised in production of functional food. Described above methodology of obtaining yeast derived natural food additives is economicly justified method of spent brewer’s yeast utilization. 130 Department of Food Concentrates and Starch Products The Department of Food Concentrates and Starch Products in Poznan, Poland, as a Department of the Institute of Agricultural and Food Biotechnology, offers comprehensive and interdisciplinary researches, development and implementation into food industry. The main areas of the Department activity range: Development of dry food mixes, including: dietetic food, food for special dietary use, functional food, food for elderly, etc. - recipes and technology Development of processing and preparing raw materials for dry mixes Enhancing of taste and healthy facilities of coffee and cereal coffee drinks Development of starches and starch derivatives Chemical and sensory food analysis including shelf life assessment Research of flexible packaging materials Food processing advisory service Pilot plant service on semi-commercial scale production. The Department is good equipped with analytical instrumentation and technical facility. The unit processes such as: extraction, drying, sterilization, extrusion, disintegration, mixing and packaging are realized in our Pilot Plant. In our Department there were elaborated and implemented into industry practice, among others: dry food mixes (soups, sauces, dishes, desserts, cakes, seasonings), including lawcalorie, sugarless and gluten-free products, technologies of herb, tea and vegetable extracts, agglomeration of powdered beverages and desserts, continuous steam sterilization of plant materials, producing of different instant cereal products by extrusion, technologies of obtaining different starch thickeners, maltodextrines and enzymatic starch syrups. The Department has developed many patented product and technologies. 131 We cooperate with clients from food industry, including SME. Institute of Agricultural and Food Biotechnology is accredited testing laboratory according to ISO 17025. Our analytical competences are confirmed by Polish Centre for Accreditation (Number of accreditation AB 452). Contact Person Data Director of Department of Food Concentrates and Starch Products in Poznan” Assoc. Prof. Marian Remiszewski Ph. D. Eng 40, Starolecka s, 61-361, Poznań, Poland phone: + 48 61 873 19 70 fax: + 48 61 879 34 83 e-mail: [email protected] www.ibprs.poznan.pl 132 Instant Cereal Groats We offer the technology of producing instant cereal groats which contain healthy ingredients. The elaborated technology is based on extrusion process which was tested in pilot plant division of our Department. The pilot plant technology line consist of screen, weigh feeder, wetting-mixing unit, screw extruder, cutting unit, pneumatic conveyer, rotary dryer, vibratory cooler. Working capacity of pilot plant is about 100kg/h of ready product. Instant cereal groats, obtaining by our technology, meet all consumer expectations for healthy, convenience and safety food. Instant groats are easy digestible, cholesterol-free, contain antioxidants, dietary fibre and big amount of complex carbohydrates; they do not contain any food additives. They have long shelf life. They are ready to eat without cooking; it is enough to pour them boiling water and wait for a while. They have also a property to rehydratation in cold/ ambient temperature water, milk or other liquid food without heating. These special rehydratation properties are obtained thanks to inner porous structure of products. This cause additional advantages – ready to eat cereal groats are not sticky, they have permanent and loose form and are friable. Thanks to their properties offered instant cereal groats, have a wide range of application – in the house keeping, tourism, catering and food industry as a component or base of other instant food. In the case of interest in implementation of our technology, please contact as bellow: Contact Person Data Director of Department of Food Concentrates and Starch Products in Poznan” Assoc. Prof. Marian Remiszewski Ph. D. Eng 40, Starolecka s, 61-361, Poznań, Poland phone: + 48 61 873 19 70 fax: + 48 61 879 34 83 e-mail: [email protected] www.ibprs.poznan.pl 133 INSTITUTE FOR ECOLOGY OF INDUSTRIAL AREAS (Instytut Ekologii Terenów Uprzemysłowionych) Organisation Contact Data Contact Person Data 6, Kossuthast, 40 –844 Katowice, Poland Head of the International Co-operation Department: Izabela Ratman - Kłosińska phone: + 48 32 60 31 ext. 243 fax: +48 32 254 17 17 phone: +48 32 254 60 31 fax: +48 32 254 17 17 e-mail: [email protected] http://www.ietu.katowice.pl/eng/index.htm e-mail: [email protected] Institute for Ecology of Industrial Areas (IETU) in Katowice, Poland is an R&D unit acting under the Ministry of Environment with a 38- year experience in applied research and consulting addressing key environmental challenges posed by heavily industrialized and urbanized environment. Our staff of 96 including 58 researchers and senior scientists represents a broad portfolio of expertise in such fields as: land management, especially post industrial areas integrated atmospheric protection management of water resources environmental risk analysis and assessment soil and groundwater remediation technologies integrated environmental monitoring and modeling solid and hazardous waste management environmental microbiology environmental management and policy including eco-innovation geostatistical analyses environmental education PROJECTS/ SPECIAL AREA OF INTEREST: We provide services to state and local administration, regulators and industry but first of all conduct research projects with partners at home and in international consortia. Vast majority of these projects is funded by the European Commission. High level of the performed scientific works combined with the personnel’s skills to cooperate in international project consortia allowed IETU to be recognized among Poland’s leading R&D centers in the number of the 134 successful applications to the EU funds. In total we participated or currently perform 43 international projects. In the years 1995- 2000 our main partner in doing environmental restoration studies and soil remediation technologies was the U.S. Department of Energy and Florida State University. Last year we successfully completed a project under the U.S. EPA Program Methane2Markets which addressed conversion of the coal mine methane from abandoned mines into LNG in Poland and we are looking forward to further explore this promising research theme as well as others such as: • integrated surface and groundwater quality management, especially in industrial and urbanized areas • integrated air quality management • technologies for soil remediation (bioremediation, phytoremedation) and site characteristics using GIS and geostatistics • health and environmental risk analysis and assessment • solutions for integrated management of post-industrial sites • environmental policy and management including environmental technologies verification issues • biodiversity issues, especially those related to the impact of contaminated environment • waste management including hazardous waste • research into eco-innovation including eco-efficiency indicators, measuring eco-innovation, LCA approaches in business practice, monitoring systems of eco-innovative technologies, etc. IETU’s Central Laboratory has been accredited by the Polish Centre for Accreditation (Certificate of Accreditation No. AB 325) for physico-chemical analyses of water, wastewater, soil and wastes. The accreditation includes 30 analytical methods and testing procedures for determining inorganic and organic compounds in different environmental components. IETU is partner in an EU funded coordination project Advance- ETV aimed at building the foundations for harmonisation and international recognition of the currently developed European environmental technologies verification scheme with the operational Canadian and the U.S. ETV systems. IETU is the main partner to the Polish Ministry of the Environment in the implementation of the European Environmental Technologies Action Plan in Poland. 135 Circular Flow Land Use Management (CircUse) Project / Technology / Solution / Achivement Description: The development of regular integrated action plans on sustainable land management and the realisation of projects demonstrating practical solutions by local and regional stakeholders are important for Central European regions. Therefore partners of the CircUse project will work on this new Circular Flow Land Use Management concept in coherence with the implementation of instruments and pilot actions. CircUse also will be strongly influenced by the goal to create climate beneficial land use structures – either by passive contributions on energy consumption by traffic, natural soil protection or actively by energy production on land integrated in interim or final land use options. Instruments will be provided by the concept of Circular Flow Land Use Management as an integrative policy and governance approach. Ecological Effect of the Project / Technology: CircUse will contribute to achieve the general spatial objective of „Developing polycentric settlements structures and territorial cooperation”. This will be adressed by the following project objectives: support of sustainable land use change (e.g. by new concepts and information tools), 136 reduction of land consumption and inner development (e.g. by integration of planning instruments, soil protection tools and brownfield revitalisation measures), increase of private investment in inner development (e.g. by risk transparency), coordination of public interventions and funding (including ERDF) (e.g. by local investment task forces), coordination of investments in greenfield, greyfield and brownfield sites to ensure cost efficient settlements (e. g. by local and regional planning). CircUse Strategy: Circular Flow Land Use Management (CircUse) represents an integrative policy and governance approach which presupposes a changed land use philosophy with regard to land utilization. This modified land use philosophy can be expressed with the slogan “avoid – recycle –compensat”. 137 Identification System of Air Pollution Inflow (SINZaP) Project / Technology / Solution / Achivement Description: The SINZaP system enables modelling the state and the forecast of the air quality and making the obtained results accessible by the Internet. The service delivers hourly communiques containing understandable air quality (AQ) information enabling citizens tune their behaviour to varying state of the AQ (e.g. allergy allerts, exceeded concentrations of pollutants, ozone etc). The modelling is realised with the use of a tool called Identification System of Air Pollution Infl ow (SINZaP). The system enables identification of air pollution infl ux, identification of emission sources location, assessment of intensity of air pollutant emission in the monitored area as well as assessment of air pollution infl ux from remote high intensity emission sources. For modeling the emission and air pollutants concentrations in SINZaP system, aback- trajectory model – BackTrack is used, which, in turn, is based on VLSTRACK model. The essential feature of the BackTrack model is application of back trajectories in the selection of emission sources influencing a given receptor. For modelling of trajectories BackTrack uses three-dimensional wind fields, friction velocity, Monin-Obukhov length and mixing layer height SINZaP consists of 4 main modules: data module including data scanner for reading public data accessible by the internet; module for preparation of meteorological data; BackTrack module for simulations of pollutants emissions and air pollutants concentrations; and Trainer module for correction of input parameters and adjusting the modelling and the observed data. Data collected by the system are used for simulation of concentrations of sulphur dioxide, nitrogen dioxide, PM10 and carbon monoxide. 24-hours traces of backtrajectories are used in simulation of air pollutant concentrations at a given time point and location. The modelled concentrations arecompared with the measured ones. This enables making corrections in the emission field and meteorological conditions. Ecological Effect of the Project / Technology: In 2005-2006 SINZaP was applied in EC MARQUIS project. Now it is used in information service on air quality in the Silesian Voivodeship (MARQUIS Light). Since 2006 SINZaP operates as a real time system for modelling of pollutants emissions and air pollutants concentrations. It 138 addresses the information needs of the specialists or decision makers responsible for air quality management Special Awards rof the Project / Technology: Due to its scientifi c and technological advancement SINZaP as well as MARQUIS Light service were presented to the Prize of the Polish Ministry of Environment and the Green Check Prize of the Voivodeship Inspectorate of Environmental Protection in Katowice 139 INSTITUTE OF ENVIRONMENTAL PROTECTION (Instytut Ochrony Środowiska) Organisation Contact Data 5/11 d, Krucza st, 00- 548 Warsaw, Poland phone: +48 22 621 36 70 fax: + 48 22 629 52 63 e-mail: [email protected] http://www.ios.edu.pl/eng/welcome.html RESEARCH PROFILE: The current activity of the Institute focuses the following research fields: comprehensive environmental research, including degradation processes and their consequences; environmental policy and environmental protection strategies, programs and plans; air protection, climate change; noise control; landscape conservation; protection of biodiversity; protection and restoration of biologically active land surface; protection of water resources and their quality; waste management; management of chemicals in the environment. ACTIVITY SCOPE: Among the basic research areas of special significance are projects aimed at assessing the risk associated with intentionally produced substances like biocides and pesticides that are introduced into the basic components of the environment - water, soil, air and living organisms in a controlled way, as well as substances which are introduced in an uncontrolled way as byproducts of many production processes, like dioxins, PCBs, PAHs and heavy metals. The findings of research concerning persistent organic pollutants and pollution with heavy metals allow to develop remedial methods for restoring degraded areas, with a special focus on areas degraded by chemicals. In cooperation with other Polish partners the Institute is involved in the preparation of a strategy for reducing greenhouse gas emissions and the adaptation of the Polish economy to climate change, preparing the first integrated climate change scenarios for Poland. Recently, 140 the Institute has developed the methodological basis for adaptation to climate change of plant production on farms representing different types of management and production scales Some projects are carried out on a permanent basis. Most of these are applied research studies for the Ministry of the Environment. Projects on environmental quality monitoring, including air pollution, noise and lakes, as well as integrated monitoring of the natural environment, and economic issues of climate change are of special importance. Research in the area of water, sewage and sludge management has been an important part of the Institute’s activity, with much attention paid to physical, chemical and biological properties of sludge, in particular sanitary research on human and animal intestinal parasites, bacteria causing hemolysis and Salmonella due to the frequent agricultural use of sludge as fertilizers. Microbiological air contamination and the spreading of odors are important research fields assessing the impact of municipal facilities such as wastewater treatment plants and landfills on the environment and human health. Research on waste management, including the management of sewage sludge, leads to cooperation with the industry as well as small and medium enterprises. The Institute’s share in research projects conducted as part of EU programs is increasing significantly.. The Institute has been working on projects dealing with the reduction of dioxin emissions from the metallurgical sector, and has been involved in the development of innovative chemical safety indicators and environmental indicators enabling integrated risk assessments in the context of accidental releases of hazardous chemical substances into the environment, and integrated assessments of the ecological state of waters, as well as projects related to ecosystems’ adjustment to climate change. Since 2005, the National Centre of the Emissions Trading System has been set up in the Institute. In 2009 it transformed within the structure of the Institute into the National Centre for Emissions Management (KOBIZE). As defined in Article 3.2 of the Law on the Emissions Management System of 17 July 2009 KOBiZE is responsible inter alia for: operation of the national system of emissions balancing and forecasting of GHG and other substances, including the national database of emissions to the air; maintaining the national registry of the Kyoto units; preparing emissions reports and forecasts; establishing methodology of setting up emissions' levels for categories of installations or industrial activities, as well as methodology of establishing emission factors per product unit, fuel or material used; collecting, processing, estimating, forecasting and collating data on the volume of emissions of GHG and other substances The Institute operates two environmental monitoring stations - in the Borecka Forest: Integrated Environmental Monitoring Station “Puszcza Borecka”, and in Warsaw: Air Pollution Measurement Station. (in collaboration with US EPA). 141 Three accredited laboratories support the Institute’s R&D projects. Namely: the Environmental Monitoring Laboratory works in the area of chemical and physical analyses of the quality of basic components of the environment; the Mobile Noise Laboratory conducts research on industrial, traffic, aircraft and impulse noise; the Borecka Forest Station for Integrated Environmental Monitoring conducts, inter alia, measurements of concentrations of ozone and other pollutants. PROPOSED FIELD OF COLLABORATION National Centre for Emissions Management Support in establishing GHG and air pollution state monitoring system as well as reporting to UNFCCC Secretariat. Verification of the GHG and other pollution emission data, both in theoretical considerations and making use of practical tools. Know-how, methodological knowledge and software IT services in elaboration and operation of the air pollutants data bases. Elaboration of the strategic development plans for different industrial branches with regards to the emission reduction of GHG and air pollution. Consulting in the area of the air pollution estimation and balancing. Other analysis related to combating the climate change and the air protection at the state and international level and their impact on economy, industry, etc. Waste Management Department The team posses a wide knowledge in the area of waste management – technology, organization, legislation. The experience is connected with waste management planning – especial municipal waste, some kinds of industrial waste, hazardous waste management especial POPs (Persistent Organic Pollutants – Stockholm Convention ). the National Implementation Plan of Stockholm Convention on Persistent Organic Pollutants (POPs) was prepared in the Institute which play role of the Stockholm Convention Focal Point for Poland in 2011. On request of UNIDO consultation in preparation National Implementation Plan in Armenia have been carried out. The team offers also advice in POPs management planning (i.e. Implementation Plans of Stockholm Convention, organization of control and reporting services). Also documents of the Conference of Parties and its bodies are analysed and national position papers are prepared . In the last years the team participated in two important projects – Waste Management in Inorganic Chemical Industry – Foresigh to 2030y. and Use of Keratine as Flame Retardant in Industrial Products (polymers) ( medaille d’Or, Concours Lepine. Paris 2011). 142 The Institute offers expert advice in waste management planning – preparation of environmental protection plans for cities and surrounding areas, hazardous waste management planning, risk assessment reports preparation, environmental impact assessment of contaminated sites. Currently the team is involved in collaboration in research in waste management of packaging materials of consumer goods. The aim of the project would be the reduction of environmental pollution throughout the changes in technology of production processes of packaging materials. 143 INSTITUTE OF METEOROLOGY AND WATER MANAGEMENT (Instytut Meteorologii i Gospodarki Wodnej) Organisation Contact Data 61, Podleśna st, 01- 673 Warsaw, Poland phone: +48 22 56-94-100 fax: + 48 22 834-18-01; (22) 834-54-66 [email protected] http://www.imgw.pl/index.php?lang=pl The Institute of Meteorology and Water Management - National Research Institute (IMGW) is a government agency under the Ministry of the Environment. IMGW offers products and services that provide various kinds of enterprises and organisations with an important foundation for decision-making. High-quality observational data and research is utilized to develop services to benefit our everyday life. Visible examples are improvement of weather forecasts, development of new expert and warning services as well as applications of the newest research results. Ground Based Remote Sensing Department The Ground Based Remote Sensing Department (OTN – Ośrodek Teledetekcji Naziemnej) is one of the branches within the IMGW. The OTN operates a network of 8 high-resolution Doppler weather radars as well as network of lightning detection system, and provides high resolution data for weather forecasting offices and other public services. The OTN also supports the aviation community through the production of several specific weather radar products. Beside providing data, the OTN is also working with research and development within atmospheric remote sensing. The main task is to improve existing methods and develop new ones to make the institute better equipped to exploit the remotely sensed data in our analysis, short-term forecasts and environmental surveillance. 144 MeteoFlight: System of Weather Hazard Monitoring for Air Traffic Control and Management The innovative, versatile and fully automatic MeteoFlight system, being developed by Ground Based Remote Sensing Department for the aviation community, produces a weather hazard index (WHI) field based on meteorological data and processes it as an input data to Air Traffic Control (ATC) systems in the form of meteorological overlay (e.g. ASTERIX format). Independently, MeteoFlight can be accessed as a web application with general access through a web browser by other users like pilots and traffic management. Figure 1: Overall scheme of the MeteoFlight system WHI is a metric, which describes a level of meteorological hazards from air traffic's point of view. The concept of the WHI is not to provide air traffic controllers with plurality information about current meteorological conditions and phenomena, but the synthetic one. From the viewpoint of ATC, information about meteorological conditions plays significant role in assessment of the air navigation safety. For air traffic management the information is directly assigned to loss in case of flight delays etc. The versatile and modular structure of the MeteoFlight system leads to easy accommodation to variety of input data sources. The basic one is the data from weather radar network and lightning detection system. But the system is open and can be adjusted to other kinds of meteorological high resolution data like satellite pictures, numerical weather prediction (NWP), lidars etc. 145 Figure 2: View of MeteoFlight web application with WHI field BUSINESS PROPOSAL Our range of expertise covers: System customization. OTN can build and deploy the application adopted to local environment, which mean working with local meteorological data, and local geographical layers. System delivery and installation. The system will be delivered with full documentation covering user and administrator manuals and trainings. Our experts will configure new hardware and install all MeteoFlight applications. System maintaining. Our experts will be ready to answer any of client enquiries. Cooperation in system development. MeteoFlight is focused on further development to provide new solutions using state-of-the-art technologies. OTN is willing to cooperate with other institutions to share experience and knowledge. For more technical information please contact: Contact Person Data Zdzislaw Dziewit phone: +48 22 569 43 53 e-mail: [email protected] 146 The range of promotion of technologies for monitoring of the marine environment state. The Maritime Branch of IMGW - PIB is a leading institute in Poland in the implementation of modern technologies in monitoring of the marine environment quality in accordance with the requirements of HELCOM, as well as the European Environment Agency. The substantial value of the Institute is the long term experience of the team involved in the marine monitoring for more than 20 years. One of the basic elements of the monitoring technology is the use of international standards of quality for the organization of the expedition, measurement, environmental sampling and laboratory analysis. This technology is compatible with the requirements of the Water Framework Directive EP (WFD) and adapted to the requirements resulting from the implementation of the Marine Strategy Framework Directive (MSFD) in Poland. The key element of the monitoring technology is the methodology of assessment of the state of the individual components of the marine ecosystem, as well as the ecosystem as a whole, using statistical methods and numerical models. The calculation tools for the classification of the ecological quality of ecosystem (in a five grade scale according to the WFD and a two grade scale according to RDSM) are the latest technologies in the field of assessment. They allow for a consistent presentation of the quality status of the entire marine ecosystem as a support in the marine environment management. The Institute offers technology transfer in the following areas: 1. Design and optimization of monitoring of the open sea and coastal water including bays and lagoons. 2. The implementation of modern technologies for the measurement of physical, chemical and biological parameters. 3. Implementation of modern analytical methods for inorganic and organic chemistry. 4. Implementation of quality assurance of laboratory analyses of inorganic and organic samples. 5. The implementation of a system of quality control for measurements of physical parameters. 6. Organization and management of measurement data by means of an oceanographic database background, which is adjusted to fit assessment procedures needs. 7. Implementation of methods generated and developed by specialized staff within the Institute, likewise within the framework of HELCOM, for analysis of the environment state in terms of eutrophication, harmful substances and hydromorphological elements. 147 INSTITUTE OF ORGANIZATION AND MANAGEMENT IN INDUSTRY ORGMASZ (Instytut Organizacji i Zarządzania w Przemyśle ORGMASZ) Organisation Contact Data 87, Żelazna st, 00 – 879 Warsaw, Poland phone: +48 22 654 60 61 ext. 206 phone/ fax: + 48 22 620 43 60 e-mail: [email protected] http://www.orgmasz.pl/uk/home_uk.htm Institute of Organization and Management in Industry ORGMASZ would like to offer cooperation at the field of green – energy. ORGMASZ with Partners offer the whole range of services aimed at implementation of technologies as well as legal services. 148 Below please find key information concerning R&D implementation: Quasi – Pyrolyze Consortium leaded by ORGMASZ We are proud to announce that our institute signed an agreement between COMPUTEX ltd. and PROKAB S ltd. and established new cooperation on 15th May 2012. The main purpose is to cooperate with extraordinary technology of utilizing wastes by quazi mineralization method. Thermal transforming by mineralization method is one of the best ways to utilize liquid and solid wastes. This method of utilization produces electricity and thermal energy. Why do we use Quasi Pyrolyze Process? The main difference between Pyrolyze and Quasi Pyrolyze Process is temperature. Pyrolyze Process operates in 800 to 1100ºC. On the contrary Quasi Pyrolyze Process needs only 400-450ºC. The final product of Pyrolyze Process is tar. Temperature of Quasi Pyrolyze Process is lower and final products are gases not tar. Utilization of all kinds of wastes in the same installation is a novelty. The other advantages of Quasi Pyrolize Process are sludge volume reduction (16 - 50 - fold) sludge mass reduction ( 20 – 100 - fold) total sludge dehydration total sludge deodorization total oxidation of organic compounds, including bacteria and viruses, to H2O and CO2 The offered technology consists of: the system which vaporize the water from bio - sludge, regardless whether this sediment is initially drained or not; the system for full disinfection of steam; the system of gasification (low – temperature quasi - pyrolysis) of the organic residue, so – called dry matter; a catalytic reactor fully oxidizing organic compounds to H2O en CO2 with efficiency of 99,9%; the system of heat exchangers, which recover catalytic, post – reaction heat to minimize energy expenditure (vaporization process); final filters which capture solid, inorganic particles and metals as well as their compounds; a series of alkaline washers (only if required by the chemical composition of the sludge) 149 For our New Cooperation the wastes are not the wastes. They are fuel. We would like to challenge the view that the wastes are only a problem. It is the final time to save environment for seriously. The new technology will support the plea for cleaner and healthier environment. Project Coordinators: Ewa Minrewska-Huńka Waldemar Snopek Arkadiusz Grzeszczak Zbigniew Krawczyk Witold Witowski 150 Energia Restitua - THE Green – Power and Legal CONSORTIUM The Consortium consists of five firms: Fund of Centre for Entreprise Supoprt, Hakon Consultancy Agency, Institute of Organization and Management in Industry ORGMASZ , „Kalwas Partners” Law Office, MS CONSULT, who carry out project in the area of renewable energy. The Consortium operates in the area of Investments in renewable energy sources by, inter alia, preparing projects and procurement of funds for project’s execution. The Consortium carries out projects with respect to: Investments in photovoltaics, heat pomp, solar collectors. Preparation of the investment task execution and transfer of information regarding undertakings on behalf of beneficiary crucial for funding of investment execution from WFOŚiGW funds with respect to installation of photovoltaic panels, heat pomp, solar collectors, in particular: Estimation of investment possibilities and estimation of effectiveness of the use of new solutions. Preparation of documentation necessary to file the application for granting a subsidy (investment documentation –project, cost estimate). Preparation of documentation regarding network connection. Preparation of the application including attachments (supervision over preparation of attachments). Supervision over correctness of an application settlement. Optimization of operating cost of: local government units, their subordinated institutions, enterprises Organization of joint purchase of energy – tenders of local government units, entrepreneurs, hospitals, in particular: Analysis of the cost reduction possibilities with respect to purchase Estimation of the possibility of joint purchase, preparation of the goods and services purchase list. Legal support (contracts between particular beneficiaries). Preparation and conduct of collective tender. Training regarding optimization of energy management costs and other operating costs. 151 „KALWAS & PARTNERS” „Kalwas and Partners” is a Polish law office founded in 1989. Since then, the firm is continually operating with major successes in both Polish and international market. “Kalwas and Partners” is a civil partnership of four legal advisors Our office is a member of the International Association of Independent Law Firms – TELFA and a member of the Polish-Spanish Chamber of Commerce. The Office Partners and cooperating lawyers have extensive experience in providing comprehensive legal assistance to Polish and foreign companies and the procedural practice with a legal representation in litigation. 152 INSTITUTE OF PLANT PROTECTION (Instytut Ochrony Roślin) Organisation Contact Data 20, Wladyslawa Wegorka st, 60 – 318, Poznań Poland phone: +48 61 864 90 02 fax: + 48 61 867 63 01 e-mail: [email protected] http://www.ior.poznan.pl/lang:1 The Institute of Plant Protection-National Research Institute in Poznan is a modern institution directly subordinate to the Ministry of Agriculture and Rural Development, covering general plant protection problems. Institute of Plant Protection-NRI provides a wide range of commercial services related to various areas of plant protection. The individual departments in the Institute offer professional consulting, trainings and identification of different type of plant pathogens. The Institute received three Ministerial Awards for development and implementation of biological methods in plant protection. The Institute obtained three patents on developed production technologies and application methods of bioproducts containing entomopathogenic viruses and bacterias. The Institute provides examination of biological efficacy of plant protection products (e.g. fungicides, herbicides etc) in agricultural and horticultural for registration purposes. We also elaborate and assessments reports of pesticide residues for the purpose of registration of plant protection products in Poland. Moreover, we analyze pesticides residues and heavy metal contents in agricultural products, soil, potable water, plant consumable products and feed derived from ecological farming using chromatographic techniques. The Institute provides also expertise’s on environmental pollution (plant, soil, water) caused by plant protection products. We organized trainings for advisors and producers. The Institute introduced several plant protection programs for growers and rendered evaluation of quality, usefulness and efficacy of new plant protection products and their occurrence in soil, potable and ground water as well as evaluation of the equipment suitability for performing plant protection treatment. The Institute offers a wide range of diagnostic services including different type of pathogens using both traditional and molecular biology methods. Newly established in 2011 ,,The Plant Disease Clinic” conducts extensive analysis and research on a wide range of plant pathogens including nematodes, viruses, phytoplasmas, fungi and bacterias. New diagnostic techniques using real-time PCR for sensitive and fast detection of viruses and bacterias in plants and seeds were developed and described. In addition, the Institute possesses the Research Centre of Quarantine, Invasive and Genetically Modified Organisms, which was formed in July 2009 at the Institute of Plant Protection - National Research Institute in Poznan. It is a modern and unique in the country 153 fulfilling the highest phytosanitary requirements’ standards (SL3). The Centre's role is to provide research facilities for researchers of the Institute of Plant Protection-NRI, and other research and development units working with IPP-NRI, leading the study on the quarantine pests, invasive and genetically modified crops. The center is equipped with the best quality equipment and modern greenhouses and laboratories to conduct studies using contra-phase microscope, scanning electron microscope, transmission electron microscope and others. 154 OUR OFFER: Department of Virology and Bacteriology Technology of vaccines against viruses Department develop technology to protect crops against viruses. There are no effective methods to fight against viruses besides complying with phytosanitary rules and using diagnostic tools. The enormous genetic variability of RNA viruses is an essential mechanism leading to their evolutionary success. This variability is owed to the short generation time, enormous population sizes and lack of proofreading mechanisms of virus-encoded RNAdependent RNA polymerases. Point mutations, if change the amino acid sequence, are potential targets for selective forces, which eliminate poorly adapted genetic variants and fix beneficial ones. The scope of genetic variability of RNA viruses often positively correlates with the ability to infect a wider range of susceptible host species, i.e. the more variability, the more species may be potential hosts. For that reason, we aimed to create stable virus variants to protect plant in the mechanism of cross-protection. It is a way of the protection against a viral infection given to a plant by its prior inoculation with a related but milder virus. The research is being performed on Pepino mosaic virus (PepMV) now consider one of the most dangerous pathogens infecting tomato plants worldwide and placed on the European and Mediterranean Plant Protection Organization (EPPO) alert list. PepMVis a highly diverse virus which evolved rapidly from emerging to endemic in tomato crops. Single nucleotide sequence differences between isolates from the same genotype have been shown to lead to the enhanced aggressiveness and symptomatology. The virus is very variable and different isolates cause wide range of symptoms on infected plants from mild mosaic, through yellowing to necrosis and plant death. Moreover, the virus creates a lot of variants and even single nucleotide substitution might be responsible for severe symptoms observed. In the Department we created infectious clone of different PepMV pathotypes and collection of viral mutants bearing single nucleotide substitution in the genome by site-directed mutagenesis. We checked them stability in the plants and potential ability to protect plants against more aggressive variants. We are working with the most stable variants and different tomato varieties coming from Poland and Spain. Our goal is to find the best variant which will protect plants against other PepMV variants and produce it in a large scale for commercial use. It will act as plant vaccines. The other way is to design of vaccines based on short artificial micro RNAs to immunize plants. Defective interfering RNAs – a way to protect plant against viruses In the Department of Virology and Bacteriology we deal with small RNAs associated with Tomato black ring virus genome which infects a wide range of plants: cucumber, tomato, potato and others. In Poland it was qualified as quarantine object on strawberry and raspberry. The virus is very dangerous because it often causes necrosis and plant death. The existence of defective interfering RNA molecules (DIs) associated with TBRV and another member of Nepovirus genus, Beet ringspot virus, has been shown. DI-RNAs are small RNA molecules 155 derived from a parental virus genome. DI-RNAs originally found in animal viruses and then they were discovered also in different families of plant viruses. It is thought that the generation of DI-RNA in due to a recombination event that occurs according to a “copy-choice” mechanism and is initiated by a strong secondary structure in the viral RNA. There are two types of defective interfering RNAs associated with plant RNA viruses. The first type contains the DIRNAs generated by a single internal deletion and the second ones are the products of several consecutive recombination events. The molecules belonging to the first were usually found in association with the virus possessing the multipartite genome. Their formation in infected cells can strongly influence virus life cycle (replication, accumulation or symptoms). Over the last few years we collected several TBRV isolates from different plant species. In the Department of Virology and Bacteriology short defective RNAs (D-RNAs) associated with Tomato black ring virus (TBRV) were isolated, cloned and sequenced. As a result, two types of D-RNAs associated with different TBRV isolates were identified. Both types were derived from RNA1. The presence of additional RNAs was connected with attenuated symptoms on infected plants. It may suggests that generated D-RNAs also interfere with replication of the parental genomes. For that reason, we are going to obtain artificial small RNAs and check their influence on symptoms development. It could be done by chemical synthesis or by creating RNA transcripts using special vector systems. The synthesis of small RNAs and immunization of plants could be a novel solution in plant protection. Small RNAs might play a role in gene silencing during the infection and can be used as a tool to protect plant against viruses. 156 INSTITUTE OF TECHNOLOGY AND LIFE SCIENCES (Instytut Technologiczno – Przyrodniczy) Organisation Contact Data 3, Hrabska st, 05- 090 Falenty, Poland phone: +48 22.628 37 63 fax: + 48 22.628 37 63 e-mail: [email protected] http://www.itep.edu.pl/english/ ITP Warsaw Branch ITP Poznań Branch 32, Rakowiecka st, 02 – 532, Warsaw, Poland phone: +48 22 542 11 00 fax: + 48 22 542 11 50 67 Biskupińska st, 60 – 463, Poznań, Poland phone: +48 61 820 33 31 fax: + 48 820 83 81 www.itep.poznan.pl Agro-environmental Research: The use of object classification of satellite and aerial imagery of selected elements of land cover, in particular: Way of land use, Natural habitats, Wetlands, Soil cover units. Exchange of experience in scope of use of remote sensing and GIS in works on landscape structure monitoring including the aspect of scale of monitored areas (local, regional, national scale). Sustainable use of natural resources in agricultural landscape. Construction of system allowing optimization of management of spatial units (administrative units, protected areas, watersheds, regions, etc.) basing on use of GIS and remote sensing tools. Development of integrated methods of inventory of valuable natural habitats in landscapes strongly influenced by human activity, particularly related to agricultural activities (using GIS and remote sensing – satellite and aerial). The relationship between carbon dioxide emission and way of use of soils rich in organic matter. Emission of carbon dioxide from natural habitats connected with wetlands ecosystems. Differentiation of indicators of biodiversity and landscapes in agricultural areas with different traditions of land use. 157 Agricultural Engineering Research: Micro installations for production of electricity and heat from the liquid and gaseous biofuels Development of universal micro installation for production of electricity and heat from gaseous and liquid biofuels (waste grease). Solution of problems connected with identification of origin of different sources of wastes basing on exchange of knowledge and experience. Development of database on wastes. Development of technology and a prototype installation operation on liquid and gaseous fuels at the same time at the small agricultural biogas plants. Works on the effective use of wastes and diffused sources of energy are carried out on a global scale. Cooperation between countries would base on exchange of experiences in scope of threats caused by production and storing of wastes as well as on ways of dealing with the problem. Basing on collected information a database would be developed. The database would contain information on characteristics of different wastes (mainly organic and grease), their amounts and sources of origin. Precise identification of the problem as well as knowledge spread among research institutes would be a foundation for development of universal, compact or modular unit for production of energy from different wastes. Animal grease as highly energetic one waste would be the main fuel for the unit generating electricity and heat while biogas would be a component of fuel-air mixture produced in combustion chamber of the diesel engine. The effect of the cooperation would be not only a regularly updated database on wastes that might be used for monitoring of waste origin but also a new technology and a prototype unit for production of energy from different wastes. The commercial product would be also a tool for defining the production potential of waste locally and a tool for their effective use. 158 MARITIME INSTITUTE IN GDAŃSK (Instytut Morski w Gdańsku) Organisation Contact Data 41/42 Długi Targ, 80 – 830 Gdańsk, Poland phone: +48 58 .301 16 41 fax: + 48 58 301 35 13 e-mail: [email protected] http://www.en.im.gda.pl/ The Maritime Institute operates as a research institute in accordance with the Act of 30 April 2010 on research institutes (Official Gazette of 2010, No. 96, it. 618). The Maritime Institute is listed in the National Court Register (Krajowy Rejestr Sądowy - KRS) under position 0000026943. In accordance with the KRS the scope of activity of the Maritime Institute in Gdansk includes among others: R&D in the field of chemical sciences, R&D in the field of earth sciences, R&D in the field of biologic and environmental sciences, R&D in the field of technical sciences, R&D in the field of economical sciences, R&D in the field of law, R&D in the field of librarianship and scientific and technical information, Activity in structure, urban and technological design, Geological and exploration activities, Survey and cartographic activities, Technical investigations and analyses. 159 CHARACTERISTIC OF RESEARCH ACTIVITIES The Maritime Institute in Gdansk implements innovative research for the needs of maritime economy, research and implementation works, feasibility studies and expert opinions, consultations in the fields of: ecology and environmental protection (biological and chemical research), maritime hydrotechnics, geotechnics, operational oceanography, maritime renewable energy, transport, logistics, spatial planning of coastal (including marine) zones, modernisation and exploitation of ports, inland navigation, tourism, flood safety, marine electronics, data bases management, monitoring of continuous phenomena. The Maritime Institute in Gdansk has an experienced and highly qualified research and technical staff, dynamically developing departments and workshops, specialised laboratories: Multipurpose oceanographic laboratory r/v IMOR, Accredited environment protection Research Laboratory – Certificate of Accreditation of Research Laboratory No. AB 646 Accredited Marine Electronics Laboratory – Certification of Accreditation of Research Laboratory No. AB 848. The Maritime Institute in Gdańsk is an inter-disciplinary unit supervised by Polish Ministry of Transport, Construction and Maritime Economy. Its activities have a direct influence on the development of widely understood maritime economy. The results of research activities of the institute are comprehensive research and development works for national government, local and regional self-government and maritime administration, also for companies connected mainly with the maritime economy and the coastal regions. The Institute’s departments cooperation results in common studies and publications. The high intellectual and technical potential allows realising international scientific projects and develop cooperation with other research institutions, also carry out the most demanding and comprehensive orders at highest level of quality in the field of maritime economy. The research and investigation activities of the Maritime Institute in Gdansk territorially cover all Polish sea areas (including the EEZ and the coastal zone) and currently are focused on six priority areas: protection and shaping of environment, environmental engineering and maritime structures (coastal protection), offshore renewable energy, monitoring and risk prevention, economics of transport and market investigation, marine technology. 160 PROPOSED AREAS OF COOPERATION Department of Economic and Law (DE&L) The Department carries out investigations connected with the functioning and development of maritime economy, including such problems as: logistics in sea transport, expert opinions and investigations of trends and prediction of development of maritime economy, marine statistics and annual publishing of the “Statistical Review of Maritime Economy” and of fire incidents on vessels statistics, economical effectiveness of investments in sea transport, EDI in international transport and trade, technological progress and organisation of intermodal transport, marketing investigations of national and international transport market, sea and coastal tourism, legal and economical analysis concerning PSSA issues, elaboration in Polish of IMO documents on safety of ships at sea and marine environment, and of connected EU documents. DE&L is interested in renewing the cooperation with Shanghai Maritime University, that was first established in the early 1960's. We wish to cooperate in the field of research and development with special focus on shipping services between the Far East and Europe. The cooperation in the 1960's was established in conjunction with the founding of the ChinesePolish Joint Stock Shipping Company "CHIPOLBROK" with its main office in Shanghai and branch office in Gdynia. Today the company successfully operates in the shipping market within the structures of COSCO (China Ocean Shipping Group Company), one of the world's largest liner shipping operators. In light of globalisation processes taking place in the maritime economy that led to the launch of direct container connection between Shanghai (and other Far Eastern ports) and Gdansk, it is particularly important to expolore research areas related to the cargo flows between Polish seaports (and other ports in the Baltic region) and the Chinese ports (and other Far Eastern ports). The joint research could include analysis of the potential of port hinterlands, transport-logistics supply chains, recent trends in shipbuilding market (demand and supply), development of port infrastructure and the development of modern intelligent transport systems (ITS). Given the fact that the vessels for Polish shipping companies (mainly Polsteam and Chipolbrok) are mostly built by Chinese shipyards, the knowledge and experience of Polish specialists in the design, construction, supervision and classification of tonnage should be shared. Department’s research team is also interested in the maritime sector’s labour market and the labour mobility in shipping, ports and shipbuilding. These issues can certainly be an area of 161 common research interests and implementation of new ideas in the field of employment, education, training and labour standards. Department of Economics and Law has also extensive experience in researching areas related to safety and security of shipping and environmental laws and regulations. In the light of recent IMO proposals associated with reducing harmful emissions from ships and installing new equipment in port facilities adapted to the stringent requirements of modern shipping techniques and technologies, it could provide an excellent platform for research collaboration between the Maritime Institute in Gdansk and the Shanghai Maritime University and other Far Eastern R&D institutions, including Shipping Research Centre at the Technical University of Hong Kong, Chinese Maritime Institute in Taipei, Korea Ocean Research and Development Institute and Japan's National Maritime Research Institute (NMRI) of Tokyo. Contact Person Data Head of Department of Economics and Law: Urszula Kowalczyk phone: + 48 58 320-32-69 e-mail: [email protected] Department of Environmental Protection (DEP) The Department performs analytic investigations for a wide range of determinations, and develops reports concerning environmental protection. It carries out physical and chemical investigations of surface, underground and marine waters, sewage deposits, bottom deposits, soil and waste in the full scope of determinations necessary for: determination of level of pollution of port waters, investigation of contamination of spoil dredged in ports, investigation of soil contamination in port and industrial areas, ecological inspection, ground- and surface water monitoring, quantitative/qualitative sewage balance, expert opinions on industrial waste and bottom sediments, water-law assessments for water consumption and sewage discharge, EIA for noxious investments (waste storage areas, petrol stations, industrial plants), technological testing of sewage treatment and water processing plants, data needed for an application for the integrated permit within the scope of water and sewage management. The Department contains a laboratory which implemented the Quality System in accordance with Polish Standard PN-EN ISO/IEC 17025: 2005, and since 1 September 2005 has a 162 CERTIFICATION OF THE POLISH ACCREDITATION CENTRE No. AB 646 confirming fulfilling of the requirements of the above mentioned Standard. DEP is interested in cooperation, including regarding the application of stabilization technology of contaminated dredged sediments as a tool for a sustainable management. The seas have many hot-spots with highly contaminated sediments in ports, estuaries etc. Human activities often take place in coastal areas and are affected by these hot-spots, e.g. land reclamation for new residential areas and dredging in ports and fairways due to more deepdraught ships. The removed material may be treated and used afterwards, or disposed of under strict environmental controls. So how to handle contaminated sediments is a major issue, also from social and economical viewpoint. Management alternatives for dredged material can be grouped into the following five main categories: sustainable relocation, beneficial use, openwater disposal, confined disposal and treatment. In the past, the only option to remediate contaminated sediments was to dredge the sediment, then treat or dispose of it. Now, in situ remediation technologies are being considered for treatment more frequently. Treatment is defined as the processing of contaminated dredged material to reduce its quantity or to reduce the contamination. Treatment methods range from separation techniques, in which contaminated mud is separated from relatively clean sand, to incineration. The stabilization of nutrients, such as nitrogen and phosphorus, has been practiced for some time as solution to eutrophication problems. Emerging treatment technologies, as the stabilisation/solidification method, make it possible to consider beneficial use of the contaminated sediments as construction material in e.g. new ports storage and transport areas. The stabilization/solidification method would reduce the environmental impact by a reduced need of natural finite resources e.g. sand. The aim of cooperation with Asia region will be to provide support for dredging actions. It would be also the base for exchange the knowledge regarding the stabilization/solidification technology, quality control (monitoring of leaching) and environmental protection. The scientific researches of the stabilization/solidification technology were performed by the University of Hong Kong (Department of Civil Engineering), Chinese Academy of Sciences (Guangzhou Institute of Geochemistry) or Pusan National University (Department of Civil & Environmental Engineering). Also contaminated sediments had been a problem in Japan. In the 1970s, Japan began to try different approaches to clean up contaminated sediments using different remediation methods, including dredging, capping, and solidification. Although the actual in situ stabilization has not been demonstrated in Japan, a dewatering project that involved in situ stabilization methods was conducted for example in the Hama River. Stabilization technology is a future for development of by-products market (e.g., fly ash, oil shale ash, slag, etc.), also for a wide international arena. 163 Contact Person Data Head of Department of Environmental Protection Barbara Aftanas phone: + 48 58 308-81-25 e-mail: [email protected] Assistant Professor: Grażyna Sapota phone: + 48 58 308-81-28 e-mail: [email protected] Department of Operational Oceanography (DOO) The Department has the following specialist laboratories and teams: Multipurpose Oceanographic Laboratory r/v IMOR Oceanographic Data Processing and Analysis Laboratory Marine Measurements’ and Survey Team Modelling Decision Support Systems Group Coastal Zone Development Group 164 With the use of the vessel – laboratory r/v IMOR, the Department specialises in realisation of highly specialised marine research services such as: investigations of ecological impact of economy on marine environment and biocenosis, pre-investment studies of sea bottom for offshore wind farms, cable and pipeline laying, sanitary collectors and artificial reefs, investigations for inventories of marine mineral resources, measurement of degree of contamination and volume of dredged spoil, services within the scope of information needed for design, modernisation and construction of maritime hydrotechnical objects, collectors port quays, marinas, investigation for improvement of safety of navigation and contingency action at sea (prediction of oil and chemical spill propagation), maritime spatial planning and ICZM strategies. The research multi-purpose vessel “IMOR” owned by Maritime Institute in Gdansk (MIG) and maintained by MIG Department of Operational Oceanography, is a good basis for complex hydrographic, geophysical, geological and other investigations in the open sea and in coastal zone. With the professional team and owned equipment we are the obvious partner for preinvestment studies for offshore constructions as harbours, marinas, wind farms, etc. Since several years we are much interested in problems of marine renewable energy, its transfer and possible storage. It includes studies for design of marine wind farms, marine telecommunication and power transmission cables, gas and oil pipelines, harbours and coastal protection structures; exploration and inspection of mining aggregate resources; maintenance of autonomous buoy system, monitoring marine state for the navigation safety of and rescue activities support, monitoring of wrecks sites in view of their environmental impact, etc. DOO is also interested in other marine renewable energy sources as wind wave energy and sea currents energy. Department of Operational Oceanography is interested to cooperate with the Asian partners in all listed fields, also for experience and knowledge exchange. Contact Person Data Head of Department of Operational Oceanography Benedykt Hac phone: + 48 58 301-87-24 e-mail: [email protected] 165 NATIONAL MARINE FISHERIES RESEARCH INSTITUTE (Morski Instytut Rybacki - Państwowy Instytut Badawczy) Organisation Contact Data 1, Kołłątaja st, 81 - 332 Gdańsk, Poland phone: +48 58 . 735 62 32 fax: + 48 58 735 61 10 e-mail: [email protected] http://www.nmfri.gdynia.pl/ The National Marine Fisheries Research Institute – Poland’s oldest marine science center The Institute’s beginnings date back to June 1921 when the Sea Fisheries Laboratory was established in Hel for the purpose of conducting research in hydrology and marine biology. This institution was closed in 1931 and then reopened in 1932 as the Marine Station. It was moved to its new headquarters, the present building of the NMFRI Gdynia Aquarium, in Gdynia at the end of 1938. After the Second World War, the Marine Station in Gdynia was reactivated under its original name of the Sea Fisheries Laboratory. In 1947, the SFL was incorporated into the Sea Fisheries Institute, which had been in operation since 1928. Beginning in 1949, the SFI was a departmental institution supervised by the Ministry of Navigation. Until 1991 it operated from its headquarters at the end of the South Pier in Gdynia when it moved to its new location on ul. Kołłątaja. Since 2000, the Sea Fisheries Institute has been supervised by the Ministry of Agriculture and Rural Development (MARD). According to the Regulation of the Council of Ministers of June 2011, the Institute has been awarded National Research Institute (NRI) status. Upon attaining the status of NRI, the National Marine Fisheries Research Institute has joined the elite ranks of Polish national research institutes. NMFRI is interested in co-operation and sale of technology in the scope of mechanic processing of carp fish and other fish of family Cyprinidae to form of semi-products and final products without the threat posed for consumers by intermuscular bones characteristic for Cyprinidae. We offer many solutions such as machines for intermuscular bones (fish bones) cutting in deheaded and gutted fish, semi-fillets and fillets of Cyprinidae. 166 Fishbone cutting machine for semi fillets and fillets Fishbone cutting machine for fillets Table fishbone cutting machines for fillets Cut fillet Fishbone cutting machine for deheaded and gutted fish Deheaded and gutted carp with cut fisbones We also offer technology of reconstruction of the deeply cut fillets to their original appearance to produce boneless carp fillets. This is possible by applying an enzymatic merging process to the cut fillet meat combined with deep chilling or freezing the fillets that are individually vacuum packed in several layers plastic. Thanks to this method, solid fillets are produced with tiny pieces of bone that are undetectable by the consumer and their sensory quality do not decreases. 167 Cut fillet after merging Sensory quality of fried "boneless" carp fillets and natural o carp fillets cold storaged for 1 year at the temperature of -20 C "Boneless" fillet Natural fillet Appearance 5 4 General assesment 3 Degree of consolidation 2 1 Texture Smell Flavour Our patented machines and technologies have positive opinions of national users and they were repeatedly rewarded for invention and innovation during international exhibitions in Gdańsk, Brussel, Paris and Moscow. Contact Person Data Department of Processing Technology and Mechanization Assoc. Prof. Andrzej Dowgiałło phone: + 48 58 73 56 189 fax: + 48 58 73 56 110 e-mail: [email protected] 168 NATIONAL RESEARCH INSTITUTE OF ANIMAL PRODUCTION (Instytut Zootechniki) Organisation Contact Data 1, Krakowska st, 32 – 083, Balice near Cracow, Poland phone: +48 666 081 133, +48 666 081 136 fax: + 48 12 285 67 33 e-mail: [email protected] http://www.izoo.krakow.pl/en/ The National Research Institute of Animal Production is one of the largest Polish scientific research institutes serving the whole country. It is accountable to the Ministry of Agriculture and Rural Development. The Institute was founded on 31 May 1950 and its mission is to carry out research and development work in the field of animal production and development of the agricultural environment. This activity is oriented towards the current and future production of inexpensive and safe food under animal and environmentally friendly conditions, and the use of farm animals for biomedical purposes. The Institute’s main and strategic research areas, in view of the changing needs of animal production, are as follows: Genetics and breeding of farm animals, conservation of genetic resources, Livestock nutrition and feed science, Biotechnological methods of animal production, Technology, ecology and economics of animal production, Quality of raw materials and products of animal origin. The Institute’s research programme is realized in the following departments: Genetics and Breeding of Farm Animals Conservation of Animal Genetic Resources Feed Science and Animal Nutrition Animal Cytogenetics and Molecular Genetics Biotechnology of Animal Reproduction Technology, Ecology and Economics of Animal Production Independent Genomics Laboratory The National Research Institute of Animal Production: 169 Provides advice and consultation on all matters related to animal breeding and management conditions Organizes courses for breeders and farmers, trainings for snail breeders, seminars and conferences on livestock production Carries out laboratory test – Main Laboratory accredited by the Polish Centre for Accreditation and the National Feed Laboratory in Lublin Offers breeding material (cattle, horses, pigs, goats, sheep, rabbits, poultry) for sale Manages animal performance testing stations and evaluates the breeding value of farm animals Cooperates with international and national research institution, Breeder’s Associations, Chambers of Agriculture and Agricultural Extension Centers all over Poland Is engaged in publishing - publishes science journal, popular science journal, conference materials, implementation and dissemination instructions Sells breeding animals in its Experimental Stations The Institute’s achievements, representing over 50 years of research, implementation and dissemination activities by its staff, resulted in the national (state) status being conferred to the National Research Institute of Animal Production on 23 November 2006 – by virtue of the Regulation of the Council of Ministers. 170 OFFER: The National Research Institute of Animal Production has the following technological offer: Individual and specific identification of animals, comparative analyses of marker maps, nucleotide sequences, polymorphism and conservation genetics of DNA (comparative genomics). Functional genomics, comprising the processes associated with gene expression, estimated on successive stages. The study of the organization of genomes based on classical and molecular cytogenetic analyses of somatic and reproductive cells, physical location of genes and comparative genomic hybridizations. Genomic evaluation of animals, estimation of the organization of a genome within chromosomes, as well as the influence of higher gnomic organization on gene expression. Embryo implantation Semen sexing Cloning of animals Transgenesis of animals Ecological breeding of animals Heat exchange device Use of alternative sources of energy in animal production New technologies of cheese production Technologies of feed assessment Assessment of the breeding value of animals Moreover, the Institute offers the following medical technologies: Technologies of feed processing Cytogenetic analysis Chimeras identification Study of the aetiology of neurodegenerative illnesses Study of microtraces Andrological diagnostics, animal sex regulation In vitro production of animal embryos Embryonic and somatic cloning of animals Animal transgenesis for the needs of breeding, pharmacy and biomedicine Cryopreservation of male and female gametes and embryos Gas chromatography and mass spectometry High efficiency liquid chromatography 171 Spectrophotometry UV – Vis Atomic absorption spectrometry Near infra-red spectometry (NIRS) Extractive Distillation and titration The departments of the Institute conduct research in the following diagnostic – analytic areas: Laboratory diagnostics in the field of feed assessment The quality of meat of farm animals Markers associated with the quality of meat Cytogenetics Molecular genetics Breeding Pharmacy Biomedicine Feed study Study of animal products Study of plant products The analysis of: vitamins, aminoacids, blood parameters, fatty acids omega3, omega6, omega9, light fatty acids and organic acids, sugar and starch, microelements, macroelements, iodine, selenium, fraction of ADF, NDF fibre and basic parameters of feeds (protein, fat, ash, dry mass). 172 NATIONAL VETERINARY RESEARCH INSTITUTE (Państwowy Instytut Weterynaryjny) Organisation Contact Data 57, Partyzantów st, 24 - 100 Puławy, Poland phone: +48 81 889 30 00 fax: + 48 81 886 25 95 e-mail: [email protected] http://www.piwet.pulawy.pl/ The NVRI was established in 1945 as a scientific unit of the Ministry of Agriculture. The major mission of the Institute is applied research in veterinary medicine, particularly concentrating on the diagnosis and prophylaxis of infectious diseases of animals, zoonoses, hygiene and toxicology of food of animal origin and feeds. Additionally, the Institute runs postgraduate training and professional specialisation, evaluates the quality of biologicals and provides the expertise and consultancy service for the veterinary administration. The Institute acts as the National Reference Laboratory responsible for the diagnosis of infectious diseases of animals, surveillance of epidemiological situation in the country, and monitoring of xenobiotics in food of animal origin and feeding stuffs. The Institute is authorised to confer the degrees of doctor of science (ScD) and doctor of philosophy (PhD) in veterinary sciences. NVRI has a completely new facility constructed in the years 2005-2007. These include 19 000m2 of laboratory area with laboratories representing high containment level (CL3 and CL3+) and animal facility with CL3+ level. Institute offers excellent training opportunities to PhD students and scientists. NVRI has large access to high-throughput PCR equipments, tissue culture core facilities, equipment four purification of bacteria and viruses, HPLC and HPLC-MS/MS. PRIORITIES/ RESEARCH FIELDS Development of diagnostic methods including molecular biology methods for zoonoses (Q fever, rabies, HPAI, brucellosis) Development and improvement of diagnostics methods for swine disease (CSF, PRRS, swine flu), poultry disease (HPAI, Newcastle, corona viruses) and cattle diseases (IBR/IPV, BVD, bluetongue, retroviruses infections) Examination of antimicrobiological resistance of Campylobacter sp., Salmonella sp., E. coli, Staphylococcus sp. Development and implementation of methods for determination of chemical residues in food of animal origin and feeds, and assessment of the risk of their occurrence. 173 RESEARCH INSTITUTE OF HORTICULTURE (Instytut Ogrodnictwa) Organisation Contact Data 1/3, Konstytucji 3 Maja st, 96 - 100 Skierniewice, Poland phone: +48 46 833 22 11 - 13 fax: + 48 46 8333186 e-mail: [email protected] http://www.inhort.pl/home_en.html Research Institute of Horticulture in Skierniewice, Poland is a governmental R&D organization supervised by the Ministry of Agriculture and Rural Development. It was established on January 1st, 2011, by merging two research units with over 50 year-long history: Research Institute of Pomology and Floriculture and Institute of Vegetable Crops. At present, Research Institute of Horticulture employs 568 people, in that 45 professors, 85 doctors and 62 research assistants. Its research programme covers all areas related to fruit, vegetable, ornamental plant and bee sciences, from basic studies on physiology, biochemistry and molecular biology, through biotechnology, creative breeding, protection of genetic resources, agronomy, plant pathology, fruit and vegetable storage and processing, food safety, horticultural engineering, economics and marketing. Due to active extension and implementation programmes and close cooperation with major stakeholders, the Institute has contributed in a large extent to the development of horticultural production in Poland. Besides research, the Institute is also involved in commercial activities, especially in food analysis. Several Institute’s laboratories has ISO/IEC 17025 and/or GLP certificates and perform analysis (pesticide residues, heavy metals, nitrites and nitrates and mycotoxins) for food producers and wholesalers. It is estimated that Institute’s laboratories have 50% share of commercial food analysis market in Poland. The Institute actively participates in building European Research Area. Cooperative links have been established with most of the horticultural research centres and clusters in Europe and several joint research project, co-financed by European Commission and other international organisations, were initiated. At present, the Institute is involved in three projects within 7th Framework Programme and in several others within Central European, LIFE and COST programmes and in bilateral projects financed by respective governments within agreements on cooperation in science and technology. Besides, the Institute is an active member of the European Fruit Research Institutes Network (EUFRIN). In Poland, the Institute is a coordinator of Centre of Advanced Technologies “AgroTech”, which is a cluster of three universities, two R&D Institutes and four commercial enterprises aiming at developing and implementing innovative technologies in Polish agri-food industry and of a network „Agroengineering for sustainable 174 development of agri-food industry and rural areas”. It is also a founding member of Polish Food Technology Platform. In September 2011 the Institute has organized conference “Food and nutrition in 21st century”, which was an official event in the frame of Polish Presidency in European Union. Institute is also an important teaching and training centre. It is authorized to conduct Ph.D. and postgraduate studies, summer schools and courses. Annually, on average five students receive Ph.D. diplomas, two D.Sc. diplomas (habilitations), and more than 700 students complete postgraduate studies and professional courses. Fruit Storage and Processing Department: The offer includes: • The assessment of the quality, authenticity and composition of clear and cloudy fruit juices and purees • Sensory evaluation of fruits, fruits products quality, consumer’s attitude • Technology and composition of dried fruit and vegetable products, including low calories fruit’ snack • The assessment of the quality and storability of apples, pears, strawberries, sweet cherries, peaches, nectarines, apricots and plums • Prediction, diagnostic and control of storage diseases and disorders of fruits • Nondestructive measurements of fruit ripening and quality of fruits • New storage technology incl. Dynamic Controlled Atmosphere (DCA), and postharvest treatment (1-MCP, hot water) Technology of cloudy juices or nectars production It was proofed that cloudy products, containing dietary fibre and phenolic compounds in particular, are healthier than the clear ones. Applying proper technology allows production of cloudy juice and cloudy nectars characterized by stable turbidity and high antioxidant contents. Use of commercial enzyme treatments in cloudy juice production is justified, however, positive effects in respect to juice yield, cloudiness stability and overall product quality may be obtained only when specific enzymes are used. At the Research Institute of Horticulture in Skierniewice technology of cloudy juices and nectars was developed. Context and rationale: Fruits contain various bioactive compounds having beneficial properties for human health. To increase consumption of some fruits in off season it is important to produce more attractive than currently available processed products. The promising products are cloudy juices containing more antioxidants and fibre than the clear juices. Some juices, e.g. apple cloudy juices, are usually produced without enzymation and clarification stages. This is not possible for berry, stone and other fruits containing large amount of pectic substances. Considering the existing problems technology of cloudy juice production was optimised in respect to enzymes used (particularly having specific pectin lyase and pectin polygalacturonase activities), their doses and treatment time. Using proper macerating mixture cloudy juices and nectars may be produced from difficult to press fruit mash. 175 I N S THE STANISŁAW SAKOWICZ INLAND FISHERIES INSTITUTE (Instytut Rybactwa Śródlądowego im. Stanisława Sakowicza) Organisation Contact Data 10, Oczapowskiego st, 10 - 719 Olsztyn, Poland phone: +48 89 524 0171 fax: + 48 89 524 05 05 e-mail: [email protected] http://www.infish.com.pl/ Founded in 1951, the Inland Fisheries Institute is a research and development institution subordinate to the Ministry of Agriculture and Rural Development. The mission of the Institute is to conduct research on inland fisheries and to disseminate the findings. The Institute is divided in fifteen units, including departments, laboratories, and sections, all of which conduct scientific research and provide scientific services within the following fields: natural science foundations for optimizing culture and rearing methods for fish and crayfish protecting fish health fishing techniques fisheries economics experimental fisheries promoting progress in fisheries The research units are located in Olsztyn, Żabieniec near Warsaw, Giżycko, Pieczarki near Giżycko, Gdańsk, and Rutki near Gdańsk. Experimental departments are located in Żabieniec and Zator near Kraków. The Institute is equipped with modern laboratories and experimental stocking facilities which permit conducting research and development in the fields mentioned above. The Institute is accredited to confer the academic degrees of doctor and doctor habilitowany (the Polish post-doctoral degree), and can also supervise proceedings to confer the title of professor. In its sixty years, the Institute has contributed extensively to the development of science and the practice of fisheries through its many accomplishments, including: developing highly effective technologies for the production of stocking material for numerous fish species; 176 developing methods for culturing sturgeon fish species on a commercial scale and for producing eggs (caviar) for consumption; implementing projects for restoring valuable fish species threatened with extinction or already extinct: salmon, Vistula sea trout, Baltic sturgeon, vimba bream, European whitefish; introducing strains of trout with different spawning periods into the fisheries, which has increased production of this fish severalfold; extensive experience in performing feasibility studies for more than 3,000 lakes, which, in addition to immediate advantages, has permitted creating a rich archive of wideranging information used by scientific, economic, administrative institutions, and others; decades of interdisciplinary research on the heated waters of the Koniń Lakes has been a scientific training ground that is unique on an international scale. The Institute cooperates actively with a number of Polish and international scientific organizations. It is also a member of international organizations such as EAS, WCSC, the Commission for Baltic Sea Research – HELCOM and NACEE. PROPOSED AREAS FOR COOPERATION The Institute proposes cooperation in research and development with interested institutions or organizations within the fields of expertise listed above. The Institute has developed highly effective technologies which are available for implementation in fish culture facilities, including: technologies for the reproduction and intensive tank culture in recirculating aquaculture systems (RAS) of predatory species: wels catfish, Silurus glanis; pike, Esox lucius; pikeperch, Sander lucioperca, and others; technology for artificial reproduction and intensive tank culture in recirculating aquaculture systems (RAS) for coregonids; technology for artificial reproduction and intensive tank culture in recirculating aquaculture systems (RAS) of sturgeon fish; creating female caviar stocks of sturgeon and harvesting eggs for caviar production; technology and equipment for recirculating aquaculture systems (RAS) for intensive fish culture 177 This page is left intentionally blank 178 Catalogue of technologies developed by Polish Research Institutes HEALTH PROTECTION AND PHYSICAL CULTURE 179 INSTITUTE OF SPORT (Instytut Sportu) Organisation Contact Data 2/16, Trylogii st, 01 - 982 Warsaw, Poland phone: +48 22 834 62 88 fax: + 48 22 835 09 77 e-mail: [email protected] http://insp.waw.pl/ MAIN ACTIVITY: Research and developmental works in the field of sport sciences Institute of Sport (IS) belongs to a group of leading Polish scientific institutions possessing the highest (A) category (in area of health protection and physical culture) awarded by Ministry of Science and Higher Education of the Polish Republic. Currently IS runs three scientific grants of European Union Commission, four grants of Ministry of Science and Higher Education, and one research program of Ministry of Sport and Tourism of the Polish Republic. Since 1984, IS has been publishing Biology of Sport - an international scientific journal which presents articles concerning basic and applied sciences in sport, physical exercise, sports medicine, pharmacology, training and testing as well as in other biological and social aspects related to sport. Biology of Sport is indexed or abstracted in Science Citation Index Expanded®, Focus On: Sports Science & Medicine®, ISI Journal Master List, ISI Essential Science Indicators, SCOPUS, EBSCO SPORTDiscus, Directory of Open Access Journals (DOAJ), CAB Abstract, INDEX COPERNICUS. We offer the opportunity of cooperation in research and developmental works in the field of sport sciences. Our main areas of interest are: Immediate and chronic physiological effects of sport activity Factors modifying organism adaptation to physical exercise Talent identification in sport Detection of banned substances in sport 180 Scientific support of training process of elite athletes Institute of Sport as a diagnostic and advisory service, cooperates with many Polish national teams in preparation of the athletes (including Olympic and world medallists) to main competitions. IS possess highly qualified staff – experts in anthropology, dietetics, biochemistry, biomechanics, endocrinology, genetics, physiology, psychology and sports medicine fields. Testing of the athletes is performed in modern and excellent equipped laboratories as well as in the field conditions (during training camps or competitions). We offer the opportunity of cooperation in sport diagnostics of the athletes trained in territory of Poland as well as abroad. In the laboratory conditions: Evaluation of training-induced changes in physical capacity, strength and power Detection symptoms of overreaching and overtraining Body structure and composition analysis Detection of vitamins and microelements shortage In the field conditions – during training camps: Monitoring of training : assessing and individual optimization of training loads Evaluation of training-induced changes in physical capacity, strength and power Analysis of rowing or canoe/kayak paddling technique In the field conditions – during competitions: Analysis of psychophysiological responses to competition Analysis of pacing strategy Doping detection Department of Anti-Doping Research is the only Polish, and one of 33 in the world, authorised laboratory to conduct anti-doping analyses in athletes. It holds accreditations of following organizations: World Anti-Doping Agency (WADA), Association of Official Racing Chemists (AORC), Polish Centre for Accreditation (PCA - certificate confirming consistence with ISO/IEC 17025 standard). Education Institute of Sport is an executor of Coach Academy - project of Ministry of Sport and Tourism dedicated for Olympic and leading non-Olympic coaches as well as support staff. Lectures, presentations, practical and theoretical trainings are conducted by prominent scientists and experts from Poland and other European countries, as well as USA. 181 MILITARY INSTITUTE OF HYGIENE & EPIDEMIOLOGY (Wojskowy Instytut Higieny i Epidemiologii im. gen Karola Kaczkowskiego) Organisation Contact Data 4, Kozielska st, 01 - 163 Warsaw, Poland phone: +48 22 838 01 29 phone/fax: + 48 22 838 10 69 e-mail: [email protected] http://www.wihe.waw.pl/ang/index.php The General Karol Kaczkowski Military Institute of Hygiene and Epidemiology (MIHE) is an independent, public, non-profit research and development entity registered under the National Registry’s no. 0000141719. Currently, MIHE is a unique research and development institution in Poland whose mission is to conduct research, prophylaxis, surveillance, and training associated with medical protection and countermeasures against different health threats, including those from use of weapons of mass destruction (WMD), including chemical, biological, radiological, and nuclear (CBRN) agents. These activities are executed in compliance with the recommendations and standards of the North Atlantic Treaty Organization which allows MIHE to cooperate with members of NATO and European Union in building of the international systems of countering the proliferation of WMD. In this regard, MIHE is the domestically and internationally recognized entity which – according to the classification of the Ministry of Science and Information Technologies – belongs to the first category of scientific institutions in Poland. Major activities of MIHE include: conducting scientific research, diagnosis, prophylaxis, and training as well as providing expertise and services in the fields of hygiene, epidemiology, microbiology, pharmacology, toxicology, radiobiology and radiation protection, applied and nutritional physiology as well as veterinary sciences, with special emphasis on the study and mitigation of health hazards associated with the use of biological, chemical, and radiological/nuclear weapons; final identification (performed at the unique in Poland biosafety level 3 microbiological laboratory of the MIHE’s Biothreat Identification and Countermeasure Centre in Pulawy) of dangerous pathogens which may be used as a biological warfare (BW) agents; functioning as a reference and expertise center for defense against biological weapons and certain aspects of toxicology, radiobiology and radiation protection; participation in development of systems of detection, identification, and countering of biological, chemical, and radiological contaminations of people, animals and the environment; 182 participation in prevention against and management of health injuries caused by natural and industrial disasters and catastrophes; examinations of bio-medical effects of and development of protective measures against highly dangerous biological pathogens and toxins (including BW agents); examinations of bio-medical effects of and development of protective measures against dangerous chemical compounds and preparations (including CW agents); examinations of bio-medical effects of ionizing (including radiological and nuclear weapons) and non-ionizing radiation with special emphasis on low-level exposures; validation of the radiation protection rules and regulations; examinations of the physical fitness and elaboration of methods of adaptation of the military and other uniformed personnel to the physically demanding conditions; assessment of the quality of food, elaboration of methods of its improvement, and studies on the physiology of nutrition of the military personnel in the barracks and during field operations; participation in national and international security systems against biological, chemical, and radiological threats. Since 2003, MIHE has been performing specific research and development tasks ordered by the Minister of Defense. These include: Defense and protection against biological warfare (BW) agents; Studies of bio-medical effects of chemical agents, ionizing, and non-ionizing radiations and development of protective and therapeutic countermeasures; Studies of ways of improvement of the sanitary-hygienic conditions of military operations carried out in biological, chemical, and/or radiological environments; Studies of physiological conditions and mechanisms of adaptation to the military operations, especially in biological, chemical, and/or radiological environments; Studies of epizootic and anthropozootic threats to the military personnel and development of protective and therapeutic countermeasures. MIHE conducts expertise, surveillance, and training activities such as: Issuing opinions on the ratification/implementation feasibilities of the NATO standardization agreements (STANAGs) and other national and international documents pertaining to defense and protection against WMD; Control of observance of the radiation protection rules by the military and other institutions employing sources of ionizing and non-ionizing radiation; Issuing opinions on hygienic, sanitary, physiological, ergonomic, toxicological, antiepidemic, and radiological properties and requirements of the military posts, offices, facilities, equipment, outfits (including individual protection garment), materiel, vehicles, etc.; Supervision of laboratory methods and procedures used at the military centers of preventive medicine; Training of physicians, veterinarians, and other specialists in microbiology, epidemiology, hygiene, toxicology, and radiation protection; Education of soldiers and other uniformed personnel in sanitary-hygienic issues. 183 STRUCTURE OF THE MILITARY INSTITUTE OF HYGIENE AND EPIDEMIOLOGY: Department of Microbiology Research activities: 1. In the field of medical microbiology: A) Pathogenesis of chronic/or recurrent bacterial infections, e.g., wound infections or respiratory diseases: studies on single- and multi-species bacterial biofilms; their properties, “net”pathogenicity and increased tolerance to antimicrobial agents; analysis of the occurrence, properties and susceptibility to antimicrobial agents of the intracellular bacteria, including Gram-negative rods and Gram-positive cocci causing respiratory tract infections; studies on the improvement of the capacity to prevent and combat biofilms occurring in the workplaces (pharmaceutical and engineering industries). Research methodology: PCR and FISH (Fluorescence in Situ Hybridization), immunofluorescence, zymography, electrophoretic analysis of proteins, Western-Blot, pulsed-field gel electrophoresis (PFGE), culture of mammalian cells, evaluation of necrosis and apoptosis in the infected host cells, analysis of cytotoxicity of bacterial isolates, and bacterial viability with fluorescent microscopy techniques. B) New formulations of antimicrobials – nanoliposomes and nanoemulsion for local therapy of the infected wounds: preparation of nanoliposomes with antibacterial agents; kinetics of the antimicrobial agents release from the nanoliposomes; in vitro antimicrobial activity of the nanoliposomes containing antibacterial agents; preparations of nanoemulsions by the high-pressure homogenization; determination of the antimicrobial activity of the nanoemulsions; the influence of nano-formulations of drugs towards Gram-negative and Gram-positive bacteria; testing of the antimicrobial activity of prototype dressings using the tissue model of the infected wound in vitro; Research methodology: high-pressure homogenization, bacterial viability assays, epifluorescence microscopy techniques. 2. In the field of environmental microbiology: development of the techniques for collection, detection and molecular identification of pathogenic microorganisms (bacteria and fungi and their spores) in bioaerosols; assessment of microbial surface contamination by pathogenic microorganisms in the work and service environments, inpatient facilities, etc.; 184 preparation of the bacterial and fungal cells of various physiological states: vegetative cells, resting forms, endospores and non-viable bacteria for detection and identification of the pathogenic organisms in the air using the advanced optoelectronic technology. Research methodology: studies on bioaerosols generated in the aerosol chambers; bioaerosol sampling using different samplers: impinger, gelatin filter sampler and six-stage viable Andersen cascade impactor; indoor air microbial quality assessment, the experimental facility for testing the capacity of the devices to clean the indoor air. 3. In the field of veterinary microbiology – the microbiological safety of food of animal origin: detection of food contamination with drug-resistant strains of pathogenic bacteria; examination of the transmission routes of the drug-resistant zoonotic bacteria: Campylobacter sp. rods isolated from poultry carcasses, coagulase-negative Staphylococcus sp. from milk samples; molecular typing of strains of Escherichia coli, Yersinia enterocolitica, Salmonella sp., Campylobacter sp. by using restriction fragment length analysis after their separation with pulsed-field gel electrophoresis; detection of enteropathogenic and enterohemorrhagic strains of E. coli, Salmonella, Campylobacter, Y. enterocolitica and Y. pseudotuberculosis by PCR multiplex; detection of verotoxin produced enterohemorrhagic E. coli strains by latex agglutination in food and feces. Research methodology: PCR, multiplex PCR, immunochemical techniques, magnetic immunoseparation, RFLP-PFGE. Department of Microbiology also provides the following services: bacteriological testing of drinking water, including determination of the number of coliforms, total coliforms faecal, faecal streptococci, total number of bacteria, according to the following standards: PN-ISO 6222:2004, PN-ISO 9308-1:2004, PN-ISO 9308-1:2004/Ap1:2005, PN-ISO 9308-1:2004/AC:2009, PN-EN ISO 7899-2:2004 and the Regulation of the Polish Minister of Health of 29 March 2007 on the quality of water for human consumption (Dz.U. 2007, No. 61, Item. 417); bacteriological testing of water for swimming pools, including the determination of the total number of bacteria, coagulase-positive staphylococci, coliforms, total coliforms and faecal streptococci, faecal, according to the following standards: PN-ISO 6222:2004, PN-ISO 9308-1:2004, PN-ISO 9308-1:2004/Ap1:2005, PN-ISO 93081:2004/AC:2009 and PZH-NIZP methodology recommended for the determination of staphylococci; bacteriological examination of water towards of Legionella bacteria, according to PN-EN ISO 11731-2:2008; 185 bacteriological examination of air with the aspiration method: determination of the total number of bacteria and fungi and the number of indicator bacteria (Actinomycetes, Pseudomonas fluorescens, Staphylococcus) in accordance with PN-EN 13098:2007 and PN-EN 14042:2010; testing the effectiveness of sterilization in accordance with PN-EN 13060+A2:2011. Contact Person Data Department of Microbiology phone/fax: + 48 22 685 32 06 e-mail: [email protected] 186 Laboratory of Epidemiology Laboratory of Epidemiology is accredited by the Ministry of Health as a training organization authorized to conduct its training in: Epidemiology for those with professional master's degree (number of training places 25) Epidemiology of military physicians (the number of training places - 9) The main tasks of the Laboratory include: ongoing monitoring of the Armed Forces Epidemiological, analysis of the risks of bioterrorism and natural infectious disease of an epidemic; specialist training in the field of epidemiology; archiving of lists of carcinogens at work and service in the Polish Armed Forces; preparation of studies and analyzes for the Inspectorate of the Military Health Service and other organizational units of the Defence; preparation for the armed forces, procedures for prevention of risks associated with the use of biological weapons and to liquidate the consequences of such use in accordance with NATO standards; conducting research work in dealing with threats from biological weapons, environmental risks, reduce the negative effects of these threats to the health of soldiers and health promotion; developing information and training materials to counter the threats from biological weapons and the treatment for the use of such weapons; participation in working groups dealing with the NATO defense against biological warfare (BioMedAC, NBC-MED, COMEDS FHP). Contact Person Data Department of Epidemiology phone/fax: + 48 22 685 31 26 e-mail: [email protected] 187 Department of Hygiene and Physiology Modern laboratory equipment, well-educated scientific workers, and highly qualified technicians of DHP constitute a setting conducive for state-of the-art performance of the following: at the Laboratory of Food Investigation and Nutrition Physiology: measurements of the energy expenditure at the workplace; assessments of the strenuousness of labor; estimations of the energy balance; estimations of the energy and nutritional demands associated with different types of work; anthropometrical evaluation of the subjects’ nutritional status; estimations of the energy and nutritive values of food products and daily food rations; verification of the appropriateness of nutrition planning and the feeding itself. at the Laboratory of Applied Physiology: evaluation of the effects of military service on the development of physical fitness and anthropometric indices in soldiers; assessment of hygienic and physiological conditions of operations in hot/wet environments; elaboration of methods of adaptation to work in protective clothing and gas masks; estimation of the effects of the selected factors of the working environment and diet on the exercise-associated metabolism in soldiers; elaboration of pharmacological ways of protection against oxidative stress. at the Laboratory of Hygiene: elaboration of non-specific methods of detection of potential biological warfare agents; assessment of the health effects devices imitating the battle-field ; elaboration of methods of prophylaxis of dermatophytosis and other skin diseases of the foot; elaboration of in-the-field methods of examination of water; assessment of contaminations of soil with heavy metals in the drill ranges; evaluation of the hygienic and ergonomic requirements of abiding in shelters in the wake of the use of weapons of mass destruction and/or industrial or ecological disasters. In addition, the Department’s staff is capable of lecturing and training in: nutritional prophylaxis of the diet- and food-related diseases; proper and rational nutrition; the food and nutrition hygiene; agro-terrorism; military hygiene and epidemiology. Contact Person Data Department of Hygiene and Physiology phone/fax: + 48 22 685 31 34 e-mail: [email protected] 188 Department of Pharmacology and Toxicology Scientific activities of the Department focus on three main areas: toxicology of chemical warfare agents and pharmacology of specific and non-specific antidotes for acute intoxications with these poisons encompassing: central effects of acute intoxications with organophosphates (OP), treatment of convulsions in the OP poisonings, effects of the excitatory amino acids (EAA)-receptor antagonists (competitive and noncompetitive for the NMDA and non-NMDA receptors) as anticonvulsants in the OP intoxications, /li> reversible AChE inhibitors as prophylactic agents in acute intoxications with OP efficacy of original compounds in reactivation and protection of AChE against irreversible inhibition caused by OP, in vitro and in vivo. pharmacology of pathologies of military impact including: pharmacological methods of the enhancement of survival in stressful conditions (e.g. extreme temperatures, isolation, pain), pharmacological methods to improve survival of hypothermic individuals in wet environments. immunotoxicology including: bacterial and parasitic infections in mice after acute poisoning with OP as host resistance models for the assessment of immunotoxicicty of agents, effects of OP on the development of transplantable tumors in mice. Patents: Individual Anti-Chemical Set" IPP 95, autoinjector against CWA" IPP-95. Contact Person Data Department of Pharmacology and Toxicology phone/fax: + 48 22 681 61 05 e-mail: [email protected] 189 Department of Radiobiology and Radiation Protection Research activities: Radiobiological Laboratory: Studies of bio-medical effects and health risks associated with exposures to ionizing radiation with special emphasis on the effects of low doses; Examinations of new radioprotective agents; Preparation of expert reports on biological and health effects of ionizing radiation; Lecturing on and training in biological effects and health risks of exposures to ionizing radiation. Laboratory of Radiological Supervision of the Workplace Control of the execution and compliance with the rules of radiological protection in organizational units supervised by the Minister of National Defence and the Minister of Interior (in cooperation with the National Agency of Atomic Energy); Preparation of expert reports and opinions on the observance and execution of the rules of radiological protection in organizational units supervised by the Minister of National Defence and the Minister of Interior (in cooperation with the National Agency of Atomic Energy); Organisation of training courses and lecturing on legal regulations and means of execution of the radiological protection rules in Poland. Laboratory of Recording and Analysis of Individual Absorbed Doses: Computation, registration and analysis of individual doses of ionizing radiation incurred by personnel of organizational units supervised by the Minister of National Defence and the Minister of Interior (in cooperation with the National Agency of Atomic Energy); Evaluation of the incurred doses and estimation of health risks associated with exposure to ionizing radiation in personnel and patients of medical units supervised by the Minister of National Defence and the Minister of Interior; Lecturing on legal regulations and means of execution of the rules of radiological protection in Poland. Laboratory of Radiological Monitoring in the Environment: Routine and occasional analysis of content of gamma- and beta-emitting radioisotopes in air, water, soil, sewage, waste, food, and plant and animal tissue samples; Preparation of expert reports on the sources, dissemination, and magnitude of as well as prevention and protection against radiological contaminations in the environment 190 Evaluation of the potential health risks associated with radiological contaminations in the environment; Lecturing on the sources, dissemination, and magnitude of as well as prevention and protection against radiological contaminations in the environment and on the associated potential health risks Contact Person Data Department of Radiobiology and Radiation Protection phone/fax: + 48 22 681 85 18 e-mail: [email protected] 191 Department of Microwave Safety Department of Microwave Safety (ZOM) has been addressing the impact of electromagnetic fields (EMF) on human health and the environment. ZOM conducts the occupational exposure assessment and environmental concerns in PEM and participates in the protection of workers and the public against electromagnetic radiation. ZOM specializes in studying effects of equipment emitting high-frequency EMF (radio frequency and microwaves), including radar and wireless communication systems (including mobile). In the structure of the Department, there are two laboratories: Laboratory for Biological Effects of Electromagnetic Fields and Laboratory of the Electromagnetic Radiation Metrology. The Laboratory for Biological Effects of Electromagnetic Fields research is conducted on the effects of electromagnetic fields on the human body, including in particular the immune system and cancer processes occurring in the body. The studio is also the issue of health risks and environmental occupational exposure to electromagnetic fields. The Laboratory of the Electromagnetic Radiation Metrology is the assessment of exposure to electromagnetic field staff in the organizational units MON, conducts research in the field of health and safety qualification devices placed on the equipment of the Armed Forces and performs measurements in health and safety and environmental protection. The Laboratory developed the original design of a digital meter (EMF-5) fields and microwave radio, which allows for precise measurement of the intensity of pulsed fields in the environment and at work. Since 2001, the Laboratory is accredited by the PCA. Measurements of the intensity of PEM for the protection of people and staff are made for military units under the program of protection against PEM, as well as on demand for civilian institutions. Laboratory also conducts research on the effects of electromagnetic fields on living organisms and structures, and environmental risks associated with the operation of military equipment generating electromagnetic radiation, develops and implements a position for the calibration of measuring instruments in pulsed electromagnetic fields. The ZOM are developed regulations on occupational health and safety in prevention and health protection of military personnel working in the range of electromagnetic radiation. Contact Person Data Department of Microwave Safety phone/fax: + 48 22 681 61 34 e-mail: [email protected] 192 Department of Regenerative Medicine Scientific activities of the Department focuses on three main directions of research: 1) Potential use of stem cells in regeneration of damaged tissues and organs, including in particular: Isolation and proliferation of stem cells isolated from various organs and tissues, Evaluation of stem cells in terms of: vitality, proliferation, specific markers and potential for differentiation, Creation of animal models, Impact assessment of endogenous and exogenous factors on growth and proliferation of stem cells, evaluation of cell-cycle and apoptosis. 2) The study of regulation mechanisms of the immune response in the course of various diseases, which include: Determination of lymphocyte subpopulations in peripheral blood, including T regulatory cells, Determination of cytokines concentrations; Exploration and study of compounds having immunomodulatory effects, The role of surface markers characteristic of the process of carcinogenesis, Examination of compounds having anticancer properties. 3) The study of damage and repair mechanisms of hematopoietic and immune system during hematological syndrome of ARD, including: Development of ways of assessing human exposure to ionizing radiation by analysis of radiation-induced biological changes; Testing of new methods in the treatment of hematological syndrome of ARD with use of stem cells. Above tasks are performed using the methods: tissue culture, flow cytometry, light microscopy and fluorescence microscopy, ELISA, cell sorting using magnetic beads, using the facilities for experiments on small animals. So far, the results of research conducted in the Department were published inter alia in: The Lancet, Blood, Journal of Cell Sciences, British Journal of Haematology, Experimental Hematology, Mutation Research, Annals of Oncology, Bone Marrow Transplantation, European Journal of Haematology, Burns and Thymus, Central European Jonural of Immunology, Polish Journal of Veterinary Sciences, in various national magazines and in several monographs (including the "Advanced treatment of radiation injuries," Pergamon Press), as well as presented on more than 60 international scientific conferences. 193 Organization: Laboratory of Cell Engineering and Research of Regeneration Processes, Laboratory of Experimental Immunology, Laboratory of Immunological Diagnosis. Contact Person Data Department of Regenerative Medicine phone/fax: + 48 22 681 61 41 e-mail: [email protected] Biological Threats Identification and Countermeasure Centre The military scientific centre in Pulawy dates back to 1949 when the Veterinary Research and Training Centre was moved there from Zamienie (near Warsaw). In the years following, some structural changes were introduced and the Centre grew into an important scientific part of the Medical Services of the Polish Armed Forces. In 1990 the Centre was incorporated into the Military Institute of Hygiene and Epidemiology while still maintaining its relatively large organizational independence. In 2002, the Centre was given its current name The Biological Threats Identification and Countermeasure Centre. The Centre has contributed considerably to the progress of medical, biological and veterinary sciences by carrying out innovative research in toxicology, radiobiology, microbiology, and food hygiene. The international prestige of the Centre has been reflected by the participation of its staff in a number of UN peace-keeping operations in the Middle East (Syria, Egypt, Iraq) and other parts of the world (Cambodia). Currently, the primary research and diagnostic activities of the Centre are focused on the detection and neutralisation of pathogens and toxins used in biological warfare. The Centre's activities have been more effective since the establishment of a biological safety level 3 (BSL-3) laboratory, the only one of its kind in Poland. The staff of the BSL-3 laboratory having trained in relevant scientific institutions in Poland, USA, UK and other countries, not to mention the research performed, has gained the lab international recognition. Contact Person Data Biological Threats Identification and Countermeasure Center 2, Lubelska st., 24 – 100 Puławy, Poland phone/fax: +48 81 886 28 22 e-mail: [email protected] 194 MAJOR RESEARCH AND DEVELOPMENT PROJECTS RECENTLY CONDUCTED AT MIHE: Development project granted by the Ministry of Science and Higher Education No. OR0000909 "Modeling and simulation of processes and procedures to determine a computer-aided risk management in food safety and nutrition." The project aims to develop a system for the support measures for risk management of food safety and nutrition in the country. Ensuring food safety requires taking action in a coordinated manner, involving both the relevant legal regulations concerning the principles of hygiene in production, processing, transport and distribution, an efficient system of official controls on food, as well as implementation in manufacturing plants and food processing food quality schemes, aimed at its safety. Inseparable component of food is water, hence ensuring adequate supplies of water quality, lies in the realm of basic steps to ensure the security of the state. Due to the real possibility of accidental contamination or contamination of food and water throughout the human food chain, as well as the possibility of using food in terrorist activities directed at the man or the agri-food industry is particularly important risk management issue of food safety and nutrition, as a permanent element of the system of supervision over its safety. Development project granted by the Ministry of Science and Higher Education No. OR00004208 „A soldier as a precise weapon – individual sets and kits: protection against CBRN weapons and environmental threats; nutrition and pharmacotherapy – survival in harsh conditions and optimization of psychophysical capacity; medical – biologically active dressings.” The project aims to develop and prepare for the production medical equipment for the individual soldier. The project entails the development of innovative solutions and complements existing ones. The area of interest in the project is to ensure the individual kits in the following areas: First Aid kits in injury, acute illness, contamination and environmental risks specific to the area of combat operations in self-aid, buddy-aid and qualified medical support, in particular: autoinjectors and individual biologically active dressings; New measures in individual packages radio-protective (IPR) for the prevention and pretreatment for operations in an environment contaminated by radiation; Kits containing selected nutrients, dietary supplements and pharmaceuticals, to ensure survival in isolation during combat missions in adverse environmental conditions while maintaining optimal psychophysical performance. The kits comprise water filter and purification device with 195 disinfection tablets that were elaborated with the support from Javel Poland www.aidpol.com, the company the specializes in products indispensible in logistics of humanitarian aid but also military operations. 196 Research project granted by the Ministry of Science and Higher Education No. N308091937 "The occurrence of infection in reservoir animal hantaviruses in terms of human cases in Podkarpackie". The project aims to demonstrate the connection between the presence of the type of Hanta virus in wild rodents hantavirus infections in humans. By identifying infections in humans hantavirus Podkarpackie will be possible to identify potential sites that are living rodent reservoir of this factor. The results confirm the coexistence of the study area in the animal reservoir of the virus, and cases of hemorrhagic fever with renal syndrome in humans of zoonotic origin. Research project granted by European Defence Agency No. B-0060-GEM3-GC-/- “Creating a database on biological agents” The project aims at establishment of an European Biodefence Laboratory Network, EBLN) and management of the network. This will lead to an increase in the degree of preparation of Europe for protection against biological weapons (Biological Warfare Agents, BWA). The project will improve Europe's ability to verify the use of biological agents in the context of the Convention on Biological and Toxin Weapons (BTWC). In case of an event indicating the use of BWA it is necessary to clearly identify a biological agent. The project will design and develop a common database of reference data by typing the microorganisms, which will constitute an essential common resource and enable reliable identification of biological agents. Development project granted by the Ministry of Science and Higher Education No. OR00001909 " Activity of non nucleoside substances against different influenza virus strains." The project for on the synthesis and evaluation of the efficacy of new antiviral active compounds which molecular structure is similar to the oseltamivir, the antiviral activity expected in the mechanism of inhibition of neuraminidase. The aim of chemical-synthetic concept of the project is to treat compounds with proven antiviral activity, including oseltamivir as lead compounds for the synthesis of new structural and functional analogues, in areas not covered by the intellectual property claims. Subsequent project phases included assessing the effectiveness of antiviral activity and cytotoxicity of selected substances in vitro and to investigate the in vitro therapeutical ability based on oseltamivir, probenecid (or its structural analogues) compared with a similar test system based on selected new analogues of oseltamivir. The planned end result was the emergence of the original substances which were effective against influenza viruses with an acceptable toxicity profile, as candidates for industrial-scale production and clinical trial design for an industrial partner. Transmission by respiratory route represents a major epidemiological problem for society, including the armed 197 forces. Experts estimate that WHO influenza pandemic could cause disease in about 30% of human population around the world. Occurrence of influenza pandemic in the general population reduces also the combat readiness of the armed forces because of the known conditions providing a high susceptibility to disease in a population of troops (having to live in crowd, in bad sanitary conditions, with increased susceptibility to infections caused by physical and mental stress). Military Institute of Hygiene and Epidemiology has the ability to validate the newly developed antiviral drugs for antiviral activity against viruses that may require high standards of safety, to the level of BSL3 (Biosafety Level Class 3). Consortium partner Pharmaceutical Research Institute - is able to identify the most likely candidates for antiviral drugs with the desired activity, and their synthesis. Industrial partner has the production capacity and sales. Economic benefit resulting from the project includes the possibility of a antiviral medicine as an alternative to the currently recommended products. This will provide a competitive environment, alternatives to the administrators of public funds in building preparedness pandemic. Research project granted by Defense Advanced Research Project Agency No. N10PC20099 “Nanobiodetector for spore forming bacteria” The aim of this study is to develop a new method of detecting spore-forming bacteria spores using an nanobiodetector. This type of nanobiodetector was already successfully used for the detection of bacterial life forms based on the interaction of bacterial cells with polymer nanofibrils that produce a specific electrical signal. A similar mechanism can be assumed in the case of spores. The device is being tested as an useful tool for the spores detected in a new way, which is very fast and easy to apply. Rapid detection of spores (in the case of spore-forming bacteria) is an important issue and remains a challenge. New nanobiodetector designed and made in the Laboratory of Physical Chemistry of Materials and Nanotechnology (NanoŚrem) is used for detection of spores quickly and efficiently. The applied procedure leads to rapid detection of bacteria forming spores and vegetative cells in liquid suspensions. Research project granted by Defense Advanced Research Project Agency No. N10PC20038 “Novel approaches to wound healing” The project aims to develop and verify the effectiveness of drug delivery system consisting of liposome nanoparticles containing antibiotics (and / or cytokine modulation of the immune response to infection (G-CSF and GM-CSF), incorporated into the polyurethane foam. Another work package in this project is to produce some of the other lysins from genetically different phages against various bacterial strains. This may allow the preparation of the composition of enzymes active against different strains of bacteria that are involved in the colonization of wounds. 198 Research project granted by the Ministry of Science and Higher Education No. N N404 138938 “Evaluation of efficacy of antimicrobial therapy and adenoidectomy as means to eradicate the non-typeable Haemophilus influenzae strains in chronic infections of the higher respiratory tracts”. Research project granted by National Science Center No. 5625/B/P01/2011/40 “The study of environmental reservoirs of Q fever endemic area Coxiella burnetii” Based on information gained during the background interview and serology in animals will be selected potential sources of C. burnetii exposure. Detection of amplification products specific for C. burnetii genome using molecular probes will be done to confirm the presence of genetic material in environmental samples tested. Another part of research will be detailed characterization of isolates of C. Burnetii by phylogenetic MLVA. Tests for the presence of C. burnetii in ticks and in environmental samples will help to determine the current threat of an environmental reservoir, and the results of work will contribute to a better understanding of the epidemiology of C. burnetii infection and their relationship to environmental reservoir. Project No. III.B.05 coordinated by the Central Institute for Labour Protection -National Research Institute “The effect of selected biocides on the organisms that live in the form of a biofilm in circulating systems for metalworking fluids ", implemented in the framework of the multiannual program" Improving the safety and working conditions” Research project granted by National Science Center “Effect of internal contamination of tritium in the non-specific antitumor immunity and inflammatory responses in mice and less sensitive to ionizing radiation”. The project aims to investigate the influence of internal contamination of the mouse small and higher doses of HTO tritium contained in the development of tumor-induced colony and therefore the effect of antitumor and / or anti-inflammatory activity of macrophages and NK cells with different sensitivity to ionizing radiation and the type of immune response to BALB / you C57BL / 6 The planned research are basic and totally original, both nationally and worldwide. The results should significantly enhance our understanding of the biomedical effects of tritium to penetrate the human body such as the action of pro-or anti-inflammatory. 199 The obtained data on the mechanisms of such actions can contribute to finding effective ways of preventing and mitigating the adverse effects of internal contamination by tritium, and to develop new strategies for the prophylaxis and / or treatment of cancer. Research project granted by National Science Center “The study of nicotinic acid derivatives in order to demonstrate their potential radio-protective and / or radio- remedial”. The goal is to identify potential radioprotective properties and / or radio-remedial selected nicotinic acid derivatives (MNA chloride-methylnicotinamide chloride, 1.4-dimethyl-pyridinium 1,4 - DMP, 1metylo-3acetylo chloride-pyridinium-1.3 MAP and nicotinamide-NA) administered at various times before and after irradiation with different doses of gamma radiation, and also understand the mechanisms underlying these properties. These results may contribute to the verification and the prevailing beliefs about the ineffectiveness of existing attempts to obtain adequate radioprotective compounds and / or severe restrictions on their use in practice due to the toxic side effects. Finally, these results should provide the basis for the development of new measures to protect against the occurrence and / or eliminate abnormal radiation in normal tissue of patients undergoing radiotherapy and for victims of radiation accidents or acts of war and terrorist use of nuclear or radiological weapons. 200 Development project granted by the National Centre for Research and Development No. O ROB 0031 01/ID 31/1 „Mobile laboratory for environmental sampling and identification of biological treats” The aim of this project is to elaborate a prototype deployable tactical field laboratory with the unmanned device for sampling. Deployable tactical filed laboratories play a vital role in confirmatory analysis of biological agents as well as expertise advice in the theatre of operation. Rapid accessible results of analysis support commanders decision in terms of adequate protection, medical prophylaxis, treatment or decontamination measures. Shortages in this area led many states to start R&D projects which will help to enhance their capabilities. For example integrated project Biological Detection Identification Monitoring Equipment Development and Enhancement Programme (BIO EDEP) was launched recently, in the frame of European Defense Agency. Polish project “ System for Rapid Sampling and Analysis of Environmental Biological Samples - SFORA” consists of two modules: biological field analytical laboratory and mobile robot for biological agents sampling. SFORA is based on 30’ intermodal container platform, which will provide appropriate deployment and transport capabilities (train, truck, air and maritime). It is supposed to work only on stable, flat surface after deployed, however. The laboratory compartment will provide safe conditions for samples handling, which are the equivalent to containment level 3 microbiological laboratories (HEPA filtration, negative pressure, laboratory decontamination, wastes sterilization and microbiological safety cabinets, pass boxes). On the other hand appropriate equipment will allow for advanced analysis of samples by molecular methods (multiplex PCR, rt-PCR, real-time PCR, and sequencing) and immunological assays (ELISA). The most important advances are introduction of the sequencing capability and rapid microfluidic PCR devices. Our laboratory corresponds to the BIO EDEP subproject 6 -Second Generation Deployable Tactical Field Biological Analysis System. Samples for analysis may be delivered by Biological Survey Teams, but SFORA is also equipped with remote controlled mobile robot (UGV), which can enter the hot zone for sampling of solids, water, air and soil. After return from the hot zone and self-decon UGV transfers itself samples to laboratory compartment by pass box. Robot will be additionally supported by GPS, video camera, NRC sensors and specific and non-specific Bio-sensors developed in frame of this project. Application of UGV will significantly decrease risk of operation related to manual sampling procedures in dangerous environment. International project granted by the European Commission and the Ministry of Science and Higher Education No 241858 “Precursors of explosives: Additives to inhibit their use including liquids” FP7-SECURITY project (the acronym: PREVAIL) project on finding inhibitors to prevent production of homemade explosives. Another project goal is to find a marker/detection system 201 to facilitate detection of illegal use. These objectives must be met without obstruction of the legitimate use of the products and without causing any adverse effects on the environment or people’s health. Project coordinator: Totalforsvarets Forskningsinstitut (FOI). MIHiE’s role: WP Leader, more about Prevail: www.prevail-fp7.eu 202 Catalogue of technologies developed by Polish Research Institutes MATERIAL AND CHEMICAL TECHNOLOGIES, MATERIAL SCIENCE, CHEMICAL AND PROCESS ENGINEERING 203 © lily - Fotolia.com FERTILIZER RESEARCH INSTITUTE (Instytut Nawzów Sztucznych) Organisation Contact Data 13 A, Tysiąclecia Państwa Polskiego st,24 – 110 Puławy, Poland phone: +48 81 473 14 00 fax: + 48 81 473 14 10 e-mail: [email protected] http://www.ins.pulawy.pl/EN/ Instytut Nawozów Sztucznych (Fertilizer Research Institute) seated in Puławy, Poland is a state research institute with a long lasting tradition. Its beginnings as Research Laboratory at United Factories of Nitrogen Compounds date back to 1935. The name was changed into the present one in 1958. INS is one of the best Polish research institutes. It enjoys a good reputation and INS trade mark is well known in Poland and abroad. The principal aim of the Institute is work for chemical industry, mainly its fertilizer and inorganic branches, which leads to making innovations and higher competitiveness of companies operating in chemistry and chemical technology areas. INS carries out research and development work in close partnership with industry employing high qualified staff and maintaining latest standards applying to research methods and procedures. It cooperates with all nitrogen works in Poland and many ones abroad. It has the unique advantage of carrying research works in pilot plants and directly on industrial plants. In the last 10 years INS signed over 100 local contracts and 65 export ones for sale of technologies, licences and products to 15 countries in Europe and Asia. Work for administration and local authorities (tasks defined in the regulation concerning fertilizers and fertilization, REACH and CLP regulations, preparation of expert opinions etc.) are an important Institute activity field. By constant development of the investigation potential, scientific and technical staff, infrastructure and research equipment the Institute is going to become a leader initiating innovatory actions competitive on the local, European and world markets in the area of chemical technology and connected branches such as chemical engineering, safety, and waste management. 204 THE SCOPE OF ACTIVITY: Research and development works including: mineral fertilizers including liquid and suspended ones, feed additives, chemical inorganic products – ammonia, nitric acid, urea, catalysts, sorbents, catalyst supports, plant extracts (hop extracts and others), selected organic products – methanol, formaldehyde melamine, selected plastics processing – trioxane, dioxolane, chemical technology and chemical engineering, environmental protection including wasteless processes of technological streams, purification and influence of organic and mineral fertilizers on agricultural production, impact of mineral fertilizers on natural environment, analysis of potential sources of pollution and contamination caused by fertilizers, sewage and smoke. Experimental production: mineral fertilizers (micro-element concentrates INSOL®; NP, PK, NPK suspension fertilizers), catalysts, sorbents, catalyst support, ceramic balls, hop extract, plant extracts, formalin (reagent grade), research apparatus – gradientless reactors. 205 COOPERATION OFFER 1. Technologies: 1) REVAMPING OF CO2 REMOVAL SYSTEM (BENFIELD/CARSOL UNIT) FROM AMMONIA SYNTHESIS GAS A unit for carbon dioxide removal from synthesis gas is one of the most energy-consuming parts of ammonia production plant and it is also "bottle-neck" limiting production capacity of the whole plant. That is why modernization of the unit is a key issue at modernization of the ammonia plant. Revamping is carried-out by an in-built system of boiler-flash tank-ejector in CO2 removal unit. Semi lean solution of potassium carbonate is directed from the regenerator to the flash tank where adiabatic steam evaporation takes place due to pressure reduction. Steam generated in the flash tank is pressurized by the ejector and is directed to the bottom part of the regenerator. Driving steam for the ejector is generated in an additional boiler which uses heat of process gas. Application of the new system allows to optimize heat utilization for solution regeneration and it increases production capacity and reduces energy consumption. Process characteristics: Process for revamping of CO2 purification units based on Benfield/Carsol technology; Heat recovery of hot solution after regeneration results in: increased production capacity of ammonia plants by 15-20%; reduction of heat consumption after regeneration from 1200 to 880 kcal/1000 Nm3 CO2; reduced natural gas consumption by approx. 25 Nm3/t NH3. INS offer includes a license, know-how, basic design and detailed engineering, supervision during erection and start-up as well as a delivery of key-equipment, piping, and control system. 206 2) IMPROVEMENT OF CARBON DIOXIDE PURITY IN BENFIELD/CARSOL UNIT Purity of carbon dioxide from Benfield/Carsol unit does not exceed 98.5%. It also contains substantial amounts of such impurities as methanol and flammable gases which creates explosion hazard of hydrogen/oxygen mixture. Saturated solution of potassium carbonate containing approx. 0.7-0.8 vol. % hydrogen and other syngas components, flows through a separator after leaving an absorber. A separator where flammable gases are released and separated before the solution enter regenerator, is placed after the expansion turbine. Due to prior inerts separation, CO2 stream from the top of the regenerator contains 99.9% CO2 and only trace impurities and can be used for urea production without further purification. The separator operating at pressure of 4-6 bar, enables a selective liberation of flammable gases from the solution, without any significant CO 2 losses – what allows to increase of CO2 stream directed to the urea production process. Process characteristics: CO2 purity improvement to the level of 99.9 vol. % ; increased pure CO2 stream for urea production by 20-25 %; elimination of explosion hazard in urea synthesis loop; reduction of CO2 compression energy consumption in a urea plant by approx. 5-8 %; increased urea plant capacity by 5 %; reduction of ammonia consumption in urea production plants by approx. 2-3 kg/t NH3. INS offer includes a license, know-how, basic design and detailed engineering, supervision during erection and start-up as well as a delivery of key-equipment, piping, and control system. 207 3) HIGH PRESSURE PURIFICATION OF PROCESS CONDENSATES IN AMMONIA PRODUCTION PLANTS A plant for high pressure condensate degassing serves for removal of ammonia and organic compounds, mainly methanol, from the process condensate. In high pressure process large heat losses are avoided what happens in case of low pressure processes. Stripping technology utilizes overheated stream directed to natural gas steam reforming at pressure of approx. 4 MPa. Impurities are recycled to technological stream and then to the primary reformer where they are decomposed to H2, CO and N2. Pure condensate containing only traces of ammonia and methanol is fed to medium and low pressure steam boilers and its surplus is recycled to a demineralization unit as a raw material for demineralized water production which can be used for feed high pressure boilers. Process characteristics: possibility of the process application in large capacity syngas systems operating with natural gas steam reforming and coal gasification processes; ammonia and methanol recovery; reduction of demineralized water consumption by approx. 1.25 t/t NH3; reduction of exhaust gas temperature by approx. 60 C; the process is not harmful to the environment. INS offer includes a license, know-how, basic design and detailed engineering, supervision during erection and start-up as well as a delivery of key-equipment, piping, and control system. 208 4) SATURATION OF NATURAL GAS IN AMMONIA PRODUCTION PLANT Technology consists in utilization of combustion gas heat and reduction of process steam consumption in reforming section of ammonia plant. A novel system for natural gas saturation with the process condensate is applied in the reforming section with the use of low-potential heat of combustible gases from the reforming furnace. Natural gas, directed to steam reforming process, flows counter-currently to the hot condensate stream which sprays the saturation column. Process condensate is heated in heater located in flue gases utilization section. Natural gas is saturated with steam evaporated from the condensate stream. Reduction of technological steam consumption is a direct effect of the saturation. The generated steam replaces middle pressure process steam. All this results in reduction of natural gas consumption for fuel. Process characteristics: novel technology which can be used in ammonia, methanol, hydrogen plants, etc. reduction of natural gas consumption by approx. 12 Nm3/t NH3 (0.42 GJ/t NH3); reduction of demineralized water consumption in high pressure steam system by 0.4 t/t NH3. INS offer includes a license, know-how, basic design and detailed engineering, supervision during erection and start-up as well as a delivery of key-equipment, piping, and control system. 209 5) SYNTHESIS GAS DRYING IN AMMONIA PLANTS Novel technology for syngas drying on molecular sives with TSA process application is proposed. After methanation process synthesis gas flows through one of 2 driers packed with molecular sieve operating in TSA (Temperature Swing Adsorption) cycle. Final gas drying to moisture content < 1 ppmv H2O and removal of remaining CO2 to the level of < 1 ppmv takes place in contact with the adsorbent. Fresh syngas stream (without any traces of residual moisture and CO2 which are ammonia synthesis catalyst poisons) is mixed with circulation gas stream just before entering ammonia synthesis conventor. As the result NH3 content in the inlet gas stream is reduced and conversion of synthesis gas during one pass through the catalyst bed is increased. This leads to reduction of gas circulation in the synthesis process and enables reduction of synthesis pressure. The final effect of process modifications are reductions of compression energy consumption and synthesis gas circulation as well as reduction of heat losses in the cooling system. Process characteristics: reduced natural gas consumption by 20 Nm3/t NH3; improved product (liquid ammonia) quality. INS offer includes a license, know-how, basic design and detailed engineering, supervision during erection and start-up as well as a delivery of key-equipment, piping, and control system. 210 6) METHOD FOR REDUCTION OF NITROUS OXIDE EMISSION FROM NITRIC ACID PLANTS Nitrous oxide (N2O) is a by-product of nitric acid production process and it is formed in catalytic ammonia oxidation. N2O is a greenhouse gas which destroys the ozone layer protecting Earth against harmful UV radiation. Iron-alumina catalyst developed in Instytut Nawozów Sztucznych (Fertilizer Research Institute) is installed in ammonia oxidation reactor, just under the layer of platinum-rhodium and palladium gauzes (for ammonia oxidation and platinum recovery). The catalyst reduces N2O emission from nitric acid plants even by 95%. Process characteristics: high and stable activity providing N2O decomposition rate in the ammonia oxidation reactor up to 95%; high selectivity – the catalysts does not decompose nitric oxide (NO) it rather increases NH3 to NO conversion rate. catalyst of high mechanical strength; low and stable flow resistance values; low production and utilisation costs of the catalyst; the spent catalysts is not harmful to the environment. INS offer includes a modernization and intensification of nitric acid plants as well as investigations and delivery of catalyst. 211 2. Products: Catalysts and sorbents for the following processes: Raw hydrocarbon desulfurization, Hydrocarbon steam refoming, CO shift reaction, Methanation of carbon oxides, Ammonia synthesis, Reduction of N2O emission in nitric acid plants, Benzene hydrogenation, Oil hardening. Alumina balls – can be applied in many processes of various branches of chemical industry. Plant extracts: Hop extract for brewing, pharmaceutical and cosmetic industries; Blackcurrant seed oil for cosmetic and food industries; Raspberry seed oil for cosmetic and food industries; Strawberry seed oil for cosmetic and food industries; Sweet red paprika extract for food industry, dietary supplements. Mineral fertilizers: Micro-element concentrates INSOL®; INSOMIX® for green-house crop fertigation; NP, PK, NPK suspension fertilizers. Reagent grade formalin Contact Person Data Head of Catalysts & Technologies Marketing & Sale Department: Bogusław Niewiadowski phone: + 48 81 473 14 83 fax: + 48 81 473 14 84 e-mail: [email protected] 212 FOUNDRY RESEARCH INSTITUTE (Instytut Odlewnictwa) Organisation Contact Data Contact Person Data 73, Zakopiańska st,30 – 418 Cracow, Poland General Manager of the Institute: Prof. Jerzy J. Sobczak, DSc., PhD., Eng. phone: + 48 12 26 18 111 fax: +48 12 26 60 870 e – mail: [email protected] phone: + 48 12 26 18 324 e – mail: [email protected] Language contacts: English, Russian http://www.iod.krakow.pl/stronaiod/strona/index.php?lang=en Foundry Research Institute was established in 1946 as a leading scientific research centre of the foundry industry in Poland. Focusing on the problems of reconstruction, first, and modernisation, next, of the domestic foundry industry, in its over sixty five year-lasting period of operation, the Institute has managed to develop and implement many successful and original solutions in the field of new materials, foundry technologies, control and measuring apparatus, and foundry machinery and equipment. In the late seventies, in cooperation with UNIDO, Foundry Research Institute became an important world training centre for the foundry personnel from developing countries. Many times, the Institute staff provided services in numerous countries in Africa and Asia, where our engineers were working as UNIDO experts and specialists in the start up of new foundries. In its present embodiment, the Foundry Research Institute is a research and development centre operating according to the modern market rules, rendering services to the foundry industry, and also to other industries, institutions, offices and international partners. The Institute's mission is to create new energy-efficient and environmentally friendly technologies and materials, and undertake various complex and interdisciplinary tasks in different sectors of the industry. The scope of the services offered by the Institute covers all forms of research and application from planning and preliminary tests to implementation and project economic analysis. The Institute activities covering all problems related with the art of making castings, including basic and applied research, the development of new cast materials and casting technologies, as well as expert studies, are performed by highly specialised staff of research workers. The organisational structure of the Institute is closely related to the scope of its activities. The scientific and technical achievements are particularly evident in the following areas: metallurgy and technology of making castings from a variety of cast materials (based on Fe, Al, Cu, Mg, Zn, Sn, Ti, Ni, Co, and metal matrix composites); 213 the technology of moulding sands, gravity and pressure die casting, investment casting and lost foam process; reclamation and recycling of foundry waste; rapid prototyping, 3D scanning, simulation of the pouring process, solidification and stress distribution; studies of: high temperature liquid state, and the reactivity and stability of liquid metals in contact with solid materials, mechanical properties and structure of cast materials, and physico-chemical and technological parameters of basic and auxiliary materials; defects in castings. The significant scientific and cognitive achievements of the Institute during the last four-year period include: determination of relationship between the manufacturing parameters and performance characteristics of titanium implants made by precision casting and isostatic compaction, development of the mechanism of pressure infiltration of porous bodies and the distribution of reinforcing phase particles to manufacture heterogeneous products with local reinforcement, determination of the effect of alloying elements and heat treatment on the structure and properties of spheroidal and vermicular graphite cast irons, including ADI (Austempered Ductile Iron), development of physico-chemical backgrounds of the synthesis of a water-based binder of the next generation for precision casting, explanation of mechanisms governing the stability and reactivity of nitrides in contact with liquid metals and alloys, determining the mechanism of multi-stage heat treatment of selected alloys, simulation of the solidification and crystallisation processes of monolithic and composite materials (including in vitro and in situ composites – on the example of a regular structure as a concentration-related picture of temperature microfield) and modelling the crack-formation process in cast alloys in a spatial state of stress, studies of the mechanism responsible for the formation of ordered porosity in highporosity media and development of a mathematical model explaining this phenomenon, determining the mechanism of isothermal transformation in ADI with nickel and copper additions austempered in salt bath, studies of the effect of the conditioning regime of sodium silicate glaze on the structure, the value of "zeta" potential and cohesive properties of hydrated sodium silicate serving as a complex binder for the chemically hardened moulding sands, 214 shaping the structure and mechanical properties of a metal - aluminium oxide joint based on physico-chemical phenomena occurring at the phase boundary, synthesis and investigation of mechanism responsible for the formation of new monolithic materials (nickel-free piston silumins and magnesium alloys) and innovative composites (lead-free bronzes, graphite-containing aluminium alloys reinforced with aluminium oxide, silicon carbide, and selected fractions of fly ash), mastering the physico-chemical fundamental rules for the manufacture of cast in situ composites of the Al-Al2O3 type, development of a method for the rheocast-type structure formation in an application approach to the technique of making products in semi-solid state (thixocasting process), developing fundamentals of the chromium-nickel cast steel nitriding process, development of a comprehensive system for the evaluation of moulding sand reclamability and reusability, studies of the effect of evaporative patterns on changes in carbon content in the subsurface layer of iron castings and on the formation of structure and properties of cast aluminium alloys and composite materials, optimising the composition of protective gas mixture in the recycling process of magnesium alloys, computer simulation of the solidification process of castings made from copper and its alloys with further experimental verification. Foundry Research Institute maintains extensive contacts with foreign institutes and companies in the exchange of scientific and technical information, and execution of joint research projects. For many years, the Institute has been very active in the development of international cooperation, carrying into effect a number of long-term international projects, among others, with Russia (All-Russia Institute of Light Alloys), Ukraine (National Academy of Sciences of Ukraine, National Metallurgical Academy of Sciences, Dnepropetrovsk), Germany (Giesserei Institut RWTH - Aachen, IFG - Institut fur Giessereitechnik, Düsseldorf, Institute of Casting Technology in Düsseldorf), China (Shenyang Research Institute of Foundry), bilateral agreements, among others, with Bulgaria (Bulgarian Academy of Sciences), Czech Republic (VSBTU - Ostrava), France (ENSGI - Grenoble and CTIF - Paris), Spain (TECNALIA-INASMET – San Sebastian), Lithuania (University of Technology - Kaunas), USA (University of Wisconsin Milwaukee and Stout, Lawrence Berkeley National Laboratory, National Research Council Washington, Energy Industries of Ohio, University of Central Florida, NASA Glenn Research Center), Japan (University of Osaka, NIRIN - National Industrial Research Institute of Nagoya). With the majority of these research institutes a long-term cooperation agreements or letters of intent have been signed, e.g. with CTIF (France) and TECNALIA-INASMET (Spain) on the research project proposals regarding the renewal and revitalisation of the national foundry industry through tighter linkage with the EU countries. 215 In 2002, at the Foundry Research Institute, a COCAFTEC Centre of Competence for Advanced Foundry Technologies was established. The programme of its activities addresses mainly the countries of Central and Eastern Europe (Baltic countries, Czech Republic, Slovakia, Hungary, Slovenia, Romania, Ukraine and others.). Its activities are supported by participation of the Institute in European projects (e.g. CRAFT - Advanced Process for the Pressure Rolling of Materials in the Foundry Industry, SARE - New Technology for Investment Casting, SUBLIB Lead Free Copper Alloys, CASTEVENTS, COST - Materials Action 531 "Lead-Free Solder Materials”, CORROSION – Detection and discrimination of corrosion attack on ships (oil tankers) with Acoustic Emission, ADI-SYNERGY – Manufacture of castings of ADI using the Lost Foam process, MAGNET – Magnetic moulding – innovative technology to improve the competitiveness and working conditions of the European foundries, ECO-IN-FOUNDRIES – Eco information in SME European Foundries, SURUZ – Scientific Network of Surfacants and Dispersed Systems in Theory and Practice, RECYSAND – Recycling of foundry sands, DIOFUR – Dioxins in Cupolas, rotary and electric furnaces, emission-free melting practises in foundries, FOUNDRYBENCH – Foundry Energy Efficiency Benchmarking, LEAN – Development of Light Weight Steel Castings for Efficient Aircraft Engines) and running the Branch Contact Point for Foundry. Designated by the State Committee of Scientific Research, an expert from the Institute has been appointed Poland’s representative to the Management Committee of the COST Action 531 "Lead Free Solder Materials", which was started in 2003. Foundry Research Institute is a member of many international organisations, such as, among others: CAEF - Committee of Associations of European Foundries, AFS - American Foundry Society, WFO - World Foundrymen Organisation. The basic research programme of the Institute is supported by the standardisation, publishing, training, and scientific-technical activities, the main aim of which is to assist foundrymen working in the industry. In the past four-year period, the Institute issued numerous books, monographs and brochures, conference and seminar proceedings, and training materials. 216 PROJECTS: 1) "Development of technology and launching the production of highquality foundry bentonite based on dried starting material and waste fractions formed in the preparation of sorbents". Contact Person Data Head of Technology Department: Irena Izdebska-Szanda, PhD, Eng. phone: + 48 12 26 18 250 fax: + 48 12 266 08 70 e-mail: [email protected] 2) "Development of technology and launching the production of highquality materials called ‘ekomix’ and of bentonite – ‘ekomix’ mixtures for foundry industry". Contact Person Data Technology Department: Zbigniew Stefański, MSc, Eng. phone: + 48 12 26 18 536 fax: + 48 12 266 08 70 e-mail: [email protected] 3) "Development of an innovative technology and launching the production of modified bentonite used in the manufacture of high surface quality steel castings". The implementation of the above mentioned three projects helped to launch the production of high quality, eco-friendly, bentonite-based materials for foundry. Currently, we can offer readymade implementation of industry-proven high-quality materials, the application of which allows improving the surface quality of castings and reduce casting defects, and has a positive impact on the environment by reducing the level of dust, the use of sorbent post-production fines in the preparation of foundry bentonite, and reducing harmful emissions evolved from moulding sands during casting, especially polycyclic aromatic hydrocarbons and volatile organic compounds. 217 Contact Person Data Technology Department: Zbigniew Stefański, MSc, Eng. phone: + 48 12 26 18 536 fax: + 48 12 266 08 70 e-mail: [email protected] 4) "Development of an innovative design and technology for the manufacture of cast components of agricultural machinery." The aim of the project was to replace the forged and welded blades in bed ploughs with blades made by the casting technology. This conversion of both material and technology has provided longer life of these elements without increasing the cost of their production. The results of operational tests have shown that the manufactured cast blades are more durable than their high quality counterparts made by forging and welding. The project was awarded a number of medals in many national and international exhibitions (Brussels, Paris, Poznan, Kielce and others). As part of this subject, in cooperation with the Industrial Institute of Agricultural Engineering in Poznan, the design and casting technology have been developed to produce a number of tillage tools, like blades for reversible ploughs and single-sided ploughs, subsoiler coulters, cultivator duckfoot, etc. Contact Person Data Head of Department of Ferrous Alloys: Zenon Pirowski, PhD, Eng. phone: + 48 12 26 18 518 fax: + 48 12 266 08 70 e-mail: [email protected] 5) “The start up of production of ferrous castings, designed for operation under extra harsh conditions of abrasive and corrosive wear and tear to replace forged and welded structures". Innovative elements of machines and equipment were designed and made by casting technology to replace elements forged, welded or rolled. The main objective of the project was to develop an innovative design of machines and equipment in terms of their shape geometry, making prototype castings from materials of a new generation intended for use under extra harsh operating conditions, and optimising the mechanical and tribological properties in terms of increased functionality and service life of the developed parts. Further aim of the project was to improve the competitiveness of machinery and equipment, mainly in areas such as agriculture, road building, environmental protection, and transportation. Under this topic, 218 among others, castings of rotor blades for shot blasting machines were developed and implemented in production. The castings won Gold Medal at an exhibition in Brussels. Contact Person Data Head of Department of Ferrous Alloys: Zenon Pirowski, PhD, Eng. phone: + 48 12 26 18 518 fax: + 48 12 266 08 70 e-mail: [email protected] 6) "Determining the impact of technological process on the quality of castings made from nickel superalloys for power, chemical and automotive industries". The project aim is to improve energy security and economic use of the available fuel that is coal, getting less greenhouse gas per 1 MWh of produced energy, reducing the amount of coal mined and transported, reducing solid waste, reducing the consumption of cooling water, and obtaining greater efficiency than with the conventional materials used so far. The scope of the studies carried out by the Institute covers comprehensive research on the properties of some heat- and creep-resistant nickel superalloys, to determine their tendency to react with the furnace atmosphere and ceramic materials used in foundry processes and to develop, based on the results obtained, a technology for casting of these alloys and making pilot castings. As part of this subject, studies have been carried out to master the technology of casting nickel superalloys, such as INCONEL and HAYNES. So far, these alloys have been used only in wrought condition. Mastering the technology of casting the above mentioned elements should enable making the “ready for use" (cast) components often of large overall dimensions and intricate shapes, thus reducing the necessary metal working and welding. Contact Person Data Head of Department of Ferrous Alloys: Zenon Pirowski, PhD, Eng. phone: + 48 12 26 18 518 fax: + 48 12 266 08 70 e-mail: [email protected] 219 7) „Studies and development of modern technology of the cast materials resistant to thermal fatigue". Based on physico-chemical interactions in a ‘liquid metal - coating - metal mould’ system, a new generation of protective and insulating coatings has been developed. The aim of the project is to develop an advanced technology for the manufature of innovative cast materials (ferrous alloys) of controlled structure, modified with alloying elements and offering increased resistance to thermal fatigue under the cyclic changes of temperature. The project also anticipates the development of a modern method for the determination of boundary parameters and dynamics of cyclic changes in temperature and state of stress in the large objects in motion; a prototype test stand to examine the destruction of iron-based alloys under the conditions of cyclic temperature changes; a database of static and dynamic operating parameters of the cast heavy equipment parts for the domestic copper metallurgy industry. The outcome of the project is expected to contribute to the reduced operating cost of numerous devices used by the steel industry, automotive and glass industries, and many other sectors of the domestic industry. Contact Person Data Department of Ferrous Alloys: Andrzej Pytel, MSc, Eng. phone: + 48 12 26 18 239 fax: + 48 12 266 08 70 e-mail: [email protected] 8) „Improving the reliability of lead-free solder joints in electronic packages." The aim of the project is meeting the EU directives prohibiting the use of hazardous substances in electronic products, obtained through improved reliability of lead-free solder joints in electronic packages, manufactured from the environmentally friendly new generation of leadfree solders, and conducting a systematic and comprehensive comparative study of the properties of various types of solder joints produced in laboratory scale and in industry, to identify the causes accounting for the loss of reliability of the connections, and to determine the influence of material characteristics, process parameters and other identified factors on the structure, and physical, mechanical and functional properties of various types of solder joints. Another aim of the project is development and improvement of the soldering process control procedures and quality evaluation of solder joints, as well as the development of solutions to improve the reliability of connections in electronic packages. 220 Contact Person Data Head of Center for High-Temperature Studies Assoc. Prof. Natalia Sobczak, DSc, PhD, Eng. phone: + 48 12 26 18 521 fax: + 48 12 266 08 70 e-mail: [email protected] 9) „Retrofitting the research infrastructure of Malopolska Centre for Innovative Technologies and Materials". The project concerns the priority of research in the field of materials technology. The immediate purpose of the project is to develop a common research infrastructure in the Malopolska Centre for Innovative Technologies and Materials through construction or purchase of new equipment, or retrofitting and/or replacement of the existing test stands with the excellent research and diagnostic apparatus and the experimental and technological equipment necessary for the joint implementation of research programme for processing of metals and materials engineering. Contact Person Data Head of Center for High-Temperature Studies Assoc. Prof. Natalia Sobczak, DSc, PhD, Eng. phone: + 48 12 26 18 521 fax: + 48 12 266 08 70 e-mail: [email protected] The Institute is in charge of the execution of a number of subjects in the strategic project entitled: "Advanced materials and technologies for their production", coordinated by the Institute of Non-Ferrous Metals in Gliwice. The overall objective of the project is to use the latest achievements of modern materials engineering to create a database and to submit an offer for advanced solutions in the field of materials and technology for industries operating in the area of non-ferrous metals. Although this area is strictly related with the non-ferrous metals industry, a number of other modern economic sectors such as electronics, photonics, transport, energy and sources of energy are also involved in the project. 221 1) Area III New light alloy-based materials Area Manager: Adam Kłyszewski, PhD, Eng. (Institute of Non-Ferrous Metals in Gliwice – Light Metals Division Skawina) “Ultralight sections extruded from the new magnesium-lithium alloys”. The aim of the project is to explore the possibility of using new super light Mg-Li alloys to shape products by casting and plastic forming, and to evaluate the possibility of obtaining a high strength/density ratio. Elements of machines and equipment are produced mostly by casting, forging and extrusion, and less often by rolling and drawing. An additional goal will be to examine structural changes occurring in the processed material during plastic forming and mechanical properties of the ready products. Efforts will also be taken to examine the corrosion behaviour of alloys of this type. The obtained information of cognitive, technological and technical character can be used in the development of a manufacturing technology of new products used in the ground and air transport, and in precision industry. Contact Person Data Department of Non-Ferrous Metal Alloys Prof. Andrzej Białobrzeski, DSc, PhD, Eng. phone: + 48 12 26 18 261 fax: + 48 12 266 08 70 e-mail: [email protected] „Elaboration of technology to manufacture special-purpose cast components from titanium alloys." The project aim is to determine optimum parameters of a technological process of making ceramic moulds for precision casting of titanium alloys. Contact Person Data Head of Center for Design and Prototyping Aleksander Karwiński, PhD, Eng. phone: + 48 12 26 18 416 fax: + 48 12 266 08 70 e-mail: [email protected] Center for Design and Prototyping Wojciech Leśniewski, MSc, Eng. phone.: +48 12 26 18 302 fax: +48 12 266 08 70 [email protected] 222 2) Area V Functional metal matrix materials Area Manager: Prof. Jerzy Józef Sobczak, DSc, PhD, Eng. (Foundry Research Institute, Cracow) “The development of squeeze casting and thixocasting technology to produce functionally graded materials and castings from non-ferrous alloys with local reinforcement". The execution of the project has enabled a comprehensive and interdisciplinary solution of the problem related with the manufacture of functionally graded materials based on non-ferrous metals, and with the fabrication of monolithic, laminated and locally reinforced products. The newest concepts of liquid-phase technology, based on the application of high external pressure exerted on the liquid or semi-solid metal during solidification (squeeze casting), combined with thixocasting, or squeeze/pressure liquid metal infiltration of porous shaped elements reinforcing the casting locally were used. Contact Person Data Department of Non-Ferrous Metal Alloys Tomasz Reguła, MSc, Eng. phone: + 48 12 26 18 473 fax: + 48 12 266 08 70 e-mail: [email protected] „Advanced, fly ash-reinforced, light metals-based, composite materials such as MAGFA and ALFA”. The aim of the project is to develop backgrounds for the manufacture of new metal matrix composite materials in which the reinforcing ceramic phase is waste material - fly ash (both materials are referred to as MAGFA® and ALFA® composites, i.e. Magnesium / Aluminium + Fly Ash), where the fly ash is formed during the combustion of coal in power plants. Due to the low value of density and thermal expansion, increased resistance to abrasion, high resistance to thermal shocks and sufficiently good mechanical properties, aluminium- or magnesium-based composites with the fly ash reinforcement are considered to be a potential solution for materials of industrial application, particularly in car transport as materials for brake discs and pistons for IC engines. Institute of Nuclear Chemistry and Technology. 223 Contact Person Data Department of Non-Ferrous Metal Alloys Paweł Darłak, MSc, Eng. phone: + 48 12 26 18 596 fax: + 48 12 266 08 70 e-mail: [email protected] Department of Non-Ferrous Metal Alloys Piotr Długosz, MSc, Eng. phone.: +48 12 26 18 596 fax: +48 12 266 08 70 e- mail: [email protected] 224 3) Area VII Disposal and recycling of materials Area Manager: Prof. IMN A. Chmielarz, PhD, Eng. (Institute of Non-Ferrous Metals in Gliwice) "Ecological foundry mould and core technologies for casting of nonferrous metals, including the recycling and disposal". Task VII.3. in the project "Ecological foundry mould and core technologies for casting of nonferrous metals, including the recycling and disposal" has as a main objective introducing new ecological binders to the process of making moulds and cores for casting of non-ferrous alloys to replace the most commonly used sands with bentonite and resin binders. The use of the new technology based on ecological inorganic binders characterised by favourable technological parameters and better knocking out properties and reclamability shall reduce the adverse effect of waste moulding materials on the environment. The methodology and studies carried out within the framework of the project will make a basis for the development of complex mould- and core-making technology with recycling and disposal of waste materials. Contact Person Data Head of Technology Department Irena Izdebska-Szanda, PhD, Eng. phone: + 48 12 26 18 250 fax: + 48 12 266 08 70 e-mail: [email protected] „Recycling of process scrap of cast magnesium alloys using an innovative method of endomodification". The aim of the project is to explore and explain the mechanism of magnesium alloys endomodification by introducing to the primary alloy a specified, in terms of both quality and quantity, addition of different grades of process scrap. The use of own process scrap additionally allows its recycling in the foundry. The end result of the project is clarifying the mechanism by which compounds contained in the scrap can affect the process of the endomodification of liquid alloys of magnesium, and developing instructions and technical documentation concerning introduction of process scrap to the metal charge (recycling) and its impact on the quality of magnesium alloy castings. 225 Contact Person Data Department of Non-Ferrous Metal Alloys Aleksander Fajkiel, PhD, Eng. phone: + 48 12 26 18 284, fax: + 48 12 266 08 70 e-mail: [email protected] Department of Non-Ferrous Metal Alloys Piotr Dudek, PhD, Eng. phone.: +48 12 26 18 473 fax: +48 12 266 08 70 e- mail: [email protected] 226 “Studies of casting properties and determination of quality requirements for products cast from magnesium alloys designated for further decorative and protective surface treatment”. The research work was carried out within the target project: UDA-POIG.01.04.00-16-001/0800/UDA-POIG.04.01.00-16-001/08-00 "Innovative technology for application of coatings on magnesium castings at Polmag " and it covered complex development of technology enabling application of decorative and protective coatings on die castings made from selected magnesium alloys, allowing for the specific character of the hot chamber die casting process. The scope of work included: identifying requirements regarding the surface condition of castings, including the casting surface defects such as folds, streaks, flower outlines, etc assessment of surface quality for the presence of elements from the technological process, including the phase analysis of chemical compounds present on the surface of castings, selection of technological parameters of the casting process for better surface quality. The composition of the decorative and protective coatings and the process of their deposition on the test magnesium alloy die castings have been developed within the framework of cooperation with the IMN OML - Skawina. The end result of the work was the development of guidelines for pressure die casting parameters to achieve the required surface quality of magnesium alloy castings necessary for the application of protective and decorative coatings. Contact Person Data Department of Non-Ferrous Metal Alloys Aleksander Fajkiel, PhD, Eng. phone: + 48 12 26 18 284, fax: + 48 12 266 08 70 e-mail: [email protected] Department of Non-Ferrous Metal Alloys Piotr Dudek, PhD, Eng. phone.: +48 12 26 18 473 fax: +48 12 266 08 70 e- mail: [email protected] 227 „Aluminium matrix composites with the textile 3-D (3D-CF/Al-MMC) type reinforcement for parts operating under complex loads in the automotive industry and machine building sector." The aim of this German-Polish bilateral project is to combine the possibilities offered by materials science, mechanical engineering and technology to develop an effective, optimised in terms of mechanical properties, and sustainable approach to the fabrication of carbon fibre / aluminium matrix composites reinforced with 3D type fabric. Within the framework of the project, theoretical and technological backgrounds will be developed to use a considerable potential of the low density metal matrix composites, and also wide opportunities to design their properties. Particular emphasis will be placed on selection of appropriate fibres and aluminium alloys, and best techniques of their modification, as well as optimising the strength of 3D shaped elements based on the available fabrics and allowing for the thermomechanical service loads under different operating conditions. Contact Person Data Head of Center for High-Temperature Studies Assoc. Prof. Natalia Sobczak, DSc, PhD, Eng. phone: + 48 12 26 18 521 fax: + 48 12 266 08 70 e-mail: [email protected] 228 „Studies of the effect of various factors on the properties of liquid and semi-solid lead-free solders for high temperature applications (COST MP0602)". The project concerns the participation of Polish research units in the European Union programme implemented within the framework of COST Action MP0602 entitled: "Advanced Solder Materials for High-Temperature Application - HISOLD" executed in the period of 20072011. The scope of work is aimed at high-temperature liquid state studies and liquid-phase technologies to manufacture alloys and soldered joints, including a comprehensive study of properties of selected alloys in the liquid state (melting point and temperature of phase transformations in the liquid state, density, surface tension of liquid alloys, the kinetics of wetting and spreading in contact with different materials) and determination of the effect of major technological factors (temperature, atmosphere, alloying additions, the technique of preparing a solid substrate, e.g. by metal coating). Contact Person Data Head of Center for High-Temperature Studies Assoc. Prof. Natalia Sobczak, DSc, PhD, Eng. phone: + 48 12 26 18 521 fax: + 48 12 266 08 70 e-mail: [email protected] „Passive protection of mobile objects (air and ground) from the impact of AP projectiles”. The project covers research and development of sandwich panels for armour components made of lightweight materials designed to be technologically innovative on a global scale, and above all competitive in many respects to the ones manufactured and used previously. The developed solution offers highly effective protection against the impact of AP type small-calibre projectiles and can be incorporated into the outer layers of a security system of the mobile transport means (ground and flying vehicles). The design of armour in terms of the materials applied (light alloys, ceramics) is characterised by a low surface weight, which significantly reduces the total weight of the vehicle, affecting the economics of use - lower fuel consumption, possible increase in the vehicle capacity. The unique solution of the armour design and the method of manufacture based on the available techniques of casting (squeeze casting) make this type of armour cheap, durable, and requiring no costly and time-consuming finishing work. 229 Contact Person Data Department of Non-Ferrous Metal Alloys Paweł Darłak, MSc, Eng. phone: + 48 12 26 18 596 fax: + 48 12 266 08 70 e-mail: [email protected] Department of Non-Ferrous Metal Alloys Piotr Długosz, MSc, Eng. phone.: +48 12 26 18 596 fax: +48 12 266 08 70 e- mail: [email protected] „The process of structure formation in the ternary Gd-Co-Ti alloys". The project aim is to determine the physical and thermodynamic properties of a new class of advanced materials, which are ternary Co-Gd-Ti alloys characterised in the liquid state by an area of limited miscibility. The scope of the planned research is directed at understanding the process of shaping a unique structure of the alloy during rapid cooling, and in particular at the clarification of the existence of an area of the limited miscibility, investigating further the composition of the coexisting phases, as well as the physical properties of homogeneous liquid phases or their mixture. The selection of alloy chemical composition is expected to enable fabrication of new metal composite materials with a metallic glass matrix. Contact Person Data Head of Center for High-Temperature Studies Assoc. Prof. Natalia Sobczak, DSc, PhD, Eng. phone: + 48 12 26 18 521 fax: + 48 12 266 08 70 e-mail: [email protected] „Technology for processing of titanium alloys by casting route for production of implants and surface treatment." The project aim is to develop the basic parameters of a technological process for precision casting of titanium alloys. Contact Person Data Head of Center for Design and Prototyping Aleksander Karwiński, PhD, Eng. phone: + 48 12 26 18 416 fax: + 48 12 266 08 70 e-mail: [email protected] 230 „Complex technologies for the manufacture of cast spare parts of the military equipment and individual medical implants using rapid prototyping techniques". For special applications, such as military vehicles used by special services - fire, medical and the like ones, numerous items are made individually and are tailored to the specific needs of a given vehicle. In this case, making models of special parts by the methods of rapid prototyping allows quick verification and finding an optimum design solution. For the needs of the project, numerous parts used in the automotive industry made so far by the traditional methods of casting (e.g. gears, rocker arms, crosses, brake calipers) were identified. At the same time, attention focused on the selection of parts that would be representative of both the precision casting process and casting in sand moulds. Precision casting technology has been used for castings with different characteristics in terms of the alloy cast, and casting geometry, shape and weight. This is a different approach to the practical application of investment casting process, which is currently used to make small but complex castings. Making models by rapid prototyping (RPS) allows for multiple and rapid, compared to traditional pattern-making techniques, changes in part configuration without having to incur the high costs of foundry pattern and mould production. In development of the operating parameters of the component and in elaboration of the casting technology, the following numerical programmes were used: Ansys, Abaqus, MAGMASOFT, Flow3D. Studies of the casting process to make the test parts included: control of metallurgical processes (metal preparation), all tests and examinations related with the lost foam patterns in ceramic layered moulds (the investment process), preparation of these moulds for pouring (e.g. determination of an optimum mould temperature). In the case of sand mould castings, the studies aimed at the selection of the most appropriate sand mixture to make these castings. Studies included monitoring and examining the accuracy of reprodution, casting surface quality, the time necessary to make a mould, and the knocking out properties.. Contact Person Data Center for Design and Prototyping Stanisław Pysz, Eng. phone: + 48 12 26 26 18 313 fax: + 48 12 266 08 70 e-mail: [email protected] 231 „Development of surface and materials technology for the manufacture of parts and components operating in a high reliability drive system for the long-term and permanent prosthetic heart." The project aim is to develop a surface engineering technology and a materials technology for the manufacture of parts and components of a high reliability drive system for the long-term and permanent prosthetic heart. Contact Person Data Head of Center for Design and Prototyping Aleksander Karwiński, PhD, Eng. phone: + 48 12 26 18 416 fax: + 48 12 266 08 70 e-mail: [email protected] „The new generation of liquid ceramic slurries for precision casting based on multifunctional binders of improved biocompatibility." The utilitarian purpose is to develop technologies for the manufacture of precision castings from reactive alloys such as titanium, using water-based binders with selected colloidal solutions (SiO2, Y2O3, ZrO2 and CeO2). Contact Person Data Head of Center for Design and Prototyping Aleksander Karwiński, PhD, Eng. phone: + 48 12 26 18 416 fax: + 48 12 266 08 70 e-mail: [email protected] „Development of an innovative casting technology using directional solidification." The outcome of project execution will be implementation of new technological solutions and application of advanced techniques in the preparation of production (CAD/CAM), verification of casting technology (computer simulation of pouring, solidification and cooling of castings), organisation and planning of production (FEM), and enterprise management (ERP). 232 Contact Person Data Head of Center for Design and Prototyping Aleksander Karwiński, PhD, Eng. phone: + 48 12 26 18 416 fax: + 48 12 266 08 70 e-mail: [email protected] “Innovative ceramic-carbon filters for metal alloys”. The project aim is to develop a technology for making filters of a new type for the filtration of liquid metal alloys and a method for the use of these filters in casting practice. The use of the ceramic-carbon filters provides the required mechanical strength and thermal stability on pouring of moulds with liquid metal, as well as a good corrosion resistance to the effect of liquid alloy. The structure of the filter wall surface forces a laminar alloy flow through the pores of the filter. An additional advantage is the high thermal conductivity of the filters. Ceramiccarbon filters are designed for the filtration of cast steel, and nickel and cobalt alloys, and can replace the zirconia filters used so far. Also important is the economic effect resulting from a lower temperature at which the filters are being fired. Contact Person Data Head of Center for Design and Prototyping Aleksander Karwiński, PhD, Eng. phone: + 48 12 26 18 416 fax: + 48 12 266 08 70 e-mail: [email protected] „Development of design and technology to make a hydroactive suspension system used in mobile unmanned vehicles resistant to IED type threat”. The aim of the project was to develop a new design of the suspension system made from new materials. The use in the suspension design of castings instead of parts forged or welded gives more flexibility in the choice of material and in shaping the geometry of the structure. The world trends are aiming at a significant reduction in labour consumption necessary to make a given part. The developed methods for computer modelling and data exchange, and the advanced modelling algorithms allow completing and limiting the physical experiments. Integrated Computational Materials Engineering ICME is a new direction in the rapid development of materials and implementation of new technologies. It provides numerous benefits, including considerable reduction in the design and lead time, mainly due to a 233 comprehensive analysis of many variants of the solution without the need for a costly and energy-intensive research carried out on true models. In the study, various programmes have been used, among others, for material analysis (Pandat), operation (Ansys, Abaqus), and the technology of manufacture (MAGMASOFT, Flow3D). The conversion of design or of both the design and material requires the use of modern materials and modern manufacturing technologies, all in close cooperation carried out between the researcher, designer and technologist. Contact Person Data Center for Design and Prototyping Stanisław Pysz, Eng. phone: + 48 12 26 26 18 313 fax: + 48 12 266 08 70 e-mail: [email protected] “Development of technology for casting responsible titanium alloy elements improving in a significant way the technical parameters of the equipment manufactured for the automotive industry, chemical industry, and medical applications”. A utilitarian objective is to develop a technology for the production of precision castings in reactive metal alloys, using water-based binders prepared from the colloidal solutions in SiO2, Y2O3, ZrO2 and CeO2, thus significantly reducing the thickness of the surface layer of casting. This should enable undertaking the commercial production of small responsible castings requiring in practice nearly no expensive machining. Contact Person Data Center for Design and Prototyping Wojciech Leśniewski, MSc, Eng. phone: + 48 12 26 18 302 fax: + 48 12 266 08 70 e-mail: [email protected] 234 INDUSTRIAL CHEMISTRY RESEARCH INSTITUTE (Instytut Chemii Przemysłowej) Organisation Contact Data 8, Rydygiera st, 01-793 Warsaw, Poland phone: +48 22 568 20 00 e-mail: [email protected] http://en.www.ichp.pl/ TECHNOLOGIES 1) Synthesis of (2R,3S)-3-phenylisoserine (2R,3S)-3-phenylisoserine-a-amino-b-hydroxyacid hydrochloride of structural formula: obtained according to the offered technology is characterized by high enantiomeric purity > 99 % and the following physicochemical properties: molar mass: 217.50 g/mol chemical formula: C9H11NO3 · HCl chemical purity: 98.0 % (HPLC, obs = 210 mm) optical rotation of sodium light: melting point: 242–244 °C solubility: soluble in water, poorly soluble in alcohols CAS No: 132201-32-2 = -14.6 (c = 0.55, 6 M HCl aq., temp. 20 °C) (2R,3S)-3-phenylisoserine hydrochloride constitutes a side chain in a particle called paclitaxel with a formula: 235 Paclitaxel is a bioactive substance isolated from the bark of yew Taxus brevifolia, vegetating at the Pacific coast of the USA. The second component in the paclitaxel particle is 10deacetylbaccatin III, available in Poland (Agropharm Company, Tuszyn near Łódź). Paclitaxel reveals activity in curing such kinds of neoplasm like ovary, breast and lung cancer. World demand for paclitaxel is 250 kg/year. A brief description of the technology In the first stage of the synthesis methyl trans-cinnamate is stereoselectively oxidized into methyl (2R,3S)-2,3-dihydroxy-3-phenylpropionate in the presence of a chiral catalyst. As a result, the synthesis produces methyl (2R,3S)-2,3-dihydroxy-3-phenylpropionate with 72 % yield and enantiomeric purity after crystallization 99 % ee. It is the key stage of the synthesis, which decides on the stereochemistry of the product. Then, after a number of reactions of type esterification, addition and reduction with hydrogen, there is obtained a product in the form of ester, which at the last stage of the synthesis is hydrolyzed, yielding white crystals of (2R,3S)-3-phenylisoserine hydrochloride with purity over 98 % and 99 % ee α 20 D 13,5 . The yield of this method related to methyl cinnamate is 23 %. Advantages of the technology offered The technology offered allows to obtain (2R,3S)-3-phenylisoserine hydrochloride with purity > 98 % and 99 % ee. Equipment The installation to produce (2R,3S)-3-phenylisoserine hydrochloride should be equipped with glass apparatus placed in specially adapted rooms, according to GLP requirements. The installation is based on two apparatus sets: an universal glass set with a glass or enameled reactor 120 l in capacity to conduct syntheses and distillations, a Simax glass set for extraction, with an extractor 200 l in capacity and 2 tanks for phase separation, 100 l in capacity each. The reactor instrumentation should include a Teflon stirrer of propeller type with speed adjustment, a sounder to measure temperature and pH of the reaction mixture, two substrate feeders, a distillation column, a condenser, a cooling bath and a distillate receptacle. The reactor blanket should be adjusted to heating the reactor up to 150 °C and cooling it contents down to -30 °C. Patents Patent application P-385 118 (2008) „(2R,3S)-3-phenylisoserine hydrochloride purification 236 method”. Market competitiveness Implementation of the technology enables to obtain the product of domestic origin and thus lowering the medication price on the Polish market. References Confirmation of high chemical and enantiomeric purity of the product by customers. Contact Person Data Barbara Kąkol, M.Sc., Chem. Eng. phone: + 48 22 568 22 97 e-mail: [email protected] 237 2) Obtaining heparin Heparin – a sulfonated mucopolysaccharide, derived mainly from animal organs in the form of crystalline sodium salt. Sodium, calcium and ammonium salts of heparin are used in the health service. Lithium heparin is used for test tube coating in biochemical research and in gasometric analysis. A brief description of the technology The process involves two stages. The first stage consists of obtaining heparic acid from a sodium salt of unfractionated heparin. A concentrated sulfuric acid is added to a 10 % aqueous solution of sodium heparin with pH 8.3 until pH 0.5 is reached. At the second stage, porophores from sulfonyl groups are substituted with metal or ammonium cations. Then the appropriate hydroxide is introduced into the heparic acid solution, resulting in full substitution of sulfonyl groups with hydroxide cations. The hydroxide is added until pH 9.2–10.2 is reached. If heparin ammonium salt is to be obtained, concentrated aqueous ammonia solution is added to crystalline heparic acid until pH 9.5–10 is reached and then full dissolution of the acid crystals is effected through stirring. Instead of hydroxides may be applied oxides or carbonates of cations to be introduced. At the third stage appropriate heparin salt is precipitated with alcohol (methanol or ethanol). The solution shall be stirred while adding alcohol. After drain-off the heparin salt crystals are rinsed a few times with alcohol and then dried. Advantages of the technology offered The technology does not require any complicated apparatus, is cheap and the product obtained with 98 % efficiency is very pure (pharmacopeial purity). Currently employed methods to obtain salts, other than sodium ones, comprise mainly running an aqueous solution of heparin sodium salts through columns filled with a cation exchange resin filled with appropriate cations, which substitute sodium cations. The electrodialysis method can also be applied, using appropriate membranes permeable to cations and anions. Both methods produce good results but the electrophoresis method requires specialist apparatus, whereas the ion exchange method causes expansion of the puncture front and hence dilution of solutions, complicating the precipitation process and lowering its efficiency. Equipment open agitators, vacuum nutsche filters, drying chambers, pH meter. 238 Patents Patent application P-386 867 (2008) „Method to obtain other heparin salts from sodium heparin”. Market competitiveness No information. References The technology has been developed on a laboratory scale. It has not been implemented. Contact Person Data Irena Grzywa-Niksińska, Ph.D., Chem. Eng. phone: + 48 22 568 20 05 e-mail: [email protected] 239 3) Obtaining morphine Morphine is known throughout the world as a pain relieving medication. A brief description of the technology The method comprises morphine separation from the aqueous extract with appropriately matched absorbents and then desorption. The product obtained is of high purity. Advantages of the technology offered In comparison to traditional methods, the method is simple as far as technology and apparatus are concerned and less power-consuming. Other methods involve multiple extraction / reextraction and then evaporation. Equipment Extractors, columns, agitators, a drying chamber. Market competitiveness No production in Poland. References The technology was implemented in the Kutno Pharmaceutical Plant. Contact Person Data Irena Grzywa-Niksińska, Ph.D., Chem. Eng. phone: + 48 22 568 20 05 e-mail: [email protected] 240 4) Separation and purification of salicylic acid Salicylic acid is an ortho-hydroxybenzoic acid. It is produced in big quantities and constitutes an important precursor to produce numerous pharmaceutical preparations. A brief description of the technology Salicylic acid is produced mainly from phenol. The post-reaction mixture contains: sodium salicylate, excess sodium hydroxide or sodium carbonate, small amounts of phenol and a number of unidentified by-products of tarry character. Salicylic acid is isolated from this solution by thinning with water and separation with hydrochloric or sulfuric acid. This way obtained raw acid has brown color and is much polluted. The developed technology to purify raw salicylic acid comprises selective absorption and desorption. Advantages of the technology offered The method of selective absorption and desorption employed to remove pollution and byproducts from the salicylic acid is less power-consuming and cheaper than the traditionally used sublimation method. Equipment three column sets (three columns each) filled with the same absorbent (in the production process two columns in each set operate connected in series and the third one is then regenerated), agitators, filtration press. Patents Patent No P-192 178 „Method to purify raw salicylic acid”. Market competitiveness The method is much cheaper and more efficient than the sublimation method. References The technology was developed on the half-technical scale and has not been implemented so far. Half-technical trials have been performed on the installation mounted in a production hall at the PSA branch of the „Polpharma” Pharmaceutical Plant in Starogard Gdañski. Contact Person Data Irena Grzywa-Niksińska, Ph.D., Chem. Eng. phone: + 48 22 568 20 05 e-mail: [email protected] 241 5) Extract from root and leafy parsley fruits Dietary supplements constitute a concentrated source of nutrients or other substances with feeding or physiological effect. Their receiving is favorable in complementing the daily diet with some lacking mineral nutrients and vitamins and in correcting nutrient deficiencies caused by dietary recommendations or social, cultural and aesthetic ramifications. There are grown two species of parsley (Petroselinum sativum Hoffm., syn. Apium petroselinum L.): leafy (subsp. macrocarpum), with hard, inedible roots, whose leaves are used for food, root (subsp. microcarpum), with edible both roots and leaves. Both species contain ethereal oils, giving them specific taste and flavor. Ethereal parsley oil contains mainly allyl-4-methoxybenzene, apiol (0.06–0.08 %), myristicin and -pyrene. According to the developed technology, two products are obtained: Loose – ground and dried parsley root with the extract deposited on it; Liquid – oily extract obtained by extraction from parsley fruits using soya oil or extract obtained by extraction from parsley fruits using liquid and supercritical carbon dioxide, thinned with soya oil. Obtained preparations constitute a feedstock into hard or soft capsules. A brief description of the technology Leafy and root parsley fruits are subjected to extraction using soya oil or liquid and supercritical carbon dioxide and then the extract is stabilized with tocopherol used in the quantity of 0.1 wt. %. As extracts from fruits of both parsley species (root and leafy) contain comparable apiol quantities, both kinds of fruits can be used interchangeably. The best extrahent of apiol from parsley fruits is supercritical carbon dioxide (apiol contents – 0.681 %). The process proceeds with efficiency about 3.4 %. In the extraction can be applied edible soya oil, which is a good apiol solvent. This simplifies the technological process and allows to skip a complicated analysis of vestigial amounts of organic solvents in the food product. Extraction with liquid and supercritical carbon dioxide A carbon dioxide stream under appropriate pressure is fed into the extractor using a pump and then the stream is decompressed using a throttling valve, down to the atmospheric 242 pressure. Then it is directed to a receptacle placed in a bath at temperature about -30 °C, goes through a rotameter and a gas meter and finally returns to the installation. Oil extraction Ground seeds of root or leafy parsley are placed in an agitator, a specified amount of soya oil is added and then the extraction proceeds for 24 or 72 h. Then the reactor contents is filtered and the extract is analyzed for apiol contents. Advantages of the technology offered The technological process of oil extraction is simple and does not require any complicated apparatus. The only labor-consuming stage is the filtration process. An advantage is also the usage of edible soya oil, allowing to avoid specific analytic check of the product, necessary if other solvents are used. Equipment Extraction with liquid and supercritical carbon dioxide requires special pressure apparatus: extractor, pump, receptacle placed in a cooling bath at temperature about -30 °C. Oil extraction: agitator, filtration press. Patents Patent application No P-381 198 (2006) „Dietary supplement, especially for diabetics”. Market competitiveness There has been obtained a liquid preparation with twice more apiol contents than in commercially available products. Contact Person Data Magdalena Jezierska-Zięba, Ph.D., Chem. Eng. phone: + 48 22 568 22 97 e-mail: [email protected] 6) Extract from celery fruits Celery, both root and leafy, is a precious source of mineral nutrients (contains i.a. potassium, zinc, calcium, iron, phosphorus, magnesium) and vitamins (C, of group B, PP, E and provitamin A). Curative properties has first of all uncooked celery. It purifies blood, slows down ageing process, produces soothing, anti-depressive and painkilling effect. 243 Characteristic, typical and lasting flavor and taste of celery give it mainly two lactones: 3-n-butyl phthalide and 3-n-butyl 2-hydrophthalide. Contents of these ingredients in oils and extracts does not exceed 1 %. Total contents of these lactones is a measure of the extract concentration in preparations to be encapsulated. Carbon dioxide in supercritical state extracts from celery fruit 0,9 % of sedanolide (3-n-butyl 2hydrophthalide) and 0,5 % of n-butyl phthalide. A brief description of the technology Fruits of leafy or root celery undergo extraction with soya oil or carbon dioxide in liquid and supercritical state. The process proceeds with efficiency of about 3.4--3.96 %. As extracts from fruits of both root and leafy celery contain comparable lactone quantities, both kinds of fruits can be used interchangeably. In the case of root celery fruits the extraction time should be longer, compared to the leafy species. Extraction with liquid and supercritical carbon dioxide A carbon dioxide stream under appropriate pressure is fed using a pump into an extractor placed in a water bath at temperature about -30 °C. The carbon dioxide stream with the extract solved is then decompressed using a throttling valve, down to the atmospheric pressure and is directed to a receptacle placed in a bath. The carbon dioxide stream goes from the receptacle to a gas meter and finally to the installation. Extraction with oil Ground seeds of root or leafy celery are placed in an agitator, a specified amount of soya oil is added and then the extraction at room temperature proceeds for 24 or 72 h. Then the reactor contents is filtered and the extract is analyzed for lactones contents. Advantages of the technology offered The extract obtained using liquid and supercritical carbon dioxide combines magnificent flavor of celery oil with intensive taste of oleoresins and also is free of macromolecular compounds i.e. waxes, fats and proteins. It can be applied as an ingredient of food flavors, soup concentrates and spices and also as an aromatizing ingredient for other food products. The extract in the form of yellow liquid and with intensive celery flavor has the following physicochemical properties: density, d420 890 kg/m3 refractive index, nD201,4800 244 acid value, (AV) 27 mg KOH/g saponification value, (SV) 236 mg KOH/g Application of edible soya oil in the extraction simplifies the technological process and allows to skip a complicated issue to analyze vestigial amounts of organic solvents in the food product. Equipment Extraction with liquid and supercritical carbon dioxide requires to use special pressure apparatus e.g.: an extractor and a receptacle placed in a water bath and a rotameter. Market competitiveness On the Polish market there are no preparations containing celery extract. References The celery extract received an approval issued by National Hygiene Institute and can be applied in production of food flavors. Contact Person Data Barbara Kąkol, M.Sc., Chem. Eng. phone: + 48 22 568 22 97 e-mail: [email protected] 245 7) Didecyldimethylammonium acesulfamate Didecyldimethylammonium acesulfamate – an ionic liquid with fungicidal and bactericidal properties. The compound may be used as an active agent in cosmetic preparations, such as: toothpastes, antiseptic mouth rinses. It has no toxic effect on warm-blooded organisms (toxicity class IV). Structural formula: O R R N + CH3 CH3 NH3C O R = C10H21 S O O chemical formula: C26H52N2O4S molar mass: 488.8 g/mol Didecyldimethylammonium acesulfamate is a thick liquid, with color from light-yellow to willow-green-lemon, specific, pleasant smell and sweet taste. Well soluble in chloroform, chloromethane and ethanol but poorly soluble in warm and cold water. Total decomposition temperature is 483 °C. A brief description of the technology Didecyldimethylammonium acesulfamate is obtained in a reaction between didecyldimethylammonium chloride and potassium acesulfamate, conducted in aqueous environment. The product is separated by extraction with methylene chloride. The ionic liquid, solved in an organic solvent, is concentrated by distillation under reduced pressure. Purification of the product is conducted with extraction methods. In order to remove water, additional drying of the product is needed, at increased temperature and under reduced pressure. Advantages of the technology offered The technology is simple, energy-saving and low-waste. The environment of the reaction is aqueous and methylene chloride used can be turned back and used in the next synthesis. A waste product is potassium chloride. The reaction proceeds with big efficiency. The technology has been implemented on the scale about 5 kg per batch. 246 Equipment A glass reactor with bottom drain valve, fitted with a high-performance, high speed mechanical stirrer, a thermometer and a dephlegmator, which can be exchanged for a distillation set. Additionally it should be equipped with a heating / cooling jacket, enabling to heat up or cool down the contents. Auxiliary equipment consists of: thermostat, membrane vacuum pump, vacuum evaporator (for final drying of the product). A precise description of analytic methods is included in a factory standard, worked out for the product. Market competitiveness Product interchangeable with commonly used biocidal constituents with similar or better bactericidal and fungicidal properties, but of better, more acceptable taste. It is non-toxic for warm-blooded organisms and price-attractive. Contact Person Data Anna Wiśniewska, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] Anna Kulig-Adamiak, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] 247 8) Didecyldimethylammonium saccharinate Didecyldimethylammonium saccharinate an ionic liquid of sweet taste, with fungicidal and bactericidal properties. May be used as an active agent in cosmetic preparations, such as: toothpastes, antiseptic mouth rinses. It has no toxic effect on warm-blooded organisms (toxicity class IV). Structural formula: O R R N + N CH 3 CH 3 S O - O R = C10H21 chemical formula: C29H52N2O3S molar mass: 508.8 g/mol Didecyldimethylammonium saccharinate is a thick, non-volatile liquid, crystallizing at room temperature, of color from light-yellow to willow-green-lemon, specific, pleasant smell and sweet taste. Well soluble in chloroform, chloromethane and ethanol but poorly soluble in warm and cold water. Total decomposition temperature is 291 °C. A brief description of the technology The compound is obtained in a reaction between didecyldimethylammonium chloride and sodium saccharinate, conducted in aqueous environment. The product is separated by extraction with methylene chloride. Resulting ionic liquid, solved in an organic solvent, is concentrated by distillation under reduced pressure. The product needs additional drying at increased temperature and under reduced pressure, in order to remove water. Advantages of the technology offered The reaction proceeds with big efficiency. The technology is simple, energy-saving and low-waste. The reaction proceeds in water and methylene chloride used can be turned back to the next synthesis. The only by-product is sodium chloride. The technology has been implemented on the scale about 5 kg per batch. 248 Equipment The apparatus set to synthesize ionic liquids consists of a glass reactor with bottom drain valve, fitted with a high-performance, high speed mechanical stirrer, a thermometer and a dephlegmator, which can be exchanged for a distillation set with a heating / cooling jacket, enabling to heat up or cool down the contents of the reactor. Auxiliary equipment consists of: thermostat, membrane vacuum pump, vacuum evaporator (necessary for final drying of the product). A factory standard worked out for the product includes description of analytic methods. Market competitiveness Product in some cases interchangeable with commonly used didecyldimethylammonium chloride. It has similar or even better fungicidal and bactericidal properties and better, more acceptable taste. Contact Person Data Anna Wiśniewska, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] Anna Kulig-Adamiak, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] 249 9) Syndiotactic polystyrene (sPS) Structural thermo-resistant polymer, with melting point 250–275 °C (depending on the catalyst used in the production process) and perfect processing properties, not requiring drying before processing, easily able to be painted and metalized. Main applications: photographic films, magnetic films of „high density” type; insulation films for electric and electronic products; heat-resistant dishes, especially for microwave ovens; car parts exposed to chemicals and high temperature: e.g. radiators, reflectors, battery covers, car body elements; machine parts working at high temperature and in contact with steam; food packaging films; machine construction materials, machine housings; pipes to transport fluids and gases (except for aromatic compounds) at temperature > 100 °C (for overheated steam – standard: 140 °C); office furniture; appliances and equipment used in medicine and dentistry, resistant to sterilization with overheated steam, ethylene oxide and UV. A brief description of the technology The process of syndiotactic styrene polymerization in the presence of catalysts [P-318774 and P-318775 (1997)], proceeds under waterless and oxygen-free conditions, in an organic solvent – hexane. The raw product is purified by extraction with organic solvents and distillation with steam, and then dried at temperature up to 90 °C in inert gas atmosphere. The process proceeds under normal pressure and at temperature up to 70 °C. Properties of the resulting product and the process yield do not diverge from those described in literature and patents. Advantages of the technology offered The process is similar to suspension propylene polymerization, what enables to use its redundant installations to produce sPS. The process, proceeding in a solvent, directly provides granulation favorable to modification with improvers increasing mechanical strength of the product. High melting point of the product (about 260 °C) enables a wide range of high--temperature 250 processing. Easy control of the process, proceeding in solvents. It is possible to use both installations and catalytic system to conduct reactions of styrene and ethylene copolymerization (INSITE DOW CHEMICAL process) and butadiene polymerization (90 % of 1,4-cis-polybutadiene), which can be used to obtain high impact strength polystyrene (HIPS). Equipment Typical reactor equipped with a stirrer, dephlegmator, drain valve, heating / cooling jacket. The reactor is coupled with a column to purify technical styrene and a filter separating the polymer from the solvent and possibly the unreacted monomer; metering pumps dosing hexane, styrene and MAO; continuous distillation columns to purify hexane and styrene; catalyst dosing device; pressure filter or centrifuge; apparatus for distillation with steam; centrifuge for aqueous suspensions; shelf dryer; nitrogen heater; sensors and elements metering temperature, flow and power consumption by the stirrer. Patents Patent No P-186 001 (2003) „Method to produce catalysts for syndiotactic styrene polymerization”. Patent No P-186 002 (2003) „Method to obtain syndiotactic polystyrene”. Market competitiveness At present only IDEMITSU company (Japan) is a producer of syndiotactic polystyrene. References Process verified in an experimental installation with a 250 l reactor (acid resistant steel and enamel), capable of obtaining about 20 kg of polymer. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 251 10) Chemosetting polymeric composites The subject of the offer is a chemosetting self-leveling polymeric composition containing unsaturated polyester or epoxy resins and (when needed) plasticizers, flame retardants, greases, stabilizers and modifiers in the total amount of 30–70 wt. %. The composition includes also a mineral filler, especially thermally conditioned phosphogypsum left from production of phosphoric acid or its mixture with other mineral fillers e.g. talc. The composition is destined for production of floor screeds, tiles, inner and outer wall facing involving the pouring method. A brief description of the technology The process includes ingredients mixing for about 1 h at temperature about 20 °C, deaeration for about 1 h and addition of the last ingredient, which is a stiffener. This way prepared mixture is suitable for pouring onto an in advance prepared ground. Advantages of the technology offered The compositions offered, due to application of waste raw materials are characterized by very low cost. Equipment Concrete mixer or other stirrer. Patents Patent application No P-194 809 (2001) „Chemosetting polymeric compositions”. Market competitiveness No similar solutions on the domestic market. References The chemosetting polymeric compositions for floor screeds has an attest issued by National Institute of Public Health - National Institute of Hygiene and Technical Approval issued by Building Research Institute. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 252 11) Polymeric composites with silica nanoparticles Polyamide (PA) and poly(ethylene terephthalate) (PET) composites with silica nanofiller content of several percent (0.5–6 wt. %), having various functional groups, show unique and enhanced properties in comparison to unfilled PA and PET polymers, such as: better barrier, mechanical and thermal properties, and in case of polyamide also increased chemical resistance. A significant influence on properties of the nanocomposites has the content and size of spherical silica particles, the number of introduced functional groups, the presence of a compatibilizer, and also processing conditions. A brief description of the technology The nanocomposite production technology comprises dispersion of spherical nanosilica with particle size between 40 and 180 nm in a polymeric matrix. The process is based on the reactive extrusion method which is carried out in a co-rotating twin-screw extruder, with screw revolution speed providing uniform dispersion. Advantages of the technology offered Composites produced according to the technology are competitive to composites containing layered nanofillers (e.g.: montmorillonite) due to ability to permanently connect the functionalized silica with the polymeric matrix and obtain at the same time system of homogeneous and high dispersion degree. Furthermore, application of compatibilizers with a defined physicochemical characteristics prevents agglomeration of nanoparticles and influences their permanent bounding into the polymeric matrix, what results in favorable properties of the nanocomposite. Equipment A intermeshing co-rotating twin-screw extruder. Patents Patent application No P-385 297 (2008) „Polyamide composite with a powdery nanofiller”. Patent application No P-389 434 (2009) „Poly(ethylene terephthalate) composite with a powdery nanofiller”. Market competitiveness 253 There are no producers of polymeric nanocomposites on the domestic market. References Awards gained on prestigious international invention and innovation exhibitions: 2 bronze medals (Geneva 2009, Nuremberg 2009). Contact Person Data Assoc. Prof. Regina Jeziórska, D.Sc., Eng. phone: + 48 22 568 24 91 fax: + 48 22 568 21 84 e-mail: [email protected] 254 12) Poly(vinyl chloride) nanocomposites prepared in-situ in suspension polymerization process PVC nanocomposites are prepared in suspension polymerization process in a typical equipment used for PVC production. The polymerization is carried out in the presence of spherical nanofillers e.g. nanosilica prepared in sol-gel process or hybrid silicone-acrylic core/shell filler. The nanofillers are added to the polymerization mixture in the amounts up to 1 wt. % per vinyl chloride monomer (VCM). These fillers do not disturb the polymerization process, do not prolong it and do not interact with initiators or other additives used in the process. The nanofillers used are dispersed in aqueous phase. Such dispersion can be stabilized with protective colloids. This form of a fillers prevents its agglomeration. Advantages of the technology offered Mechanical properties (impact strength, tensile strength) of the nanocomposites prepared by the method described are better than those of standard PVC prepared by standard suspension method. The nanofiller addition improves impact strength about 20–50 % dependently on the blend composition and does not influence the final product hardness. Preparation of nanocomposites in the polymerization step is advantageous in comparison with applying of nanofillers in PVC processing as it gives excellent dispersions of the nanofillers in PVC grains and let use smaller amounts of them to reach the same properties improvements. The process can be applied for the preparation of PVC nanocomposites of any molecular weight (full range of K value). Silica nanofiller allows controlling the polymer molecular weight in some range. Equipment The process can be used in every plant of VCM suspension polymerization. Any tank in the lines of media dosage to the polymerization reactor can be used as a nanofiller tank. Patents Polish patent application P-384 835 (2008) „Method of the suspension polymerization of vinyl chloride in the presence of a nanofiller”. Polish patent application P-388 960 (2009) „Method of the suspension polymerization of vinyl chloride in the presence of a nanofiller”. European patent application PCT/PL2009/000087 (2009) „Method for the suspension polymerization of vinyl chloride in the presence of a nanofiller”. 255 Market competitiveness There is no PVC nanocomposites in the world market in spite of intensive works of many research centers, known from the published papers and patents. The only known to us trial of the production of such nanocomposite is introduction of the pilot plant for physical mixing of emulsion PVC latex and bentonite aqueous dispersion. The dried product is a blend called NanoVin®. Production in the industrial scale has not started yet. References PVC nanocomposites production (at reactor 1 m3 of capacity) in Spolana a.s. in Czech Republic (ANWIL SA Group) showed that suspension polymerization of VCM in the presence of spherical nanofillers is possible. Contact Person Data Maria Obloj-Muzaj, Ph.D. phone: + 48 22 568 21 86 fax: + 48 22 568 21 84 e-mail: [email protected] 256 13) Thermoplastic starch (TPS) Biodegradable and compostable thermoplastic starch produced from renewable natural raw materials is characteristic of high homogeneity degree, a favorable set of mechanical properties, and products made of it have good dimensional stability in application conditions. TPS in granulated form is a ready material to manufacture products with methods used on conventional thermoplastic polymers or it can be used as raw material to produce starchpolymeric composites, useful in organic recycling. Thermoplastic starch can be used for manufacture of any kinds of packaging, such as: films, bags (for shopping or waste) and one-off products (e.g. catering equipment pieces) and in this area it can be an equivalent substitute of conventional materials like polyolefins or PVC. A brief description of the technology The technology to produce thermoplastic potato and corn starch involves the destructurization of the native starch in specific dynamic-thermal conditions. The process is carried out in a corotating twin-screw extruder in the presence of a plasticizer, where due to pressure and high shear rates crystalline starch structure is disrupted and the starch is converted into homogeneous, amorphous material, suitable for thermoplastic processing. Advantages of the technology offered The technology to produce the new polymeric material, which is thermoplastic starch, relies upon renewable raw materials of vegetable origin. It provides for becoming independent of traditional raw material sources, and simultaneously allows for organic recycling and biodegradation of waste products i.e. decay in composting conditions. Equipment A intermeshing co-rotating twin-screw extruder. Patents Patent application No P-376 985 (2005) „Method to produce biodegradable polymeric material”. Patent application No P-386 832 (2008) „Biodegradable composition containing thermoplastic starch”. Patent application No P-392 109 (2010) „Method to produce thermoplastic starch”. 257 Market competitiveness At present, thermoplastic starch is not produced in Poland. References Awards received on prestigious international invention and innovation exhibitions: 2 gold medals (Geneva 2008, Brussels 2009), 2 silver medals (Seoul 2008, Shanghai 2008), 1 bronze medal (Warsaw 2008), Cup of the Minister of Economy of Poland, deputy Prime Minister Waldemar Pawlak (Brussels 2009). Contact Person Data Barbara Świerz-Motysia, Ph.D., Chem. Eng. phone: + 48 22 568 28 93 e-mail: [email protected] 258 14) Polyurethane sealants and coatings – Elastofix PU Polyurethanebitumen sealants and coatings – Elastofix PU-B Those products have been developed for application in construction, specifically for waterproofing insulations as moisture-curable, single-component materials. They can however be applied also in two-component systems, what significantly accelerates curing process. Elastofix can be used also in mining and in production of window panels. Elastofix grades of enhanced chemical resistance and enhanced glass adhesion properties are also available. They are supplied in a form of a paste with thixotropic and self-leveling properties, with lightcreamy color in case of Elastofix PU, and black in case of Elastofix PU-B. Elastofix PU does not contain organic solvents, whereas Elastofix PU-B contains only a small amount of aromatic hydrocarbons mixture (from just few to over a dozen percent). A brief description of the technology The process to obtain Elastofix PU products comprises two steps. The first step is to disperse fillers in a starting polyol, then the mixture is dehydrated under reduced pressure and subsequently the polyaddition process of polyol and diisocyanate is carried out, at increased temperature, in inert gas atmosphere and in the presence of a plasticizer. In case of the thixotropic grade, the product obtained is additionally mixed with colloidal silica. The process to obtain Elastofix PU-B products includes mixing of Elastofix PU mass containing as a filler coal flour (and possibly carbon black) with asphalt-isocyanate adduct (produced in a reaction between molten asphalt and diisocyanate). Advantages of the technology offered The technology allows to obtain products forming elastic joints or coatings, well adhering to construction materials and resistant to outdoor environmental factors. The special grades are also resistant even to chemical agents, especially acid and base solutions. Equipment typical reactor with an anchor stirrer and a heating / cooling jacket, able to keep inert gas atmosphere and conduct the process under reduced pressure, high speed mixer, tanks to store reactants, planetary mixer (in case of the thixotropic grade), a device for pneumatic discharge of the planetary mixer bowl (optional). 259 Laboratory equipment: equipment to determine the hydroxyl value and NCO groups contents, viscometer or rheometer, equipment for testing the properties of sealants and coatings. Patents The technologies were patented, but the patents have already expired. Market competitiveness At present there are market-available polyurethane sealants and coatings, including polyurethane-bituminous ones, but those are no moisture-curable products. References Elastofix PU and Elastofix PU-B (containing coal pitch adduct instead of asphalt adduct) were produced on the industrial scale (up to 300 TPY) in the eighties of the last century by Pilchem Company on site of the former Paints and Coatings Company in Pilawa. Production of Elastofix PU masses was then moved to „Silikony Polskie” Chemical Plant in Nowa Sarzyna, but after a few years was abandoned due to a reduction in the production profile of the plant to solely silicone products. All grades of Elastofix PU and Elastofix PU-B products designated for construction applications received certificates of Building Technology Research Institute (ITB). Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Jarosław Przybylski, M.Sc., Chem. Eng. phone: + 48 22 568 26 46 ; + 48 22 568 26 47 e-mail: [email protected] 260 15) Polyurethane, silicone-urethane, polyurethane-acrylic and silicone-urethane-acrylic aqueous dispersions – DPU-PJ DPU-PJ aqueous dispersions were developed for application as paint and lacquer binders, applied on wood, metals or plastics and also to be directly applied as coating materials (of wide hardness range) or as additives to coating materials based on other aqueous dispersions, e.g. acrylic dispersions. DPU-PJ dispersions can form coatings cured by UV irradiation or oxygen from air (with a siccative). Choosing suitable composition enables to produce DPU-PJ dispersions with various raw material cost, forming coatings with wide range of hardness, elasticity and adhesion. Based on the developed dispersions, two-component compositions (dispersion + hardener) can be obtained. DPU-PJ dispersions have the form of opalescent liquids of low viscosity, pH about 8 and solids content about 33 %. A brief description of the technology At the first stage the starting polyol (or polyol mixture) is dehydrated under reduced pressure, and then, at increased temperature and in inert gas atmosphere, a polyaddition of polyol, dihydroxy carboxylic acid and cycloaliphatic diisocyanate is carried out in the presence of small (several percent) amounts of a diluent – N-methylpyrrolidone (NMP). Resulting NCOterminated prepolymer containing carboxyl groups is neutralized with a tertiary amine, obtaining a concentrated prepolymer-ionomer solution in NMP. At the second stage the concentrated prepolymer-ionomer solution is dispersed in water and then the polymer chain is extended with polyamine. Advantages of the technology offered The technology allows to obtain dispersions forming coatings of wide range of properties. Equipment typical reactor with an anchor stirrer and a heating / cooling jacket, capable to keep inert gas atmosphere and perform the process under reduced pressure, high speed mixer with a heating / cooling jacket, tanks to store reactants. Laboratory equipment: equipment to determine the hydroxyl value and NCO groups contents, viscometer or rheometer, 261 pHmeter, equipment for testing coating properties. Patents The technology was not patented. Market competitiveness There are polyurethane and polyurethane-acrylic dispersions available on the market, special grades forming coatings cured by UV irradiation or by oxygen from air (with a siccative). However, neither silicone-urethane nor silicone-urethane-acrylic dispersions are commercially available. Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Jarosław Przybylski, M.Sc., Chem. Eng. phone: + 48 22 568 26 46 ; + 48 22 568 26 47 e-mail: [email protected] 262 16) General purpose silicone greases A grease to seal up and/or secure ground glass joints in laboratory apparatus and metal surfaces, decreasing glass joints clotting due to grease leaching by solvents, especially in glass apparatus operating at increased temperature (-50 °C–250 °C) and/or under reduced pressure (3–5 mm Hg). The greases are also handy in lubrication and securing water fittings. A brief description of the technology The process to obtain the greases offered includes very fine grinding of silicone oil with fillers, until uniform consistency is not reached. Advantages of the technology offered Greases produced according to the technology are marked by very good resistance to solvents, especially at temperature range between 100 and 180 °C and under reduced pressure, thus guaranteeing very good effectiveness in securing ground glass connections in laboratory apparatus. Equipment kneader or Z mixer, tube, box or glass jar packing device. Patents We offer our know-how, the technology is not protected with any patent. Market competitiveness The main advantage of the technology offered is a big added value to be earned from this production. It results from a big difference between the price of materials and labor costs, and the sale price. Potential customers are chemical, medical and biological laboratories supplied by distribution companies, e.g. POCH S.A. References According to the technology developed, since 2004 is produced a grease for pipette plungers for HTL S.A. Company. Over 90 % of pipettes produced by the company is sold to world markets (USA, Europe). Contact Person Data Maria Zielecka, Ph.D. phone: + 48 22 568 28 40 e-mail: [email protected] 263 17) Associative non-ionic polyurethane thickeners (Pseudo-plastic and Newtonian Grades) The thickeners can be applied to control the rheological profile of a number of products containing aqueous polymer dispersions as binders, such as paints, coatings (for both indoor and outdoor use) and adhesives. They are applied especially in products cured by UV irradiation or by oxygen from air (with a siccative). The thickeners are 40 % solutions of active agents in a mixture of water and organic solvents of low viscosity (facilitating their dosing) and have density of about 1.03 g/cm3. They are well soluble in water, forming viscous, opaque and opalescent liquids. The pseudo-plastic grade thickeners may be applied e.g. to increase viscosity in the range of low shear rates, enabling this way to reduce an unfavorable phenomenon of binder and filler particles sedimentation, and their amount in the product depends on required rheological effect. Usually 0.1–2 wt. % of the thickener is used relative to the final product mass. The Newtonian grade does not cause such big increase in viscosity in the range of low shear rates as the pseudo-plastic version does. The thickeners can be added at any manufacturing stage of the coating production. A brief description of the technology The process comprises a two-stage reaction of addition of poly(oxyethylene glycol), alcohol and isocyanate, and then dissolving the obtained thickener in a mixture of solvents. Advantages of the technology offered The thickener synthesis process is performed in the bulk, without any organic solvents, what is favorable from both the ecological and economical point of view. It allows to avoid a costly process of solvents recovery or utilization. Advantageous is also big simplicity of apparatus washing at each production stage. Equipment two reactors with an anchor stirrer and a heating / cooling jacket, capable to keep inert gas atmosphere and conduct the process under reduced pressure, high-speed mixer, tanks to store reactants. Laboratory equipment: equipment to determine the hydroxyl value and NCO groups contents, 264 viscometer or rheometer. Patents Patent application No P-390 104 (2009) „Method to produce modifiers of rheological properties of aqueous polymeric dispersions”. Market competitiveness At present, there are numerous market-available technologies to obtain associative non-ionic polyurethane thickeners, to be applied in paints and coatings based on aqueous polymeric dispersions. They have, however, no ability to permanently build themselves into the product structure. On the contrary to thickeners presently available on the market, the thickeners developed are able to build themselves into the structure of the coating and participate in formation of the coating under UV irradiation or with a siccative, together with the binder contained in the coating material. It allows to improve water-resistance of the coating in comparison to coatings obtained with using traditional thickeners. Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Jarosław Przybylski, M.Sc., Chem. Eng. phone: + 48 22 568 26 46 ; + 48 22 568 26 47 e-mail: [email protected] 265 18) Modified nanofillers based on mine halloysite This new group of fillers has a hybrid structure of type: inorganic core / organic envelope. Such construction of the filler improves its dispersibility and miscibility in polymeric matrices, especially in polymeric mixtures. Polymers filled with them, both thermo- and duroplasts, are characterized with very significant improvement in mechanical properties (first of all in impact strength and flexural strength). A brief description of the technology The modification of halloysite proceeds with the cladding method, using optimal recipes and process parameters. Advantages of the technology offered A new technology, no comparison. Equipment An ultrasonic bath, a reactor with the ability to take out the solvent of the modified compound, a dryer. Patents Patent application No P-386 380 (2008) „Method to produce modifiers of epoxy resin and method of modification of epoxy resins”. Patent application No P-386 833 (2008) „Method to produce modifiers of polypropylene and method of obtain modified polypropylene”. Patent application No P-386 455 (2008) „Method to produce polyolefines composites”. Patent application No P-390 410 (2010) „Method to produce modifiers of polymers and polymeric nanocomposites”. Patent application No P-390 578 (2010) „Method to produce modifiers and polymeric nanocomposites”. Patent application No P-390 868 (2010) „Method to produce modifier of polystyrene and polystyrene nanocomposites”. Market competitiveness So far, no similar products on the Polish market. 266 References Awards received on abroad invention and innovation exhibitions. Gold medal for „Modifiers of epoxy resin based on halloysite”, Brussels-Innova 2009 (BrusselsEureka), Brussel. Bronze medal for „Modifiers of epoxy resin based on halloysite”, Geneva PALEXPO, Switzerland, 2009. Contact Person Data Assoc. Prof. Izabella Legocka, D.Sc.. phone: + 48 22 568 26 51 e-mail: [email protected] Ewa Wierzbicka, M.Sc., Chem. Eng. phone: + 48 22 568 26 93 e-mail: [email protected] 267 19) New generation engineering polymers from PET waste This innovative, ecologic technology, counted among „top 10 export hits” – most interesting Polish technical achievements in recent years, considerably reduces an overflow of nondegradable environmentally waste. It allows to produce engineering polymers used as material for practically all technical products. Application of the new polymer in the electric and electronic appliance sector includes high precision bearings, levers, cog wheels and device housings with specified mechanical and electrical functions, e.g. office devices, computers, monitors, printers, cooking equipment, light bowls, photographic accessories and also electric sockets, plugs and capacitor cores (resistant to creeping current). Automotive industry can make use of the new polymer to manufacture such products as fuel system parts (fuel pumps and filters) or parts of braking system and air conditioners. This polymer can also be used to produce sports equipment, e.g. ski bindings and sailing gear. A brief description of the technology The technology utilizes the method of reactive extrusion using a modifier, facilitating creation of compatible heterogenic structures with enhanced adhesion at phase boundaries. Processing in a co-rotating twin-screw extruder results in chemical reactions between functional groups of processed polymers and functional groups of the modifier, creating permanent covalent or ionic bonds. Hence, the resulting polymer presents properties of engineering polymers. Advantages of the technology offered New generation engineering polymers made of secondary PET materials are equivalent and simultaneously cheap replacements of conventional polymers like poly(butylene terephthalate), high impact polystyrenes or reinforced with glass fiber species of polyamide 6, polyamide 66 or polycarbonates. They are also competitive to products of world leading companies. Equipment A co-rotating twin-screw extruder. Patents Patent application No P-183 370 (1996) „Thermoplastics recycling method”. 268 Market competitiveness At present no engineering polymers from PET bottles are produced in Poland. References Awards received on prestigious international invention and innovation exhibitions: 3 gold medals (Geneva 2000, Brussels 2002), including a WIPO gold medal for a woman inventor (Brussels 2002), 2 silver medals (Nuremberg 1999, Gdañsk 2001), a distinction in the VIth edition of the competition „Polish Product of the Future” in the technology category, V th International Competition „EKO-2003” on solutions in the area of environment protection and Grand Prix of the VIth International Plastic Fair PTS 2003 (Warsaw 2003). Contact Person Data Assoc. Prof. Regina Jeziórska, D.Sc., Eng. phone: + 48 22 568 24 91 e-mail: [email protected] 269 20) Polymeric composites made from polycarbonate waste The technology is based on most recent achievements in the area of chemical modification of thermoplastics, guaranteeing obtaining polymeric composites with excellent properties and a wide spectrum of technical application capabilities. A filler additive allows to obtain materials with diversified properties, e.g.: graphite additive allows to obtain sliding properties and increases wear resistance. Such a material is hence excellent to produce belt and chain conveyors used i.a. in food and packaging industry, for lining dock walls with special battens to protect ship boards from bouncing against quays and for runners in bowling alleys. Another example is addition of glass fiber, providing heat resistance and suitable stiffness and hence good damping of mechanical vibrations, dimensional and shape stability. Such composites can find their application in the automotive industry (motor housing, carburetor, filters, cable holders), in household appliances (housings of vacuum cleaners or fryers), they can be material for cog wheels, self-sealing rings, parts of rotary and metering pumps, valves, faucets, filtration plates and frames etc. Nanosilica added in very small quantities radically changes properties of a nanocomposite, improving among others its stiffness, mechanical strength and reducing flammability. A brief description of the technology The essence of the process is employment of the reactive extrusion process with simultaneous filling (with e.g. glass fiber, graphite or nanosilica). In a relatively small processing device, which is a co-rotating twin-screw extruder, occurs a process of chemical modification of compact disk waste (the process runs rapidly – within only several dozen seconds, whereas „traditional” polymerization used to obtain new kinds of polymeric materials takes usually over a dozen hours). Advantages of the technology offered The developed solution, based entirely on Polish technical thought, is at the highest technological level of a new, intensively developing area of reactive extrusion. Polymeric composites made of polycarbonate waste, including compact disks, depending on modifiers and fillers used, are equivalent and simultaneously cheap replacements of conventional engineering polymers. They belong to the group of products, which for many years will be used in leading industries, like: machine-building, automotive, electronic and electrical. Equipment A co-rotating twin-screw extruder. 270 Patents Patent application No P-378 227 (2006) „Method to produce polymeric composites from polycarbonate waste”. Market competitiveness No composites with engineering polymers properties involving usage of waste compact disk are produced at present in Poland. References Awards received on prestigious international invention and innovation exhibitions: 2 gold medals (Budapest 2006, Brussels 2008), 3 silver medals (Moscow 2006, Nuremberg 2006, Warsaw 2007), 1 bronze medal (Geneva 2006), a distinction in the XIth edition of the competition „Polish Product of the Future” in the future technology category, a special prize funded by Gorodissky & Partners Company from Russia (Brussels 2008). Contact Person Data Assoc. Prof. Regina Jeziórska, D.Sc., Eng. phone: + 48 22 568 24 91 e-mail: [email protected] 271 21) Polyester plasticizers Synthesis of polyester plasticizers using waste poly(ethylene terephthalate) (PET) proceeds in four stages: Ist stage – glycolysis of waste poly(ethylene terephthalate) with diethylene glycol, at temperature 220–230 °C in the presence of a catalyst, IInd stage – condensation of mixtures of glycols, PET oligomers and adipic acid, performed at temperature 200–210 °C, until acid value > 50 mg KOH/g is reached, in order to obtain dicarboxylic polyester, IIIrd stage – esterification of dicarboxylic polyester with 2-ethylhexyl alcohol, at temperature 150–180 °C, until acid value < 10 mg KOH/g is reached, IVth stage – flash distillation and distillation under reduced pressure, allowing to obtain plasticizers of proper volatility. Distillation under reduced pressure is performed up to the moment when volatility of di(2-hydroxyl)polyester drops below 0.7 % at temperature 180 °C for 30 min (check using a thermo-balance). Advantages of the technology offered Because of big molecular mass, polyester plasticizers using poly(etylene terephthalate) are characterized by low volatility and low migration tendency, and hence will not be washed out from final products. Big thermal stability of PVC products obtained using polyester plasticizers guarantees much longer usage of these products, and to much extent this will bring about lower amount of worn-out products. Good miscibility and good efficiency of developed plasticizers produced from PET (comparable to polymeric plasticizers produced from petrochemical constituents on the industrial scale in Organika-Sarzyna Chemical Plant) will broaden the offer. Lower price of polyester softeners produced from PET compared to plasticizers available on the domestic market (produced by Organika-Sarzyna Chemical Plant and imported) will increase interest among purchasers. Equipment The synthesis is performed in a typical installation to synthesize polyesters in a reactor equipped with a stirrer, a distillation column and a thermometer. Patents In preparation. 272 Market competitiveness Attractive price, compared to prices of polyester plasticizers. References Implemented production of polyester plasticizers from petrochemical constituents in Z.Ch. „Organika-Sarzyna” S.A. in 2002. Contact Person Data Elżbieta Wardzińska, Ph.D. phone: + 48 22 568 28 46 e-mail: [email protected] 273 22) Porous hoses made of polyolefin composites and vulcanized rubber scrap Porous hoses are produced from polymeric composites, obtained entirely or partly from waste polyolefins and vulcanized rubber scrap. Typical outer diameters of these hoses are 15 and 19 mm. Porous hoses 19 mm in diameter are prepared for Gardene connectors, enabling them to be attached to an irrigating system. A brief description of the technology Porous hoses are produced by extruding polymeric composites obtained from polyolefin waste and vulcanized rubber scrap. The mixture consists of: Polyethylene or polypropylene (primary or waste) 10–60 wt. %, vulcanized rubber scrap 40–90 wt. % and porophor, playing an important role as a porosity regulator. The composition can also contain greases, mechanical properties modifiers, anti-frictional additives, fillers and stabilizers. Advantages of the technology offered An advantage of the technology is obtaining cheap hoses of good quality, which thanks to their porosity (open micropores, uniformly spaced throughout its whole mass) enables homogeneous pouring of water throughout the irrigation zone either on the surface or underground. They can be also applied in fertigation (irrigation joined with fertilization). Application of porous hoses provides a new, ecological and economical soil fertilization and irrigation system. Another advantages of pipes produced according to the technology developed by Industrial Chemistry Research Institute are: water savings by 40–60 % relative to the amount used in traditional systems (installed underground, delivering water directly to roots of vegetation); ability to feed plants with fertilizers soluble in water; easy installation and dismounting; low working pressure of the system < 1 · 105 bar (optimal 0,2 · 105 bar); water throughput 140 l/h · m. Equipment Single-screw extruder, screw diameter 45 mm, head of special construction (patented). 274 Patents Patent application No P-175 637 (1995) „Device to produce porous pipes from polymeric compositions containing comminuted vulcanized rubber scrap”. Patent application No P-177 682 (1995) „Thermoplastic polymeric composition containing comminuted vulcanized rubber scrap”. Market competitiveness No similar home-made porous hoses on the Polish market. References Silver medal IENA 95 (Nuremberg, Germany, 1995). Diploma GENIUS ’96 (Budapest, Hungary, 1996). Gold medal Casablanca’97 (Morocco, 1997). Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 275 23) Ground stabilizing nets (geonets) The subject of the offer are ground stabilizing nets called geonets (globnets) produced from waste materials. They are produced from a mixture of comminuted vulcanized rubber scrap (particle size < 1,6 mm) from car tires (20–50 wt. %), mineral fillers (up to 30 wt. %) and polyolefin recyclate, e.g. PE-LD film agglomerate (50–80 wt. %). A brief description of the technology A mixture of comminuted vulcanized rubber scrap, polyolefin agglomerate and mineral filler (0– 30 %) is extruded in the form of bands 15 mm thick and of free to choose width. The bands are connected in such a way, that they create a structure of „honey-comb” type when unfolded, with uniform mesh size, and when folded they are superimposed one layer upon another. The extruded and cooled band displays the effect of double-sided knurling without any additional tools. Due to knurling, meshes between bands can be filled with soil with vegetation, ground from excavations, sand, aggregate, etc., providing increased ground stabilization and restricting migration of ground crumbs or sand. This facilitates vegetation rooting and constitutes additional effective and attractive protection form for escarpments and slopes. Advantages of the technology offered Offered by the Industrial Chemistry Research Institute technology to produce geonets, due to utilization of thermoplastic recyclates, is marked by very low cost of constituents, by 1/3 less than the cost of other widely applied geonets produced from primary high density polyethylene. Equipment extruding line with a long tape receptacle to cool down the band for geonet, terminated with a calender and a cutter to cut the band into straps of suitable width; a device to weld or glue the band in the form of honey-comb. Patents Patent P-205 736 (2004) „Cellular ground stabilizing nets made of bands from waste materials and the method to produce them”. Market competitiveness The domestic market offers only geonets made of primary high density polyethylene. 276 References A piece of geonet, produced on the industrial scale, was mounted on the Polish coast near Jastrzębia Góra. It has been perfectly fulfilling its strengthening role. During 5 years of usage its properties have practically not deteriorated. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 277 24) Large-size road traffic security devices The subject of the offer is a technology to obtain big-size road traffic security devices like: stands for emergency traffic signs, speed bumps, parking bollards, etc., made of waste from polyolefins or poly(vinyl chloride) and vulcanized gum (particle size < 5 mm). A brief description of the technology Polyolefin composites containing vulcanized gum waste are obtained by their mixing in an appropriate mixer or by extrusion in granulated form. These composites can be processed with standard methods of extrusion, compression molding or injection molding. Advantages of the technology offered The composites offered, due to the usage of thermoplastic recyclates in production, are characterized by very low cost. Equipment screw or drum mixer, extruder with screw diameter over 60 mm, press or injection molding machine. Patents Patent PL-177 682 (1995) „Thermoplastic polymeric composition containing comminuted vulcanized rubber scrap”. Patent PL-188 466 (1997) „Thermoplastic polymeric composition”. Market competitiveness No similar solutions on the domestic market. References A speed bump produced with the form extrusion method is since 10 years mounted at the site of Industrial Chemistry Research Institute and works without any problems. Silver medal at Moscow International Salon of Industrial Property Archimedes 2006, Moscow, Russia. Bronze medal at International Exhibition “International Warsaw Invention Show” (IWIS) 2007. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 278 25) Complex processing of the pyrolysis tar to naphthalene and high-boiling aromatic hydrocarbon fractions The technology relates to comprehensive processing of pyrolysis tar (liquid residues from gasoline pyrolysis), produced in PKN „Orlen” S.A. in Płock, till now fully disposed of as a component of heavy heating oil C-3. Using the pyrolysis tar produced in PKN „Orlen” S.A., there is a possibility to produce petrochemical naphthalene, used to manufacture phthalic anhydride and b-naphthol in quantity about 10 thousand TPY. Processing of pyrolysis tar, would also enable to produce scrubbing oil, in short supply on the domestic market, used in coke oven plants (about 20 thousand TPY) and highly aromatic oil to produce carbon black (about 35 thousand TPY). Total market value of the products mentioned is about Є 1520 mil. A brief description of the technology The technology comprises separation of pyrolysis tar by distillation under reduced pressure, using flash distillation and rectification. It allows to obtain suitable hydrocarbon fractions with boiling point in defined temperature ranges, which (except for naphthalene fraction) can be ready market products. Obtaining pure naphthalene from pyrolysis tar involves distilling separation of the hydrocarbon fraction enriched in naphthalene, with boiling point usually between about 210 and 225 °C and containing > 70 wt. % naphthalene. This fraction is then subjected to the crystallization process and centrifugation or directly to fractional crystallization from the melt. This process allows to obtain naphthalene of 98–99.5 wt. % with high efficiency. Advantages of the technology offered Application of the technology of complex processing of pyrolysis tar would contribute to increase in the degree of crude oil processing and consequently to improvement in technical and economical indicators of the Olefin Plant in Polish Petroleum Concern „Orlen” S.A. in Płock. Patents Patent application No P-390 411 (2010) „Method to separate naphthalene from oil residues from olefin pyrolysis of gasoline”. Equipment The technology to process pyrolysis tar can be used in petrochemical refineries possessing a 279 distillation installation equipped with columns for vacuum rectification and flash distillation. In order to produce pure naphthalene, there is necessary an equipment for crystallization with centrifugation or fractional crystallization. References The technology of complex processing of pyrolysis tar with this method has been investigated on the 1/4-technical scale. Obtained products: naphthalene, aromatic oil for manufacturing of active carbon black and methyl naphthalene fraction (scrubbing oil for coke oven plants) have been successfully tested, respectively, in: ZAK S.A., carbon black plant in Jas³o Refinery and Institute for Chemical Processing of Coal in Zabrze. Contact Person Data Małgorzata Jamróz, Ph.D., Chem. Eng. phone: + 48 22 568 20 21 e-mail: [email protected] 280 26) Modified petroleum asphalt The technology relates to modification of utility properties of asphalts using fractions of pyrolysis tar, boiling at temperature > 300 °C (liquid residues from gasoline pyrolysis). Commercialization of the petroleum asphalt technology will be possible after PKN „Orlen” S.A., or another company, implementation of the comprehensive processing technology of pyrolysis tar (a by-product from the process of olefin pyrolysis of gasoline in PKN „Orlen” S.A.). A brief description of the technology The technology to modify petroleum asphalts comprises mixing petroleum asphalt with a fraction of post-pyrolysis oil (bp > 300 °C) at temperature 110–125 °C, and then holding at temperature of 120–125 °C. Optimal quantity of the added post-pyrolysis oil fraction is 5–20 %. Production of asphalt compositions with this method is technologically easy. The compositions obtained do not contain any substances harmful to the natural or operating environment. Advantages of the technology offered Petroleum asphalt compositions produced from the modified asphalt are characterized by increased resistance to deformations at high temperatures and also very good adhesion to mineral aggregate, ensuring good resistance to high shearing forces on road pavement, caused by heavy vehicle loads. Patents Patent No P-205 644 (2005) „Modified petroleum asphalt”. Equipment The technology does not require any special apparatus and may be applied in all domestic petroleum processing plants, producing asphalts for highway engineering. Contact Person Data Małgorzata Jamróz, Ph.D., Chem. Eng. phone: + 48 22 568 20 21 e-mail: [email protected] 281 27) Silica and titania-silica nanomaterials for high-tech applications Functionalized and non-functionalized nanomaterials are new group of nanomaterials with unique properties resulting from exactly defined structure of these materials. Silica and titaniasilica nanomaterials are characterised by desired uniform spherical particle size within the range of 30–600 nm, specific surface area within 300–1500 m2/g as well as the defined kind and content of functional groups. These nanomaterials assigned for high-tech applications, especially as nanofillers for polymer nanocomposites and as nanocatalysts. A brief description of the technology The process of silica and titania-silica nanomaterials manufacturing according to sol-gel process is realised in precisely defined conditions (mixing speed, temperature, pH) in water-alcohol medium by using silane and titania precursors. This technology gives the possibility of various modification of nanosilica according to application needs. The process is waste less. Advantages of the technology offered The most important advantage of this technology is the possibility of steering the synthesis process enabling acquisition of unique products characterised by the properties focused on given application. The main direction of production based on volume of production is manufacturing of nanofillers for polymer nanocomposites. Equipment The production line should contain enamel autoclave of the proper volume equipped with dosing system, heating-cooling jacket for synthesis in the temperature range 20–25 °C, solvents regeneration unit and drying unit (e.g. spray drier). Patents Patent application No PL 198 188 (2008): „The method of manufacturing of silica nanopowders, also functionalized”. Patent application No PL 204 519 (2010) „The method of manufacturing of titania-silica nanopowders”. 282 Market competitiveness On the Polish market there are not manufacturers of silica and titania-silica nanomaterials. References Pilot scale production in Chemical Plant POLISH SILICONES Ltd. The manufactured sols and nanopowders were applied for the production of PVC nanocomposite in SPOLANA Works Anwil Group and for the production of nanocomposite in GEO GLOBE POLSKA Ltd. Awards on prestigious inventions fairs (gold medal Brussels 2005, Moscow 2007, Warsaw 2007, silver medal Genève 2006). Contact Person Data Maria Zielecka, Ph.D. phone: + 48 22 568 28 40 fax: + 48 22 568 23 90 e-mail: [email protected] 283 28) Copper powders and nanopowders The method for obtaining copper powders and nanopowders from industrial electrolytes, including waste waters through electrodeposition of metallic copper on the cathode was developed. The technology solves the problem of the necessity of using an electrolyte of appropriate purity and concentration, and of using additional electrolytes and other substances. Potential sources of metal nanopowders produced according to the technology are three types of (waste) electrolytes: electrorefining electrolyte, decopperised electrolyte, flotation waste waters destined for dumping. Products which can be manufactured according to the technology include i.a. additives to polymers, lubricants, dye, antibacterial agents and microprocessor connections. Nanopowders of copper or its alloys can find their application in microelectronics, as sorbents in radioactive waste purification, as an additive to cooling fluids and also as catalysts in fuel cells. The most recent application of copper nanopowder is connected with obtaining electronic circuits printed with the Ink jet method, superseding the traditional electrochemical method. Copper nanopowder additive has also positive influence on tribological properties of machining oils. A brief description of the technology The method consists in application of the pulse potentiostatic electrolysis with or without change in the electric current direction using the cathode potential value close to the plateau or on the plateau of the current voltage curve corresponding to the potential range between 0.2 and -1.0 V. A moveable or static ultramicroelectrode or an array of ultramicroelectrodes made of gold, platinum or stainless steel wire or foil is used as a cathode, whereas metallic copper is used as an anode. The process is carried out at temperature from 18–60 °C, and the electrolysis lasts from 0.005 s to 60 s. Copper nanopowders of 99–99.99 % purity can be obtained using that method. Depending on the size of the electrode, metal the electrode is made of, conditions in which the electrolysis is carried out and particularly the kind of electrolysis, temperature and copper concentration in the electrolyte, powders or nanopowders of different shapes, structure and dimensions can be obtained. Advantages of the technology offered Electrochemical methods used so far to obtain copper nanopowders are complicated and expensive. They require costly preparation of substrates (solutions, reagents of suitable purity, reductive agents, auxiliary substances etc.), which results in very high market prices of 284 nanopowders. The main benefit for purchasers of our technology is to increase competitiveness of their enterprises due to innovative solutions included in the method and significantly lower production costs, compared to traditional methods. Equipment To produce nanopowders in the industrial scale, programmable pulse rectifiers enabling change of electric current direction in less than 10 s will be necessary. Such rectifiers are available at a price of about $ 25.000. The applied current from 500 to 10 000 A, will depend on the electrolyzer size and the cathode used (pilot and industrial process). To study the structure and composition of obtained powders and nanopowders, scanning electron microscope (SEM) equipped with energy dispersive spectrometer (EDS) as well as instruments to determine particle size will be needed. Patents Patent application No P-387 565 „Method for obtaining copper powders and nanopowders from industrial electrolytes including waste idustrial electrolytes” and international patent application No PCT/PL2010/000022. Market competitiveness It is estimated that 15 % of total world industrial production will be based on nanotechnology in 2014 and market share of nanopowders will be over 80 %. The product based on the offered technology has surely a very dynamically developing market and will not require much marketing expenditures. The technology should be of interest for entrepreneurs ready to introduce innovative production methods, i.a. in the area of nanotechnology, electronics, polymer plastics industry, paints and lacquers. 285 References The technology for obtaining copper nanopowders from industrial waste waters has already resulted in signing a license agreement with NanoTech Ltd. from Wroc³aw. The technology has been qualified to Global Partnership Programme, in which a free assessment of the project, including preliminary market value assessment was performed. Contact Person Data Assoc. Prof. Przemysław Łoś, D.Sc. phone: + 48 22 568 20 61 e-mail: [email protected] Aneta Łukomska, Ph.D. phone: + 48 22 568 23 19 e-mail: [email protected] 286 29) Volatile brazing flux The object of the offer is a technology for producing volatile flux for brazing steel, copper, brass and zinc bronze with a gas torch (burner). The active substance of the flux is trimethyl borate, obtained in the form of its azeotrope with methanol. The flux in liquid form is fed into the brazing zone with a flammable gas supplying the torch. The gas flame saturated with the flux vapours exhibits a reductive effect on the most metal oxides and provides an effective screening of the brazing zone from atmospheric oxygen, thus safeguarding metallic purity of the joint, required anti-corrosiveness and aesthetics of the product. Such a way of brazing eliminates the burdensome necessity to clean joints from slag, what is characteristic of using classical fluxes in the form of powder or paste. The preparation is a uniform, colorless, clear liquid with a characteristic, acrid smell. It contains about 70 % azeotrope of trimethyl borate with methanol. Remaining ingredients are potassium fluoride with its stabilizing and activating influence and ethylene glycol. A brief description of the technology Synthesis of trimethyl borate proceeds according to the simple equilibrium reaction scheme: In order to ensure reaction progress in the expected direction to create the product it is necessary to separate the product from the reaction mixture. The synthesis is performed at the boiling temperature of the reaction mixture (72–78 °C). The distillate of azeotrope of trimethyl borate with methanol (about 70 wt. %) is separated from the reaction environment by the rectification method in the range of temperature 53–57 °C. In order to separate the azeotrope enriched with trimethyl borate, there is a necessary to apply a rectification column. Depending on the technical parameters of the applied apparatus set (including the resolution capacity of the fractioning column) there can be different: speed of the process to separate from the reaction environment the azeotrope of trimethyl borate with methanol of required composition, the time to bring the system to the equilibrium state and the yield of the synthesis. Water created in the synthesis slows down the trimethyl borate creation process, until the equilibrium of the reaction is shifted to the substrates. Then the synthesis should be treated as completed, despite the fact that the reactor still contains unreacted boric acid and methanol. Advantages of the technology offered The offered technology allows to obtain, in a simple and a safe way, a home-made preparation of a quality comparable to foreign ones. 287 Equipment The base of the installation is a periodic rectification apparatus set. The rectification tub acts at the same time as a reactor and it should be fitted with a stirrer and a drain valve. The rectification system consists i.a. of a column with filling, a condenser, a cooler and a receptacle. The installation should be equipped with a control-measuring apparatus, allowing to keep technological parameters i.a.: temperature of the reactor, temperature of the rectification column and temperature of the column’s top. Installations of all electric devices, mechanical ventilation and lighting should be explosionprotected and non-sparking. Patents Patent application No P-376 168 (2005) „Method to obtain volatile brazing flux”. Market competitiveness The technology allows to obtain the product from cheap constituents (boric acid and methanol) and it enables to separate the product from the reaction environment by the rectification of azeotrope of trimethyl borate with methanol. The price of the product is competitive to offers of foreign companies, e.g. German Company Chemet and characteristics of trimethyl borate in the brazing process is comparable with other foreign products. References Based on brazing tests, the preparation received a positive opinion by the Welding Institute in Gliwice – ruling No ZT/227/06. Contact Person Data Lidia Lewicka, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] 288 OFFERS FOR COOPERATION 1) Izowin-S – a bioactive preparation Izowin-S is used as a dietary supplement in prophylactics of obesity, cellulite and in anticancerogenic therapy. A brief description of the technology The technology comprises isomerization of linoleic acid, a constituent of vegetable oils rich in this acid. The process is performed at temperature 130–190 °C, under normal pressure, using as a substrate edible vegetable oils. The product contains 55–70 % bioactive isomers 9c, 11t + 10t and 12cC18:2. Advantages of the technology offered Preliminary studies proved retarding influence of Izowin-S on hyperplasia of neoplastic cells. Carrying out of the planned researches will allow to introduce it on the market as a bioactive preparation supporting anti-neoplastic therapy. Equipment The production process can be carried out using typical apparatus and devices i.e. a reactor, a sedimentation tank and an evaporator. Advancement of proceedings The technology has been developed on the laboratory scale. Preliminary application studies have been already carried out and there has been received an attest issued by National Institute of Hygiene (PZH). It is necessary to carry out wider-ranging application studies. Patentability Patent PL No P-195 040 (2007) „Method to separate a fraction rich in isomers of linoleic acid with conjugated double bonds from natural fatty acids”. Patent PL No P-199 216 (2008) „Preparation with anticancerogenic activity”. Subsequent patent application in progress. 289 Market competitiveness At present no similar preparation on the market. Type of expected cooperation Cooperation in financing of application studies, production organization and commercialization of the undertaking. Contact Person Data Wiesława Walisiewicz-Niedbalska, Ph.D., Chem. Eng. phone: + 48 22 568 22 45 fax: + 48 22 568 26 33 e-mail: [email protected] 290 2) Spinalpep – a nutraceutical combining peptides and yeast This nutraceutical can be applied as a dietary supplement and support therapy of sclerosis multiplex. A brief description of the process Production can proceed in pressure-less conditions, at temperature 80 °C, raw material – pork spinal cord. Advantages of the technology offered Due to the combination of yeast and a mixture of short peptides, Spinalpep can be applied as a nutrient or in support of the sclerosis multiplex therapy. Short peptides are able to pass the intestinal barrier, get into the blood circulation and perform there a specific biological role. Therefore obtaining and administering of short peptides as nutraceutical components has huge potential application in both feeding healthy organisms and in therapeutic support. Equipment The production process can be performed in typical apparatus and devices used in enzymatic and fermentation processes. Advancement of proceedings There has been developed a technology to produce protein hydrolyzates (pilot scale) to be used as a nutraceutical. Talks concerning industrial implementation of the technology are under way. Patentability Patent application No P-386 296 (2008) „Method to obtain peptide preparations for oral administering”. Market competitiveness The preparation has properties supporting therapy of sclerosis multiplex. The technology allows to obtain peptide mixtures from any sort of protein fractions. Selection of proteins and of created from them peptides can be made depending on the desired final effect. No similar preparation on the market. Type of expected cooperation Cooperation in production organization. Contact Person Data Prof. Andrzej W. Lipkowski, D.Sc. phone: + 48 22 568 28 48 fax: + 48 22 568 26 33 e-mail: [email protected] 291 3) Hydrogenated block (SBS / SIS) copolymers The presence of double bonds in block copolymers styrene-butadiene-styrene (SBS) and styrene-isoprene-styrene (SIS) renders them vulnerable to weather conditions. Hydrogenation of these bonds allows to obtain new plastics with participation of polyethylene (SBES) or polypropylene (SBPS) blocks, more resistant to chemical and weather factors and to low temperature. A brief description of the process The SBS / SIS copolymers hydrogenation reaction is performed in waterless and (favorably) oxygen-free conditions in cyclohexane, at temperature 100 °C under pressure of 10·105 Pa of hydrogen, in the presence of a catalytic system. After the reaction is completed, the polymer is precipitated from the solution with methanol and then it is filtered and dried to a constant mass. Advantages of the technology offered Due to very good properties, i.a. good resistance to weather factors and low temperature, hydrogenated block (SBS / SIS) copolymers find wide usage i.a. in glues, freezeproof shoe soles, as freezeproof modifiers for bituminous mixtures (including i.a. road and roof asphalts) and as cosmetics ingredients. Equipment pressure reactor fitted with a stirrer, agitators, dryer. Advancement of proceedings There have been defined optimal conditions to hydrogenate commercial SBS / SIS copolymers (KRATON - Schell) on the laboratory scale (a 500 ml reactor). Patentability Patent application No P-382 997 (2007) „Method to hydrogenate block copolymers of styrene with butadiene and styrene with isoprene”. 292 Market competitiveness Neither SBS / SIS nor hydrogenated forms of these copolymers are produced in Poland. SBS / SIS copolymers are however accessible on the international market and hydrogenated forms of SBS and SIS are produced by Shell and Repsol Companies. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 293 4) Modification of thermoplastic materials with waste from annual plants The subject of this research are composites, with a matrix in the form of polyolefin waste or poly(vinyl chloride), left from the process to recover copper from cables, filled with comminuted waste from annual plants (straw from: rape, oats, barley, rye, wheat and triticale), processed by extruding, compression molding or injection molding. A brief description of the process Components of the composite are mixed in an extruder and then processed with the injection molding method. If the composites are used to obtain extruded cross-sections, the granulation step can be omitted in the extrusion process. Advantages of the technology offered Straw from annual plants is a kind of waste of virtually no use (they are used as bedding for domestic cattle or incinerated). The proposed solution will allow to use them as fillers (in the amount up to 50 wt. %) in composites made of waste thermoplastic materials. Equipment extrusion granulating line, injection molding machine, press. Advancement of proceedings Laboratory scale. Patentability Patent application No P-383 568 (2007) „Poly(vinyl chloride) composition with a natural filler”. Patent application No P-383 567 (2007) „Polyolefin composition with a natural filler”. Patent application No P-385 117 (2008) „Biodegradable polymeric composite”. 294 Market competitiveness No similar solutions on the domestic and foreign market. Silver medal at Brussels Eureka „The Belgian and International Trade Fair for Technological Innovation” 2009. Type of expected cooperation Assistance in carrying out of extrusion and injection molding tests on the industrial scale. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 295 5) Polystyrene with reduced flammability obtained by suspension polymerization method A brief description of the process The process pertains to a method to produce polystyrene with reduced flammability by polymerization of styrene in aqueous suspension. As flame retarding additives are used halogen-free compounds. Suspension polymerization of polystyrene is performed in the presence of initiator, by adding a solution or styrene dispersion of phosphorous burning reducing additives to water mixed with a suspension stabilizer. There can also be added a modified or unmodified mineral with nanometric layered structure, especially modified montmorillonite and in justified cases also porophor. The product obtained is characterized favorable parameters of horizontal and vertical flammability (according to PN-EN-60695-1110:2002 standard) and favorable parameters of oxygen index (according to ASTM D 2863-97 standard). Advantages of the technology offered In the industrial practice, flammability of polystyrene obtained with the suspension polymerization method is reduced mainly with halogen additives, e.g. bromine compounds. The technology offered reduces flammability of polystyrene in a pro-ecological way, without using noxious, halogen flame retardants. Equipment The process can be performed using industrially available apparatus to produce polystyrene. Advancement of proceedings Laboratory works have been completed. Patentability Patent application No P-386 868 (2008) „Method to obtain polystyrene with reduced flammability using suspension polymerization”. Market competitiveness The proposed solution is competitive in relation to currently used methods to reduce polystyrene flammability with halogen additives, whose application is now being restricted by the European Union legislation. 296 Type of expected cooperation Cooperation in industrial implementation of the proposed solution. Contact Person Data Piotr Jankowski, Ph.D., Chem. Eng. phone: + 48 22 568 24 63 e-mail: [email protected] 297 6) Obtaining of polystyrene with reduced flammability A brief description of the process The method to produce the polystyrene composition with reduced flammability comprises polystyrene modification by creation of a premix with a flame retardant and possibly an auxiliary substance, in order to better homogenize the constituents. As flame retardants are used organophosphorus compounds. In the industrial practice it is favorable to incorporate the process to perform the flame retarding modification into the polystyrene production node. Advantages of the technology offered The technology offered reduces flammability of polystyrene in a pro-ecological way, without using noxious, halogen flame retardants. Equipment The process can be performed using industrially available apparatus to produce polystyrene. Advancement of proceedings Laboratory works have been completed. Patentability Patent application No P-379 453 (2006) „Polystyrene composition with reduced flammability and the method to produce the polystyrene composition with reduced flammability”. Market competitiveness The solution is competitive in relation to methods to reduce polystyrene flammability with halogen additives, whose application is being restricted by the European Union legislation. Type of expected cooperation Cooperation in industrial implementation of the proposed solution. Contact Person Data Piotr Jankowski, Ph.D., Chem. Eng. phone: + 48 22 568 24 63 e-mail: [email protected] 298 7) Application of graphite and graphite nanofillers to reduce flammability of plastics The offer pertains to obtaining plastics with reduced flammability with graphite or its derivatives including: polystyrene with reduced flammability produced in the suspension polymerization process, polyester or epoxy compositions. A brief description of the process Graphite additives are introduced into ready polyester or epoxy resins as a composition constituent and into polystyrene during its obtaining by the suspension polymerization method. Advantages of the technology offered Graphite and its varieties raise mounting interest as additives able to effectively reduce flammability of plastics. Graphite is practically neutral to the environment, and its action comprises i.a. restriction of oxygen access to the flame zone and creation of non-flammable decomposition products. Unfortunately, application of graphite alone in many cases (e.g. polystyrene) does not warrant sufficient reduction in the plastic flammability and hence there is a need to modify graphite or use additional supporting flame retardants. Proposed solutions are of pro-ecological character. Equipment The process can be performed using industrially available apparatus to produce polystyrene. Advancement of proceedings At present laboratory works are under way. Patentability Patent application in preparation. Market competitiveness The solution is competitive in relation to currently used methods to reduce plastics flammability with halogen additives, whose application is now being restricted by the European Union legislation. 299 Type of expected cooperation Co-financing of research works. Cooperation in industrial implementation of the proposed solution. Contact Person Data Piotr Jankowski, Ph.D., Chem. Eng. phone: + 48 22 568 24 63 e-mail: [email protected] 300 8) Polyesterols for polyurethanes A brief description of the process Polycondensation of the reaction mixture is carried out at temperature 200–230 °C in a inert gas, with continuous stirring and condensate collecting. In the technology waste poly(ethylene terephthalate), vegetable oils (rape, soya and sunflower), by-products and waste products emerging in technologies dealing with processing of various chemical products (glycerin, mixtures of dicarboxylic aliphatic acids, aromatic acids, hydroxyacids and their derivatives) are used. Advantages of the technology offered Usage of up to 80 % waste materials. They are characterized by a wide range of physicochemical properties (acid number, hydroxyl number, viscosity, functionality, reactivity, molecular weight etc.), what enables their widespread application and allows to obtain products of various utility properties. Economical advantages – consumption of cheaper and available waste materials, by-products and bio-renewable materials in the amount up to 80 wt. % of input raw materials (depending on the polyesterol type) substantially reduces production cost, compared to the input cost if technical petrochemical raw materials were used. Ecological advantages – usage of waste materials (PET), by-products (alcohols, multi-carboxyl acids) and bio-renewable materials (oils of agricultural origin), contributes to protection of the environment. Equipment Typical apparatus to produce polyesters (unsaturated polyester resins, alkyd resins and polyesterols). Advancement of proceedings Works of the laboratory scale have been completed. In case of some types of polyesters there have been completed studies on the experimental (half-technical) scale. Patentability There have been received patents for the method to obtain polyesterols. If in further researches were obtained original solutions, new patent applications are anticipated. Market competitiveness 301 Wide-ranging assortment for various applications. There has been stated full usability of the new polyesterol group to produce polyurethane foamy materials, glues, lacquers, solid screed masses and as modifiers (plasticizers) for epoxy and phenolic resins. Significantly reduced input material cost. Type of expected cooperation Production launching. Research concerning application of polyesters to manufacture new polyurethane products. The Institute has compiled Material Security Data Sheets for products worked out within the development project and depending on the interest by receivers and destination of particular type of polyesterol we are able to hand over these materials to potential clients, with guidelines concerning their application. Contact Person Data Elżbieta Wardzińska, Ph.D. phone: + 48 22 568 28 46 e-mail: [email protected] 302 9) Halogen-free flame retardant epoxy compositions The offer pertains to halogen-free epoxy compositions with reduced flammability. The composition is destined to obtain the flame retardant halogen-free plates for manufacturing of printed circuit boards. Flame retardancy of the composition is achieved through the use of a polymeric compound containing phosphorus. An organophosphorus compound is build into the resin structure by means of a chemical reaction. The obtained composition gives a product of required non-flammability degree, good mechanical properties, high glass transition temperature and low water absorption. A brief description of the process The halogen-free flame-retardant epoxy composition is obtained in a multistage process. The first stage is a modification of a commercial epoxy resin with a polymeric organophosphorus compound. At this stage functional groups of the organophosphorus compound react with epoxy groups of the epoxy resin. The synthesis proceeds with an excess of epoxy groups in relation to functional groups of the organophosphorus compound in the presence of an appropriate catalyst, at temperature 100–130 °C in a inert gas atmosphere. After the assumed parameters of the synthesized resin are obtained, the resin is dissolved in an organic solvent. At the next stage to a solution of resin containing organically bound phosphorus is added a curing agent, dissolved in an organic solvent and a curing catalyst. In the next step prepregs are prepared by impregnating a glass fabric with the epoxy composition and precuring at temperature 150–170 °C. The obtained prepregs are pressed under pressure of 50 kG/cm2 at temperature 170–180 °C. The plates obtained using the offered composition meet a UL 94 rating of VO. Their glass transition temperature is about 170 °C (DMA) and water absorption 0.033 % (the acceptable value is 0.150 %). Advantages of the technology offered The technology offered allows to reduce the flammability of epoxy compositions in a proecological way, without using harmful, halogen flame retardants. The organophosphorus compound applied is build into the structure of the epoxy system, thus allowing to avoid disadvantages related to the usage of additive flame retardants (worse mechanical and chemical properties, plasticization effect and lower glass transition temperature). Equipment Epoxy resins modification process: reactor equipped with a stirrer with the possibility of heating up to 130 °C and the possibility of dissolving the resulting product in an organic solvent. 303 The process to obtain plates for production of printed circuits industrial-available apparatus to produce epoxy laminates. Advancement of proceedings There have been carried out preliminary industrial tests to obtain halogen-free flame-retardant plates coated with copper film to produce printed circuit boards. Patentability Patent application No P-392 982 (2010) „Method to obtain epoxy resin with reduced flammability”. Market competitiveness The proposed solution is competitive in relation to currently used technologies to reduce epoxy materials flammability with halogen additives (mainly bromic ones), whose application is being restricted by the European Union legislation. Type of expected cooperation Finding a partner for industrial implementation of the proposed solution. Contact Person Data Barbara Szczepaniak, Ph.D., Chem. Eng. phone: + 48 22 568 20 55 e-mail: [email protected] Piotr Jankowski, Ph.D., Chem. Eng. phone: + 48 22 568 24 63 e-mail: [email protected] 304 10) Polymer miscibility modifiers A brief description of the process The method to produce the modifiers comprises joining selected small-molecular compounds or oligomers (hydrocarbon resins) to macromolecules of polypropylene, polyethylene or block (SIS / SBS) co-polymers. The reaction is performed in alloy. The process is waste-free. Advantages of the technology offered Obtained modifiers, due to the presence of reactive groups in macromolecules, more favorably interact with constituents of polymeric compositions, influence morphology of the compositions and stabilize their phase structure. Therefore it is possible to obtain „tailor-made” materials. Equipment Heated agitators with sigma type stirrers or extruders (most favorably twin-screw). Advancement of proceedings Laboratory works have been completed. Patentability Patent application No P-388 949 (2009) „Method to produce polymer miscibility modifiers”. Patent application No P-387 336 (2009) „Method to produce polystyrene impact modifiers and modified low-impact polystyrene”. Market competitiveness The modifiers are new products of diversified chemical construction, and hence they have a wide spectrum of applications in mixtures of various polymers. Moreover they can be based on both primary and secondary waste polymers. References Bronze medal for „A novel modifier for the enhancement of miscibility and mechanical properties of thermodynamically immiscible polymers”, IENA 2009, Nuremberg, Germany. Silver medal for „A method of strengthening the low-impact polystyrene”, Concours Lépine, Paris, France, 2010. 305 Type of expected cooperation Cooperation in order to carry out application studies and then implementation undertakings. Contact Person Data Assoc. Prof. Izabella Legocka, D.Sc.. phone: + 48 22 568 26 51 e-mail: [email protected] Ewa Wierzbicka, M.Sc., Chem. Eng. phone: + 48 22 568 26 93 e-mail: [email protected] 306 11) Polymeric composites with metal nanopowders for applications in electromagnetic interference (EMI) shielding The offered product is innovative in relation to traditionally used metal shields due to its properties characteristic of electromagnetic metamaterials. A brief description of the process The fillers of the composites are powders, nano-powders and/or nano-flakes of copper and other metals obtained from industrial waste waters and electrolytes according to the ICRI patent pending technology. The extrusion method is used to produce polymeric composites based on the polymer (e.g. EVA/HFFR) matrix with added copper nanopowder filler. Advantages of the technology offered The technology is based on the most recent achievements in the production of a qualitatively new group of metal nano-fillers in the form of copper and other metals powders and flakes. Since the nanopowders fillers are obtained from industrial waste waters the technology promotes pro-ecological manufacturing practices. Another key advantage of the patent pending technology is low production cost of both the nanofillers and composites. In comparison to metal shields traditionally used to reduce electromagnetic interferences (EMI), polymeric composite materials are characterized by low specific weight, good corrosion resistance, elasticity and easy processability. Equipment Nanopowders are produced on the laboratory scale using a two-electrode system with a potentiostat of type AUTOLAB GSTST30 made by EcoChemie. The following procedure is used in order to obtain polymeric composites with nanopowders fillers: single- or twin-screw extruder, electrically heated metering mixer for PLASTI-CORDER device produced by BRABENDER Company, hydraulic press. The mechanical and dielectric properties of the obtained composites are studied. In order to observe the structure and to perform qualitative chemical analysis of the composites a SEM with EDS is used. 307 Advancement of proceedings The technology has been developed to obtain a group of polymeric composites, displaying low electric conductance and simultaneously characterized by very good ability to EMI shielding. For preliminary laboratory scale tests on the laboratory scale a material with the desired properties was selected and subsequently, after scale-up of the manufacturing process (to pilot scale) the obtained composite was tested in a company dealing with cable production (in Poland and Israel). Patentability Patent applications: PCT/PL2010/000022 and UP RP P 392 282. Market competitiveness The technology employs modern, pro-ecological, innovative nanotechnology (which is in-line with EU policy see e.g. FP7 projects calls). The technology is cost effective and based on recycling of copper recovered from industrial waste waters, hence its potential patent rights purchasers might have opportunity to get e.g. EU and public financial support for its implementation. Type of expected cooperation Cooperation with flash-investors and cooperative scientific-research works. Contact Person Data Assoc. Prof. Przemysław Łoś, D.Sc. phone: + 48 22 568 20 61 e-mail: [email protected] Assoc. Prof. Regina Jeziórska, D.Sc., Eng. phone: + 48 22 568 24 91 e-mail: [email protected] 308 12) Modification of thermoplastic materials with natural polymers The subject of the offer are composites with polyolefin or poly(vinyl chloride) matrix filled with cellulose fiber of various origin (e.g.: waste from newspapers or chipboards grinding and waste cellulose from paper industry or wood flour), destined for processing with extrusion, compression molding or injection molding. A brief description of the process The composite granulate is obtained by extrusion and then various products are made from it with the injection molding method. If the composites are used to obtain extruded crosssections, the granulation step can be omitted in the extrusion process. Advantages of the technology offered Thermoplastic materials used in the composites can be primary or they can be partly or entirely substituted with appropriate waste material. It can be an agglomerate from packaging foil or PVC waste left from copper recovery from cables. Equipment extruding line for production of granulates or extruded cross-sections, injection molding machine of size depending on the obtained product. Advancement of proceedings The composite granulate have been obtained by extrusion in semi-technical tests. The tensile properties, flexular properties and impact strength have been carried out. Investigations of degradability by aging in different conditions of use have been carried out too. The various products about different largeness are made from the composites by the injection molding and compression molding (e.g. flowerpots). Composites have been used to obtain extruded crosssections without the granulation step. Patentability PL 194 586 (2006) „The method of manufacture of cellulose fibre from waste paper”. Market competitiveness Silver medal at Brussels Eureka „The Belgian and International Trade Fair for Technological Innovation” 2009. 309 Type of expected cooperation Assistance in carrying out of extrusion and injection molding tests on the industrial scale. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 310 13) Melamine salts The subject of the offer are salts of melamine and organic acids (cyanuric acid – melamine cyanurate) or inorganic acids (phosphoric – melamine phosphate, melamine pyrophosphate, polyphosphoric – melamine polyphosphate, boric – melamine borate). The above-mentioned salts are solids with decomposition temperature > 260 °C. They are applied as flame retardants to thermoplastic materials, especially polyamides. A brief description of the process Melamine salts are obtained in a direct reaction between melamine and appropriate organic or inorganic acid in aqueous suspension. These reactions do not require any catalyst. Advantages of the technology offered Flame retardants used so far were based on chlorine or bromine compounds. An advantage of the offered technology is synthesis of ecological halogen-free flame retardants. The process of preparation of salts of melamine proceeds in aqueous suspension with 100 % efficiency, without by-products. Equipment A reactor equipped with a reflux condenser, a temperature recorded and a heating medium. Advancement of proceedings The melamine salts synthesis has been developed on the laboratory scale. It is necessary to reach appropriate degree of fineness of obtained salts. There is also necessary to refine the method to introduce the obtained composites into polymeric materials. Patentability Patent application in preparation. Market competitiveness Halogen-free flame retardants constitute a competitive solution compared to flame retardants containing chlorine or bromine compounds. Type of expected cooperation Cooperation to increase the scale of synthesis of melamine salts and further research concerning application aspects of the obtained compounds. Contact Person Data Dorota Kijowska, Ph.D., Chem. Eng. phone: + 48 22 568 25 05 e-mail: [email protected] 311 14) Utilization and recycling of the wastewater and technological streams in the galvanizing plant The innovation of this technology is the application of filtration and membrane processes for separating of selected streams into clean water and concentrated solution of metals. Both resulting streams are fully subjected to recycling. The technology has been developed for the hot-dip galvanizing plant in which zinc sulfate solution is used as an electrolyte. A brief description of the process wastewater evaporation demineralized water electrolyte without Fe ION EXCHANGE UNIT ELECTROLYTE PROCESS WATER washings electrolyte with Fe water from ionite bed washing washing retentate NANOFILTRATION permeate Selected technological streams and wastewater from different processes realized in the galvanizing plant are collected together and sent to the membrane unit (in this case, nanofiltration unit), where the separation into recovered water and concentrated solution of metals goes on. The products of the separation are turned back to the electrolyte. Advantages of the technology offered reduction of the amount of wastewater only to the streams from the regeneration of the ionite column high degree (> 99 %) of the zinc recovery from technological streams and wastewater which underwent membrane process reduction of the water consumption by the galvanizing plant by over 70 % Equipment In this technology different membrane modules are used, all of them are commercially available. Customization of the technology to the conditions in the particular plant, e.g. the hot-dip galvanizing plant, must be preceded by the semi-technical and pilot researches. The Institute has the appropriate apparata and installations for performing such studies. 312 Advancement of proceedings Implementation of this technology requires the performance of studies which are necessary to adjust it to the conditions in particular industrial plant. Patentability Depending on the range of the customization work, the technology can be offered as „knowhow” of the Industrial Chemistry Research Institute or it can be the subject of a patent application. Market competitiveness The technologies of recycling of technological streams, including recovery of water and other natural raw materials, offered by other companies, can be competitive to this technology. Type of expected cooperation Co-operation with industrial plants concerning elaboration of technological concept to the conditions of the particular company. Customization works and researches will be performed primarily at the location of the interested company. Contact Person Data Tadeusz Porębski, M.Sc., Chem. Eng. phone: + 48 22 568 20 12 e-mail: [email protected] 313 15) Usage of waste materials to produce acoustic screens The subject of the offer are acoustic screen panels of a new type for highway engineering applications. A brief description of the process Polyolefin composites containing comminuted rubber scrap are obtained by mixing of components in a suitable mixer or they can be extruded in the form of a granulate. These composites can be processed with standard methods, like extrusion, compression molding and injection molding. Advantages of the technology offered Disposing of waste polymeric plastics and comminuted rubber scrap from tire. Equipment granulation line with a single-screw extruder, single-screw extruder, screw diameter > 60 mm, used in the extrusion molding method, hydraulic press, injection molding machine. Advancement of proceedings Laboratory scale. Patentability W 60273 (1998) „Sound-absorbing panel”. Patent No P-201 467 (2004) „Thermoplastic composition”. Patent No P-201 466 (2004) „Polyolefins-based thermoplastic composition”. Patent No P-206 725 (2004) „Method to produce sound-absorbing screen panels”. Market competitiveness No similar solutions on the domestic market. Market competition in the area of acoustic screens is high. Plastic screens used nowadays are transparent panels made from poly(methyl methacrylate) or polycarbonate. Keeping these screens clean is very difficult and after a few years they are useless. Type of expected cooperation Trial fabrication of screens on the production scale. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 314 16) Revulcanization of comminuted tire rubber scrap The subject of the offer are utility goods fabricated from comminuted rubber scrap made of waste tires or other comminuted rubber scrap revulcanized using sulfur. A brief description of the process Rubber panels made of comminuted rubber scrap are obtained with the developed method to revulcanize this waste with sulfur, using the compression molding technique. Advantages of the technology offered Results of preliminary inspection of mechanical properties and wear resistance of these composites are only slightly different from the characteristics of primary rubber. Equipment mixer; hydraulic press. Advancement of proceedings Laboratory scale. Patentability Patent application No P-381 070 (2006) „Method to produce utility goods from comminuted rubber waste”. Market competitiveness The current recycling offer is insufficient in relation to steady growing amount of vulcanized waste, especially waste tires. Type of expected cooperation Partial financing of research works. Assistance in performing an attempt to press bigger fittings. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 315 17) Hydrometallurgical recovery of materials from waste zinc-carbon and alkaline batteries A brief description of the process The proposed and verified on the big-laboratory scale process of hydrometallurgical recycling of zinc-carbon and zinc-manganese cells comprises a number of stages: mechanical disassembly and separation of cells, leaching, concentration and purification of solutions and obtaining products containing zinc and manganese. At the first stage intermingled primary battery waste is mechanically disassembled, allowing direct recovery of iron, constituting housing of these cells. From one ton of waste this process recovers about 220 kg of iron. Then by aerial separation is recovered polymeric plastic and paper, and remaining black mass is transferred for leaching with sulfuric acid(VI). This stage, performed at elevated temperature and under permanent stirring, results in creation of a mass containing manganese oxides and graphite and a solution of zinc and manganese sulfates. The resulting black mass is undergoes further technological processes. These processes produce material which can be used for production of new zinc-carbon cells. Obtained solutions are concentrated and separated with membrane techniques and heavy metals are separated out of them. At the last stage, with chemical and/or electrochemical methods, zinc and manganese are recovered from concentrated solutions (with 98 % efficiency). Solutions left from this process are turned back again to the process of dissolving black masses. Advantages of the technology offered The developed process of hydrometallurgical recycling of primary cells is characterized by: recycling efficiency compliant with EU regulations, i.e. exceeding 55 %, recovery of chemical compounds of zinc and manganese, directly applicable in the economy, production of new electrode material for zinc-carbon cells, significant reduction in mercury contents in battery waste, small amount of created waste, small energy consumption, small consumption of the leaching reagent. Equipment To perform 1/4-technical scale tests there is necessary to build a recycling line consisting of leaching tanks at least 1 m3 in volume, filtration presses, a pumping system, etc. 316 Advancement of proceedings Based on results of the works on the big-laboratory scale (there have been processed about 270 kg of battery waste) there have been specified parameters to perform a 1/4-technical scale test, which will allow to develop a technological documentation to construct a recycling line for zinc-carbon and alkaline cells. Patentability Patent applications protecting the developed solution are in preparation. Market competitiveness EU Directive No 2006/66/EU introduced for the first time the obligation to collect zinc-carbon and alkaline cells and reach 50 % recycling rate of waste materials from them. Hence, as of 26.09.2011 there will not be allowed to use simple recycling methods e.g. Waelz process, used in Poland. This is why it became necessary to develop an alternative method to manage this waste, allowing to recover cathode electrode material (MnO2 + carbon). It can be successfully used to produce new zinc-carbon cells. Cells produced from the recovered waste material have working parameters similar to commercially available cells. Taking into account the iron recovery level, repeated usage of MnO2/C mixture and over 95 % zinc recovery, the estimated recycling level is at least 55 %. Increase in efficiency of this process is related to i.a. repeated turning back the obtained solution to the process, allowing to reduce the amount of waste. Obtained results indicate unequivocally, that the proposed method to recycle zinc-carbon and zinc-manganese cells meets the requirements set out for EU member states. Type of expected cooperation Participation in implementation works, construction of a pilot installation. Contact Person Data Tadeusz Porębski, M.Sc., Chem. Eng. phone: + 48 22 568 20 12 e-mail: [email protected] 317 18) Modification of waste from electric / electronic equipment Waste from Electric and Electronic Equipment (WEEE) in nowadays a major problem. The developed technology allows to modify this waste with other plastics and/or glass fiber, allowing to obtain modified WEEE with properties comparable to primary plastics. A brief description of the process Composites are obtained by its processing into a granulate with the extrusion method and making of them various products with the injection molding method. Advantages of the technology offered The developed technology aims at modifying these waste plastics with other plastics and/or glass fiber. This way we aim at obtaining modified WEEE waste with properties comparable to primary plastics. Equipment extrusion granulating line, injection molding machine. Advancement of proceedings Laboratory scale. Market competitiveness No similar solutions on the domestic market. Type of expected cooperation Partial financing of works. Carrying out of extrusion and injection molding tests on the industrial scale. Contact Person Data Prof. Wincenty Skupiński, D.Sc., Chem. Eng. phone: + 48 22 568 21 83 fax: + 48 22 568 22 33 e-mail: [email protected] 318 19) Production of glycerol polyalkylethers as biofuel components Glycerol di- and triethers obtained from glycerol, a by-product in biofuels production from vegetable oils (fatty acid methyl esters), can be used not only as an additive to biofuels or diesel oils, but also to gasoline, increasing its octane number. The presence of glycerol polyalkylethers in biofuel influences effectiveness of hydrocarbon combustion, by reduction of emission of noxious substances into the atmosphere. These ethers have also a positive influence on physicochemical properties of biofuel, by reducing its viscosity and temperature of cloudiness. Process description Glycerol polyalkylethers are obtained in a reaction of glycerol with olefins contained in the isobutene fraction (containing ca. 60 % isobutene), performed in the presence of an acid heterogeneous catalysts, at 80–120 °C and under pressure of 10–20 · 105 Pa. The process is carried out in the fixed-bed reactor. The product contains also isobutene dimers (isooctenes), a full-value raw material to produce isooctane, which can be separated from the ethers with flash distillation. Advantages of the technology offered Glycerol polyalkylethers are a very valuable additive to biofuels used in self-ignition engines. The developed technology allows to dispose of market surplus of glycerol, derived from transesterification of triglycerides contained in vegetable oils. In the Institute of Biofuels and Renewable Energy there were performed physicochemical investigation of the biofuel (from industrial process of rape oil transesterification) modified with tert-butyl glycerol ethers. A significant reduction in cold filter plugging point, viscosity reduction and increased cetane number was recognized. Equipment The glycerol ethers production proceeds in a column reactor with a catalyst bed, operating under pressure 10–20 · 105 Pa. Products can be separated by distillation in high-performance rectification columns. The state of technology The laboratory studies has been finished. The catalyst has been selected and the conditions to carry out the process have been established. Patents 319 Patent No P-200 500 (2004) „Method to produce glycerin polyalkylethers”. Patent No P-206 797 (2006) „Method to produce biofuel for self-ignition engines”. Type of expected cooperation Cooperation in research on a bigger scale and establishment of foundations to build a 1/4technical installation. Assistance in the range of application research. Contact Person Data Małgorzata Jamróz, Ph.D., Chem. Eng. phone: + 48 22 568 20 21 e-mail: [email protected] 320 20) Gliperol – a new biofuel Product used directly as a biofuel or as a biocomponent for diesel fuel. A brief description of the process Gliperol is obtained in a cross-transesterification reaction between triacylglycerols of vegetable oils or fats and low-molecular-weight esters, e.g. methyl acetate, at temperature 110 °C, under normal pressure, except for the solvent recovery stage, which is performed under reduced pressure. It is a single-stage process, without the necessity to drain the glycerin fraction as a by-product. Advantages of the technology offered In the classical method to obtain fatty acid methyl esters (FAME), i.e. transesterification of triacylglycerols with methyl alcohol, the glycerin fraction emerges as a by-product, which must be purified and disposed of. In the proposed technology as a biofuel component is used glycerin in the form of ester derivative. Production cost of the new biofuel is 30–35 % less than the cost to produce FAME and usage of glycerin as a biofuel component decreases ecological threat related to its purification and processing. During Gliperol combustion in an engine the amount of greenhouse gases (CO 2, CO) and HC created is smaller than from combustion of petrochemical fuel or classical fatty acid methyl esters (FAME). Equipment The synthesis is performed in typical apparatus made of acid-resistant steel, employed to obtain fatty acid methyl esters using the classical method (with minor additions). Advancement of proceedings There have been developed foundations of the technology to obtain the new biofuel – Gliperol and initial application research has been performed. Patentability Patent No P-197 375 (2002) „Biofuel for self-ignition engines and the method to obtain biofuel for self-ignition engines”. Patent application No P-359 907 (2003) „Method to obtain biofuel for self-ignition engines”. Patent application No EP-1 580 255 A1 (2004) „A biofuel for compression-ignition engines and a 321 method for preparing the biofuel”. Patent application No P-378 096 (2005) „New biofuel components and the method to obtain new biofuel components”. Patent application No P-389 394 (2009) „Biofuel component, method to obtain it and its application”. Market competitiveness No similar technology on the market. FAME production costs are so high, that their production without financial donations is unprofitable. The technology proposed allows to reduce the cost to obtain biofuel by 30–35 % compared to the cost of the classical FAME production method and to evade problems concerning disposing of the glycerin fraction. Type of expected cooperation Cooperation in development of the technology, taking into account the scale, ramifications concerning constituents and capabilities of the contracting party. Contact Person Data Prof. Andrzej W. Lipkowski, D.Sc. phone: + 48 22 568 28 48 fax: + 48 22 568 26 33 e-mail: [email protected] 322 21) Benzalkonium lactates Benzalkonium L-lactate and benzalkonium D,L-lactate are ionic liquids with excellent biocidal properties. They contain an expanded ammonium cation, displaying biocidal properties and a mandelate anion, non-toxic and pharmaceutically acceptable. Biological activity of benzalkonium lactates against a number of microorganisms is from several to several dozen times bigger than active substances widely used in preparations available on the domestic market. Their biocidal action is most effective against the following microorganisms: Staphylococcus epidermidis, Moraxella catarhalis, Bacillus subtilis, Rhodotorula rubra. They are food deterrents against insects e.g. khapra beetle Trogoderma granarium (larva), i.e. chemical substances, which act on taste organs of insects, reducing their appetite, up to total stopping of foraging, what eventually brings them to death. They belong to the group of cationic surface active compounds. They display also electrostatic properties. Benzalkonium L-lactate and benzalkonium D,L-lactate can be ingredients of: biocidal preparations, insecticidal preparations, and disinfecting/washing preparations. R1 = C12H25 (60 %), R1 = C14H29 (40 %) Benzalkonium lactates are thick liquids, soluble in water, acetone and ethanol, thermally stable, with decomposition temperature > 180 °C. They have no toxic effect on warm-blooded organisms (toxicity class IV). A brief description of the process Benzalkonium lactates are obtained in reaction between benzalkonium chloride and a potassium salt of L-lactic (or D,L-lactic) acid, in aqueous environment at temperature 40 °C. The product is separated by distilling off water under reduced pressure and filtering off the byproduct – potassium chloride. In order to remove water it is necessary additional drying of the product at elevated temperature and under reduced pressure. Advantages of the technology offered 323 The technology is simple, low-waste and substrates are cheap. The environment of the reaction is water and the by-product is potassium chloride. The reaction yield is high. Equipment The apparatus set comprises a glass reactor with bottom draining valve, equipped with a highspeed mechanical stirrer, a thermometer and a dephlegmator (which can be exchanged for a distillation set) and a heating-cooling jacket, allowing to heat up and cool down the contents. Auxiliary equipment comprises: thermostat, membrane vacuum pump, vacuum evaporator (to distillate off water from the post-reaction mixture and for final drying of the product). Advancement of proceedings There has been compiled documentation concerning physicochemical properties and analytic methods have been developed. Acute toxicity studies have been performed. There have been performed trials to obtain benzalkonium lactates on the scale of 1.5 kg of the product. Patentability Patent application No P-380 976 (2006) „New quaternary ammonium salts of lactic acid and a method to obtain new quaternary ammonium salts of lactic acid”. Patent application No P-383 743 (2007) „Application of benzalkonium lactate as a food deterrent”. Patent application No P-382 950 (2007) „Application of benzalkonium lactate in washing and disinfection”. Market competitiveness New ionic liquids are novel compounds with fungicidal and bactericidal properties. The effect of benzalkonium lactates is against some microorganisms many times more effective than commonly used benzalkonium chloride, so they can be applied in preparations in low concentrations. 324 Type of expected cooperation Cooperation in compiling registration documentation, deployment and launching production of the preparation. Contact Person Data Anna Wiśniewska, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] Anna Kulig-Adamiak, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] 325 22) Dialkyldimethylammonium prolinates Didecyldimethylammonium L-prolinate and benzalkonium L-prolinate – ionic liquids containing an ammonium cation, giving them biocidal properties and an anion originating from L-proline amino acid. Biocidal activity of these compounds is comparable or greater than commonly used didecyldimethylammonium chloride and benzalkonium chloride. Their biocidal action is most effective against the following microorganisms: Micrococcus luteus, Staphylococcus epidermidis, Staphylococcus aureus, Moraxella catarhalis, Enterococcus faecium, Escherichia coli and two fungi: Candida albicans and Rhodotorula rubra. Due to the high level of anti-microbial activity, obtained ionic liquids can be used in preparations in small concentration. They are probably low toxic to warm-blooded organisms, although appropriate tests have not been performed. Dialkyldimethylammonium prolinates belong to the group of cationic surface active compounds. They display also electrostatic properties. They can be constituents of: biocidal preparations, disinfecting/washing preparations. They can also serve as catalysts in some types of reactions in asymmetric organic synthesis. Benzalkonium prolinate n = 9 60 % n = 11 40 % Didecyldimethylammonium prolinate They are thick, waxy compounds soluble in water, methanol, methylene chloride and acetone. A brief description of the process Dialkyldimethylammonium prolinates are obtained in a reaction between benzalkonium (didecyldimethylammonium) chloride and a potassium L-proline salt in aqueous environment at temperature 60 °C. The product is separated by vacuum distilling off water, dissolving in organic solvent, precipitating and filtering off by-product, i.e. potassium chloride and concentrating the ooze. Dialkyldimethylammonium L-prolinates require additional drying at elevated temperature 326 and under reduced pressure. Advantages of the technology offered The technology is simple, low-waste and substrates are cheap. The environment of the reaction is water and the by-product is potassium chlorine. The reaction yield is high. The technology has been awarded with a silver medal at PALEXPO Exhibition (Geneva, 2010). Equipment The apparatus set comprises a glass reactor with bottom draining valve, equipped with a highspeed mechanical stirrer, a thermometer and a dephlegmator (which can be exchanged for a distillation set) and a heating-cooling jacket, allowing to heat up and cool down the contents. Auxiliary equipment comprises: thermostat, membrane vacuum pump, vacuum evaporator (to distillate off water from the post-reaction mixture and for final drying of the product). Advancement of proceedings There has been compiled documentation concerning physicochemical properties and analytic methods have been developed. No acute toxicity studies have been performed. Patentability Patent application No P-388 195 (2009) „New ionic liquids from the ammonium group, a method to obtain them and their application”. Market competitiveness New ionic liquids are novel compounds with fungicidal and bactericidal properties. Due to their big efficiency, obtaining the desired effect requires only small concentration of these compounds in preparations. 327 Type of expected cooperation Cooperation in compiling registration documentation, deployment and launching production of the preparation. Contact Person Data Anna Wiśniewska, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] Anna Kulig-Adamiak, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] 328 23) Dialkyldimethylammonium mandelates Dialkyldimethylammonium mandelates can occur in the form of a racemate (R,S) or optically active isomers (S)-(+) or (R)-(-). These compounds contain an expanded ammonium cation and a mandelate anion, biocidally active against microorganisms. For instance (R,S) benzalkonium mandelate is most effective against the following microorganisms: Micrococcus luteus, Staphylococcus epidermidis, Staphylococcus aureus, Moraxella catarhalis, Enterococcus faecium, Escherichia coli, Proteus vulgaris, Pseudomonas aureginosa, Serratia marcescens and two fungi: Candida albicans and Rhodotorula rubra. Dialkyldimethylammonium mandelates belong to the group of surface active cationic compounds and display also electrostatic properties. These compounds can be constituents of: biocidal preparations, disinfecting/washing preparations. Didecyldimethylammonium mandelate Domiphen mandelate Benzalkonium mandelate n = 9 60 % n = 11 40 % Dialkyldimethylammonium mandelates are thick, waxy compounds, soluble in water, methanol, methylene chloride and acetone, with decomposition temperature > 180 °C. A brief description of the process Dialkyldimethylammonium mandelates are obtained in a reaction between dialkyldimethylammonium chloride (bromide) with a potassium salt of mandelic acid [or (R)-(-) – mandelic acid or (S)-(+) – mandelic acid] in aqueous environment at temperature 60 °C. The product is separated by vacuum distilling off water, dissolving in organic solvent, precipitating and filtering off the by-product – potassium chloride and then concentrating the ooze. In order 329 to remove water, additional drying of the product in elevated temperature and under reduced pressure takes place. Advantages of the technology offered The technology is simple, low-waste and substrates are cheap. The environment of the reaction is water and the by-product is potassium chlorine. The reaction yield is high. The technology to synthesize these compounds has been awarded with a silver medal at PALEXPO Exhibition (Geneva, 2010). Equipment The apparatus set comprises a glass reactor with bottom draining valve, equipped with a highspeed mechanical stirrer, a thermometer and a dephlegmator, which can be exchanged for a distillation set and a heating-cooling jacket, allowing to heat up and cool down the contents. Auxiliary equipment comprises: thermostat, membrane vacuum pump, vacuum evaporator (to distillate off water from the post-reaction mixture and for final drying of the product). Advancement of proceedings There has been compiled documentation concerning physicochemical properties and analytic methods have been developed. No acute toxicity studies have been performed. Patentability Patent application No P-388 194 (2009) „New ammonium ionic liquids, a method to obtain them and their application”. Market competitiveness New ionic liquids are novel compounds with fungicidal and bactericidal properties. Due to their big efficiency, obtaining the desired effect requires only small concentration of these compounds in preparations. 330 Type of expected cooperation Cooperation in compiling registration documentation, deployment and launching production of the preparation. Contact Person Data Anna Wiśniewska, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] Anna Kulig-Adamiak, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] 331 24) Didecyldimethylammonium lactates Didecyldimethylammonium L-lactate and didecyldimethylammonium D,L-lactate are new biocidal compounds, containing an expanded ammonium cation, giving them biocidal properties and a lactate anion, non-toxic and pharmaceutically acceptable. Their biocidal action is most effective against the following microorganisms: Micrococcus luteus, Staphylococcus aureus, Staphylococcus epidermidis, Enterococcus faecium, Escherichia coli, Bacillus subtilis, Moraxella catarhalis, Rhodotorula rubra. Didecyldimethylammonium lactates are food deterrents against insects e.g. khapra beetle Trogoderma granarium (larva) and wheat weevil Sitophilus granarius (beetle), i.e. chemical substances, which act on taste organs of the insects, reducing their appetite, up to total stopping of foraging, what eventually brings them to death. They belong to the group of cationic surface active compounds. They display also electrostatic properties. Didecyldimethylammonium L-lactate and didecyldimethylammonium D,L-lactate can be constituents of: biocidal preparations, insecticidal preparations, disinfecting/washing preparations. R = C10H21 Didecyldimethylammonium lactates are thick liquids, soluble in water, acetone and ethanol. They are thermally stable compounds, with decomposition temperature > 200 °C. They have no toxic effect on warm-blooded organisms (toxicity class IV). A brief description of the process Didecyldimethylammonium lactates are obtained in reaction between didecyldimethylammonium chloride and a potassium salt of L-lactic (or D,L-lactic) acid, in aqueous environment at temperature 40 °C. The product is separated after distilling off water under reduced pressure and filtering off the by-product potassium chloride. In order to remove water it is necessary additional drying at elevated temperature and under reduced pressure. 332 Advantages of the technology offered The technology is simple, low-waste and substrates are cheap. The environment of the reaction is water and the by-product is potassium chlorine. The reaction yield is high. Equipment The apparatus set comprises a glass reactor with bottom draining valve, equipped with a high-speed mechanical stirrer, a thermometer and a dephlegmator (which can be exchanged for a distillation set) and a heating-cooling jacket, allowing to heat up and cool down the contents. Auxiliary equipment comprises: thermostat, membrane vacuum pump, vacuum evaporator (to distillate off water from the post-reaction mixture and for final drying of the product). Advancement of proceedings There has been compiled documentation concerning physicochemical properties and analytic methods have been developed. Acute toxicity studies have been performed. There have been performed trials to obtain didecyldimethylammonium lactates on the scale of 1.5 kg of the product. Patentability Patent application No P-380 976 (2006) „New quaternary ammonium salts of lactic acid and a method to obtain new quaternary ammonium salts of lactic acid”. Patent application No P-383 744 (2007) „Application of dialkyldimethylammonium lactate as a food deterrent”. Patent application No P-382 951 (2007) „Application of dialkyldimethylammonium lactate in washing and disinfection”. Market competitiveness New ionic liquids are novel compounds with fungicidal and bactericidal properties. Due to their big efficiency, obtaining the desired effect requires only small concentration of these compounds in preparations. 333 Type of expected cooperation Cooperation in compiling registration documentation, deployment and launching production of the preparation. Contact Person Data Anna Wiśniewska, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] Anna Kulig-Adamiak, M.Sc., Chem. Eng. phone: + 48 22 568 21 93 e-mail: [email protected] 334 25) Production of alkaline hydrogen peroxide solution for pulp bleaching The subject of the offer is a technology to produce alkaline hydrogen peroxide solution, which can be used to bleach paper or textile pulp and to produce perborates and percarbonates. In a reaction of this solution with carbon dioxide it is also possible to obtain sodium bicarbonate solution and hydrogen peroxide suitable for concentration. A brief description of the process In the developed method, a diluted soda lye solution is enriched in hydrogen peroxide by electrolysis of gaseous oxygen (pure or from the air). On the cathode occurs electroreduction of molecular oxygen to the ionic form of hydrogen peroxide: O2 + H2O + 2 e → HO2– + OH– On the anode takes place either hydrogen oxidation: H2 + 2 OH– → 2 H2O + 2 e or oxygen release: 2 OH– → 1/2 O2 + 2 e + H2O In the first case, electric energy does not have to be supplied (it can be even recovered). The reaction can then be represented by the following summary equation: H2 + O2 + OH– → HO2– + H2O In the second case, electric energy needs to be supplied, but according to the summary equation less oxygen is consumed and no water is formed: 1/2 O2 + OH– → HO2– As a result of both the above overall reactions the number of hydroxyl groups decreases, but an equivalent number of them emerges in bleaching due to decomposition of HO2– . Alkaline hydrogen peroxide solution with H2O2 concentration up to 7 wt. % and up to 14 wt. % of NaOH is ready to be used at the bleaching stages. The lye recovered from the bleaching is recycled to the electrolysis stage in order to enrich it in hydrogen peroxide again. The electrolysis is performed in an aqueous solution of soda lye at the temperature of 50–60 °C under atmospheric pressure. Advantages of the technology offered the method eliminates the necessity to purchase concentrated hydrogen peroxide, transport it and mix it with lye (independence from H2O2 suppliers and no risk of handling concentrated H2O2); the process is well scalable (device modularity); the product obtained is of high purity; the method is waste-free and safe; 335 low energy consumption (possibility of recovering the energy released in the reaction). Equipment The basic reactor unit for oxygen electrolysis consists of a cathode, an anode and an ionic conductive membrane. Fittings from lye-resistant plastics work well. The electrodes used are made of carbon, carbon-nickel or carbon-platinum. The electrode separator is made of Nafion™. Technology development stage An electrolyzer has been tested on the laboratory scale (a few grams of H 2O2 per hour) in twoweek continuous operation, which gave a steady H2O2 current efficiency > 90 %, a steady mass ratio of NaOH to H2O2 in the product = 2:1, an adjustable product concentration of 2–5 wt. % H2O2, and simultaneous production of electric energy and useful H2O2 solution using a hydrogen anode. Patentability Patent No P-184 363 B1 (2002) „Method to obtain alkaline hydrogen peroxide solution”. Market competitiveness Taking careful assumptions (current parameters of the electrolyzer process are not optimal), the total cost to produce H2O2 with this method in the form of alkaline solution is comparable to the cost to obtain the solution by mixing purchased H2O2 with soda lye. Type of expected cooperation At the present stage, it is purposeful to develop a new electrolyzer construction maximizing the electrodes’ utilization (measured in grams of H2O2 per unit of time per unit of electrode area). Work should be conducted initially on the laboratory scale, then on the 1/4-technical scale. We are interested in obtaining funding from its final user (paper mills, textile producers and chemical plants) for the further development of the technology in return for the rights to use the technology. Contact Person Data Piotr Piela, Ph.D. phone: + 48 22 568 29 08 e-mail: [email protected] ANLYTICAL SERVICES 336 1) Analysis and characterization of materials Since 1997, the quality management system according to the PN-EN ISO/IEC 17025 standard has been implemented in all laboratories of the Department of Analysis and Characterization of Materials. Selected methods are included in the scope of accreditation, confirmed by the accreditation certificate No. AB 113 issued by the Polish Centre for Accreditation (PCA). Department is also notified as the approved laboratory that according to the Regulation of European Parliament and Council No. 648/2004 on detergents is competent to carry out the biodegradation tests required by the regulation (Official Journal of The European Union 2009/C 39/05). The following studies can be carried out within the scope of accreditation: identification of polymers, plastics and plastics additives (e.g. fillers, stabilizers, plasticizers, antioxidants etc.) by infrared spectroscopy method (qualitative analysis). Such substances are identified, the IR spectra appear in the directories of the standard spectra. Contact Person Data Joanna Sołtysiak, Ph.D. phone: + 48 22 568 24 41, + 48 22 568 24 67 fax: + 48 22 568 20 48 e-mail: [email protected] determination of metal content by Flame Atomic Absorption Spectrometry (FAAS) method: barium (1–100) mg/l, cadmium (0.1–10) mg/l, chromium (0.2–20) mg/l, lead (1–100) mg/l, antimony (1–100) mg/l in aqueous solutions not requiring mineralization; determination of metal content by Flame Atomic Absorption Spectrometry (FAAS) method: barium (0.0015–0.15) % (m/m), cadmium (0.00015–0.015) % (m/m), chromium (0.0003–0.03) % (m/m), lead (0.0015–0.15) % (m/m), antimony (0.0015– 0.15) % (m/m) in colourants of plastic materials coming into contact with food; determination of metal content by Flame Atomic Absorption Spectrometry (FAAS) method: barium (0.0010–1) % (m/m), cadmium (0.0001–1) % (m/m), chromium (0.0002–1) % (m/m), lead (0.0010–1) % (m/m), antimony (0.0010–1) % (m/m) in plastics and vegetable materials. 337 Contact Person Data Dorota Kolasa, M.Sc. phone: + 48 22 568 23 25 phone/fax: + 48 22 568 20 51 e-mail: [email protected] Beata Arndt, M.Sc. phone: + 48 22 568 23 26 phone/fax: + 48 22 568 20 51 e-mail: [email protected] evaluation of inorganic, organic and total incrustation of cotton fabric after wash; evaluation of loss in tensile strength of cotton fabric after wash, in %, force range: 0.5– 2500 N. evaluation of aerobic ultimate biodegradation of organic chemical products, including detergent products and surfactants by manometric respirometry in the range of 0– 100 %; evaluation of aerobic ultimate biodegradation of organic chemical products, including detergent products and surfactants, with Dissolved Organic Carbon (DOC) Die-away method in the range of 0–100 %; determination of Chemical Oxygen Demand (COD) in the range of 30–660 mg/l; determination of Dissolved Organic Carbon (DOC) in the range of 0.05–4000 mg/l. Determination of biodegradability, COD and DOC done acc. to law as of 9.01.2009 (Journal of Laws 2009 No 20 pos. 106), Council Regulation (EC) No 440/2008 of 30.05.2008, Regulation (EC) No 648/2004 of the European Parliament and of the Council of 31.03.2004, OECD Procedures No 301 and 209 and Standards No: PN-EN ISO 9408:2005, PN-EN ISO 7827:2001, PN-ISO 6060:2006 and ISO 8245:1999. Contact Person Data Renata Dudek, Chem. Eng. phone: + 48 22 568 22 94 phone/fax: + 48 22 568 20 50 e-mail: [email protected] Anna Bolińska, M.Sc. phone: + 48 22 568 26 14 phone/fax: + 48 22 568 20 50 e-mail: [email protected] Elżbieta Dłuska-Smolik, M.Sc. phone/fax: + 48 22 568 25 89 e-mail: [email protected] 338 the studies of surface structure and morphology of solid samples by the Scanning Electron Microscopy (SEM) method. Contact Person Data Assoc. Prof. Przemysław Łoś, D.Sc. phone: + 48 22 568 20 61 e-mail: [email protected] Aneta Łukomska, Ph.D. phone: + 48 22 568 23 19 fax: + 48 22 568 20 50 e-mail: [email protected] 339 2) Analysis of organic compounds, polymers and plastic materials identification of organic compounds, polymers, plastics products, paints, glues, binders, etc. by spectrophotometric and chromatographic methods; identification of the structure of non-volatile organic substances, e.g. synthetic and natural polymers, biochemical and geochemical products by the Py/GC/FTIR method; determination of average molecular mass and molecular mass distribution of polymers by Gel Permeation Chromatography (GPC) method; organic synthesis process control by FTIR and UV/VIS absorption spectrometry methods; FTIR studies of the hardening and cross-linking of polymer materials (functional and structural groups determination); composition analysis of organic compounds mixtures (identification of volatile components) by GC/MS and GC/AED methods; determination of trace amounts of toxic substances (monomers and solvents) in plastic products and in other materials by GC method using head-space technique, flame ionization detectors (GC/FID), atomic-emission detectors (GC/AED) and electron capture detectors (GC/ECD); determination of CFCs and halons in aerosols by GC method; determination of the C1-C3 alcohols in household chemistry products and pharmaceutical products by the GC/FID method; determination of organic acids, hydrocarbons, alcohols, esters and ketones in the gas samples by GC/FID method; studies on gases composition in closed cells of polyurethane foam by GC/FID and GC/TCD methods; studies on migration of trace contaminants from plastics by spectrophotometric and chromatographic methods; purity control of raw materials and technological processes control with GC, FTIR and AAS methods; determination of water content by the Karl Fischer method. 340 Contact Person Data Joanna Sołtysiak, Ph.D. phone: + 48 22 568 24 41, + 48 22 568 24 67 fax: + 48 22 568 20 48 e-mail: [email protected] Elżbieta Zimnicka, M.Sc. phone: + 48 22 568 23 72, + 48 22 568 23 73 phone/fax: + 48 22 568 20 51 e-mail: [email protected] Anna Bajszczak, M.Sc. phone: + 48 22 568 23 76 phone/fax: + 48 22 568 20 51 e-mail: [email protected] molecular modeling of structure and IR, Raman, VCD and NMR spectra of molecules of technological importance; interpretation of the experimental and theoretical vibrational spectra of organic molecules. Contact Person Data Prof. Jan Dobrowolski, D.Sc. phone: + 48 22 568 24 21 e-mail: [email protected] determination of formaldehyde contents in cosmetic products and their raw materials by HPLC method (according to the Decree of the Minister of Health as of 16.07.2004, Journal of Laws No 206, pos. 2106 as of 22.09.2004); determination of the composition of fatty acids in vegetable oils and animal fats by GC method (according to PN-EN ISO 5508:1996 and PN-EN ISO 5509:2001 standards); determination of nitrogen contents by Kjeldahl method. Contact Person Data Hanna Gwardiak, M.Sc., Chem. Eng. phone: + 48 22 568 23 54 e-mail: [email protected] 341 development of analytical methods and procedures involving high pressure liquid chromatography; determination of organic compound mixtures of especially complicated and difficult to analyze composition by HPLC method. Contact Person Data Jarosław Kamiński, M.Sc. phone: + 48 22 568 20 36 e-mail: [email protected] 3) Inorganic analysis determination of metal content in aqueous solutions, organic and inorganic samples and samples with mixed organic-inorganic matrix by Atomic Absorption Spectrometry (AAS) method, including: – determination of metals in water and wastewater; – purity control of raw materials; – determination of metal content in paints and dyes for the manufacture of paints, in varnishes, plastics and colourants of plastic materials; – chemical composition analysis of catalysts and aluminosilicates; – determination of metals in vegetable materials and oils; – determination of trace amounts of toxic metals (Ba, Cd, Cr, Pb, Sb, Hg, As) in the articles of plastics, cosmetics, detergents, etc.; – determination of trace metal content in the articles of paper; – studies on toxic metals migration from the colourants in plastic materials coming into contact with food and from utility products made of plastics (packaging, toys, stationery, etc.); determination of anions in inorganic samples, water and wastewater. 342 Contact Person Data Dorota Kolasa, M.Sc. phone: + 48 22 568 23 25 phone/fax: + 48 22 568 20 51 e-mail: [email protected] Beata Arndt, M.Sc. phone: + 48 22 568 23 26 phone/fax: + 48 22 568 20 51 e-mail: [email protected] 343 4) Real life scale and laboratory scale testing of non-food market products, including consumer panel tests laundry products: evaluation of primary and secondary detergency washing performance, incrustation, loss in tensile strength, fabric greying and yellowing, fabric shrinkage, dye transfer, fabric whiteness, fabric softening effect; liquid dishwashing agents: evaluation of washing performance by the IKW test, determination of fat emulsification power; toilet cleaning agents: evaluation of lime scale dissolution power; scouring milks and powders: evaluation of cleaning performance and surface damage; oxygen and chlorine bleaches: determination of stain removal power, fiber damage, color maintenance and fabric yellowing; fabric softeners: evaluation of softening effect, change in fabric whiteness and fabric rewetting power; window cleaners: evaluation of cleaning power, dry matter and alcohol content; shampoos: determination of foaming power by Ross Miles method; product quality evaluation tests including consumer tests of household chemistry consumer chemicals, cosmetics, personal hygiene products, candles, cemetery candles and other domestic use products in panel groups; evaluation of activated sludge respiration inhibition by raw materials and final products; selected analytical and physicochemical tests of raw materials and final products. Contact Person Data Paweł Kikolski, Ph.D. phone: + 48 22 568 22 92 fax: + 48 22 568 20 49 e-mail: [email protected] Renata Dudek, Chem. Eng. phone: + 48 22 568 22 94 phone/fax: + 48 22 568 20 50 e-mail: [email protected] Anna Bolińska, M.Sc. phone: + 48 22 568 26 14 phone/fax: + 48 22 568 20 50 e-mail: [email protected] 344 5) The structural studies of solid samples by the Scanning Electron Microscopy (SEM) method and qualitative analysis of their composition structural studies of solid samples in the magnification range of 5–300 000x; investigation of polymers, polymer composites and films made of PP, PE, PVC, PS, etc.; characterization of materials used in electrolytic and batteries cells; investigation of powders, sintered plastics and lacquer coatings; nanoparticles studies; studies of structural defects and impurities in materials and the environment; microanalysis of materials - elements from boron to uranium, detection level for light elements above 0.5 wt. %, for other above 0.3 wt. %. Contact Person Data Assoc. Prof. Przemysław Łoś, D.Sc. phone: + 48 22 568 20 61 e-mail: [email protected] Aneta Łukomska, Ph.D. phone: + 48 22 568 23 19 fax: + 48 22 568 20 50 e-mail: [email protected] 345 6) Physicochemical analysis Differential Scanning Calorimetry (DSC) and Thermogravimetric Analysis (TGA) studies on physical and chemical transformations (e.g. melting, crystallization, glass transition, curing, and phase transitions) in polymers and other substances; purity determination, e.g. for pharmaceutical raw materials; determination of the oxidation induction time (OIT) by DSC method; studies on degradation and decomposition of materials by TGA method; determination of thermal stability of polymers and other substances by TGA method; determination of the oxygen index, flash point, ignition and flammability testing of various polymers and plastics (according to UL 94 and HTL-15). Contact Person Data Joanna Sołtysiak, Ph.D. phone: + 48 22 568 24 41, + 48 22 568 24 67 fax: + 48 22 568 20 48 e-mail: [email protected] determination of tensile properties; determination of flexural properties; determination of compressive strength; determination of Izod and Charpy impact strength; determination of dynamic thermomechanical properties (DMTA) in the temperature range from -160 °C to 500 °C; determination of hardness (ball indentation method and Shore A and D scale); determination of tensile-impact strength; determination of Vicat softening temperature; determination of the melt mass-flow rate (MFR); determination of temperature of deflection under load; determination of kinematic viscosity. Contact Person Data Maciej Studziñski, M.Sc. phone: + 48 22 568 24 87 e-mail: [email protected] 346 determination of particle size in the range from 5 to 5000 nm by Photon Correlation Spectroscopy (PCS) method; determination of the zeta potential. Contact Person Data Assoc. Prof. Przemysław Łoś, D.Sc. phone: + 48 22 568 20 61 e-mail: [email protected] Aneta Łukomska, Ph.D. phone: + 48 22 568 23 19 fax: + 48 22 568 20 50 e-mail: [email protected] determination of dynamic viscosity of liquids, viscosity and shear stress vs. shear rate, determination of plasticizing stress. Adjustment of experimental data to the rheological model; determination of viscosity according to PN-EN ISO 3219 standard; determination of rheological properties of viscoelastic materials. Determination of changes in: loss modulus, storage modulus, complex modulus, complex viscosity, phase difference angle as a function of frequency; monitoring of resin curing processes, according to ASTM D 4473-01 standard; monitoring of gelling process during (polyurethane) foam formation. Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Jarosław Przybylski, M.Sc., Chem. Eng. phone: + 48 22 568 26 46 ; + 48 22 568 26 47 e-mail: [email protected] determination of relative hardness of coatings on a glass substrate or – in justified cases (e.g. following the method the coating is made) – on a metal substrate, according to PN79/C-81530 standard. monitoring of film formation from aqueous dispersions of polymers and copolymers, according to PN-90/C-89415 standard. 347 Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Izabela Ofat, M.Sc., Chem. Eng. phone: + 48 22 568 26 52 e-mail: [email protected] determination of apparent viscosity of liquid polymers, resin emulsions or polymer dispersions using Brookfield apparatus (according to PN-ISO 2555:1999 standard); determination of apparent viscosity of petrochemical products (according to PN-83/C04023 standard); determination of UV curability of coatings, adhesives and other materials (ICRI own procedure); accelerated ageing of polymers and coatings in cycles (1 cycle = UV irradiation + moisture condensation). Number of cycles and ageing conditions – as agreed with the client or according to the relevant standard; ageing of polymers, coatings and other materials in summer and winter conditions in climatic chambers providing fixed temperature and humidity or under variable conditions (in cycles); samples conditioning at fixed temperature and humidity, according to the relevant standard, before the actual examination described in the standard is performed; determination of the percentage share of open and closed pores volume in rigid porous materials (according to PN-ISO 4590:1994 standard, clause 9). Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Jarosław Przybylski, M.Sc., Chem. Eng. phone: + 48 22 568 26 46, + 48 22 568 26 47 e-mail: [email protected] Krystyna Sylwestrzak, M.Sc., Chem. Eng. phone: + 48 22 568 26 46 e-mail: [email protected] 348 determination of static and dynamic contact angles, computerized calculation of surface free energy of solids based on contact angle data, determination of surface and interfacial tension with the hanging drop method. Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Jarosław Przybylski, M.Sc., Chem. Eng. phone: + 48 22 568 26 46, + 48 22 568 26 47 e-mail: [email protected] Izabela Ofat, M.Sc., Chem. Eng. phone: + 48 22 568 26 52 e-mail: [email protected] determination of coating gloss at the angle 20, 60 and 85 (according to PN-EN ISO 2813 standard) along with the statistics and transfer of results to a computer using PC software; nondestructive determination of thickness of coatings placed on various substrates, such as ceramics, glass or plastics (according to PN-EN ISO 2808 standard). Thickness range 13–1000 m; determination of elasticity of coatings placed on a metal substrate according to PN-EN ISO 1519 standard; determination of coating resistance to scratching (scratching of a sample with an appropriate stylus tip under a defined force 0–20 N); cupping test performed on coatings on a metal substrate according to PN-EN ISO 1520 standard; determination of abrasion resistance of coatings and polymeric materials with the friction wheels (Taber) method; determination of coating impact resistance with the falling weight method according to EN ISO 6272 standard; determination of coating-substrate adhesion with the cross-cut method according to ISO 2409 standard; determination of leveling characteristics of paints and coatings according to ASTM D 2801 standard; 349 determination of viscosity of liquid materials according to PN-81/C-81508 standard (Ford viscosity cups); determination of surface drying time and degree of dryness according to PN-79/C81519 standard; determination of coatings elasticity by bending method according to PN-76/C-81528 standard; determination of coating-substrate adhesion according to PN-80/C-81531 standard; determination of coatings resistance to water according to PN-76/C-81521 standard; determination of mechanical stability of aqueous dispersions and suspensions in a centrifuge in the temperature range from -10 °C to 40 °C (at up to 18.000 rpm); determination of sedimentation of aqueous dispersions according to BN-74/6351-01 standard. Contact Person Data Assoc. Prof. Janusz Kozakiewicz, Ph.D., Chem. Eng. phone: + 48 22 568 23 78 e-mail: [email protected] Jarosław Przybylski, M.Sc., Chem. Eng. phone: + 48 22 568 26 46, + 48 22 568 26 47 e-mail: [email protected] Izabela Ofat, M.Sc., Chem. Eng. phone: + 48 22 568 26 52 e-mail: [email protected] Krystyna Sylwestrzak, M.Sc., Chem. Eng. phone: + 48 22 568 26 46 e-mail: [email protected] 350 PROCESS SAFETY 1) Process safety We offer services concerning: comprehensive risk assessment concerning dangerous chemical substances and processes involving these substances; The Regulation of Minister of Economy from 8 July 2010 concerning minimal requirements of Heath and safety due to possibility of explosive atmosphere in the workplace (Dz. U. No 138, item 931 from 30 July 2010) needs, that employee is obliged to assess the risk of presence of explosive atmosphere in the workplace, examination of materials and technological processes in order to establish how much they are harmful to the human health; Industrial Chemistry Research Institute is on the list of the Regulation of Minister of Heath and Social Care from 12 July 1996 concerning bodies which are able to examine materials and technological processes, development of safety reports and emergency plans, according to the „Law on environment protection”; „Law on environment protection” (unified text Dz. U. No 25, item 150 from 2008) states, that operator of upper tier establishment is oblige to prepare safety report and emergency plan, development of environment influence analyses for chemical industry plants, in relation to their build-up or privatization; „Law on environment protection” (unified text Dz. U. No 25, item 150 from 2008) states, that in the vicinity of towns and urban regions the build-up of establishments posing the risk of major accident is allowed under the condition, that it will diminish the risk. Contact Person Data Andrzej Milczarek, M.Sc. phone: + 48 22 568 23 33 e-mail: [email protected] 351 2) Preparation and verification of Material Safety Data Sheets (MSDS) We offer our capacity in preparation of MSDS Almost every company involved in production, import or placing on the market will sooner or later come across substances or mixtures requiring preparation of Material Safety Data Sheets. If some hazardous properties of a substance to be placed on the market come into sight, e.g.: explosive, oxidative, extremely flammable, highly flammable, flammable; toxic or very toxic, harmful, corrosive, irritant, sensitizing; carcinogenic, mutagenic, toxic for reproduction (CMR); dangerous to environment; fulfilling PBT (persistent, bioaccumulative, toxic) criteria substance is not classified as dangerous but: contains at least one substance depicted in the relevant regulations as causing harm to human health or environment, present in concentration of at least 0.1 wt. % in case of non-gaseous substances or 0.2 vol. % for gases; or contains above the same concentration of CMR (cat. 1 or 2); or for which workplace exposure concentration limits were established, or a Material Safety Data Sheet in an official language of a country where product is placed on a market is required. Preparation of that data sheet is an obligation of a manufacturer, formulator or importer (from outside EU). Material Safety Data Sheet is dedicated for professional users and enables them to adopt all occupational safety, health and environmental protection measures. It also provides consumer (through proper labeling) with a complete information about potential risks which may arise from using a particular substance or mixture. A format of Safety Data Sheet which forms a set of information about dangerous properties of substances or mixtures and rules and recommendations for their safe use was set out in a EU Commission Regulation 453/2010 of 20 May 2010. It is possible to prepare a Safety Data Sheet individually, on a basis of relevant knowledge (in particular while being a manufacturer) or, on a basis of one being delivered by a supplier (in case of being an importer or trader). Very often however a SDS prepared by a supplier doesn’t fulfill the requirements of polish law. Direct translation of an original text results in missing requirements of polish law and lapse in verification of e.g. classification provided by manufacturer. 352 If you would like to be sure that Safety Data Sheet which is in use in your company and which you present to your customers fulfills the requirements of UE law regarding chemicals and a label was designed properly, and in the same time you are of the opinion that our ancestors were right inventing societal sharing of duties, you are invited to use our assistance. Contact Person Data Marcela Palczewska-Tulińska, M.Sc. phone: + 48 22 568 20 39, + 48 22 568 20 06 e-mail: [email protected] 353 EXPERIMENTAL PRODUCTION 1) Experimental production Services concerning: mixing of loose materials An agitator of „Nauta” type, 1 m3 in volume, ability to mix loose materials and packing in 50 kg sacks grinding Pebble mills (200, 100 and 50 l in volume) - ability to grind and sift ground materials conducting of chemical reactions Reaction apparatus sets including chemical reactors (1000, 500, 200, 100 and 50 l in volume), fit with slow-rotating stirrers, with cooling capability, deaerated through reflux condensers distillation Simple distillation apparatus sets including a distillation tub (500 and 200 l in volume), fit with a heat exchanger, a condenser and a receptacle rectification Apparatus sets including a rectification tub 1000 l in volume, a distillation column with filling, a phlegm separation funnel, a heat exchanger, a condenser and a receptacles conducting of unique processes on the half-technical scale Contact Person Data Marek Leszczyński, M.Sc., Chem. Eng. phone: + 48 22 568 24 86, + 48 22 568 23 48 fax: + 48 22 568 24 99 e-mail: [email protected] 2) Products offered by the Industrial Chemistry Research Institute Konsil Z Konsil Z Super Two-component silicone waterproofing agents for external use on stone (sandstone, marble, granite and terrazzo) and for maintenance of masonry, walls, sculptures, monuments, tombs, bricks and other porous construction materials. Konsil Z Super also features anti-fungus and anti-lichen properties. Konsil Z and Konsil Z Super packaging available: 1 l, 5 l, 10 l, 30 l and 60 l. 354 Acid-based cleaning agent Agent for chemical cleaning of building facades, stone surfaces (sandstone, granite, terrazzo and clinker bricks) and skylights, industrial facilities, glasshouse walls. Packaging available: 1 l and 5 l. Leposil K1 Two-component silicone binding agent used with putty and mortar to fill in creases and dents in sandstone, limestone, marble, brick and gypsum. Packaging available: 0,5 l and 1 l. West marine glue Two-component epoxy glue, used for cold gluing of wood, especially in boat-building. Packaging available: 5 kg glue + 1 kg hardener. Kolakryl Acrylic glue used in manufacturing of various adhesive materials such as tape, labels and wallpaper. Sold by the kilogram. Motofix – liquid seal Liquid polyurethane sealant used for sealing flat and threaded metal surfaces. Packaging available: 4 kg. Pollena Jod K Iodophor cleaning agent (killing bacteria, mold and viruses), used for sanitizing facilities, equipment and vehicles applied in transportation of farm animals. Packaging available: 1 l (1.25 kg), 5 l (6.25 kg), 10 l (12.5 kg) and 30 l (37.5 kg). 355 Peel-off lacquer Lacquer used for insulating parts during plating (electro-galvanizing) of various products e.g. knife edges during silver-plating. It provides protection of transported metal goods from the elements. Packaging available: 3 kg. Contact Person Data Marek Leszczyński, M.Sc., Chem. Eng. phone: + 48 22 568 24 86, + 48 22 568 23 48 fax: + 48 22 568 24 99 e-mail: [email protected] 356 INSTITUTE FOR CHEMICAL PROCESSING OF COAL (Instytut Chemicznej Przeróbki Węgla) Organisation Contact Data 1 Zamkowa st., 41-803 Zabrze, Poland phone: +48 32 271 00 41 fax: + 48 32 271 08 09 e-mail: [email protected] http://www.ichpw.zabrze.pl/?setlang=en Institute for Chemical Processing of Coal (IChPW) was established in 1955 as an R&D centre of coal processing industry. The scope of the Institute's activity includes the following areas: biomass processing technologies (pyrolysis, gasification and combustion), thermal waste processing, dispersed heating systems, fossil, renewable & alternative fuels, coal & biomass fired power plants, coke making & carbochemistry, high temperature refractories for industry oven. The Institute employs 240 persons including 13 professors and 34 doctors. Our works are addressed to economy, ICHPW is also an active partner in large strategic projects. The Institute has a management system according to ISO 9001. Our testing laboratories operate in accordance with the ISO/IEC 17025 system. Proficiency Testing Centre of the Institute, assures that it appointed, implemented and maintains a management system corresponding with the scope of activity and including the type and scope of the skill researches, which is offered. The system is compliant with the requirements of the accreditations set in the ISO/IEC 17043 norm and in the PCA DA PT-01 document. Partners of the Institute comprise largest domestic universities and many foreign institutes, including those from the USA, P.R. of China, Japan and the EU. The main commercial partners of the Institute are: coal carbonization plants (coking and steel industry), power and CHP plants, industrial and municipal heating stations. 357 Examples of research themes and activities addressed by the Institute include: gasification of coal in fixed and circulating fluid bed, development and deployment of co-firing technology, procedures and certification in Poland (over 20 power and CHP plants), industrial application of a biomass gasification unit 5 MWth, development and dissemination of analytical standards for biomass, development of high efficiency dedusting system for medium size boilers (20 - 200 MWth), establishment of industrial supervised laboratories for power plants LABIOMEN, development and licensing for manufacturing high efficiency small capacity boilers in the range 25 - 500 kWth. coal drying in an impact dryer of 100 kg/h scale, carbon dioxide removal in an absorption reactor in the scale 20 - 100 m3/h gas input containing CO2 (new project), Mathematical modeling and process simulations. PROJECTS / SPECIAL AREA OF EXPERTISE Biomass and coal co-firing systems for municipal purposes, certification of solid fuels fired power boilers of small and medium power – 1100 certificates Biomass co-firing technologies – over 20 cases of “green certificates” implementation for the power industry Coal pyrolysis and gasification technologies in shaft, rotating and fluidised bed reactors (several plants) Valorization of waste organic products Industrial gases conversion technologies Establishment and management of National Network of Supervised Laboratories “LABIOMEN” – 44 licensed industrial research laboratories Accreditation of a group of testing laboratories at the Polish Centre for Testing and Certification – 114 accredited testing methods. Smokeless fuel and granulated fuels production technology based on coals and biomass Fluidized bed ash management technologies Coke-oven batteries construction, reconstruction and start-up technologies (21 batteries) Char production and coal powder for injection to a blast furnace preparation technologies (2 steelworks) 358 1) Biomass Gasification – Electricity and Heat Generation in Dispersed Sources The conversion of biomass chemical energy into the energy of inflammable gas in the process of solid fuels gasification substantially increases the scope of solutions applied for energy biomass use. The application of process gas in gas CHP cogeneration systems, which cogenerate electricity and heat and/or cold seems especially attractive. The IChPW has a technology of electricity and heat generation from biomass. The plant comprises: an innovative gasifier with a solid bed (GazEla), a system for dry purification of gas and an electricity generator. The Institute has implemented a bench scale plant of 60 kWt power and a demonstration scale plant of 1.5 MWt power. The gasifier with a solid bed features a novel design enabling collection of gas directly from the gasification zone, a system for dry purification of gas and a dual-fuel piston engine. The plant enables generation of electricity and heat. Such systems may be used in all places, where there is a demand for electricity and heat and also where local biomass sources exist. Potential buyers of the technology include timber processing plants (sawmills, briquettes and pellets manufacturers) and farms. The use of biomass – production waste – seems especially attractive, as it may be effectively used as a fuel for cogeneration plants. Contact Person Data J. Zuwała e-mail: [email protected] 359 2) Removal mercury from coal using low-temperature pyrolysis The process is based on thermal treatment of coal (‘low-temperature pyrolysis’) before combustion/gasification. Results of research (carried out at the Institute for Chemical Processing of Coal) has shown promise for the substantial reduction of mercury in fuel using the process of low-temperature pyrolysis (60 and 90% reduction for hard and brown coal respectively). The process allows for high efficiencies in Hg separation without exerting a significant influence on the properties of cleaned coal (slight decrease in volatiles content and in chemical enthalpy of the fuel and an increase in calorific value). Plant for coal cleaning consists of drying and pyrolysis zones. Heat carrier for the process is a flue from additional coal combustion. Coal fed into the system is divided into two streams. One stream is directed to a combustion chamber where the flue is generated, as the heat carrier in the process. The second stream of fuel (mercury removal) is directed to a fluidised bed dryer. After passing through the dedusting system (e.g. bag filter for separation of fine fuel particles carried from the drying unit), the flue gas from the drying system is partly recirculated to the dryer and partly released to the atmosphere through a heat exchanger, where the water removed from the fuel is condensed and the heat recovered. The dried fuel is directed to a pyrolysis reactor (indirect heated rotary reactor). From the pyrolysis reactor, mercury is swept with the pyrolysis gas and with an inert-carrier gas additionally fed to the system (the carrier gas is nitrogen in the concept considered here). The carrier gas with a high concentration of mercury is directed to a mercury separator, where Hg is extracted from the gas e.g., by adsorption in a fixed bed reactor. The flue from the pyrolysis reactor system is divided into two streams: one is recirculated to the system and the other cooled in a cooler, where the moisture contained in it is condensed and the heat recovered. The cleaned coal is directed to a storage yard or directly to combustion/gasification (the most favourable option because of the use of the physical enthalpy of the hot fuel). Technology is under development, research work in large laboratory/bench scale and detailed technical-economic analyses are in progress. Technology is dedicated to power and coal mining industries. Contact Person Data T. Chmielniak e-mail: [email protected] 360 3) KARBOTERM - waste plastics utilisation in cokemaking industry The problem of utilisation of non-biodegradable waste plastics is the one of the nonfully solved environmental problems. In Institute for Chemical Processing of Coal it was elaborated the technology of waste plastics processing making possible to use them in coke production. The essence of the technology is the thermal preparation of broken-up waste plastics in the presence of bitumens (hydrocarbons mixture). As the result of temperature (350 0C) a chain decay of polymer is observed. If the process is carried out in the presence of bitumens (waste plastics/bitum weight ratio = 4/1) the yield of liquid products from polymer decay is minimised. It is the two-stage process where we can control the hydrogen chloride release and therefore minimise the chlorine content in the product. As the result of waste plastics thermolysis the hot liquid product is obtained which is next directly cooled by contacting with a hard coal of natural moisture content. The final product is called the karboterm - it is the substitute of coal. A combustible process gas as well as hydrochloric acid are also released in the process. The broken-up waste plastics from selective waste collection and municipal waste sorting-lines are a feedstock. In the technology also bitumens are applied (e.g. coal-tar pitch, asphalt, anthracene oil) received on a commercial scale as by-products in Polish coking and petroleum industries. The karboterm is a solid fuel of full value recommended in cokemaking industry as a component for coal blend. The karboterm is a solid material of physicochemical properties nearing to hard coal. The amount of waste plastics in karboterm is about 20 %. The karboterm can be also applied in heat-generating and power industries. The ecologically clean and market attractive Karboterm technology can be applied e.g. in coking plants. Contact Person Data A. Sobolewski e-mail: [email protected] 361 4) System for the automatic control of the coke oven battery’s firing „System for the automatic control of the coke oven battery’s firing” has been developed in the Institute for Chemical Processing of Coal, based on the analysis of collected technological data (calorific value of the fuel gas, coal charge humidity, implemented schedule of coal chamber charging, crude coke oven gas temperature, temperature in the control heating flues, temperature alongside the pushed coke). The system selects valid temperatures in the heating flues and adjusts gas pressure in the side pipelines and duration of firing break. The amount of air flowing through the battery’s heating system is reduced during the firing break thanks to some modifications in the battery’s reversing system. As our research and observation have proved, this method of adjusting the battery’s firing system has, most of all, excluded the need for burdensome adjustment of the battery’s hydraulic parameters with every change in production capacity level, or even coal charge parameters. In a natural way, temperature in the heating flues has been lowered in compliance with the changes in production capacity, and temperature distribution on the particular walls remained practically unchanged, with no need for adjustment elements exchange. Even though, the coke oven battery is still a device with limited possibilities of production capacity adjustment (because of its construction material, namely silica), implementation of the automatic firing control system has significantly improved this capacity and, most of all, has limited the influence of manual analysis. Our experience has also shown that the developed method enabled a considerable lowering of heat usage for coking process (5-10%) compared with the previous methods of controlling the firing conditions. Our system has been implemented and tested in several operating coke oven batteries in Poland. Contact Person Data L. Kosyrczyk e-mail: [email protected] 362 INSTITUTE FOR ENGINEERING OF POLYMER MATERIALS AND DYES (Instytut Inżynierii Materiałów Polimerowych i Barwników) Institute for Engineering of Polymer Materials and Dyes consists of: Institute for Engineering of Polymer Materials and Dyes in Toruń Branch House for Elastomers and Rubber Processing in Piastów Branch House for Paints and Plastics in Gliwice INSTITUTE FOR ENGINEERING OF POLYMER MATERIALS ABD DYES IN TORUŃ Institute for Engineering of Polymer Materials and Dyes in Toruń 55, Marii Skłodowskiej-Curie st, 87 – 100 Toruń, Poland Phone / fax: +48 56 650-03-33 secretary: + 48 56 650-00-44 e-mail: [email protected] http://www.impib.pl/ Technological Laboratory Laboratory performs assessment of physicomechanical properties of polymers and plastic products. Post of resistance tests comprises of tensile testing machine (TIRA GmbH) with computer controlled that makes possible performing measurements with simultaneous plotting of data: mechanical properties at static tensile, compression and bending according to the standards PN-EN ISO 521 1-3, PN-EN ISO 178, tear resistance by a trouser tear Elmendorf tear strength according to the standard PNEN ISO 6383-1-2, resistance to tear off of layers according to the standard PN-88/C-89099, index of the bond strength according to the standard PN-C-89258-1 p3.18, coefficient of static and dynamic friction according to the standard PN-EN ISO 8295, interadhesion of film layers according to the standard PN-71/C 89095. 363 Capillary plastometer (Dynisco) offers assessments of indexes of mass (MFR) and volumetric (MVR) flow of polymers according to the standard PN-EN ISO 1133. Moreover we asses: impact resistance (Charpy, Izod and impact tensile method) according to the standard PN-EN ISO 179-1, impact strength assessed with falling dart method according to the standard PN-EN ISO 7065-1, change of linear dimension during heat treatment according to the standard PN-EN ISO 11501, gloss, light transmittance, haze according to the standard PN-EN ISO 13468-1, ASTM D1003-11, density with gas pycnometer according to the standard PN-EN ISO 1183-3, microscopic assessment of multilayered films, time of thermal stability of PVC blends, watervapour permeability (Dansensor apparatus) according to the standard PN-EN ISO 15106-1, gas permeability (e.g. oxygen, helium, nitrogen, argon) according to the standard PNEN ISO 2556. Concurrent twin screw extruder BTSK 20/40D is available for technological tests of manufacturing of composites of polymer plastics, by addition of other polymers, powder extenders and modifying agents. These composites are processed on injection moulding machine Battenfeld Plus 35/75 into profiles – bars, dumbbells, plates that are subjected to testing. Tests and trials of extrusion of films made of various polymers and mixtures in each layer are preformed on the assembly line type 3xW25 for manufacturing of 3-layer films. As our research activity covers also activation of films and sheets by corona charging, Technological Laboratory offers measurements of their free surface energy with Kruss goniometer and wettability with model liquids. We sell testers – ink or stick - for evaluation of level of surface activation, with measuring range from 30 to 73 mN/m. Section of Technological Testing We develop new technologies for manufacturing of utility products made of polymer plastics. We produce ready profiles, containers and shapes in low-tonnage scale as well as granulates of 364 composites and nanocomposites based on polymers. In addition our staff offers its service in issues concerning choice of right raw materials for high-quality products. Our Section of Technological Testing is equipped with: assembly line for extrusion of profiles (Barmag extruder L/D=45), assembly line for co-extrusion of profiles coated with monolayer (screw extruder L/D=32), assembly line for manufacture of polymer composites as granulate with concurrent twin screw extruder 2T40W with gravimetric dosage system, assembly line for manufacture of flat film of width up to 500 mm, stand for testing extrusion processes of polymer profiles with screw extruder Barmag L/D=45, assembly line for blowing extrusion for manufacture of containers (1 – 10 l), milling assembly for polymer waste – mills UR 250 and UR 16. Equipment and machinery for plastics processing offered by IMPiB Technological assemblies for manufacture of PE, PP, PS, PET, PVC films Technological assemblies are designed for production of single and multilayered sleeve films. Design solutions of particular technological units (extruder, extrusion head, fused plastics filter, receiving or winder set etc.) are adjusted to properties and field of use of film as well as to the needs of a customer. Technological assemblies for production of PE, PP, PVC pipes and profiles We offer technological assemblies for production of pipes with diameters up to 400 mm and of profiles (sidings, window sills, profiles for construction industry, sheets and traceways for electroinsulating wires). Technological assemblies for PE, PP and PS waste granulation Our technological assemblies are designed to reprocess (regranulate) waste – in form of agglomerates or a milling. Reprocessing may be done either in cold or in hot regime, according to the demand of a customer. 365 Single and twin screw extruders single screw extruders for PE, PA, PS, PP, PET and PVC processing, concurrent cylindrical twin screw extruders for processing of PE, PP, PA, PS, ABS also with mineral fillers, backward cylindrical twin screw extruders for processing of PVC dry-blends. Plasticizing units (cylinders, screws) of extruders are optimized for a particular uses and quality demands set for the product. Concurrent screws, because of their purpose, have segmented structure of a cylinder and a screw. Additional fittings of extruders e.g. controlling system, graphical visualisation and saving processing data are also possible. Equipment UFP series for forming containers This equipment is designed for blowing extrusion of PE, PP and PVC containers of volumes up to 5 dm3. Additional fitting is possible e.g.: a set for regulation of a wall thickness of an extruded “hose” or a set conveying granulate to the extruder. Intensive mixers MJI and MDI type one-stage MJI (with one chamber) of mixing capacity up to 1200 kg/h, designed for mixing powdered materials. Blends are used in food, pharmaceutical and other industries. two-stage MDI (with two chambers) of mixing capacity up to 1200 kg/h, designed for mixing powdered PVC with solid additives. Blends are used for profiles or pipes production Equipment UR type for grinding PE, PP, PVC waste Mills are used to grind various types of wastes (pipes, profiles, containers, foils, packs) made of all range of thermoplastic polymers. Capacity of mills reaches 1200 kg/h. This equipment may have additional features e.g conveyor sets for transportation a waste to the mill’ funnel and sets collecting grinded waste (e.g. pneumatic sets with dust separators) and also soundproof casing. 366 Equipment A and AZ type for thickening of PE and PA films waste A and AZ type equipment is designed to thicken clean and contaminated film’ waste. It has low energy and water consumption, an agglomerates produced with A and AZ type equipment have bulk density of 0.4 kg/dm3. Equipment for activation of PE, PP, PA, PET, PVC films Designed to run modification process of an upper layer (activation) of a film (up to 2500mm width), and pipes activators (up to the diameter of 1200 mm). Training Activity of Institute for Engineering of Polymer Materials and Dyes Institute organizes trainings and courses for entrepreneurs and personnel working in plastics processing industry. The scope of those trainings and courses is determined each time separately to meet needs of our customers. Lectures are given by scientific staff of our Institute, who are experts in plastics processing. Training and courses: Basics of plastics processing plastics, properties and use, manufacturing of plastics products by extrusion. Construction of equipment and tools for extrusion of plastics screw extruders, one and twin-screw plasticizing systems, power transmission systems of screws, cylinders heating-cooling systems, control systems, assemblies for extrusion, control of extrusion, activation of films. Practical problems of PVC processing manufacture, types, properties of PVC, PVC v. recipe components, 367 gelation of PVC, extrusion technologies, co-extrusion, plasticizing systems of extruders, construction demands and heads for PVC. Extrusion Processing of Packaging Films theoretical basis of film extrusion, technologies and equipment for film extrusion (blowing extrusion and flat films), control and stabilization of extrusion, optimization of the structure of multilayered films, films defects and methods of avoiding them, laboratory – methods of evaluation of properties, recycling of film waste. Intellectual and industrial property patents for inventions, copyrights and exclusive rights, protection of trademarks and utility patterns, rights resulting from registration of patterns, topography of integrated circuits, geographical sign. 368 Institute runs secretariats of following Standardization Committees: KT 140 for Pipes, Profiles and Fittings made of Plastics System standards relating to all aspects of areas of use of plastic pipes: drainage systems, sewage systems, water supply systems, heating systems, gas and industry systems as well as for test methods. KT 168 for Plastics Products Aspects related to plastics processing, plastics products, semi products including properties and test methods of thereof, porous and strengthened materials and self-adhesive tapes. KT 175 for Paints and Varnishes Paints and varnishes and products of a similar type and raw materials for paints and varnishes (excluding pigments and extenders) – terminology, classification, demands, test methods including test methods for various usage areas; preparation of steel surfaces prior to paint application and paint-like products. KT 240 for Machinery and equipment for Processing Plastics and Rubber Blends Machinery and equipment for processing plastics and rubber blends including: extruders and additional machinery, special purpose press, injection moulding machinery, blenders, machinery for waste processing and instrumentation and technologies related to those machines/equipment. PRIK Our institute is a proud member of a The Polish Association of Plastic Pipes and Fittings Producers (PRIK). PRIK activity focuses on integration of the branch of pipe and fittings producers. PRIK acts as representative body of the branch in contacts with administrative and legislative bodies, as well as other national and international organizations in issues concerning legislation and standardization, directives and recommendations on plastics processing, usage and recycling or pipes and pipe-like plastics profiles. 369 BRANCH HOUSE FOR ELASTOMERS FOR AND RUBBER PROCESSING IN PIASTOW Branch House for Elastomers and Rubber Processing in Piastów 30, Harcerska st, 05 – 820, Piastów, Poland phone: +48 22 723-60-25 to 29; +48 (22) 723-60-20 fax: + 48 22 723-71-96 e-mail: [email protected] www.piastow.impib.pl Research and Development Activity Our mission is R&D tasks activity leading to new technical and technological solutions, supporting development of the rubber industry and increasing its level of innovation and competitiveness, to keep up with or gain over foreign companies. Main activities: Our activity is focused on R&D in chemistry and technology of elastomers, in particular: elaboration and implementation of rubber processing, designing novel rubber products, tests concerning strengthening of, adhesion, crosslinking and miscibility of elastomers and other materials used by the industry, elaboration of manufacturing methods of elastomeric nanocomposites, structure and properties testing, elaboration of preparation methods of rubber blends for powder latexes and powdered pre-mixtures of latexes and extenders in continuous blending process, utilization of materials from renewable sources as components of rubber blends modification and synthesis of elastomers, improvement of test methods of elastomeric systems, exploitation of specialty elastomers in military and aviation industries, compatibilization of latex blends, elimination of the negative influence of the rubber industry on the environment, recycling issues and devulcanization of rubber. 370 Our partners represent all sorts of industries: car producers, aviation industry, military industry, agriculture, construction industry, mining, food processing industry, medical equipment producers. 371 Dissemination of Knowledge Informative activity of the Elastomers and Rubber Technology Division includes gathering, elaboration, processing and dissemination of information about chemistry, physics and processing of elastomers. Division possesses: collection of specialist books, wide range of specialist magazines, both polish and foreign ones. We also edit magazine “Elastomery”, published bimonthly and focused on issues important for rubber industry. Both scientific and technical articles describing results of R&D investigations of polish and foreign research institutes and industry research teams are published in “Elastomery” magazine. “Elastomery” is listed in the Polish Scientific Committee register of leading scientific-technical magazines. Articles are published either in English or in Polish languages, abstracts are always bilingual. All articles submitted to the editor are reviewed. “Elastomery” are reported in Chemical Abstracts and Rapra Abstracts Apart from publishing activity we also: prepare specification on given subject, prepare lectures and literature surveys, organize specialist courses and trainings concerning rubber industry for the process engineers, personnel of the factories test laboratories and for the technical surveillance personnel. PCA Accredited Laboratory Labgum Accreditation Certificate No AB 147 Chemical Properties Testing Unit tests of raw materials for conformity with specifications, tests of rubber products that come in contact with foodstuffs, analyses of the composition of blends and vulcanizates for the estimation of their use in recipes, for monitoring the composition, to solve exploitation and technological problems, estimation of the presence of trace amounts of N-nitrosamines, identification of blooms on the surface of a rubber, tests of thermal properties of materials. 372 Physical Properties Assesment Tests of: processing properties of latexes and blends, durability of rubber, basic physical properties of rubber, hardness, density, elasticity, wear resistance, resistance to liquids (fuel, oils), resistance to elevated temperatures (accelerated ageing) and to ozone, resistance to the influence of low temperature, relaxation and attenuation. 373 BRANCH HOUSE FOR PAINTS AND PLASTICS IN GLIWICE Branch House for Paints and Plastics in Gliwice 50 A, Chorzowska st, 44 – 100, Gliwice, Poland phone: +48 32 231 90 41 fax: + 48 32 231 26 74 e-mail: [email protected] www.gliwice.impib.pl Paint and Varnish Laboratory Activity of Paint and Varnish Laboratory focuses on technical consulting, assessment of properties of paints, varnishes, resins and binders as well as the development of technologies for paint industry. Our offer is addressed to producers and users of paints and varnishes. We develop: new technologies of manufacturing of resins and binders for technical purposes, new manufacturing technologies of coatings for substrates (metal, wood, plastics, mineral) for specific purposes, technologies of removal of coatings. We test: properties of new materials for synthesis of binders and coating materials, properties of pigments, extenders and additives, properties of liquid paints and dry coatings, resistance of coatings to weathering (in natural and accelerated conditions), recycling. Implementation of: ecologically friendly technologies as alternatives to existing ones, new raw materials for production of coatings. Expertise of: state of coatings applied to various substrates. 374 Production of: coatings materials for special purposes, developed and prepared according to customer demands. Technical consulting. Plastics Laboratory The activity of Plastics Laboratory focuses on: development and implementation of masterbaches with PE, PP, PS and other carriers, development of manufacturing technology of thermoset and thermoplastics, physical and chemical modification of plastics, selection of raw materials for manufacturing of defined product, expertise of raw materials and product quality, solving of problems occurring during plastics processing , physicochemical tests of plastics and products performed according to Polish (PN), European (EN) and other standards (ISO, DIN, ASTM), market overview, assessment of demands concerning quality of plastic products, expertise of innovation potential of technological processes of polymer production, development of fire retandancy of thermoset resins and polyolefines by using halogenfree additives, development of oxo-degradation technology, processing of biodegradable plastics and manufacturing of packaging made of them (PLA, photo-oxo-degradable plastics), testing of stabilisation and degradation processes polymers, mainly polyolefines, technology of material and plastics recycling (including reused plastics mixtures and wastes, development of technology production of single and multilayered sleeve films (blown and cast). Laboratory equipment for plastics processing: rolling mill, 375 press, Brabender plastometer, Brabender absorption meter, hot-cold fluid mixer. Equipment for determination of flammability of polymer materials cone calorimeter, stand for testing of oxygen index, stand for determination of flammability classification. Equipment for determination of physicochemical properties of polymer materials: Instron testing machine, absorption meter, plastometer. Bureau for Standardization and Certification of Products (BNC) Certification of products is performed according to the procedure comprising of: tests and evaluation of project quality (type), evaluation of suppliers quality system, supervision by periodical controls of suppliers quality system as well as testing and evaluation of the quality of the control samples taken from the suppliers and/or purchased on the market. BNC is accredited by Polish Centre for Accreditation (PCA) and the scope of accreditation covers: paints and varnishes, plastics products, including pipeline systems, diluents, packaging. 376 The scope of accreditation is available on PCA and Institute’s web sites – www.pca.gov.pl and www.impib.pl respectively. Certification Unit is authorised to certify products for conformity with international, European and national standards, instructions, technical criteria and technical approvals. Certification Unit is also authorised to certify products for conformity eco-sign “E”. Eco-sign “E” is reserved by Institute. Conformity certificates are valid for three years. All tests covered by the scope of accreditation are performed by Accredited Laboratory (accreditation No AB 163) that operates within the organizational structure of IMPiB - Paints and Plastics Division. The tests may be also performed by other national laboratory possessing PCA accreditation. Bureau for Standardization and Certification of products is responsible for ensuring confidentiality and impartiality of its staff, contractors, members of the Technical Committees and Certification Unit Council regarding all information gained during the certification procedures and supervision, except of the law enacts. Analytical Laboratory Analytical Laboratory is accredited by Polish Centre for Accreditation (PCA) No AB 163 and performs: a) tests performed by accredited methods: properties of liquid paints, physicomechanical properties of coatings, evaluation of VOC levels in paints by means of Gas Chromatography, accelerated weathering tests of coatings and plastics (using light emitted either by xenon or fluorescent lamps), neutral salt tests to estimate corrosion resistance of coatings and zinc films, tests of child-resistance packaging, endurance tests of plastics products and pipes, fixtures and profiles made of plastics, tests of thermal properties of polymers by means of DSC and TGA, estimation of softening point by Vicat apparatus, 377 estimation of the amount of vinyl chloride monomers by GC, estimation of concentration of Pb, At, Cd, Cr, As and Ba by means of AAS. b) tests performed by non-accredited methods test of global migration into model liquids products made of plastics, identification of organic and inorganic compounds by means of FTIR and spectrophotometry, identification of composition of solvents – GC analysis, tests of viscoelastic polymers with DMA. Disssemination of Knowledge Paint and Plastics Division edits two bimonthly magazines in the field of science and technology devoted to paint and plastics entitled “Paints and Varnishes” (in Polish: Farby i Lakiery) and “Plastics Processing” (in Polish: Przetwórstwo Tworzyw”). Both magazines are listed in Polish Scientific Committee register of leading scientific-technical magazines. Articles are published in Polish; abstracts are published in Polish and English. All articles submitted to the editor are reviewed. Paint and Plastics Division is a regular organiser of international conferences devoted to paints and plastics entitled “Advances in Coatings Technology “ and “Advances in Plastics Technology”. Each conference is organised every second year. Representatives of leading European and world enterprises present in English their latest achievements in the field of paints and plastics. 378 COOPERATION OFFER/DESCRIPTION OF TECHNOLOGIES 1) Removable, sustainable composites on the base of polymeric materials reinforced by micro- and nanofibres. The usage of composites in modern industry, and other areas of economy, is growing especially in building and transportation (aircraft, train, car industry). For this reason, also supported by the growing environmental awareness, it is very important, that future composites have to be generally produced from renewable and sustainable row materials. Recent reports about negative role of carbon nanotubes on human health have brought more attention to lignocellulisic micro and nano-fibres as reinforcing material to polymers, which can be produced from renewable resources. Polymers from renewable resources such as: polyhydroxy alkanate and succinic acid can be converted to many commercial polymers and fibres. New and recently developed techniques for extraction of micro- and nano- cellulosic fibres i.e.: enzymatic, ultra sound steam explosion help to process lignocellulosic row materials to more fine and homogeneous fibres. These can be successfully used as excellent filler and reinforcing fibrous materials for modern composites, also can be designed to work under extremely conditions. 2) Development of low combustible and stable against biodeterioration polymer nanocomposites with nano-dispersed fillers including carbon nanotubes. The important problem of many produced and applied composites is their flammability and non-stability against biodeterioration. In order to improve above mentioned features, composites with addition of flame retardants and biocides (to prevent them against virus, bacteria and fungi attack) need to be made. Generally, these additives (very often more than 10 % w/w of flame retardants and biocides) decrease the physicomechanical properties of composites. The latest research showed, that nanodispersed flame retardants and nanobiocides significantly used below 10 % weight (concentration 2 – 3 times lower) have a positive effect; decrease flammability and biodeterioration ability of composites. There are many known examples of an effective use of carbon nanotubes, nano-clay and nano-melamine-polyphospate. Many of the nanofillers show also synergistic effect and in some case intumescent, fire barrier effect. 379 3) Application of an effective biocide against microbial attack as component polymers and coating materials. In order to get protection against biodeterioration, many different biocides are being used in majority of produced polymers composites and coating materials. They are active against gram plus and gram minus bacteria, viruses and fungi. Many of the commonly used biocides are environmentally hazardous and they do not meet of REACH systems demands. The very wide application’s area of polymers, paints and composites such as: building industry, transportation, agriculture and packaging demand to avoid decomposition and functionality decrease of the material due to biodamages. The problem of biodamages comprises a wide range of scientific and practical tasks. These are associated with protection of row materials, intermediates and products against damaging by bacteria, fungi, insects and rodents during long terms production, storage, transportation and the use in different climatic conditions. Biodamages can influence on properties of polymers, rubber composites, textiles, wood, leather, paper, building causing significant change in their functionality, quality reduction and in some cases even completely destroy them. Special attention will concentrate on natural biocides (which are more environmentally friendly) such as agrofine chemicals – like essential plants oils, bioactive polypeptides and their relatives, and relatives of 2 qinolino-carboxylic acids and some nano-compounds. 4) Mutli layer composites on the base of fabrics and rubber. The textile-rubber goods, in which textiles are a main constituent, are designed to take advantage from properties of reinforces textiles and resistance of rubber coating in order to operate in environmental conditions. Besides properties of both bonded materials, durability of these good is determined by adhesion between both materials. In their production process the increase of bond strength between synthetic textiles and elastomers is usually achieved by coating of cords or textiles in the RFL bath. A modern, less awkward and recently developed way is incorporation into rubber compounds special chemicals called adhesion promoters e.g.: (Patent No. 187856 “Method of bonding textiles to rubber without impregnation”) Adhesion between rubber and cords (polyamide PA, polyester SP or viscose VISC) in all experimental compounds of carboxylated-butadiene rubber (XNBR) is seven times higher in comparison to adhesion between standard natural rubber compound and polyester (or polyamide) cords, but coated by RFL system. Appropriate selection of fillers and curing agents (convectional or unconventional) ensures required properties for textile-rubber products. Usage of adhesion promoters is less complicated and inconvenient, that adhesive impregnation from technological and technical point of view. Rubber coated fabrics can be used as a semi product for lining of driving belt with a driving strand made from oriented polyamide foil. Multilayer driving belts are used in many industrial branches. 380 5) Sealing mass on the base of polymer for modern building applications. This proposal concerns the establishment of an innovative product, a sealing mass for production of tapes and sealing profiles with the usage of rubber waste. The use of rubber waste for production of sealing masses has a proecological effect. Currently used sealing masses exposed to high temperatures i.e.: roof accessories, where temperature can easily reach 100 °C, increase their fluidity, what has an adverse impact on their functionality. Development of suggested technology should help to eliminate this serious disadvantage of currently used products. In this proposal it is expected to investigate the influence of compound such as: resins, oils and fillers as well as multilayer (lamellar) fillers on the plasticization of rubber. Lamellar fillers effectively improve barrier properties of the material by decreasing diffusion of gases and liquids. They also decrease migration of plasticizers to the surface of the product, what prolong the product lifetime by the increase in resistance against aging in environmental conditions. That is why lamellar fillers will be optimized for control viscoelastic and barrier properties of the materials. The main aim of this proposal is to establish technology, in which the correlation between cohesion in sealing mass and its adhesion to the surface can be found. The study of adhesion and cohesion properties of the sealing mass will be investigated as follows: tack – with the accordance to international standard AFERA 4015, adhesion – with the accordance to international standard AFERA 4001, cohesion – with the accordance to international standard AFERA 4012, destruction of the adhesive – tearing the layer of sealing mass from the surface, destruction of the cohesion – destruction of the sealing mass. 381 6) New technology of bisphenol A A new technology for the production of the highest grade Bisphenol A (BPA) is offered, which can be further applied as the key component to obtain epoxy resins and polycarbonates, respectively. The last represent modern plastics commonly applied in building construction, electronics, optics, aviation and car industry. Intellectual property of the offered BPA technology is protected by two European patents, No. EP 1809589, EP 2090562 A1 and one international PCT patent application No. PCT/PL2011/000010. The older version of the technology in question was implemented industrially in the “Blachownia” Chemical Works, Kedzierzyn-Kozle, in the year 1978 (now PCC Synteza S.A.) and further became the subject of license exported 8 times to: China, India, Korea, Iran and Taiwan, within the years 1987-1999. Among the years 2006 and 2009 a new, upgraded energy saving version of the technology was developed by the authors in the Institute of Engineering of Polymer Materials and Dyes, located in Torun. It is presently offered as the “Chemwik® BIS process”. The New BPA technology was verified industrially in the years 2008-2009 in a scale of 15 000 t/y, at PCC Synteza reference plant located in Kedzierzyn-Kozle, Poland. The technological offer includes: licensing, basic design, technical services - like personnel training, author supervision on purchase and accomplishment of equipment and start-up of the plant, as well as further development and implementation of improvements for the licensee. Two dedicated multimedia presentations are available for interested clients, whereas one presents the offered BPA process (35 min.) and the other visualizes of the PCC Synteza reference plant (40 min.), respectively. 7) New, anti-static paint for the production of surgical mattresses. The invention relates to a technology of producing and applying a new, anti-static paint intended for coating of flexible polyurethane foams used to manufacture of mattresses for surgical tables. Compared to the previously used anti-static paint, the paint made according to the invention distinguishes itself by improved chemical resistance. This allows the surgical mattresses to withstand repeated disinfecting and maintain permanent electrostatic properties, with an extensive range of used disinfectants, containing such active substances as alcohols, aldehydes, peroxides or quaternary ammonium salts. The invention ensures more effective protection against microbiological contamination in hospitals. 382 8) Waterborne paint for decorative-protection painting of polyurethane foams for building industry. The subject of offered technology is a new ecological paint for protection of foams against UV radiation used for thermo- and hydro insulation of roofs in building industry. The paint protects effectively the surfaces of polyurethane foams in the way friendly to the environment. Developed ecological paint fulfils high technical requirements for coating materials for protection of PUR foams. Although the paint does not contain organic solvents, the properties of developed coatings are the same like for classical solvent- borne coatings. A proper choice of wateborne binder – water polymer dispersion of glass temperature below 0° C and the development of optimal composition of paint enabled obtaining the paint of required technical parameters like very good adhesion to thermo insulating material and high resistance of coatings exposed to sun radiation and variable atmospheric conditions. 9) Technology of coating system containing white anti-static paint used for painting of industrial protective helmets. An innovative white anti-static paint based on polyurethane binder has been developed. The paint possesses a surface resistance at the range of 107, excellent adhesion to polyester-glass substrate and good impact and scratch resistance. The paint together with the developed white polyurethane primer can be used for painting of protective helmets in mining. Developed coating system has been already implemented in Polish industry. 10) New pigment compositions of low sun radiation absorption used mainly for coatings applied on roofs and building façades. The subject of offer is a new technology of coating systems containing pigment compositions of defined absorption-dissipative properties decreasing the temperature of heating of objects under the influence of sun radiation. The colouristic of developed coatings was designed in accordance with market demand for paints used for roofs and façades. 11) The method of producing medical polymeric dressing based on chitin copolyesters. For the research purpose, material compositions in the form of staple fibres of 5-7 mm coated with chitin copolyester in the form of an alcoholic solution were prepared. The solution was selected in the way, that amount of active substance on the non-woven surface was approximately 2 % w/w. The composite was pressed and circles with a diameter of 70 and 90 mm were cut out for further study of biological activity. Before pressing, non-woven was subjected to carding process, which increases its volume 15 times. Such a composite structure is different from the currently used gel dressings. 383 12) Method of manufacturing piezoelectric materials by using polymers. The piezoelectric effect in the PP film modified with inorganic nanocompound (nanoclay) was discovered and studied. The generated voltage is similar to that generated by the piezoelectric PVDF films. The effect of piezoelectric voltage appears only in crystalline systems (both mineral and some organic). The piezoelectric effect depends on the correct orientation of unidirectional film combined with corona discharge activation. 13) Preparation of biodegradable PLA packaging. The technology for producing thermoplastic film of polylactide PLA intended for the manufacturing of containers for packaging or food products storage was developed. Film is produced by extrusion of strip. The containers are manufactured by thermoforming. The material is modified by various additives in order to ensure suitable flexibility in further processing. 14) Development of the technology and production start up of mulitilayer fireproof barriers The project aims to develop innovative, lightweight, flexible as well as rigid fireproof barriers with high thermal and fire insulation at the reduced thickness, also resistant to biodeterioration. Objective will be achieved by the use of swollen and functionalized vermiculite and wollastonite fibres, mineral fibres and binding agents on the basis of expanded silicates. To strengthen the effectiveness of fire proofing barrier they will be covered with Al films with swelling coatings. Innovation of this solution relies in the synergistic selection of components of barrier layers, which will gain a flexible and rigid barriers, easy to apply and shape, to be used in construction, transport, defence and fire protection. 384 15) Equipment for the manufacture of environmentally friendly polymeric composites using renewable raw materials. Nowadays, manufacturing technologies and processing of polymer composites play a key role in many industries. Research on new polymer technologies, that help protect our environment, are areas subjected to a current priority of generated visions of technological development in various fields, such as chemical industry, processing and manufacturing of plastic products and creating a modern industry based on biotechnologies. New technologies of low-cost polymer composites with the required and pre-defined properties, are obtained by applying a large amount of cheap fillers, which also act as modifiers and allow to obtain the properties of these composites. Preparation of advanced polymer composites using natural materials with excellent properties will greatly expand the applicability of this type of material in various industries. 16) Equipment for laboratory testing of rheology, structure, technological and functional properties of polymer composites The study of rheological properties of polymeric materials are designed to determine their flow and deformation under the influence of stress. Precision and control of conditions during the tests allows for an analysis of the relationship between the state of stress, strain state and their time derivatives. This provides the information required for classification of the rheological behaviour of the examined materials. 17) Equipment for the recycling of filled polymers. The modern world is based mainly on plastics. Products made from them are an indispensable part of our daily lives. However, some important issues are related to the production of plastics, and these are the depletion of raw materials for their production, high production costs and difficulties associated with recycling. The consequence of this is to change the direction of production and testing of plastic products. Currently on the market, there are eco-friendly, innovative production technologies of thermoplastic composites with cellulosic fillers. Our research will also focus on the development of the equipment for recycling of plastics from composites, and products made out of it, containing metals and nano-additives. 385 INSTITUTE FOR FERROUS METALLURGY (Instytut Metalurgii Żelaza im. Stanisława Staszica) Organisation Contact Data 12 – 14 Karola Miarka st., 44-100 Gliwice, Poland phone: +48 32 234 52 05 fax: + 48 32 23 45 300 e-mail: [email protected] http://www.imz.pl/en.html Institute for Ferrous Metallurgy (Instytut Metalurgii Żelaza) is a research entity with 65-year long tradition. Mission of Instytut is to conduct research and development works as well as to render research, consulting and training services in favour of steel manufacturers, steel users and institutions, in that public institutions, related to the iron and steel industry. Scientific and research activity of the Institute is mostly of the nature of the applied research, the result of which is implemented or utilized in the industry. Partially, the research is of the basic nature. Basic research is carried out mostly prior to the intended utilitarian works and makes it possible to obtain initial understanding as to purposefulness of dealing with practical issue and problem solution are concerned. It also contributes to scientific development of the Institute personnel as well as development of research methodologies applied in the Institute. Research works and services executed by the Institute cover the following fields: Investigation of technological processes including research carried out by means of advanced methods of physical and numerical simulation Development and implementation of new and improved metallurgical technologies in scope of: primary processes, including hot metal, steel and ferroalloys production continuous and conventional steel casting steel products hot forming (long and flat products rolling, die and blacksmith forging) cold working heat treatment of steel products including direct treatment using the heat of hot working Development and implementation of the technologies of: waste recycling, sewage treatment, dedusting of waste gases, recycling of dusts and sludge in steel plants Development of technology of advanced processing and manners of products’ properties adjustment to the requirements of consumers 386 Development and improvement of steel and construction alloys; developing chemical composition and designing internal structure of material from the point of view of the required properties of product Development and implementation of new product ranges and improvement of quality of the manufactured semi-products and steel products Examination of chemical composition, properties and structure of materials, expert assessments of materials, including: tests of products for their compliance with standards, diagnostic material tests of power engineering equipment and analyses of steel products’ defects. Consulting activity of the Institute includes: Scientific consultancy in scope of research methodology, in particular material tests and analysis and interpretation of tests results Technical consultancy in scope of selection of equipment and units for steel manufacturing and steel processing Technical consultancy in scope of selection of steel (and to some extent other materials) for various practical applications Business consultancy including: macroeconomic analyses, marketing studies, financial analyses, strategic analyses, planning and assessment of efficiency of business undertakings, monitoring and analysis of implementation of the restructuring programmes. 387 1) Technology of new slag-forming MgO carrier. In cooperation with the Company PEDMO S.A., the Institute for Ferrous Metallurgy developed manufacturing technology of new MgO carrier to be used in steel melting and ladle treatment as well as in foundry. The developed material contains more than 60% MgO and is in form of a granulate of diameter 9-11 mm. It is characterized with high mechanical strength and moistness below 2%. The Institute developed two options of material: the first one mainly for slag foaming in electric furnace, containing carbon, and the second, universal, which may be used in all processes. Moreover, the manner of preparation of mix for granulation was developed (composition, binding agent, moistness and proportion). Parameters of new material pelletizing in industrial conditions were developed by PEDMO S.A. and the latter is the owner of know-how in this regard. The present industrial experiences imply that regular and expert application of the new material in ladle furnace results in significant extension of the time of lining usage and does not deteriorate refining parameters of slag. Both electrical steel melt plants and foundries are recipients of the material. Significant increase in demand would occur in the case of material application in converter process. At present the domestic demand is met by PEDMO S.A. There are numerous cheaper substitutes in the market, of worse parameters, therefore increase in demand requires promotion campaign. Contact Person Data Mariusz Borecki, MSc. Eng e-mail: [email protected] 388 2) Energy-efficient ignition furnaces for ore sintering belts Energy-efficient ignition furnaces designed and built by the Institute for Ferrous Metallurgy are recommended for iron and other metal ore sintering belts up to 4m wide (see below): Ignition furnace characteristics The energy-efficient ignition furnaces consist of steel structure, roof, refractory lining, battery of injector burners, piping, damping chambers and supporting tracks. They have the following outstanding characteristic: - - - low heat-consumption (50-70 MJ/ton of sinter) without adverse influence on physical properties of the sinter; concentration of energy in peripheral zones of the belt (better ignition at belt sides); construction costs lower by more than 50%; the use of special injector burners which eliminate the need of compressed air system for combustion and reduce electric power consumption; furnace cooling system is eliminated with consequent reduction in water and electric power consumption; simple and compact desing reducing thermal losses and facilitating maintenance and repairs (the weight of the furnace is 60-70% lower than of comparable conventional furnaces); the furnace is mounted on wheels for easy repairs, replacement of parts of the furnace itself; possibility of firing with gases with various heating values (7.5-35 MJ/m3); lower environmental hazards (lower emissions of SOX, CO2 and NOX and less noise). 389 Score of supplies - supply of complete ignition furnaces; documentation of assembly of the furnaces; quality attestation for refractories used in furnaces; supervision of assembly and start-up of the furnaces. Time of delivery Delivery of the furnaces within approximately 6 months after the signature of contract. Warranty Warranty is given for the period of 12 months beginning from the date installation. Contact Person Data Janusz Stecko, Dr. Eng., e-mail: [email protected] Marian Niesler, Dr. Eng. 390 3) Method of Liquid Steel Reheating in Hot Top and/or in Tundish and Cover for this Aim A liquid steel in hot top after bottom pouring it into mould assembly is reheated after pouring by the cover with high isolating refractory material till a moment of metal contraction in volume, and in a case for tundish, adequate insulating-reheating cover is used fo reduce heat loss and superheating of liquid steel during continuous casting operation. Above mentioned method results in high cleanness and internal quality of continuous casted bloom, billet and slab. Contact Person Data Bogdan Zdonek, Dr. Eng e-mail: [email protected] 391 INSTITUTE OF BIOPOLYMERS AND CHEMICAL FIBRES (Instytut Biopolimerów i Włókien Chemicznych) Organisation Contact Data Contact Person Data 19/27, Skłodowskiej-Curie st, 90 – 570 Łódź, Poland Proxy International Cooperation: phone: + 48 42 6376744 fax: +48 42 6376214 e – mail: [email protected] http://www.ibwch.lodz.pl, Mr. Alojzy Urbanowski phone: + 48 42 638031 e – mail: [email protected] Director: Danuta Ciechańska, Ph.D. COOPERATION OFFER We are an R&D unit active in biopolymers like cellulose, chitin, chitosan, keratin, starch, alginates and other, and preparation of chemical fibres for mainly special, non-apparel application. An exhaustive information on the Institute can be found under www.ibwch.lodz.pl. We would like to establish cooperative links with R&D and industrial units in Asia in following areas : 1. Cellulose fibres. In our Institute two proprietary processes have been developed for the manufacture of cellulosic fibres as alternatives to viscose process . The processes consist in modification of cellulose by either enzymatic or hydrothermal treatment which leads to cellulose directly soluble in alkalis. Fibres are spun from the solution in a wet-spinning process. 2. Chitosan fibres. A process has been developed to produce chitosan fibres. We run a small pilot scale line enabling production of chitosan fibres in amount of few kgs. per week. The fibres are mainly designed for uses in medical devices including implants. 3. Biodegradable non-woven directly spun from the melt of bio-based polymers 4. Composite keratin materials. We are active in the utilization of waste feathers from chicken breeding. Obtaining materials may be used for different purposes. For above items know-how is available sufficient for up-scaling of the processes to pilot scale and further on to industrial scale. We are ready to give exhaustive presentations 392 INSTITUTE OF CERAMICS AND BUILDING MATERIALS (Instytut Ceramiki i Materiałów Budowlanych) Organisation Contact Data 9, Postępu st., 02-676 Warsaw, Poland phone: +48 22 843 19 65; 22 843 52 96 fax: + 48 22 843 17 89 e-mail: [email protected] ; [email protected] http://www.icimb.pl/icimb_en/ The only scientific-research institute in Poland which covers all areas of non-metallic science and industry such as well as mineral processing, production technology of ceramic materials and glass, refractory and building materials, mineral binders and concrete products. RESEARCH AREA: glass, ceramics and bioceramics building and refractory materials mineral raw materials environmental protection development and improvement of materials production technology LABORATORY TESTS: mineral raw materials glass and ceramics products refractory materials building materials environmental pollution SERVICES: expert opinions and technical advisory services scientific and technical information specialist trainings schemes: www.icimb.pl power engineering and production engineering audits industrial measurements 393 CERTIFICATION: glass, ceramic and concrete products building materials factory production control (FPC) quality management systems PRODUCTION: technical ceramics and composites building and refractory materials bioceramics frits, engobes and glazes ceramic pigments and colours 394 1) APPLICATION OF ROASTED LOW-CALORIE COAL-ASSOCIATED SHALES IN BUILDING TECHNOLOGY The Glass and Building Materials Division of the Institute of Ceramics and Building Materials and the Department of Building Materials Technology of the Faculty of Materials Science and Ceramics of the AGH University of Science and Technology, basing on their research and development works, have elaborated an innovative technology: a method of roasting of lowcalorie coal-associated shales or clays containing no combustible parts in an annular fluid layer, and a reactor with an annular fluid layer for their roasting. Roasted low-calorie coal-associated shales are used in building as a low-weight concrete filler. A special area of their application is the cement industry, where the product obtained by means of the new technology may be used as a pozzolan additive. The additive consists of silty materials obtained from coal-associated shales or roasted clays, dehydrated in the process of roasting in a fluid layer. The application of diverse mineral additives, including waste materials such as coal-associated shales, as well as improvements and changes of the technology of cement and concrete production, will allow to manufacture "a better composite from worse materials". The necessary technological development in that area is made possible, for example, by using active hydraulic powders, by designing concrete composition that matches its applications more accurately, and by modernizing the technology of its production. To achieve this, it is necessary to develop theoretical foundations of properties and mutual interactions of concrete components, including pozzolan mineral additives. Coal-associated shales - one of the components of the gangue obtained in the process of hard coal extraction - are materials with very promising future applications as additives in the production of cement and high-quality concrete. The gangue, including the shales, is stored in mine dumps in the areas where coal is produced. The waste is usually inert, but it may still pose a potential threat for the environment since the salts contained in the waste material are leached and thus constitute a source of pollution of the underground and surface waters and soil; moreover, the waste contributes to polluting the adjacent areas with the dust from the dumped material; also, thermally active dumps emit considerable amounts of air-polluting 395 gases (including CO and CO2) and may endanger the local population in case of their insufficient protection. The described invention has been submitted to the Polish Patent Office under the title “A method of roasting of low-calorie coal-associated shales or clays and a reactor for its application.” The invention was part of the project entitled Patent protection and commercialization of innovative technological solutions in the field of plastering mortars produced on the base of Roman cement and of the method of coal-associated shale roasting within the "Patent Plus" Programme of the Ministry of Science and Higher Education. 396 2) INTERNAL PROTECTION OF CONCRETE AGAINST SULFATE CORROSION The target area of the application of the invention are plants manufacturing cement concretes based on Portland cement. Under the influence of water containing sulfates, Portland cement concrete undergoes dangerous destruction during exploitation that is connected with the loss of chemical and mechanical properties as the result of sulfate corrosion. The mechanism of sulfate corrosion consists in the destruction of cement matrix as a consequence of a series of chemical reactions leading to ettringite or gypsum crystallization and decalcification of CSH phase that determines concrete strength. As a result of these processes, a number of microcracks arise that weaken concrete in initial phase of corrosion and, in the final stage, cause destruction of concrete structures. The disadvantage of the known methods of increasing the resistance of concrete to sulfates is the lack of the protection of the entire mass of concrete in the course of time. Cements established to be resistant to sulfate corrosion protect concrete only during relatively short exploitation time and do not warrant the protection of concrete structures made from these cements in the long run. In case of cellular concrete, they do not protect groundwater from contamination by sulfates. The internal protection of concrete against sulfate corrosion consists in the addition of dicalcium silicate containing variable amounts of barium in solid solution in an amount of 3% to 10% by mass of cement to the concrete mix during its preparation. Barium forms solid solutions with dicalcium silicate in a wide range of compositions. The solid solution of dicalcium silicate and barium added to the concrete mix does not react with water during the initial maturation of concrete mass and during its treatment in autoclave. The reactivity of the silicate is activated after the migration of water into the concrete during its exploitation or after crushing concrete and its storage in an open area, for example on a heap, where it undergoes rapid hydrolysis releasing barium hydroxide. The invention is part of the project entitled “Science for industry - the commercialization of inventions resulting from R & D” within the "Patent Plus" Program of the National Centre of Research and Development. 397 3) METHOD OF APPLICATION OF NANOSTRUCTURED, REFLECTIVE, COLOR AND/OR COLORLESS COATINGS ON GLASS AND COATING DEVICE FOR CARRYING OUT THE COATING PROCESS. The main disadvantage of the known commercial methods of coating glass sheets for building windows is the lack of possibility to use such methods for the placement of colored or colorless durable protective coatings on a surface of glass items with irregular shapes, such as bottles, containers and the other glassware products, especially of common use. The technology has been developed with the aim to obtain container and glassware glass products with metal (-s) oxide films characterized by solar control and decorative properties. Additionally, the thin film coatings obtained using this technology are bonded to the glass surface layer with strong chemical bonds. In effect, practically independent of metal oxide composition, the glass surface protective features can be obtained even with a coating thickness as low as about over 20 CTU (1 CTU ≈ 3-4 Angstroms Å, 1 Å =0,1 nm), endowing the glass product with the lubricity and surface damage resistance as well as impact strength increase of several % to about 20 %, depending on the thickness of the coating. This feature is especially important in terms of avoiding the losses during filling and transportation of the glass containers. It also allows to increase the range of glass containers recycling, to obtain saving of the raw materials and energy cost and also, is advantageous for the environment protection. With aim to avoid the drawbacks of the existing state of coating technology the present invention proposes applying to the common use glass products of the coloured or colourless metal oxide films characteristic of ability to decrease solar radiation transmittance, especially of the UV and NIR range. In accordance to this invention, the coatings on the glass products are produced by chemical pyrolysis method depending on whether they undergo dipping in the next high temperature treatment /or spraying the solutions of the metal oxide coating precursors immediately to the hot glass surface after the products are formed. Thus obtained metal oxide coatings are colourless or coloured and reveal resistance to the outside atmospheric conditions and cleaning agents of common use for glass. The coatings obtained in this technology are able to reflect and also selectively absorb solar radiation of UV and NIR ranges which are responsible for degradation of the contents of the glass packages. 398 This coating technology allows to apply the durable metal oxide films with solar control and mechanical protective properties on the surface of glass items commercially produced. The application of this technology is especially advantageous when applied “on-line” immediately after the formation of the glass products and it also allows to obtain uniform coatings on the glass products with complex shapes. 399 4) PRODUCTION TECHNOLOGY OF AUTOCLAVED AERATED CONCRETE Autoclaved aerated concrete is a light-weight and warm building material that possesses high strength parameters. It is used for construction, insulation and insulation-construction purposes in civil engineering. Depending on local conditions, various production technologies of autoclaved concrete are applied, according to the following formulas: binding material (cement + lime or only lime), aggregate (sand or fly ash from burning brown or hard coal or sand + fly ash), porosity adsorbent (aluminium powder or aluminium paste), surfactant facilitating the blending process of elements and the reaction of the porosity adsorbent with elements concrete mix, water. We also offer to develop formulas fit for AAC technology with other raw material as specified by the Customer. The production technology of autoclaved aerated concrete is characterized by low-wear raw materials and energy-efficiency as opposed to other technologies of wall building materials production. This is the result of low concrete density and appropriately conducted processes. It is a waste-free, environmentally friendly process. Elements from autoclaved aerated concrete can be applied in the housing industry 1-2 concrete family for erecting walls and, moreover, in industrial and public facilities. It should be emphasized that houses form AAC are built in all European countries, as well as on other continents in different climate zones, and in seismic areas the advantages of this material has been put to a test. The properties of masonry elements from autoclaved aerated concrete are covered in the EN 771-4. The concrete density in the dry state range from 300 to up to 750 kg/m 3, the compressive strength, respectively 1,8 – 8,0 MPa. It is possible to make warm single-ply outer walls U≤ 0,3 W/m2K from autoclaved aerated concrete of low density classes: 300, 400, 500,. Single-ply walls are recommended particularly in one, two-family buildings, terraces, in which the insulation properties of autoclaved aerated concrete may be taken full advantage of. It is possible to make layered walls from AAC also in combination with insulation and brickwork. A wide range of products is offered for building walls: elements of small-dimension as well as elements for carrying lintels, beam-and-block flooring. These are elements fit for thin joints with the thickness of 1-3 mm (to adhesive mortars). Elements of small-dimension may have smooth surfaces, with shaped faces adapted to the feather and, additionally, with a handgrip facilitating bricklaying. 400 ICiMB provides the production technology of autoclaved aerated concrete, including: establishment formulas adjusted to the raw materials the Customer has at her/his disposal establishment the course of technological process selection of machines and devices about the determined output capacity. Moreover, we offer the contact and cooperation with Polish companies that manufacture and design AAC as well as manufacture machines and devices. We develop the technology production of AAC with the use of fly ashes from burning biomass with coal and fly ashes produced from coal combustion in fluid boilers involving concurrent flue gas desulphurization (details enclosed). Currently, development works are being conducted. The technology drawn has received numerous awards at international exhibitions. 401 5) LEAD FREE COLOURS FOR GLASS DECORATION The harmful activity of lead compounds present in ceramic colours forces to seek solutions eliminating harmful agents both during the colours production stage as well as during their application. The characteristic feature of the invention is that the colours made according to this technology do not contain lead compounds and their chemical composition guarantees giving shine to decorated surface and intensity of colour comparable with colours based on lead fusing agents which were previously used. The solution according to the invention implies 6 pallets of colours for firing in the temperature range from 800°C to 1250°C. on-glaze metallic ceramic colours for decorating porcelain ceramic colours for decorating ceramic tiles on-glaze ceramic colours for decorating porcelain under-glaze colours majolica colours colours for decorating glass using the fusing technique The colours manufactured on the basis of these developed technologies are applied by various ceramic factories as well as small and medium-size companies. The colours are produced by Institute of Ceramics and Building Materials. A particular attention should be paid to colours applied for glass decoration. The worked out colours became base for starting of new production of glass tiles and strips, decorated from the fitting side. 402 6) SPOUT INSERTS OF CERAMIC – METALLIC COMPOSITE ZRO2 –Mo The subject of the invention are spout inserts made of new refractory material from zirconiummolybdenum (ZrO2-Mo) composite for application in casting of molten soda-lime glass. The composite is a sintered product based on zirconium–oxide (ZrO2) with content >80% mass. and molybdenum (Mo) with content up to 10% mass. Addition of molybdenum improves mechanical strength of the ceramic matrix of the composite and improves erosion resistance of composite, while keeping its high refractoriness. The composite material used for spout inserts were is statically formed under pressure ~ 200MPa and pressureless sintered in an atmosphere at 16000C. Composite material for spout inserts features: high apparent density >5g/cm3, low open porosity <10%, high cold crushing strength >400 MPa high corrosion resistance to molten soda-lime glass 403 7) AGRO-SINTERS CERAMIZED FERTILIZER COMPOSITES The invention involves ceramized fertilizer composites referred to as agro-sinters. A characteristic feature of agro-sinters produced in the form of granulate with the dimensions of 1 to 5 mm is their slow decomposition in the soil environment, accompanied by gradual, longterm feeding to the soil of the macro- and microelements released, which are necessary for correct plant development. This gives agro-sinters a significant advantage over the commonly used artificial NPK fertilizers which dissolve easily and can be washed out quickly by atmospheric precipitation. Argo-sinters also de-acidify the soil, increasing its pH and decreasing hydrolytic acidity, as well as improve soil structure. Due to their prolonged action over several years, they can be used to improve soil structure and the balance of the soil components in places where agrotechnical procedures are no carried out frequently: In the areas of forest plantations, recultivated wasteland, waste dumps, dunes or other undeveloped land. The basic components of agro-sinters are clays, mineral waste material and accompanying minerals. The production methods involves granulation of the material set and heat treatment of the granules at the temperature of 700oC. 404 8) CERAMIC BACKING USED TO PROTECT ROOTS OF WELD WITH INERT GAS, IN SPECIAL WELDING Welding high-alloy steels (such as for instance duplex and superduplex), nickel alloys stainless steels, steels for power engineering, copper alloys and titanium alloys requires inert gas protection of weld root. This problem is solved either by direct blowing of the inert gas on welded spot and double-sided welding or by using copper backing conveying the inert gas to the weld root, with a shape adapted to the shape of the welded elements. Normally, such backing is used to weld specific joints and it is impossible to change its shape. The ceramic backing for welding with inert gas protection of the weld root that has been developed presents the following features: 1. a segment structure making is possible to form long sequences and to convey gas along the welding line (variant a); 2. a shape making it possible to weld curved surfaces (variant b) with diversified radius; 3. possibility of multiple use; 4. diversified thermal conductivity making it possible to adapt the device to the type and thickness of the plates welded (table); 5. possibility to obtain a uniform joint and a varied weld surface from the backing side; 6. reduction of the amount of gas used, making single-sided welding possible. 405 9) INSTALLATION FOR SCRAP TIRES COMBUSTION IN CEMENT KILNS Institute of Ceramics and Building Materials, Building Materials Engineering Division in Opole offer its own technology and full technical documentation for system of scrap tires delivery to cement kilns (scope of documentation supply: mechanical construction, electrical, automation and control). The solution is developed for tires (dimensions Qmax1200 x 400mm, G max = 4,0 t/h) or rubber waste that can be delivered as an alternative fuel to the inlet chamber of socalled cold end of the cement kiln. Tires, after weighing are inserted through a sluice into the kiln. Transportation and dispensing system is connected to kiln control system operating in automation. Burning tires as an alternative fuel is an environmentally friendly action because it allows for the safe liquidation of waste and the recovery of thermal energy contained there. This solution allows us to save non-renewable reserves of conventional fuels and at the same time to reduce the size of the landfills storage area. Depending on the preferences of the investor and the tires stock locations, there are two basic solutions, as mentioned below, concerning the transportation from the ground level to the level of the dispensing system on the heat exchanger tower: An inclined conveyor with especially shaped sills, to prevent tires from slipping onto tape (photo) Vertical elevator with protruding handles, especially designed for hanging tires Transportation is carried out horizontally by means of roller conveyors, and is controlled automatically. Weighing device is usually located on the tower exchangers allowing for controlled dispensing of tires to the kiln. The installation is equipped with a system for technological and movement security. The installation was developed by an engineering- research team of the Institute of Ceramics and Building Materials from the Department of Process Engineering in Opole. Our Division conducts investment supervision and commissioning of the installation. Examplary technological parameters of the cement kiln with co-incinerated waste tires: Heating fuel substitution technology - up to 20% Heating value of scrap tires - approximately 26 kJ / kg The number of tires dispensed into the furnace – up to 2.5 t / h Substitution of coal dust from tires 1Mgw /1Mg tires 406 Requirements for burning tires: - Coefficient of air excess in the chamber is 1.15 -1.20 - Real air consumption 9.6 -10.0 m3n/kg tires 407 10) PRODUCTION TECHNOLOGY OF WARM MORTAR - TERMOR N OF IMPROVED THERMOINSULATION PROPERTIES AND HIGHER EFFICIENCY The wall is a composite comprising different materials, starting from masonry elements, and mortars for construction purposes, as opposed to the previously used glue and plaster. There is no doubt that all the components must be selected with due care in order for the best effect to be achieved. ICiMB CEBET has designed the heat-insulating TERMOR N mortar. The mortar is produced in the form of dry elements (cement, lime, fly ashes, fine powder from autoclaved aerated concrete, polystyrene foam or perlite, refined additions). Before on-site application, it only take to mix it with water. This mortar is characterized by a favorable thermal conductivity and better working properties in terms of mixing, adhesion to base, productivity output. This mortar is intended for the construction of outer walls from small-dimension elements of autoclaved aerated concrete or other materials with similar thermal conductivity. Thickness of the joint of 8-10 mm. With heat-insulating mortar it is possible to join elements with the admission of greater deviations in respect of target dimensions (± of 3 mm to ± of 5 mm). The amount of mortar required for the preparation of, for instance, a 1m 3 wall from AAC blocks with the thickness of 36 cm is c. 18 kg. Termor N Mortar is not applied for foundation construction and underground walls. It warrants thermal homogeneity of walls, without the formation of "small bridges of cold" at joint interfaces. This reduces the power consumption required for heating buildings and helps protect the atmosphere and environment. Buildings erected with the use of autoclaved aerated concrete are long-lasting and energy-efficient. 408 Basic Technical Properties Dry blend: - bulk density - ≤ 500 kg/m3 - working life - 3 months from the date of the production - density (max) - 580 kg/m3 - compressive strength - ≥ 3 MPa - bending strength (min) - 1,15 MPa - adhesion to base - ≥ 0,3 MPa Mortar hardened: - thermal conductivity λ in the dry state -0,13 W/(mK) in-service humidity state -0,15 W/(mK) Our offer for the manufacturing of Termor N: - selling know-how for production, - elaboration of documentation for production line, - consultation at all phases of implementation, - testing of finished products. 409 11) PRODUCTION TECHNOLOGY OF THIN JOINTMORTARS Thin joint mortars are intended for the construction of walls of small-dimension elements from autoclaved aerated concrete and allow for thin joints with the thickness of 1 - 3 mm, or other materials about with a similar thermal conductivity. It allows to obtain thermally homogeneous walls. Thin joint mortars are produced in the form of dry blends on the basis of cement. Preparing mortars on the building site is simple and consists in mixing mortars with water in a container with a mechanical agitator until homogeneous consistency is obtained. Mortars are designed for the connection of elements with similar dimensions and shapes (acceptable deviation from ± 3 mm to ± 1 mm). Basic Technical Properties Dry blend: - bulk density - 1300 - 1500 kg/m3 - working life - 3 months from the date of manufacture Fresh mortar: - time of retaining working properties retention exceeding 3 hours - time for elements readjustment/until full setting 7 minutes Hardened mortar: - compressive strength - ≥10 MPa - adhesion to base - ≥0,3 MPa Thin joint mortars are registered under the patent No. 185365 „Dry glue mortar blend, dedicated for the connection of elements from autoclaved aerated concrete. Thin joint mortars is simple in preparation and application on the construction site. The considerable thermal homogeneity of walls made with the thin joint mortars enables to reduce the power consumption for heating the building. The dry blend is much more efficient as opposed to the traditional mortar. The amount of mortar required for the preparation of, for instance, 1 m2 wall from blocks from autoclaved aerated concrete with the thickness of 36 cm is : - 40 kg of dry components of the cement-lime mortar at the traditional method of building walls 410 - 8 kg of the dry blend of the mortar for thin joints Our offer for the production of thin joint mortars: - marketing license - elaboration of documentation for production line - consultation on all phase implementation - testing of finished products 411 INSTITUTE OF ELECTRONIC MATERIALS TECHNOLOGY (Instytut Technologii Materiałów Elektronicznych) Organisation Contact Data 133, Wólczyńska st, 01-919, Warsaw, Poland phone: +48 22 835 30 41 – 49 fax: +48 22 864 54 96 e-mail: [email protected] http://www.itme.edu.pl ITME has already had a certain experience in R/D collaboration with Asian countries, realized through exchanges of scientists (Japan), participation in international fairs and scientific conferences(China, Japan, Taiwan), execution of common research programs. (Japan, Qatar) or execution of research projects commanded by Asian companies. We are interested in developing scientific and R/D cooperation and execution of common research projects in following areas: novel materials for electronics and photonics such as: graphene, meta-materials, topological insulators, self-organizing materials, photonic crystals and gradient composites. glass and ceramics fabrication with desired mechanical and optical characteristics (transparent, laser) , and optical guides, photonic crystal fibers, diffraction lenses included. epitaxial structures on silicon, silicon carbide, III/V compounds, YAG and GGG oxide crystals for electronic and photonic devices. development of innovative lasers, photo detectors, diodes and transistors. ITME offers also: The realization of research requested by industrial partners. Development and eventually small scale production of materials, epitaxial structures, active and passive components according to requirements. Highly qualified consultants in the area of technology and characterization of materials and components. A short description of our Institute is included in the appendix and more detailed information concerning the Institute of Electronic Materials Technology can be found on our webpage http://www.itme.edu.pl 412 INSTITUTE OF HEAVY ORGANIC SYNTHESIS „BLACHOWNIA” (Instytut Ciężkiej Syntezy Organicznej „Blachownia”) Organisation Contact Data Contact Person Data 9, Energetyków st., 47 - 225 Kędzierzyn - Kożle, Poland phone: +48 77 487 34 70 fax: + 48 77 487 30 60 e-mail: [email protected] Adriana Muszynska phone: + 48 77 487 36 40 mobile: +48 694 467 497 e – mail: [email protected] http://www.icso.com.pl/index.php?id=44 Institute of Heavy Organic Synthesis „Blachownia" (ICSO) is a research Institute of organic chemistry sector. For 60 years it has been a successful partner for both, domestic and foreign organizations, within the range of developing, implementing and improving chemical processes, production and sale of chemical goods. ICSO belongs to the top research units in Poland. Institute carries on the R&D and implementation works within the scope of chemical sciences, performs the research and chemical analyses. The confirmation of Institute’s competence and experience are numerous publications, patents and implementations. During its activity the Institute has implemented nearly 900 technologies into the industry, obtained almost 1,5 thousand patents in Poland and abroad, signed 14 contracts for export of technologies (among others: China, Iran, Korea, Spain) and published about 2 thousand of scientific works. ICSO performs scientific research and R&D works concerning the chemical processes, especially in the range of: organic synthesis and technology acrylic, phenolic and epoxy resins with their properties modification, polycarbonates and others separation of gases, hydrogen and pressure processes processing renewable raw-materials petro- and carbochemical processes homo- and heterogenic catalysis chemistry and technology of polymers and plastics, their modification and processing surfactants and household chemistry auxiliaries for various branches of industry chemical analysis physical chemistry chemical engineering environmental protection and waste utilization. INSTITUE OFFERS 413 scientific research research and development works chemical technologies analytical and design services In order to meet the expectations of industrial partners processes offered by ICSO, technical solutions, branch products and provided services are brought into line with worldwide standards. Institute obtained and maintains a Quality Management System ISO 9001 and performs analyses according to a Good Laboratory Practice (GLP) rules. 414 1) An innovative process of propylene bioglycol production Process Description The innovative technology for production of propylene bioglycol through hydrogenation of glycerol deriving from biodiesel production from fatty raw material. The technological line process comprises three stages: glycerine purification through distillation under reduced pressure hydrogenation of glycerol to propylene glycol on the catalyst in a heterogeneous flow reactor: purification of the product through distillation. Process Advantages The presented technology for manufacturing of propylene glycol is an innovation on a national and world scale. As particularly innovative in the proposed technology must be considered: the use of renewable and easily available resource for production which is glycerin fraction (a by-product in the used on a wide scale biodiesel production technologies) method for purifying of the glycerol fraction dedicated specifically for the needs of the process and providing glycerin with the desired quality and favorable price the developed by ICSO heterogeneous catalyst used in hydrogenation of glycerol to propylene glycol with high selectivity and activity, produced from easily available raw materials and with high regenerative qualities (waste-free) to obtain an environmentally friendly product with high added value diversification of raw materials for the chemical industry based on propylene bioglycol no solvents and toxic substances in the process the use of small quantities of non toxic by-products in the process concept of the reaction system, conducting of process and product emission optimized flow of the process streams for the total utilization of the raw material and energy. 415 2) A new generation of epichlorohydrin technology with use of bioglycerin as a raw material Process Description Innovative method of epichlorohydrin production uses totally different raw-material base than the traditional process, which utilizes chlorine and propane of petrochemical origin. The new process uses hydrogen chloride (hydrochloric acid) and glycerin, the main waste product of rapidly developing biodiesel industry. The method is based on the replacement stages of propylene chlorination stages to allyl chloride ones and via well-known reaction of glycerin with hydrogen chloride, allyl chloride converts to dichloropropanols: glycerin + hydrogen chloride ( gaseous ) dichloropropanols final stage of dichloropropanols conversion proceeds just as in the traditional method: dichloropropanols + alkaline agent epichlorohydrin Obtaining epichlorohydrin with the use of renewable glycerin is two-staged process based on the following chemical reactions: Process Advantages simplification of the technological process in comparison with the traditional one basing the method on less expensive, renewable raw-material - glycerin significant decrease of energy factors (steam and electricity) radical decrease of waste products amount (chloroorganic compounds) radical decrease of sewage amount non-toxic and non-flammable substrates and half-products are used 416 Economic Aspects several times lower raw-material unit cost considerable reduction of waste products amount (mainly glycerin derivatives which are easier to utilize) multiple reduction of the sewage amount, which are additionally less toxic (lower content of AOX) substantial lowering of variable costs of the new EPI production method in comparison with the traditional one. 417 3) EPOXY RESINS Product Quality Several types of high performance epoxy resins can be obtained in the process offered. The table below presents exemplary quality parameters for Epidian® 6 and Epidian® 012 and Epidian® 011B. Specification Appearance Epoxy value, val/100g Epoxy equivalent Viscosity at 25oC, mPa·s Hydrolyzing chlorine content, % Colour, Hazen scale Epidian® 6 clear liquid 0.52 - 0.55 182 - 192 12,000 max not more than 0.02 not more than 50 Colour, Gardner scale Softening point, oC Non-volatiles content, % Bromine content, % <1 not less than 99,9 - *) 40% solution in dioxane Epidian® 012 clear flakes 0.10 - 0.125 800 – 1000 not more than 0.02 not more than 50*) <1*) 93 - 105 not less than 99,9 - Epidian® 011B clear flakes 0.19 - 0.22 455 – 526 not more than 0.08 <2**) 63 - 80 not less than 99,9 not less than 20 **) 40% solution in butyldiglycol Other types for special applications: other conventional epoxy resins, various modified epoxy resins, epoxy – novolacs based on phenol and o-cresol novolacs can be also offered. Process Description Liquid epoxy resin (Epidian®6) synthesis is a two-stage process: during the first stage, epichlorohydrin reacts with bisphenol A in the presence of the sodium hydroxide. During the second stage – dehydro-chlorination, the reaction is finished and the chlorine content of the resin is reduced. After dehydrochlorination the resin is washed. Water from washing is further utilised and the solvent is recovered from organic phase. Solid epoxy resin (Epidian®012) and brominated epoxy resin (Epidian®011B) are obtained through the polyaddition, in which bisphenol A (or respectively tetrabromobisphenol A) is reacted with Epidian®6 in the presence of highly active catalyst. The process runs continuously or periodically depending on needs. Process Advantages High product quality, with low hydrolyzing chlorine content and bright colour Stability and repeatability of product properties The process is environmentally safe. No off-gas is removed outside the synthesis process. Sodium chloride is recovered from aqueous solutions in the solid form, whereby the presence of organic in the effluent is practically eliminated. Low consumption of raw materials and utilities Highly active catalyst in polyaddition process. 418 4) Concentrates of Fire-Resistant HFAE Hydraulic Fluids for Mining Industry (two types: emulsyfing and microemulsion) Benefits approved by Polish Central Mining Industry Institute (GIG) passes approval testing at 0,5 - 2 % concentration in mine specific water licensed/produced in Poland biodegradation in accordance with ISO 7827 and OECD 302B compatible with all commonly used longwall fluids stable in water hardness up to 750 ppm CaCO3 Mixing The fluids are delivered as concentrates and mix with water for use in roof supports. The products mix easily with water of all types. Recommend concentration is 1 % for both type of concentrates (emulsyfing and microemulsion). Typical Properties of concentrates Appearance pH freeze point viscosity @ 40 °C (mm2/s): clear amber solution 9,5 -3 °C emulsyfing microemulsion 60 40 TYPICAL PROPERTIES of emulsion/microemulsion Appearance white emulsion clear microemulsion Rust prevention passes at 0,5 - 2 % (ISO 12922, 7th Luxembourgh Report) Contain bacteria and fungi preventive additives. May contain a dye for easy underground leak detection. 419 5) VPSA O2 and VSA-O2 Process for Production of Oxygen with the Purity of 90÷95 %Vol. from the Air and 92±1% vol. O2 in standard Application The process for production of oxygen with the purity of 90 - 95% vol. from air at the place of application can be employed in: Oxygenation of fish ponds Metallurgy and metallurgical industry – iron-making, sintering, oxidative smelting of metals, metallurgy of copper, nickel and zinc Glass-making industry and ceramic industry: thermal treatment of glass, concrete, magnesite, glaze, high-performance ceramic lining, etc Environmental protection: oxidative purification of waste water, potable water treatment, incineration of wastes, treatment of cellulose waste water Biochemistry: bio-fermentation processes Bleaching of cellulose, substitute for chlorine Process description 3 Capacity: 100÷5000m N/h. The air is compressed under pressure of 150 - 180kPa abs in a blower and then cooled to 30oC and separated in three section adsorber where VPSA process is employed. The adsorber is filled with new generation zeolite molecular sieve – LiLSX. Desorption of adsorbed nitrogen is conducted under pressure of 50kPa. In addition rinsing of molecular sieve, with use of oxygen. Energy consumption no more than 0,4 kWh/1Nm3 92±1%vol O2. 420 Advantages The plant needs no operators. The initial investment and operating costs are low. Oxygen produced is dry (its dew point is -70C) and its concentration reaches 90-94% with the impurities being nitrogen and argon. References Trout Farm, Spain (07.2008) - oxygen purity: 92%volO2, capacity: 150 m3N/h 421 6) Two-stage PSA process for production of oxygen with purity of 99,7÷99,9% vol. O2 Application Oxygen production from atmospheric air at the place of application to cut thick steel details in machine-shops, shipyards, steelworks and scrap yards. Oxygen with high purity can also be used in hospitals and ambulances. Process description Production capacity: 20 ÷ 100 m3N O2/hour. Atmospheric air is compressed to the pressure of 500kPa of volume, filtered, cooled down to the temperature of 20oC, drained and separated in Io PSA installation filled with zeolite molecular sieve. The oxygen with purity of 95% of volume, contaminated only with argon, is manufactured. The oxygen is still purified from argon in the IIo PSA installation filled with MSC3A carbon molecular sieves. The oxygen with purity of 99,7÷99,9% vol. O 2, created in desorption phase, is obtained. The oxygen is compressed and partly turned back to II o PSA process to wash out the argon. In another technology 99% purity oxygen is produced in one stage PSA with use of carbon molecular sieves (CMS) and zeolite molecular sieves (ZMS). Advantages - the possibility to manufacture oxygen with high purity at place of application low investment costs low exploitation costs no problems with wastes possibility to adjust the size and capacity of the plant to the needs of client. References 3 Two plants with capacity of 25 m N /h of oxygen with purity of 99,7÷99,9/vol. O2 in Kopalnia Węgla Brunatnego (Brown Coal Mine) „ Konin”. 422 7) VPSA-N2 and PSA-N2 Pressure Swing Adsorption process for production of nitrogen with purity of 99,999%vol. from air Application Swing pressure VPSA-N2 process for production of nitrogen with purity of 99,999% vol. from air at the place of application can be employed in: food packing metallurgy and aluminium processing food storage after liquefying in: cryogenics inert atmosphere protection used tyres processing with use of cryogenic method Process description 3 Capacity: 10÷500m N/h. The air is compressed in a compressor to 700÷800 kPa, filtered, cooled to 20 oC, dried, and separated in two adsorber PSA plant with use of carbon molecular sieve – MSC-3A. PSA-N2 process utilizes two stage desorption of adsorbed oxygen where during the second stage oxygen is desorbed under pressure of 20kPa. In addition rinsing of adsorbents with nitrogen is employed. Advantages Low cost of high purity nitrogen production. There is no need to use Deoxo process. 423 References Biodiesel Works Wratislavia - purity 99,9%volN2 capacity 200 m3N/h 424 8) Pressure-Swing Adsorption (PSA) Process for Hydrogen Recovery Application Hydrogen recovery from a variety of-gases: gas resulting from steam reforming or semi-combustion of methane coke-oven gas and purification coke oven gas for gas engines ammonia purge gas and argon recovery high purity hydrogen from methanol The scale available is from 500 to 50 000Nm3/h of H2. Process description The PSA process is effected in plants comprising 3-12 adsorbers filled with activated carbon and zeolite molecular sieves. The process combines adsorption at an elevated pressure and desorption at a close-to-atmospheric pressure, using special procedures for gas purging and elimination of over-pressure. By-products No by-products arise in the process: all the products resulting from gas separation are utilized. Process novelty Novel technique for gas purging and elimination of over-pressure; computerized plant control system. 425 Process advantages - High purity of hydrogen: 99.9 – 99.999% mol. Increased purity of hydrogen (99.9999% mol) on request. High efficiency of hydrogen recovery: up to 90%. Low investment and operational costs. Complex process control. Commercial plants 10.000 Nm3/h of H2 for OXO synthesis at the ZAK S.A. (Nitrogen Works) 50 Nm3/h pilot plant for high-purity H2 (99.999% mol) at the Instytut Ciężkiej Syntezy Organicznej “Blachownia” (Institute of Heavy Organic Synthesis “Blachownia”). 426 9) KOTAMINA PLUS - anti corrosion and anti scaling agent Application Kotamina Plus is a high-efficient multi-functional product based on thermo-stable alkylamines Primene TM for chemical treatment of boiler water in energy systems in the power industry. The quality of water decides about efficiency of heat exchange and economics of performance of energy systems. The up to now idea of water conditioning consists in addition of protective formulation into boiler feed water, most often hydrazine and phosphates. ICSO has developed technology with application of multifunctional amine formulations, which improve heat exchange in the boiling and condensation processes, reduce operating deposits and decrease corrosion. Kotamina has been used in several plants in Poland since 1993. Application of the new technology KOTAMINA PLUS for chemical treatment of boiler water, based on thermostable amines (PRIMENE TM) produced by Rohm and Haas might be a breakthrough in boiler water conditioning in energy systems in power industry. Description The application method consists in proper continuous addition of Kotamina Plus to the boiler feed water or to the make-up water. Advantages Kotamina Plus is a new product, which combines long-term experience from industrial application of Kotamina and research efforts of international consortium co-operating in the EUREKA project: E! 2426 BOILTREAT. The advantages of application of Kotamina Plus may be summarized as follows: Improvement of boiler performance Reduced failure frequency of power units Savings on water and fuel Reduced resistance of flow within a system Kotamina Plus offers: exceptional protection against corrosion and deposit formation competitive technology both in economical and ecological aspects, giving considerable improvement of water quality and reduction of raw materials consumption, and decreasing contaminants emission to environment higher efficiency of boilers performance and extended life of equipment 427 References Numerous electric and thermal-electric power stations in Poland use Kotamina protective agent. Kotamina is used in electric power stations with total power of about 5 000MW. In thermalelectric power stations and heat-generating stations Kotamina is used with the of the total systems capacity of over 400 000 m3. The list of reference plants includes among others electric power stations in Połaniec, Bełchatów, Adamów, Dolna Odra, Pomorzany, Konin, and thermalelectric power stations in Chorzów, Tychy, Łódź, Kielce, Elbląg, Białystok. Kotamina Plus has already been successfully implemented in Połaniec, Białystok, Elbląg. 428 10) PHENOLIC RESINS Application Phenol formaldehyde resins are widely used as binders, adhesives, modifying and laminating agents in different branches of industry, including manufacture of wooden derived boards, insulation materials from mineral and glass wool, electro-insulating and construction laminates, insulation foams in buildings and coal mines, foundry, refractory and friction materials. Advantages Versatile range of resins of both types - resol and novolacs High quality - the characteristics is designed to ensure expected functional parameters of the final products, including good mechanical strength, high water, heat and flame resistance Special care is taken as regards environmental safety. The products with very low free monomers are available. Flexibility and innovation - modification and adjustment of the process and resin characteristics to meet the specific application requirements and changing market needs Proved methods for quality control Processes for resins manufacture are commercialized Performance of the resins has been proved in industrial applications Close co-operation of research team with resins producer and end user Research background - more than 30years of research experience, well equipped research facilities, including computer-aided synthesis, advanced analytical methods (TG, DSC, HPLC, GPC, GC,GC-MS, FTIR) References ZTS Erg S.A. Pustków, Poland - Versatile range of products is produced, capacity up to 35,000t/yr. Raw materials phenol formalin catalyst modifiers from the cumene method technical grade basic catalyst of technical grade technical grade 429 11) ISOBIS – New generation of Bisphenol A manufacture process Application Bisphenol A is a raw material for: production of plastics, in particular polycarbonates and epoxy resins production of flame-retardants (mainly tetrabromobisphenol A and recently bisphenol A phenylphosphates) thermal stabilizers of PVC production of phenoplasts unsaturated polyester resins polysulfones, polyetherimide and polyaryl resins plastics antioxidants production of raw materials for polyurethane synthesis. Process Description Synthesis of p,p-BPA isomer through phenol and acetone condensation method in liquid stage in acidic environment with two-stage separation and purification system of synthesis product and by-product concentration control system consisting of parallel running isomerization and catalytic distillation with simultaneous phenol regeneration. The continuous process for the p,p-BPA manufacturing is divided into three stages: 1) p,p-BPA isomer synthesis in two flow reactors operating in series with intercooler control of the reaction temperature and concentration of water, acetone and by-products; 2) separation of p,p-BPA isomer in the form of adduct with phenol from phenol solution through suspension crystallization method and thermal adduct decomposition, as well as purification of crude p,p-BPA isomer through fractional crystallization; 3) by-products concentration control in technological streams circulating in the p,p-BPA isomer synthesis unit and in the unit of its separation and purification based on parallel realized processes of partial isomerisation of by-products contained in mother liquor with catalytic distillation of mother liquor from suspension crystallization. Process Advantages High quality of Bisphenol A Appropriate combination of synthesis, separation and purification units connections and process parameters Control of by-product concentration to obtain high selectivity and capacity of p,p’-BPA isomer Competitive raw material consumption figures Competitive energy consumption No waste problems No batch-operated centrifuges, instead of them continuous filters Increased catalyst lifetime 430 References ICSO “ Blachownia” having 40 years of experience in R&D of BPA process, 7 contracts for granting license to foreign partners for the process to manufacture of Bisphenol A is now offering a new generation process, protected by patents and patent applications, distinguished at numerous international inventions fairs and exhibitions (Intern. Exhib. of Invent. "Geneva Inventions" 2012 – golden medal, Intern. Exhib. of Invent. -SuZhou 2008 – silver medal, Seoul Intern. Invent. Fair 2010 – gold prize, The Belgian and Intern. Trade Fair for Techn. Innov. 2008 – golden medal). 431 INSTITUTE OF NATURAL FIBRES AND MEDICINAL PLANTS (Instytut Włókien Naturalnych i Roślin Zielarskich) Organisation Contact Data 71 B, Wojska Polskiego st., 60 – 630 Poznań, Poland phone: +48 61 84 55 865, + 48 61 848 00 61 fax: + 48 61 841 78 30 e-mail: [email protected] http://iwnirz.pl/index.html The Institute of Natural Fibres and Medicinal Plants is an interdisciplinary research centre with international standing, involved in complex research on obtaining and processing of fibrous and herbal raw materials. The Institute is involved in a number of national and international research projects; cooperates multi directionally with numerous research centres worldwide; works for agriculture, environment protection, construction, transport, food and pharmaceutical industries and medicine. The Centres for Excellence CELLUBAST and Medicinal Plants in Nutrition and Medicine, Accredited Flammability as well as Textile Laboratories (Polish Centre for Accreditation No. AB 225) operate at the INF&MP. These centres and laboratories use the state-of-the-art equipment allowing for conducting flammability tests of different materials, including textiles, specific for the area of application and physico-mechanical tests of these materials The main fields of INF&MP activities: Biotechnology, Breeding new cultivars of fibrous and medicinal plants, agronomy and preliminary processing, Extraction and processing technologies of natural fibres and their modification for textile and non-textile applications, Agro-fine chemicals obtained from plants, nutrients and dietetic products, New applications for oil cultivars of fibrous plants (dietetic and medicinal products), Bio-fuels obtained from fibrous plants, Development of renewable, biodegradable raw materials for industry, Technologies of fire- and bio-retardants production, Environmental protection in natural fibres processing, Recipes and technologies for Polish herbal medicinal products, Complex research on biologically active substances i.e. quality evaluation, development of analytical methods and their validation as well as stability testing, 432 Pharmacological and microbiological testing of herbal raw materials and products, Expert’s reports on new food products in terms of human health or life hazard, Expert’s reports and consultations for state and local government authorities and commercial companies, Research on herbal plants, herbal products, plant medicines, dietetic and functional food. The research conducted at the Institute covers also utilization of polluted land by cultivation of non-food crops, use of co-products from processing of textile raw materials and modern composite materials based on textile raw materials. We are also involved in production of textiles made of natural fibres and blends. Nanotechnology (nano-fibres from natural resources and nano-modifiers for intumescent fire retardant systems) is also of interest for the Institute’s research staff. The outcomes of this work are patented fire retardants and fire retardant systems developed at the Institute – Fobos and intumescent varnish for wood Expander FR. Another fire retardant product developed at the Institute is fire barrier composite resistant to long time effect of temperatures reaching 1200oC used as a filling in steel fire door. Another field of research conducted at the INF&MP is determining the physiological effect of fibres, fabrics and other textile products on human organism. We would like to present 3 technologies from our catalog: 433 1) "Methods of manufacturing cellulose fibers and nanofibers containing silver nanoparticles" (PCT/PL2007/000007) Cellulosic fibres, due to their excellent properties ensuring comfort in use are commonly used in production of garments, hygienic materials and wound dressing. Use of these fibres as wound dressing requires bactericidal and bacteriostatic properties. Such properties are given to wound dressing by textile finishing process introducing superficially active bactericidal pharmaceuticals. This method is expensive, changes physico-mechanical properties and often the colour of wound dressing and causes relatively easy transmission of pharmaceuticals into human body, assuming that these are the wound dressing for homogenized use, e.g. bandages. Such wound dressing require relatively high amounts of pharmaceuticals offering relatively low biocidal effect obtained at complicated finishing process. Taking into account the negative features of manufacturing biocidal wound dressing by finishing method, a new method of biocidal wound dressing manufacture was developed using cellulosic fibres containing the biocidal agent in the structure of fibres. The fibres are characterized by permanent biocidal properties and wound dressing made thereof can be washed many times with no negative effect on biocidal activity. This effect was obtained by homogenous distribution of nano particles of silver in cellulose solution. Homogeneous distribution of nano-sized silver particles in fibre structure ensures excellent bactericidal and bacteriostatic properties of fibres at low silver content. Experiments conducted shown that introduction of silver particle into spinning solution of cellulose by "in statu nascendi" method allows to obtain fibres with bactericidal properties even if the silver content in the fibre is 0.01%. The same bactericidal and bacteriostatic effect can be shown introducing silver into the spinning solution in the form of powder of nano particles in the amounts of one hundred times more. Thus, introducing silver into the fibre by the "in statu nascendi" method allows to obtain fibre with excellent biocidal properties without negative effect on physico-mechanical properties and without any colour changes. The biocidal effect of these fibres is permanent and does not change as a result of multiple washing or dry cleaning due to a permanent presence of silver in fibre structure. Additionally, the biocidal effect is obtained at silver content many times lower in the fibre as compared to effects obtained by other methods of introducing of biocidal substances into the fibres. The fact worth special emphasizing is that process of introducing of silver nano particles into the fibres is fully environmental friendly – causes no pollution of the natural environment. 434 2) Butter modified with flaxseed oil and its production method (PCT/PL2007/000003) Butter is a high fat product obtained in a process of churning of extracted and properly prepared cream. It is a product consisting of the same components like milk but found in a different proportion. It contains also precious natural vitamins: A, D, E and K. A commonly known butter is an easy-to-digest product of unmatched nutritive value. Butter that we present here confirms the above thesis, combining classical advantages of butter and cold-pressed flaxseed oil, contributing qualities that cannot be found in any other vegetable fat. In production of the oil no preservatives or improving substances were used. The methods by which the flaxseed oil is produced have specially been developed for this product, based on scientific knowledge and production experience. The flaxseed oil “Linolia” used in this product is a new assortment of oil. It is obtained from new cultivars of oil flax, specially selected for its applicability for production of edible flaxseed oil. The proportions of fatty acids contained in the oil, provide the high rank among products with positive effect on cholesterol and lipid metabolism in human body. “Linseed butter” is reccomended to everybody, especially for eldery people. A specific taste of butter, given by the flaxseed oil, surely will find customers using it in direct consumption or in cooking or baking. 435 3) An intumescent fire retardant and the methods of its manufacture (PCT/PL2005/000057). A technology of a new, effective intumescent fire retardant system, which contains modifiers in nano scale has been developed for protection of wood and lignocellulosic composites against fire. It does not change a natural appearance of protected material thanks to transparency of a coating. The fire retardant varnish provides coatings, which swell and increase their volume as the result of heat or flame and create a thick carbonized and porous layer. This perfectly isolates the covered material from the excessive rise of temperature and oxygen penetration and thus protecting flammable materials against thermal decomposition and in consequence against loss of mechanical properties. The solution is very effective as compared to conventional intumescent fire retardants. The performance of the coating is achieved by proper selection of carbonizing, foam-forming, dehydrating agents and modifiers, including very effective high dispersion components in nano scale. Application of modifiers in form of nanoparticles significantly improves the fire retardancy and thermal insulation effectiveness of the system. High degree of particle dispersion causes changes in decomposition processes as well as combustion of coating. In consequence, the time of carbonized layer formation is reduced, also the structure of carbon skeleton improved towards small-cell structure (this allows reducing the amount of system used and by this reducing the costs of protection). Intumescent system effectively protects wood and different wood derivatives (plywood, particleboard, high and low density fiberboard) in non-flammable degree, at only 250-350 g/m2 of the system applied. Forming an intumescent carbonized coating effectively protects materials against thermal decomposition by delaying ignition, reducing the amount and rate of released heat, effective heat of combustion, and mass loss rate, which are important in the initial phase of potential fire. The fire retardant and coating formed by this system does not emit toxic substances and poses no threat to the environment nor to human health. This allows for the system application in places permanently occupied by people. It can be used in different branches of economy, especially in construction industry (roofs, flat roofs, struts, beams, supporting structures, suspended ceilings, etc. in housing, public buildings, warehouses and on factory sites) and transportation. 436 INSTITUTE OF NON – FERROUS METALS IN GLIWICE (Instytut Metali Nieżelaznych) Organisation Contact Data 5, Sowińskiego st., 44 - 100 Gliwice, Poland phone: +48 32 2380 200 fax: + 48 32 2316-933 e-mail: [email protected] http://www.imn.gliwice.pl/ Institute of Non-ferrous Metals in Gliwice would like to present its interest in establishing a wide cooperation in the area of research and technology transfer with the countries of South East Asia. The Institute of Non-Ferrous Metals in Gliwice (IMN) is the main research and development centre of Polish non-ferrous metals industry, of a very wide scope of activity covering processing of non-ferrous ores and other mineral materials, pyro- and hydrometallurgical processes of metals recovery from ores and concentrates as well as recovery of by-product metals, waste treatment and utilisation, new alloys and composites, processing of metals and alloys, environmental protection, analytical chemistry of metals. The Institute provides services in most areas related to non-ferrous metals (such as Cu, Pb, Zn, Al, Mg, Ag, Re, Se, Co) production and application, such as development of technologies for enrichment of a wide range of materials, especially non-ferrous ores, coal, waste and secondary materials; pyrometallurgical processes of metals production from ores, concentrates, scrap and waste; hydrometallurgical technologies for production of primary metals as well as by-products metals; basic and applied research into new metallic materials and composites, such as amorphous and nanocrystalline soft magnetic materials and intermetallic compounds; development of new technologies for production of cast, rolled, extruded and drawn products from metals and alloys; as well as research works and application studies into manufacturing, modernization and testing of primary batteries, rechargeable batteries and fuel cells. The Institute produces also specific machines and equipment, including automated flotation machines of various sizes for non-ferrous ores enrichment, of cell capacity up to 100 m3. The range of the products offered by IMN covers also small batch production of modern products (sintered metal filters, electric contacts, welding dies, brazing alloys, soft magnetic, amorphous and nanocrystal cores, Cu and Ni based amorphous alloys), certified reference materials for spectroscopic and chemical analysis, lead alloys, zinc compounds and water purificators, etc. In our opinion cooperation between our Institute and partners from South East Asian region could be fruitful for both parties and we are ready to start discussion on the possibilities and scope of potential cooperation. 437 INSTITUTE OF NUCLEAR CHEMISTRY AND TECHNOLOGY (Instytut Chemii i Techniki Jądrowej) Organisation Contact Data 16, Dorodna st., 03 - 195 Warsaw, Poland phone: +48 22 5041220, +48 22 5041000 fax: + 48 22 8111917, + 48 22 8111532 http://www.ichtj.waw.pl/drupal_eng/ Institute of Nuclear Chemistry and Technology (INCT), located in Warsaw, Poland, is an interdisciplinary institute started in 1983. General director is Prof. A.G.Chmielewski. The INCT is Poland’s most advanced institution in the fields of radiochemistry, radiation chemistry, nuclear chemical engineering and technology, application of nuclear methods in material engineering and process engineering, radioanalytical techniques, design and production of instruments based on nuclear techniques, environmental research, cellular radiobiology, etc. It has 270 employees , including 15 professors, 13 associate professor; 56 senior scientists (Ph. D) and 21 Ph. D. Students. The Institute is listed in the category I of scientific institutions group in accordance to the Ministry of Science and Higher Education The results of work at the INCT have been implemented in various branches of the national economy, particularly in industry, medicine, environmental protection and agriculture. Basic research is focused on: radiochemistry, chemistry of isotopes, physical chemistry of separation processes, cellular radiobiology, and radiation chemistry, particularly that based on pulse radiolysis method. With its nine electron accelerators and 3 Co-60 sources in operation and with staff experienced in the field of electron beam application, the Institute is one of the most advanced centers of science and technology in this domain. The Institute has four pilot plants equipped in six electron accelerators: for radiation sterilization of medical devices and transplantation grafts; for radiation modification of polymers and semiconductors; for removal of SO 2 , NOx f and VOCs from flue gases; for food hygiene. The electron beam flue gas treatment in EPS Pomorzany with the accelerators power over 1 MW is a biggest radiation processing facility ever built. The Institute trains many of IAEA’s Fellows and plays a leading role in agency regional projects. Because of its achievements, the INCT has been nominated the IAEA’s Collaborating Centre in Radiation Technology and Industrial Dosimetry (www-naweb.iaea.org/na/collaboratingcentres.html). The INCT has begun the implementation of several projects in the program “Innovative Economy” POIG, granted on the basis of high evaluation of the Institute’s achievements. The mission of the INCT is the implementation of nuclear energy for social development, health and environmental protection. The Institute represents the Polish Government in Euroatom Fuel Supply Agency, in Fuel Supply Working Group of Global Nuclear Energy Partnership and in Radioactive Waste Management Committee of the Nuclear Energy Agency (Organization for Economic Cooperation and Development). Scientific Council has rights to grant D.Sc. and Ph.D. degrees in the field of chemistry,and the Institute carries out third level studies (doctorate) in the field of nuclear and radiation chemistry. The INCT also is editor of the international scientific journal “Nukleonika” (www.nukleonika.pl) . 438 INSTITUTE OF PRECISION MECHANICS (Instytut Mechaniki Precyzyjnej) Organisation Contact Data 3, Duchnicka st., 01 – 796 Warsaw, Poland phone: +48 22 560 26 00 fax: + 48 22 663 43 32 e-mail: [email protected] http://www.imp.edu.pl/impgb.html Institute of Precision Mechanics, one of the oldest and best known Institutes in Poland, is a research and development centre, focussed on methods of improvement of metal products by enhancing their corrosion resistance and raising their mechanical properties, especially fatigue strength, and wear resistance in service processes involving friction. The Institute conducts scientific and technical research, the aim of which is first of all the development of new technological methods, as well as commercial service and implementation activity. 439 The Institute offers, among other, the following: methods of mechanical and chemical preparation of surfaces for deposition of protective coatings, along with equipment and chemicals methods of depositing of electroplated, varnish, thermal spray and immersion metallisation-type coatings and chemicals for their deposition methods of heat and thermo-chemical treatment of tooling and machine components, as well as accomplishment of these processes on a semi-technical scale work in the field of material strength, including, among other, fatigue and friction testing and measurement of stresses cleaner production methods, recovery of raw materials, methods of wastewater decontamination in surface treatment of metals An integral part of the Institute is the Scientific Council which has the necessary authorisation and confers degrees of Doctor of Technical Sciences in the field of materials engineering. Within the scope of its activity, the Institute cooperates with the industry since many years. Among the big industrial plants, the following should be mentioned here: Z.M. Tarnów, HSW Stalowa Wola, WSK Rzeszów, Z.M. Siemianowice Śląskie, MESKO S.A. Metal Works, Radom Arms Factory, Z.M. „BUMAR-ŁABĘDY” S.A., Z.M. „NOWA DĘBA”, Warsaw Mechanical Works “PZL-WZM”, PZL – WOLA S.A. Mechanical Works and the Warsaw Radio Factory “RADWAR”. The Institute cooperates very closely with Polish research centres: technical universities, institutes of the Polish Academy of Sciences and industrial research institutes. Within this scope of cooperation, the Institute conducts shared research and markets own intellectual property and products. Such cooperation is carried on with, among other, Warsaw Technical University, Poznań Technical University, Gdańsk Technical University, Mining and Steelmaking Academy, the Institute of Fundamental Technical Problems of the Polish Academy of Sciences, Electrotechnical Institute, Industrial Institute of Automation and Measurements, Institute of Nuclear Problems, Institute of Electronic Materials Technology, Częstochowa Technical University, Silesian Technical University, Military Technical Academy, Institute of Service Utilisation Technology, Institute of Physical Chemistry of the Polish Academy of Sciences. 440 International cooperation is carried out by research collaboration, as well as by direct sale of own developed methods, equipment and services. Special emphasis in international cooperation is placed by the Institute on technical research collaboration, accelerating and raising the level of research carried out. Currently, the Institute cooperates with several research centres and laboratories of big industrial plants, among other with the Technische Universität (Chemnitz, Germany), Helsinki University of Technology (Helsinki, Finland), Instituto Superior Technico (Lisbon, Portugal), Technical University (Lyngby, Denmark), Institute of Materials (London, UK), Commissariat à l'Energie Atomique (Fonteney-aux- Roses, France), University of Southern California (Los Angeles, USA), Pye Metallurgical Consulting Inc. (Meadville, USA), Nitrex Metal Inc. (Québec, Canada), National Institute of Aviation Technology (Moscow, Russia), Karpenko Physico-Mechanical Institute UAS (Lviv, Ukraine), E.O. Patton Welding Institute (Kiev, Ukraine), Physical-Technical Institute National Academy of Science of Belarus (Minsk, Belarus) and other centres. The Institute coordinates or participates in major international programmes and research projects, among other in the "Education in Ecological Surface Finishing (TEMPUS JEP)", "Cleaner Technology and Eco – Management Transfer Programme for the Electromechanical Industry in Poland" (0160/Denmark), "UE Network of Integrated Scenario Analysis of Metal Coatings" (ISACOAT), "Model for Multi-pollutant Impact and Assessment of Threshold Levels for Cultural Heritage" (MULTI-ASSET) as well as in the Visegrad Programme "The Improvement of Safety and Equipment and Application of Corrosion Protection". The Institute presents its work by publishing articles in internationally circulating periodicals, such as "Journal of Materials Science", "Physico-Chemical Mechanics of Materials", "Materials Science and Technology", "Surface and Coatings Technology", "Galvanotechnik", "Transactions of the Metal Finisher's Association of India" and other, as well as in several domestic journals. Papers by scientists of this Institute are delivered at many international and domestic research and technical conferences. The Institute is itself the publisher of a technical-research quarterly "Inżynieria Powierzchni" (Surface Engineering), as well as monographical research materials, published in book form. The "Inżynieria Powierzchni" is a periodical encompassing all of Poland, which also publishes works by foreign authors. The monographic publications present, among other, habilitation (post doctorate ) dissertations by employees of the Institute. 441 The Institute very actively participates in international and domestic standardization activity. Employees of the Institute lead the ISO TC107/SC7 Sub-Committee: „Metal Coatings and other nonorganic – methods of investigation” and participate as experts in the proceedings of the ISO TC/156 Committee: “Corrosion of Metals and Alloys”, as well as the ISO TC35/SC12 Sub-Committee: “Paints and Varnishes – preparation of steel substrates for deposition of paints and similar products”. The Institute also sponsors three domestic technical Committees: KT-106 (concerning corrosion and corrosion protection), KT-262 (concerning heat treatment of metals) and KT273 (concerning mechanical security equipment. The Institute presents its achievements at international fairs and exhibitions, earning gold medals and other distinctions, among other at the International Innovations and Inventions Fair (e.g. in London, Nuremberg, Brussels, Seoul and Moscow). Taking part in domestic competitions, the Institute has repeatedly been awarded the prestigious title of Champion of Technology, the last time for „Development of multicomponent surface layer, resistant to wear and corrosion, obtained in conditions of glow discharge”. 442 1) GLOW DISCHARGE ASSISTED NITRIDING AND NITROCARBURIZING IN THE AUTOMOTIVE INDUSTRY – EXAMPLES OF PRACTICAL APPLICATIONS A brief description of the technology 1. INTRODUCTION The automotive industry in Poland is among the fastest developing recently. Fundamentally important for automotive components are quality, service life and enhanced user properties. Fulfilling these requirements in practice, given the need to limit manufacturing costs – depends to a great extent on surface engineering processes. These processes yield service properties for components made from different grades of steel, aluminum alloys, as well as titanium alloys, nickel alloys and more recently magnesium, working in conditions of corrosion, friction, wear and oxidation at elevated temperatures. Classical heat treatments, such as hot dip galvanizing, electrochemical and electroless deposition of metallic coatings, phosphating, chrome plating, electrophoresis, gas and vacuum carburizing processes, anodic oxidation or induction hardening are all widely used in the automotive industry. These processes have made possible the modern vehicle with among other features, a 12 year warranty on bodies, as well as longer life and better engine performance, largely due to reduction of friction in the power train. Surface engineering technologies are designed to control microstructure, chemical and phase composition, residual stresses, and surface topography of outer layers on treated components from the viewpoint of achieving the required service properties. Among these properties are wear and corrosion resistance, improved fatigue strength and heat resistance. Achieving such properties represents the most economical means of meeting requirements placed on structural materials, over on a wide range of operating conditions [1-10]. Such requirements are very often met by glow discharge treatments, including glow discharge nitriding and nitrocarburizing processes. These methods utilize non-equilibrium low temperature and non-isothermal plasma formed in conditions of glow discharge. The result of glow discharge nitriding of steel depends predominantly on process parameters such as: chemical composition of gas mix and its pressure within the reaction chamber, and on the location of the load: at the cathodic potential or in the plasma zone. These factors affect both the type of particles responsible for the formation of the surface layer, as well as the physico-chemical phenomena taking place at the interface of low temperature plasma and treated component. Phenomena such as cathode sputtering and chemisorbtion, in turn, affect the diffusion processes, controlled by the temperature of glow discharge nitriding. 443 Thus, the following factors have a fundamental effect on the results of glow discharge nitriding: Type of glow discharge, i.e. dc or high frequency (so called pulsed plasma) because in the latter case, there is a higher proportion of active nitrogen particles (atomic nitrogen, N+ and N2+ ions, as well as NH radicals) and, consequently a higher concentration gradient Location of the treated load at the cathodic potential bias or the plasma zone, which, in turn, determines the effectiveness of cathodic sputtering. Most effective is placement at the cathode potential [11-14]. By selection of the chemical composition of the nitrogen–hydrogen gas mix and type of electrical activation of the gaseous environment, it is possible to control the phase composition of the nitrided layers, their surface topography and microstructure, and in this way their user properties. Given the advantages of these processes, such as: Potential for treatment of components with complex geometry low consumption of electrical energy and reactive gases elimination of labour-intensive finishing treatment after the process full control of microstructure, phase and chemical composition, surface roughness and state of residual stresses in the layers formed, as well as their diffusion character possibility of treating diverse steel grades, including austenitic, at temperatures as low as 400ºC this treatment is increasingly widely used in the automotive industry. 2. APPLICATION EXAMPLES The advantages of glow discharge nitriding and nitrocarburizing be obtained under conditions of precise process control in which surface phenomena at the interface of reactive atmosphere – treated material and layer growth kinetics are controlled by selecting process parameters: temperature, time, pressure and atmosphere composition, as well as surface activation resulting from the phenomenon of cathode sputtering. Application possibilities may be extended by pulsed-plasma nitriding with higher frequency current [6]. 444 The new, improved version of the pulsed plasma process developed at the Institute of Precision Mechanics has global potential. It was first applied in 2006 at the AMP Paradowscy SJ company in Ursus/Warsaw, Poland. The equipment was developed along with the process (Figs. 1 and 2). Fig. 1. General view of equipment for glowdischarge nitriding of valves Fig. 2. Pulsed-plasma nitrided automotive valves The output of the installation is 6 thousand valves per 24 hours (ca 1.2 million pieces annually). The equipment is designated for nitriding automotive valves using glow discharge generated by pulsed plasma. Performance tests on the valves have shown that this method offers increased service life for the valve seat and stem and prevents the formation of carbon deposit in the seat zone. Fig. 3 shows the microstructure of the nitrided layer formed on automotive valves. These valves are characterized by good corrosion and wear resistance [9]. The method, by comparison with processes previously carried out at the same plant, i.e. chromium plating and salt bath nitriding, is superior also from the standpoint of workplace safety; it is environmentally friendly. 2 11 2 Fig. 3. Microstructure of nitrided layer obtained on automotive valves by pulsed-plasma nitriding. Magn. 250 X. Nitrided valve X45/X53 – place of welding: 1 – valve made of martensitic steel H9S2 – surface hardness HV after nitriding – 1020 HV0.2, thickness of layer – 24 µm; 2 – austenitic steel 21-4N – surface hardness HV0.05 after nitriding - 890 HV0.2, thickness of layer – 12 µm 445 A typical example of the use of the ferritic nitrocarburizing with plasma is the camshaft for the DAEWOO 1.6 GLI engine. Previously, the process was induction hardening using 10kHz generators. The depth of hardening was 3 to 7 mm on the cam lobe and on the opposite side (taking into account stock for finish grinding). The hardness was 47 HRC and 52 HRC, respectively. Induction hardened camshafts were used in engines with mechanical cam follower control (to limit play). Fig. 4. Equipment for glow-discharge nitrocarburizing of camshafts at DAEWOO (a) and view of camshafts for one load of 140 pieces for nitrocarburizing treatment Improvements to engine design using hydraulic cam followers and multi-point injection of fuel produced the need for a method which would ensure the formation of layers with improved tribological properties. For this reason, the ferritic pulsed plasma process, meeting all the above requirements, was selected [10]. The method was awarded a First Degree Award by the RS-NOT Organization in the ‘Master of Technology’ competition in Warsaw in 1999. From investigations carried out in actual industrial service conditions it follows that the surface hardness of layers formed of the order of 500 – 560 HV1 has a significant effect on wear properties. Special equipment was developed and built for pulsed-plasma ferritic nitrocarburizing process on camshafts (Fig. 4). The next example of application of ferritic glow discharge nitriding of cast iron components is cylinder liners for high compression engines (Fig. 5) which, after a road test of 100,000 km, showed less wear than chromium-plated liners. It should be added that in the case of cast iron, besides good wear resistance, nitrocarburized layers ensure resistance to seizure in conditions of insufficient lubrication [15]. Fig. 6 presents the installation designed by IMP for glow discharge nitriding of crankshafts, at the Diesel Works in India; Fig. 7 shows the microhardness profile [15] 446 Fig. 5. Cylinder liners for automotive engines after glow-discharge nitrocarburizing (a) and microstructure of layer produced on W1C grade cast iron (b). Magn. 200 X. Hardness after nitrocarburizing - 600HV1 Fig. 6. Equipment designed by IMP for glow-discharge nitriding of crankshafts Fig 7. Crankshafts made of 25H3M grade steel after glow-discharge nitriding (a), microstructure (b) and hardness profile (c) in nitrided layer; hardness after glow-discharge nitriding - 600HV10. Magn. 200 X. 447 Fig. 8. Examples of nitrided piston rings Fig. 9. Examples of nitrided layers produced on piston rings by glow-discharge nitriding . Magn. 100 X Fig. 10. Effect of reactive atmosphere pressure on microstructure of layers produced on piston rings made of ductile cast iron, grade S-14 by glow-discharge nitriding. Process parameters: a – temperature - 480 C, treatment time - 6 hours, pressure 1.7hPa, b – temperature - 480 C, treatment time - 6 hours, pressure – 2.5hPa 448 Another application example of the glow discharge nitriding process is piston rings. This method is competitive with the currently used chromium plating, because the layers formed are characterized by good wear and corrosion resistance, as well as meeting the requirement for surface roughness [16]. Moreover, the relatively simple possibility of local (selective) nitriding, achieved through masking, proved to be an effective means of avoiding deformation of piston rings with special shapes. Fig. 11. Glow-discharge nitrided gear wheels made from grade 31CrMoV9 steel for electric locomotives produced by General Electric (Germany). Photograph taken at AMP Paradowscy S.C. in Kunowo Twardość HV1 1000 800 600 400 200 0 0 0,1 0,2 0,3 0,4 0,5 0,6 0,7 0,8 Odległość od powierzchni [mm] Fig. 12. Microstructure and hardness profile of glow-discharge nitrided layer. The layer was produced on a gear wheel made from grade 31CrMoV9 steel. Equipment for the treatment was developed and built by IMP, installed in the AMP Paradowscy S.C. plant 449 Figs 8 and 9 show nitrided piston rings, and Fig. 10 their microstructure. The next example of application of the glow discharge nitriding method is gear wheels (Figs. 11 and 12). [17]. 3. FINAL REMARKS The scope for glow discharge nitriding and nitrocarburizing is broadening. The processes also constitute the basis of future hybrid processes, combining these processes with other surface engineering methods. This will give the treated material unique properties, such as resistance to oxidation at elevated temperatures, thermal shock and overloading, as well as reduction of the coefficient of friction [16-18]. Such properties are important in, among other things, engine components, exhaust systems and power trains, i.e. those working in extreme conditions. A significant challenge to broader application of the technology is the enhancement of resistance to contact fatigue (pitting), especially in the case of gears. Intensive investigations in this field are being conducted at the Institute of Precision Mechanics. 450 2) PEEN–IMP - new shot peening technology and device for ceramics and metals with high hardness surface layers A brief description of the technology The main aims of the PEEN-IMP technology and device invented in Institute of Precision Mechanics were the reduction of exploational costs of shot-peening process and the widering of fields of application of shot-peening process on hard materials such like ceramics, high hardness steels, steel elements coated by hard PVD and CVD layers. Basic ideas of the PEEN-IMP technology - worked surface is placed inside of upper part of the closed working chamber is treated "from underside” by strong stream of mixture of air with shot, shot after realization of work falls down because gravitation and it mixes again with stream of air, mixing process of particles (crumbled shot or powder) with stream of air follows in lower part of working chamber, stream of air and shots has vertical direction "from down to top” and moreover a stream is introduces into circulated movement, the most profitably into movement on a cone surface. It is possible to introduce additionally powders of some chemical elements refining treated surface to the working chamber, also in form of liquid solutions. Shot-peening process under the PEEN-IMP technology in comparison with actual well known processes marks considerable shortening of shot return road to circulation, 200-250 times decrease of required quantity of shots, 50-times decrease of a level of required pressure (even to 0,05 Mpa), use of powders (considerably smaller from shot), also in form of liquid solution. The decrease of required quantity of shot allowed the use of expensive bearing balls and other expensive shots e.g. sintered carbides and tungsten. 451 3) The technology of the vacuum brazing of the “ honey comb” seals in gas directing apparatuses of aircraft engines A brief description of the technology The technology of the vacuum brazing of seal rings in form of a "honey comb” to the internal surface of gas directing apparatuses applied in the most modern aircraft engines is the object of the invention. These elements works in changed thermal tension and mechanical conditions, as well as in atmosphere of corrosive gases. They are also exposed onto constant long-lasting dynamic burdens. Directing apparatuses are produced in a form of very precision casts from nickel based alloys consisted from body and blades. The “honey comb” seals are used as the seals between gas directing apparatus and shaft because very responsible character of work – they are ones of the most modern solutions. The seals are made from the Hastelloy alloys with the structure of a "honey comb” – they are soldered perpendicularly by edges of individual cells to cylindrical surface of apparatus. About complexity of problem testifies the fact, that in distinction from typical soldered connections, in which the joint is a flat surface, in this case the solder among two different alloys on the nickel base can be compared with the simultaneous brazing of thousands' thinwalled capillary tubes. The worked out technology concerns by productions of joints by of solders Ni-Cr-B -Si in form of tapes and pastes produced from powders with a suitable adhesive and it consists from following technological processes. nickel-plating of apparatus bodies; spreading of solder; tacking of the “honey comb” seals with apparatus body before the brazing; vacuum brazing; cleanings of surface after brazing; quality control The working out technology for serial production makes a possibility to obtain high quality products fulfilled the conditions defined by air-equipment users, with a retain of criterion of minimization of defects in production process. 452 4) Nanocrystalline Cobalt Alloy Plating for Replacement of Hard Chrome A brief description of the technology The present invention relates to the pulsed electrodeposition of nanocrystalline cobaltphosphorous(nCo-P) coatings, as a viable alternative to electrolytic hard chrome plating. This technology uses pulse plating to control the nucleation and growth of grains within the coating, creating a nanocrystalline structure. The nCo-P coating application does not cause hydrogen embrittlement of high-strength steels, which is a significant problem with electrolytic hard chrome plating. Performance testing showed that the nCo-P coatings demonstrated superior salt fog corrosion behavior compared to the hard chrome coatings. As a result of Hall-Petch strengthening, nCo-P alloys display significant increase in hardness relative to their coarser grained counterparts due to their ultrafine grain size. A further increase in hardness, can be obtained by annealing the as-deposited coating to induce the precipitation of cobalt-phosphites from the supersaturated solid solution at elevated temperatures. The process is non hazardous and produce stable coatings free of hexavalent chrome. It meets the requirements of ELV, RoHS and WEE directive. An application of the invention is recommended particularly for automotive and aerospace components 453 5) WibroTermoFluid® - fluidal heat treatment method A brief description of the technology The method of the fluidal heat treatment of metal elements is the subject of invention (patent application in Patent Office of Poland under Nr P-392916 since 2010.11.10). There are known methods for heat treatment of metallic elements, which consist of fluidization of heated, granular and chemically inactive bed with the technologica atmosphere. Such way requires the use of large quantities of technological atmosphere for fluidization, several times larger quantities of technological atmosphere, than it would be necessary to perform only the treatment alone. This is the reason of high production costs. . The purpose of this invention was to develop the way to perform treatment with reduced costs, through decrease of the usage of technological atmosphere. The core of fluidal heat treatment, according to our invention, consists of fluidization of granular, heated and chemically inactive bed with technological atmosphere in the retort, which is elastically mounted, mostly vertically, and subjected to mechanical vibrations of specified amplitude and frequency. Performed tests have shown that with optimal choice of strings and vibrations amplitude and frequency, the consumption of technological atmosphere decreased to 50% without the decrease of treatment's quality. This lessened quantity of technological atmosphere would not be enough to fluidize the bed by itself, but is enough to fulfill the needs of heat treatment process. This treatment method, according to our invention may be used interchangeably with the old method in technologies of fluidal heat treatment. 454 6) Nanostructured Co-P coating as a diffusion barrier in electronics A brief description of the technology The invention relates to the preparation of cobalt alloy electroplanting coatings with phosphorus using the method of galvanic current pulse. Depending on the characteristics of the current deposition is possible to obtain coatings of amorphous or nano-structure ( 5 to 20 nm). They provide excellent diffusion barrier under gold coating used in electorinc circuits utilized especially at elevated temperatures (above 200oC) which allows their use in automotive, military and aerospace characterized by electronic components operating temperatures to 400oC. Co-P (2 – 8% of the masses) coatings exhibit better barrier properties than those used Ni-P coatings in both SnPb solders and leaf free. SnAgCu solder contact angle for the Co-P coatings is three times smaller than the Ni-P coatings. Co-P/Au immersion coatings exhibit lower diffusivity of lead-free solders and the absence of intermetallic compounds, which greatly improves the performance of connections. Corrosion tests in nitric acid vapor shower a good resistance coatings Co-P/Au-Co already at small thickness, respectively 0.1 and 0.3 um Au-Co, which indicates the possibility of such a multilayer coating to cover the pins and contacts, especially with due to the high hardness of the Co-P coatings at elevated temperatures and similar to the Ni-P coating, ductility which would significantly reduce the thickness of the gold coating. 455 7) Nickel-Tungsten Alloys as Protective Coatings for Glass Moulds A brief description of the technology Application of rationally selected protective coatings for glass moulds is remarkable method of production yield increasing, particularly if small dimensional tolerances and increased surface quality of product are required. These necessities concern significant part of glass manufacturing branch e.g. lightweight containers, optical devices, colour picture tubes, displays, vacuum accessories, glass insulators. Within required physical and mechanical properties of coatings the most important are abrasive wear resistance, high temperature resistance, ability of appropriate heat extraction from the product and ability of proper and reasonable surface finishing Only specially designed permanent coatings may be applied in such a case. Structure stability, high ductility, high cathodic electrochemical potential and thermal anisotropy which prevents from rapid heat extraction outside regions of warmest glass there are ideal features of such a coating. It was found that Ni-W alloys of 20-40 wght% of tungsten content have excellent mechanical, thermal and chemical characteristic which let use them as protective coating for various purposes and exclusively for glass panel plunger application. Studies the Ni-W alloys electroplating process shown that satisfactory results of treatment on a industrial scale may be reached applying the bath of high content of hydrocarboxyl acids /particularly citric acid/ with high tungstenes content which lessens the coating hydriding. Stable process of electroplating is gained by soluble nickel anodes implementing and less than usually applied acidity of the bath /pH 3.8-5.5/.This modified plating technology of plunger has been applied in practice Independent research of Ni-W alloys considered for other specialized applications /MEMS, LIGA processes, catalysis, shielding gaskets/ indicate low coating surface attraction to environmental impurities in hot work conditions. 456 INSTITUTE OF SECURITY TECHNOLOGIES MORATEX (Instytut Technologii Bezpieczeństwa) Organisation Contact Data 3, Marii Skłodowskiej-Curie st., 90-965 Łódź, Poland phone: +48 42 637-37-63 fax: + 48 42 636-92-26 e-mail:[email protected] http://www.moratex.eu/en/ Institute of Security Technologies MORATEX in Łódź exists since 1953. It develops modern designs and technologies of textile technical goods and implements them to the industry. In 90s the R&D workload has been moved towards developing of personal life and health protection means for individuals exposed to threats from bullets, fragments, impacts, harmful chemical or biological agents and unfavourable factors, as fire, temperature, water etc. The works focused mainly on solutions related to technologies dedicated for services subordinated to the Minister of Interior and Administration and to Minister of National Defence. Since 1999, according to the decree of Prime Minister, the Institute is the R&D body supervised by the Minister of Interior and Administration. Starting with that moment all the effort of the Institutes management and employees is driven to satisfying the expectations and requirements of the Police, Fire Service, Border Guards and The Government Protection Bureau. Executing the tasks set, with co-operation with those services, MORATEX developed in 20012006 new and modern uniform assortment, equipment and means of individual protection. The quality management system, compliant to the requirements of the Standards: PNEN ISO 9001, PN-N 19001 has been implemented to the Institute and confirmed by certificate from The Polish Centre for Testing and Certification. The Institute has been awarded the Notified Body position by the European Committee within the scope of directive 89/686/EEC – Personal Protective Equipment, ID No. 1475. The quality of newly-developed goods is confirmed by the certificates from accredited Certifying Bodies, including: CIOP, WITU, CNBOP. The Products Certification Department works at the Institute, to issue certificates of conformity of the products offered by the suppliers of textile protective goods and uniform elements. High level and modernity of material, technical and design solutions of developed products, are proven by positive opinions of end users as well, as the medals and awards from both domestic and international organisations. The novelty of scientific and technological 457 solutions is confirmed by the protection rights assigned by the Polish Patent Office. The Institute has gained more than 100 patents and more than 140 utility model reservations. www.moratex.eu 458 Key Project WND-POIG.01.03.01-10-005/08 „Modern ballistic body armours and covers for transportation means as well as for buildings, made on a basis of textile composites” Realisation: 01.09.2007 – 30.06.2012 Project Value: 12 940 000 PLN European Union Fund: 10 999 000 PLN The Key Project is realised within the frame of INNOVATIVE ECONOMY, NATIONAL COHESION STRATEGY 2007-2013, Priority 1 - Research and development of new technologies, Axis 1.3 Support for R&D projects for entrepreneurs carried out by scientific entities, Subaxis 1.3.1 Development projects. http://ergobal.poig.eu THE COMPONENTS DEVELOPED: 7 variants of ballistic inserts for bullet- and fragment-proof vests Ballistic resistance Ballistic resistance according to Type of ballistic panel according to PN-VPN-V-87000:2011 Standard 87000:1999 Standard Composite K2 , K4 K3/A [7,62x39mm; PS; 720±15 m/s] K3/A [7,62x39mm; PS; 720±15m/s] Ceramic & Composite K2 , K4 , K3/B [5,56x45mm; SS109; of type I resistance to SS109 bullet 950±15m/s] K3/A [7,62x39mm; PS; 720±15m/s] Ceramic & Composite K2 , K4 , K3/C [7,62x51mm; FMJS; of type II resistance to 54R bullet 840±15m/s] K5/A [7,62x51mm; AP; 820±15m/s] THE PROTOTYPES DEVELOPED: 3 prototypes of bullet- and fragment-proof vests 2 prototypes of quick-release bullet- and fragment-proof vests; a prototype of two-part bullet- and fragment-proof vest (vest and hip belt). FINAL SOLUTIONS DEVELOPED: The bullet- and fragment-proof vest dedicated for the area of internal security. The bullet- and fragment-proof quick-release vest dedicated for the area of internal security. 459 Modular quick-release bullet- and fragment-proof vest dedicated for the area of internal security. Hybrid ballistic helmets Resistance to bullets as well as to fragments complies with PN-V-87001:2011 Standard. Helmet protects the head at front – above the eyebrows level, at sides – above the mid-ear level behind the cheekbone, and at back – above the occiput, for the V50 > 600m/s at the acceptable dynamic deflection (trauma) below 20 mm (class O3). Ballistic shield 7,62x51 308 Winchester FMJ at the bullet velocity of V=828±15 m/s; 7,62x39 AKM PS 43 at the bullet velocity of V=710+15 m/s. The Project realised within the frame of INNOVATIVE ECONOMY, NATIONAL COHESION STRATEGY 2007-2013, is co-funded in 85% by the European Union from the European Regional Development Fund and in 15% by the Polish Ministry of Regional Development. CAMOUFLAGE TEXTILE MATERIALS One common title „Camouflage textile materials” covers the following material and design solutions submitted for protection to the Patent Office of Republic of Poland: W.120169 „Camouflage woven fabric” and P.396078 „Antistatic openwork knitted fabric”. They are products made with methods: weaving and knitting. They are dedicated for masking men and their individual equipment under visible, IR and radar spectra. The properties originate from proper both qualitative and quantitative selection of compound materials i.e. basic yarns (background material) and conductive yarns (with due share of metal and soot). The design itself of each material is no less important to reach specified properties. The application of optimum weaving and knitting pattern allows for suitable arrangement and deterioration of each yarns group on the surface of final product i.e. fabric/knit. An extra trump of the materials is low weight, rare among such products full of functionalities, masking men and their individual equipment. The camouflage textile materials, have been developed within the frame of Key Project no. POIG.01.03.01-00-006/08 co-financed from the funds of European Regional Development Fund under Operational Programme Innovative Economy. PROTECTIVE VEST The vest protects against small arms bullets, fragments, knife, needle and stab according to: bullet-proofness class 3 according to PN-V-87000:1999 Standard „Light ballistic armours. Bullet- and fragment-proof vests. General requirements and tests.”, 460 knife- and stab-proofness class 1 according to procedure PBB-08:2006 ITB „MORATEX” „Impacting tests. Determining the resistance of personal armour to an edge – procedure compliant with NIJ STANDARD 0115.00 needle-proofness class 2 according to procedure PBB-12:2008 ITB „MORATEX” „Impacting tests. Determining the resistance to puncture with needle” Due to its innovative design, the vest features ergonomic shape which allows for easy adjustment to the wearers silhouette. An interesting solution is disjoint, yet durable way of fastening the vest on shoulders which prevents undressing the officer by an attacker. A special way of joining two elements of back belt and mounting it on back part of vest was introduced. It is a system of thin ropes, holes, technical bands and metal frames. Whole vest is covered with MOLLE band system MOLLE. The protective vest was submitted to Patent Office of Republic of Poland, to gain the protection rights for utility design, application no. W-119599, dated 22.12.2010. Weight of L-size vest is ca. 6.6 kg. 461 METAL FORMING INSTITUTE (Instytut Obróbki Plastycznej) Organisation Contact Data 14, Jana Pawła II st., 61 – 139 Poznań, Poland phone: +48 61 657 05 55 fax: + 48 61 657 07 21, e-mail: [email protected] http://www.inop.poznan.pl/?set_language=en The Institute performs research, development, implementation works and participates in domestic and international projects on non-metallurgical metal forming. The Institute has well experienced and creative staff backed with advanced computer systems, modern scientific and research facilities. High quality of the research and development works is ensured by the Quality Management System conform with ISO 9001:2008 and the Accredited Investigation Laboratory meeting the requirements of PN-EN ISO/IEC 17025:2005. The Institute’s scope of activity includes: innovative technologies, machines, devices and tools for: net shape forging, orbital forging, extrusion, forging by the TR method, stamping, spinning and flow forming, forming of precision metal powder parts, including the application of nanotechnology, mechanizing and automating devices, special centres and production lines, computer designing, modelling and simulation of processes and tools, research of metal structures and properties, heat and thermochemical treatment, standardization activity, scientific and technical information – databases, publications, among others, “Metal Forming” periodical, assessment of machine and device conformance, consulting, training and promotion activity, manufacturing of prototype machines and devices, manufacturing of parts by the metal forming methods. 462 Achievements of the Institute: licences sold to many countries of the world, hundreds of modern technologies, machines and devices implemented in industry, many publications and patents, both in Poland and abroad, many individual and team prizes, awards and medals, membership in important scientific organizations and networks, status of the Centre of Excellence of the Metal Forming Institute. The Metal Forming Institute offers: elaboration and implementation of technologies, design, execution and implementation of devices, machines and tools for metal forming processes, investigation of technologies, devices, machines and tools, investigation of metal structures and properties, technical consulting. The Institute participated and coordinated many EU and nationally funded projects like: Framework Programme funded projects (FP5, FP6, FP7) like NANOMINING, EUREKA funded projects like NEGFORT, projects within the Innovative Economy Programme (POIG) like I-Centrum, NANOMET, development projects, Institute’s own research projects. 463 1) NANOMINING Nanomining is a project dedicated to the development of new nanocomposites using materials from mining industry The NANOMINING Project is carried out within 7th Framework Programme of the European Commission within joint EU-Mexico call Adding Value to Mining at the Nanostructure level, NMP Program Priority: NMP.2010.1.2-4. Project background: Silver nanoparticles and silver based nanostructured composites are being frequently used in a variety of biomedical and industrial applications, such as an antimicrobial agents, lead-free solders, electric contact materials, gas-sensitive sensor, etc. The most complicated Silver using problems to be considered in the Project are: recovery of silver from ore waste materials; the controlled synthesis of metal nanoparticles of well-defined size, shape and composition; nanoparticles incorporation to desired implant surfaces synthesis of Silver based nanostructured composites for industrial purposes. Project goals: The main goal of the Project is to develop: Clean and efficient procedure of silver recovery from waste: Combined Mechanical Activation – Thermal Oxidation Processing of jarosite type residues to alleviate and accelerate the following precious metal leaching; Combined nanotechnology of biological synthesis (using Mexican plants) of Ag nanoparticles and its deposition on implant surfaces by electrophoretic, spraying and other techniques; Nanostructuring technology of Silver based nanocomposites manufacturing for electrical contact applications. Pilot production and trials of developed Ag nanoparticle modified implants and Ag based nanostructured composites: Hydroxyapatite Ca10(PO4)6(OH)2) coated implants which are widely used in orthopaedic surgery because of their good biocompatibility related to the osteoconductive properties of calcium phosphate coating; 464 Ag-SnO contacts for electrical systems; these composites combine high resistance to welding and to electric arch erosion of the refractory phases with the high electric and thermal conductivities. Currently, IT infrastructure of the Institute is modernized, as part of the project entitled “ICenter” – computer centre for managing research processes in the Metal Forming Institute in Poznan, implemented under the Operational Program Innovative Economy 2007-2013, Priority 2 Infrastructure of R&D. In the “I-Center” project, a computer center for managing research processes in the Metal Forming Institute in Poznan is created. The project aim is to create an innovative ICT infrastructure, fostering the development of the Institute by supporting the management of research projects and a wide sharing of results for scientific, research, economic and educational purposes. The Project will result in consolidation of resources and structures of managing research processes, utilizing the available human resources, research equipment, repository of knowledge and the creation of an informational service platform. Certificate ISO 9001:2008: In the Metal Forming Institute a Quality Management System according to ISO 9001:2008 is applied (certificate GDK0003185 Lloyd’s Register Quality Assurance Limited– LRQA). The System is applicable to design of manufacturing processes, machines, installations and tools for metal forming and research works. Manufacture of parts by metal forming methods. Collecting, processing and distribution of scientific and technical information. INOP possesses a testing laboratory designed to fulfill metal forming industry needs, certified by the Polish Centre of Accreditation PCA (Certificate AB 105, expiry date 12.01.2015), performing its activities in accordance with norms PN-EN ISO/IEC 17025:2001 and ISO 9001:2008. Prizes and awards: Diplomas of the Minister of Science and Higher Education for the Metal Forming Institute for projects awarded with medals of the 4th and 5th International Warsaw Innovation Show, IWIS 2010 and IWIS 2011: Method for manufacturing of nanocomposite graphene-like greases and unit for manufacturing of nanocomposite graphene-like greases and unit for manufacturing nanocomposite graphene-like greases- Gold Medal with distinction Method for hemming of sheet metal products, especially thick ones, and unit for hemming of sheet metal products, especially thick ones- Gold Medal Unit for surface treatment of top layers, especially of metal- Silver Medal. 465 Method for stamping shaped elements of metal sheet and unit for stamping shaped elements of metal sheet- Gold Medal Method for the modification of top layers of working surfaces of machine parts- Silver Medal Method for increasing the strength properties of bearing sleeves and unit for increasing the strength properties of bearing sleeves- Silver Medal Protection of the inventions is provided due to the realisation of the project entitled “Protection of industrial property in the scope of manufacturing and introducing graphene-like particles” included in the Innovative Economy Programme, Sub-action 1.3.2, Support of the protection of industrial property created by scientific entities as result of R&D works. The promotion emblem, “Now Poland” of the fourth edition of the “Now Poland” (‘Teraz Polska”) competition for innovative ventures, for the solution, “Innovative numerically controlled MWS-700 machine for rotary forming of complex parts of machines” implemented in FLAKT Bovent Ltd in Ożarów Mazowiecki. (Warsaw June 6, 2011) Award of the President of the National Economic Chamber „Innovatica” 2010 in the category of „ Innovative product – innovative technical or technological salution” for the Innovative technology of crimping the coupling ends of transmission shafts Gold Medal of International Fair Trade Poznan 2009, 2010 and 2012 in category: “Transfer of the scientific research findings into economic practice” for: „Technology and device for flow forming complex products of metal sheets” implemented in Flakt Bovent Sp. z o.o. (2009) „The technology of forming rings for flexible buffers” implemented in Więcborskie Zakłady Metalowe WIZAMOR Sp. z o.o. (2010) “Automatic line type UR 291 for manufacturing the front beam of railway wagon trolley together with an innovative technology of spatial bending” implemented in INTERMECH Ltd. in Stalowa Wola (2012) A prize in the category of "Technology of the Future" in the IV edition of competition, "Polish Product of the Future", organised in 2000 with the honourable sponsorship of the Prime Minister, for the elaboration entitled "New Technology of obtaining high density precision parts of powder alloy materials in mass production" Distinction in the category of invention in the field of product or technology economic prize of the Wielkopolska Region 2003 for the elaboration and implementation of production technology for high-density precision parts made of iron matrix alloy powder materials for the demands of automotive, machine and other industries". 466 2) Rotary forming of axisymmetrical parts The Metal Forming Institute offers elaboration and implementation of rotary forming technologies and machines. The methods of rotary forming of products on a rotating templet by means of roll are spinning and flow forming. Manufacturing single parts or short production series by traditional stamping is often very expensive. Manufacture of the same element by methods of rotary forming is much quicker than stamping and the tooling cost is much lower. The technologies of rotary forming allow for manufacturing high quality axisymmetrical parts with high productivity. Spinning and flow forming are performed on special machines - spinning machines and flow forming ones. Lathes can also be adapted for the realization of spinning and flow forming processes. Spinning machines do not require large forces on the forming roll. Forming products with curved side walls and the application of complex radial-motions require very precise control of the spinning roll. Most often a hydraulic templet or computer control are applied. MWS 700 spinning machine Flow forming machines require the application of large forces, therefore their construction is adequately compact and robust. Flow forming is effected mostly on products with rectilinear side wall and, consequently, the control system is simpler. Elongating flow forming is superior to drawing with thinning in that it requires lower forces and the flow forming machine takes less room than a vertical press. On a flow forming machine, execution of a cone can be effected in one operation, while execution on a press requires at least several operations. Advantages of the products made by rotary forming: good dimensional accuracy, high surface quality, improvement of strength properties - in the case of flow formed parts, complex shapes of products. 467 Effects of implementation of the rotary forming technologies: reduction of labour intensity of production, reduction of material consumption, reduction of electric energy consumption, reduction of manufacturing cost. Parts made by rotary forming The spinning machine MWS 700 with innovative tool head is used for forming from metal sheets complex shaped products used for ventilation, air conditioning and cooling devices. The spinning machine with the technology was implemented in Fläkt Bovent company from Ożarów Mazowiecki and replaced the manufacture of products made so far from a few separate parts, welded afterwards. The machine meets the requirements of the Machine Directive 98/37/WE and the Low Voltage Directive 2006/95/WE (designation CE). The spinning machine MWS 700, together with the technology, has been awarded Gold Medal of the Poznań International Fair 2010 in the category of “Transfer of investigation results to the economic practice”, as well as the Polish Promotion Emblem, “NOW POLAND” 2011 for innovative undertakings. The invention used in the machine entitled: “Method for stamping shaped elements of metal sheet and unit for stamping shaped elements of metal sheet”, (no. patent application: P.389731, date: 1 December 2009r.), was awarded with Gold Medal of the IV International Warsaw Invention Show IWIS in 2010. The Metal Forming Institute offers: elaboration and implementation of rotary forming technologies, design, execution and implementation of machines for rotary forming, adaptation of lathes for spinning and flow forming, technical consulting. 468 3) Innovative technology and devices for plastic forming of the coupling ends of transmission shafts The Metal Forming Institute offers innovative technology and special devices, THC-17 and THC-19, intended for cold plastic forming of solid coupling transmission shafts applied in harvesters. The new technological process consists in forming the tube ends by the method of push broaching, in operations of the tube end diameter reduction and THC-17 device forming an end with hexagonal cross section. The devices work in the semi-automatic mode with a productivity of 6 pcs per minute. The devices meet the requirements of the Machine Directive 98/37/WE and the Low Voltage Directive 2006/95/WE (designation CE). The device for forming tube ends consists of a horizontal hydraulic press, a tube holder (to THC-19 device prevent buckling), a tube transfer feeder and an auxiliary table. The tubes are stored on a supply table from where they are taken by the operator and placed in the feeder paws. Next, they are moved by the feeder to the working zone of the individual operations and, after the process of end forming is completed, they are dropped to a container. The technology and devices, implemented in the production of coupling transmission shafts for harvesters manufactured by CNH Polska, Płock, have replaced production of shafts welded of a tube and two ends made by the methods of machining. Innovative technology and special devices, THC-17 and THC-19, are intended for cold plastic forming of solid coupling transmission shafts applied in harvesters. ● THC-17 device is intended for forming tube ends with the diameter of 38 mm and length of 2000 mm, in 4 operations. ● THC-19 device is intended for forming tube ends with the diameter of 76 mm and length of 2000 mm, in 6 operations. 469 Implementation of the technology and devices has resulted in: ● better dimensional accuracy, ● better smoothness of the shaft end surface, ● better strength properties and life time of the transmission shafts, ● higher productivity, ● less material consumption, ● less labour demand in production, ● lower manufacturing cost. Formed tube ends The technology and devices have been granted ”Innovatica” 2010 award of the President of the State Economic Chamber, in the category of “Innovative product – innovative technical or technological solution”. The Metal Forming Institute offers: elaboration and implementation of the technology, design, execution and implementation of the devices for cold plastic forming of the tube ends, technical consulting. 470 4) Forging crankshafts by the TR Method The common feature of the TR - Method is that the normal working stroke of a press is used to generate horizontal as well as vertical force. In this way, in specially designed TR forging devices, combined upsetting, bending and squeezing operation with simultaneous gripping of the bar enable such items as crankshafts to be formed. The devices are extremely simple, compact and versatile and can be installed on forging presses of capacity up to 100 MN. Advantages: - material savings, diminished labour consumption, high quality of forgings (i.a. proper grain flow), possibility of forging bigger crankshafts on relatively smaller forging presses . Crankshaft forging Licensees: Thyssen; Kloeckner; Krupp – Germany, Sulzer – Switzerland, Italsider – Italy, Forjas y Aceros de Reinosa S.A. – Spain, Endo Co; Japan Steel Works; K.E.F. – Japane, Wuhan, Forging Works – China, Hyundai – Korea, Alfing-Kessler – Germany, Ellwood – USA. The Metal Forming Institute offers: design, manufacture and implementation of forging devices elaboration and implementation of forging technology technical consulting licences. 471 5) Innovative metal powder parts forming technology Powder metallurgy is a highly developed manufacturing method of precision parts; the method consists in: mixing chemically pure or initially alloyed powders, die pressing and sintering of compressed parts in a protective atmosphere. This technology allows to obtain homogenous structure without defects and intermetallic intercalations. Metal powder parts Due to the application of the technology, the following effects have been obtained: high abrasive wear resistance, high abrasive strength, crushing strength and compressive strength of the product made, obtained product density up to 7.7 g/cm3 for iron powder parts, reduction of production energy consumption, possibility of forming parts with complex shape and parts working in hard exploitation conditions such as gears, possibility of application for products of any shape, any destination, particularly for ones of required high strength like gears, bearings, etc. Advantages of the technology: good mechanical and tribological properties of products, repeatable dimensional accuracy, elimination of finishing machining, high degree of raw material utilization, positive environmental impact, reduction of manufacturing cost. The technology has been awarded following prizes and awards: Award of the Wielkopolska Regional Authority in the category of “Invention in the field of product or technology of the Wielkopolska region economic prize”, Nomination to the economic prize of the President of the Republic of Poland in the category of “Invention in the field of product or technology”, Award in the 4th edition of the competition “Polish product of the future”, Award in the Stanislaw Staszic competition “Research and development entities for the economy and society”. 472 The technology can be applied for the manufacturing of the following products: parts of shock absorbers, sleeves, elements of pumps and brake systems for the automotive and aircraft industry, bearings, rings, racks, latches for the industry of household appliances, elements of locks for doors and windows for the building industry, machine elements, gears, spacing sleeves, bearing rings and others. The Metal Forming Institute offers: elaboration of the technology for manufacturing of products made of iron powders, a circular line for forming powder material sleeves with the outer diameter of up to 22 mm and height of up to 10 mm, technical consulting, short series production of iron matrix powder material parts. 6) Method for increasing the strength properties of bearing sleeves and unit for increasing the strength properties of bearing sleeves Increasing the strength properties of bearing sleeves in the process of surface layer modification with the use of pressure device, results in lower friction coefficient and prolongation of the sleeve working time. The process consists in modification of the inner layer of the bearing sleeve with solid lubricant nanoparticles, in most cases with graphene like molecules of molybdenum disulfide. The process is carried out in the PC-1 pressure device, which was designed, made and tested in the Institute. The modification process is based on infiltration of solid lubricant nanoparticles into the pores of a bearing sleeve made by powder metallurgy; the remaining particles form a lubrication film on the inner surface of the sleeve. Pressure device PC-1 for modification of the surface layer Impregnation socket of the PC-1 device Example of sleeve surface layer after modification process in PC-1 device 473 Effects of implementation: increase of durability and working life of bearing sleeves, decrease of friction coefficient, improvement of tribological properties, reduction of energy consumption and decrease of operating costs, possibility of application of bearing sleeves in extreme environment (aircraft or rocket engines), reduction of production and operating costs. The invention entitled: “Method for increasing the strength properties of bearing sleeves and unit for increasing the strength properties of bearing sleeves”, was awarded with Silver Medal of the IV International Warsaw Invention Show IWIS in 2010. 474 7) Surface Engineering and Tribology The Laboratory is concerned mainly with materials and machine parts research as well as biomaterials and implants material research. Materials and machine parts research The Laboratory carries out its materials land machine parts research Rusing the following control and measuring devices: Tribological tester T-10 Tribological ball-on-disc tester type. The device is used for assessing the tribological features of new materials used for gliding elements of machines, mainly thin sheaths. Using the T-10 device you can precisely examine the resistance for wear and the coefficient of friction of any material association working in gliding motion, depending on the speed of gliding, surface pressing and other factors. Tribological tester TWT-500N Own construction tribological tester used for research of dry friction of machine parts. This tribological tester is used for research in temperatures from room temperature to 600 0C. 475 Samples Tribological tester T-05 Device T-05 is used for research of tribological features of lubricants i.e. solid lubricants, oils, plastic lubricants as well as resistance to wear of materials used for gliding elements of machines. What should also be mentioned are: Device for hardness tests in elevated temperatures in Rockwell scale BT-G01 It allows for hardness measurements in HRA, HRB and HRC scale in temperatures up to 500 °C. The sample surface is protected from oxidation by protective gas blow in test chamber. Device for hardness and microhardness tests in elevated temperatures in Vickers scale BT-G02 It allows for hardness measurements in Vickers scale, with various loads, in temperature up to 500°C. The use of special clamps allows for small samples testing. Device for small dimension samples compressing in elevated temperature HC-V01 Device allows for performing compression tests and flow curves determining for small samples, even Ø2x3mm, in temperature up to 500°C. Manufacturing of sulfide graphene-like nanoparticles using the „Rolling Cleavage Technology”. 476 8) Research on biomaterials and materials used for implants Increased lifetime of humans resulting from the ability to make use of a number of technical devices as well as progress in the diagnostics and curing of illnesses generates the demand for various types of implants. Such fields as orthopedics, traumatology, dentistry, cardiosurgery, laryngology, ophthalmology, etc. Using different types of implants, so called “surrogate organs” such as joints endoprostheses, coronary stents used widely in cardiosurgery or spine implants has become the challenge of contemporary civilization.. In order for the implant to meet the requirements it needs to be constructed in a specific way and needs to be made of a suitable biomaterial. Due to this fact regardless of the progress in implant construction constant research is being conducted in order to improve the chemical composition and biomaterials specificity. The group of implants used in the human osteo-skeletal system where tribological processes play a role are composed of: hip-joint endoprostheses mainly the „ball-socket” locomotor system, knee-joint endoprostheses: the runner-polyethylene insert system, joints endoprostheses: brachial, cubital, crurotalar, intervertebral spinal disc implants, teeth implants. In the group of elements exposed to heavy wear surgical instruments should also be named. INOP has: workplace for friction and wear research of biomaterials (testers named above i.e. T05, T-10, etc.), workplace (simulators) for friction and wear research on implants. The Metal Forming Institute in Poznan designed and constructed some of the simulators for tribological research on implants i.e.: simulator for research on hip-joint endoprostheses made in two different versions of attachment, simulator for research on knee-joint endoprostheses, simulator for research on intervertebral spinal discs. Each of the simulators has an automatic registration system for the researched parameters. Main aims of tribological research on implants run on simulators are: 477 determination of the friction resistance in the researched motion node of the implant for different material associations, determination of the intensity of wear of the researched materials of the friction couple (for example ball and socket). collection and research on the products resulting from wear (their quantity, size, chemical composition). research on other destructive processes such as: biocorosion, material fatigue, quantity of metalic ions impacting the metal, the so called metalosis effect, etc., possibility of assessing the durability of an implant. Main advantage of the Simulator run tests is the fact that they are conducted on prototypes of real implants (for example endoprostheses of joint, spinal implants, etc.)before they are introduced to the medical practice. Simulators a) Simulator of the hip-joint endoprosthesis: i) arrangement compliant with the human biological system, ii) reverse arrangement 478 b) Example of a simulator used for research on hip-joint endoprosthesis c) Example of a simulator used for research on implants of intervertebral spinal disc 479 POLISH WELDING CENTRE OF EXCELLENCE (Instytut Spawalnictwa) Organisation Contact Data 16 - 18, Bł. Czesława st., 44 – 100 Gliwice, Poland phone: +48 32 231 00 11 fax: + 48 32 231 46 52 e-mail: [email protected] http://www.is.gliwice.pl/en/indexen.php Instytut Spawalnictwa (The Institute of Welding) is engaged in development and transfer of knowledge in the field of joining advanced structural materials in order to ensure innovation and competitiveness of producers of welded structures. Established in 1945, Instytut Spawalnictwa is a leading and key welding research centre in Poland. In its long-standing activity the Institute has been solving problems in welding technology, coordinated numerous R&D projects and strengthened close links with industry and research centres. Instytut Spawalnictwa is the only organisation of its type in Poland and has the status of the Centre of Excellence and functions as: ANB – Authorised National Body – in European Federation of Welding, Joining and Cutting (EWF) and International Welding Institute (IIW), authorised for qualification of welding personnel, ANBCC – Authorises National Body – in EWF – authorised for certification of enterprises according to PN-EN ISO 3834 standards, Accredited in Polish Centre for Accreditation (PCA) organisation for certification of welding products and processes, Factory Production Control systems, welding and NDT personnel and quality management systems, Notified Body in the European Union in the scope of 2006/95/WE, 97/23/We and 87/404/WE Directives. Institute has the certified quality management system in accordance with PN-EN ISO 9001:2009 standard. Applied and development research constitutes the basis of the Institute’s activities. Instytut Spawalnictwa in Poland deals with processes of joining of structural materials with the use of advanced technologies of welding, brazing and thermal cutting as well as allied technologies. 480 Areas of activity: development and applied research into welding and allied technologies weldability of steels and non-ferrous metals mechanical, structural and non-destructive testing environmental engineering expert opinions, advisory service testing for CE marking, certification and approvals transfer of innovation into industry education and supervision of welding education in Poland certification of welding personnel, quality management systems and products, welding processes and Factory Production Control systems testing and qualification of welding technologies qualification of industrial enterprises, supervision of structures manufacture standardization scientific, technical and economic information collaboration with Polish and foreign organisations professional publications, seminars, conferences 481 SCIENCE FOR INDUSTRY Instytut’s team of technologists highly experienced in conducting research and development works as well as collaborating with industry, offers a wide range of research and expertise services including assistance in transfer of innovative technologies into industrial practice. The offer includes collaboration and consulting services in solving problems such as reduction of costs, quality and competitiveness improvement of product and manufacture of welded structures. The offer includes the following services: Consultancy and technical assistance in development and transfer of new technologies into industry On the basis of technological audits and information about currently applied technologies, Instytut researchers offer assistance in the planning of technology development and improvement of welding work quality and selection of innovation technologies. Development and implementation of welded technologies Development of welding technologies includes conditions for preparation of joints, selection of parameters, consumables and equipment, conditions for joints examination, heat treatment etc. Research/test results are available in the form of reports and/or WPS/BPS. Implementation includes vocational guidance as well as authors’ supervision over new technology acquisition and pre-production batch manufacturing. Qualification of welding technologies Acting as a third party, Instytut Spawalnictwa qualifies technologies of welding, surfacing and brazing in accordance with PN-ISO EN and PN-EN standards as well as other standards and regulations specified by the Customer. Instytut issues documents of technology qualification in the form of WPQR, WPAR, PQR and BPAR stating that the technology fulfils specified requirements. Weldability of materials and testing of welded structures Instytut Spawalnictwa conducts research works devoted to weldability of metals and welded structures. Structural, mechanical and non-destructive testing, stress analysis and fatigue testing is performed in order to provide assistance for designers and producers of welding consumables and structures. 482 Environmental Engineering The specialists offers a wide range of research and services in work safety, health protection and ecology in welding processes. The offer includes investigation of dust and gas emission, noise and electromagnetic fields, microclimate of work environment, optical radiation, and welding consumables and processes in respect of pollutants emission. Training of personnel in implementation of new technologies Apart from a wide range of training dedicated to welding personnel, Instytut Spawalnictwa offers specialist training adapted to conditions and requirements specified by enterprises. The scope of collaboration includes the following technologies: - laser welding and cutting plasma welding and cutting arc welding preventive surfacing and rebuilding brazing, soldering and braze welding resistance and friction welding robotic and mechanised welding Laser Welding and Cutting Instytut offers research/testing, technology and consultation services in the range of laser welding and cutting processes aiming at improvement of quality, repetitiveness and reduction of costs of welded products. Works are conducted by means of numerically controlled and robotised laser welding and cutting stations with CO2 and YAG lasers processing centres for welding and cutting of two and three-dimensional elements. The laser stations reproduce the real industrial conditions. Laser welding enables: - joining of materials without edge preparation and necessity to use welding consumables obtaining very narrow welds with restricted heat affected zone and minimum distortions in welded joints i.e. welding “ready-made” products welding of elements of diversified thickness simplification of the structure and manufacture of products by applying advantages of laser welding 483 Laser cutting enables: - ensuring high quality and repeatability of cut-out elements elimination of additional machining of edges cutting of coated plates, pipes and stamped elements, etc. saving materials due to optimum layout of elements 484 Plasma Welding and Cutting In the range of plasma welding the offer includes: development of welding technologies for 0.1 ÷ 2 mm thick materials made of unalloyed and alloyed and galvanised (without damaging of zinc coating) steels used in electronics, medicine, precision engineering, food and automotive industries, etc. implementation of welding systems with welding technologies pre-production or prototypes batches Great stability, high level of concentration and ionisation as well as high power density of plasma arc ensure very good quality and appearance of joints. In the range of plasma cutting the offer includes: cutting with the use of water shielding resulting in reduction of stresses and distortions technical advice in cutting technology and organisation of work stations Arc Welding Instytut offers extensive collaboration in welding of steels, aluminium, titanium, copper and other metals with MIG/MAG, TIG, A-TIG, SAW and MMA processes as well as hybrid laser + MIG/MAG welding process. The collaboration includes: development of welding technologies advice on process and consumable selection process development aimed at improvement of applied technologies manufacture of pre-production and prototype elements welded with different methods Preventive Surfacing and Rebuilding The offer of Instytut covers: MIG/MAG, SAW and MMA surfacing plasma and gas surfacing of elements made of unalloyed, alloyed and non-weathering steels, cast steels and some cast irons; the surfacing is conducted with metallic powders such as nickel, cobalt, iron or copper-based alloys assistance in development of surfacing technologies on the basis of analysis of abrasive wear of elements of equipment and machinery development, manufacture and implementation of specialised iron and nickel-based tubular cored electrodes for surfacing meeting specified exploitation requirements 485 Brazing, Soldering and Braze Welding The offer of technological collaboration in the range of soldering and brazing includes: flame brazing with the use of conventional and volatile fluxes (manufacture of feeders of volatile flux) induction brazing of tools and machine parts oven brazing in vacuum and argon blanket soldering of parts of machines, tools, heat exchangers and other metal devices Instytut offers specialised filler metals, fluxes and pastes for brazing and soldering as well as assistance during their implementation. MIG/MAG braze welding is an alternative to arc welding and brazing of plates covered with anticorrosion coating and sheets of alloyed and unalloyed steels. This method enables obtaining high quality joints with retaining original anticorrosion properties of the base material. Instytut offers development and implementation of the technology of robotised and semirobotised MIG/MAG braze welding of galvanised and alloyed steels. Resistance and Friction Welding Instytut offers support in problemshooting and development of technologies enabling the manufacture of products with the use of: spot resistance, projection and butt welding friction welding including friction stir welding (FSW) ultrasonic welding braze welding A relatively new FSW method enables: joining aluminium sheets and plates, depending on equipment size, of thickness up to 50 mm in single run, without shielding gases and edge bevelling welding dissimilar materials such as aluminium to copper welding of non-ferrous metals which cannot be welded using other processes reducing costs of welding Cost reduction is the result of simplified preparation of plates for welding, absence of consumables, limited necessity of application of protection measures (indispensable in arc welding of aluminium and its alloys). 486 Robotic and Mechanised Welding Processes Within the range of robotic and mechanised welding Instytut offers: economic analysis of profitability of implementation of robotised stations for specified applications development of assumptions of the best possible configuration of welding station and assistance in selection equipment suppliers development of technology of robotised welding or braze welding support in implementation of robotised welding technologies 487 THE RESEARCH AND DEVELOPMENT CENTRE FOR BUILDING INSULATION INDUSTRY (Centralny Ośrodek Badawczo Rozwojowy Przemysłu Izolacji Budowlanej) Organisation Contact Data 193 A, W. Korfantego st., 40 – 157 Katowice, Poland phone: +48 32 2581 373 ; 32 2580 572 phone / fax: + 48 32 2583 553 e-mail: [email protected] http://www.cobrpib.katowice.pl/ang/angindex.htm We are interested in cooperation in range: 1/ Technology offer Title: Flame retardancy of bitumen materials for roof waterproofing Short description: Technology allows to obtain bitumen materials for roof waterproofing with increased resistance to fire in relation to traditional products. During production of bitumen layer for preparing reinforced flexible sheets for waterproofing or during production of bitumen compounds, solutions and dispersions some additives are added, which decrease a spreading of fire during its action. 2/ R&D offer Cooperation: Research of the heat transfer in materials or products for thermal insulation in range of temperature from -160 ºC to 700 ºC. 488 WOOD TECHNOLOGY INSTITUTE (Instytut Technologii Drewna) Organisation Contact Data 1, Winiarska st.,6- - 654 Poznań, Poland phone: +48 61 849 24 00 fax: + 48 61 822 43 72 e-mail: [email protected] http://www.itd.poznan.pl/en/ The Wood Technology Institute (in Polish: Instytut Technologii Drewna, ITD) is the only research and development unit in Poland which, since 1952, has been comprehensively dealing with issues concerning wood processing, its application, and the creation of new composites based on wood as a raw material. The mission of the Institute is to conduct research aimed at achieving the sustainable development of the wood industry, maintaining the high competitiveness of the Polish wood sector, developing innovative materials, technologies, and machining techniques, as well as improving education and awareness in a knowledge-based society. The Wood Technology Institute’s activity involves research, certification, normalization, information dissemination, and training for the forestry-wood sector companies. The institute co-operates with numerous national and foreign entities and companies within and outside the forestry-wood sector (e.g. ministries, the State Forests, regional and local authorities, various associations and industry chambers, national courts, technology platforms, wood companies). Research activity encompasses the following areas: structure, quality, properties, and protection of wood, wood products and wood materials, production processes in the wood and furniture industries, biotechnology, wood industry organization and economics, markets in roundwood, sawnwood, wood-based panels, furniture and other wood products, product quality, environmental protection and safety at work. 489 The Institute is an EU Notified Body (No. 1583) and acts as an Independent Controller (No. TPC-19) of composite wood product manufacture within the area of formaldehyde release, conferred by the California Air Resources Board (CARB). The Institute has in its structure a Testing Laboratory of Wood, Wood-Based Materials, Packaging, Furniture, Constructions and Woodworking Machines which performs tests according to requirements of national, European, and international standards, and is divided in eleven sections (A: Anatomical and Taxonomical Testing, B: Physical Testing, C: Chemical Testing, D: Furniture Testing, E: Packaging and Construction Testing, F: Environmental Protection and Safety Testing, G: Wood Preservation and Conservation Testing, H: Surface Testing, K: Inflammability Testing, L: Woodworking Machines and Machine Tools Testing, and M: Solid Biofuels Testing). The laboratory is accredited by the Polish Centre for Accreditation (PCA). The Institute also has a Certification Centre for Wood Industry Products which is authorized to issue product certificates (on average it issues 50 certificates a year) and a Quality Policy Department. In its activity he Institute follows the principles of a Quality Management System acc. to ISO 9001:2008 standard. Since 2005 the Institute has been coordinator of the Polish Forest-Based Sector Technology Platform, which is a national support group of the European Forest-Based Sector Technology Platform (FTP). The Institute also has office of the Polish National SME Services Network. The Institute co-operates with the following Technical Committees of the European Committee for Standardization (CEN/TC 38 Durability of wood and derived materials, CEN/TC 175 Round and sawn timber, CEN/TC 142 Woodworking machines – Safety, CEN/TC 112 Woodbased panels, and CEN/TC 207 Furniture) and ISO Technical Committees (ISO/TC 136 Furniture, ISO/TC 218 Timber, ISO/TC 89 Wood-based panels, and ISO/TC 39/SC4 Woodworking machines). The Institute has numerous patents and pending patent applications, for example: “A method of reducing the content and emission of formaldehyde in boards from lignocellulosic particles bonded with amine resins”, “A method of testing initial adhesion of plywood glues and a sample for testing of initial adhesion of plywood glues”, “An adhesive and method of bonding flat surfaces and a method of spatial objects production”, “Agents for surface and deep protection of wood against moisture and a method of surface protection of wood against moisture”. 490 TECHNOLOGY FOR COMPOSITE PANELS MADE OF UNCONVENTIONAL LIGNOCELLULOSIC RAW MATERIALS This offer encompasses sale of technology and its adjustment to raw materials and regional conditions, including: the manner of grinding and obtainment of chips (flakes and fibrous chips), the choice of glue resin and glue formula, taking into account pH and buffer capacity of lignocellulosic raw materials, the structure and formulas of the panel, pressing parameters, tests of panel properties. The developed technology enables the production of furniture panels and indoor equipment panels, interior and exterior load shift panels, and building panels, i.e. structural and insulating panels, with the use of chips obtained from agricultural waste, fast growing plants (from agricultural and forest plantations), and root offshoots. The below table compares chosen properties of panels produced according to the ITD technology with the properties of popular building OSBs. Requirements of the Results of PN-EN 300:2006 standard for panel testing Panel properties OSBs, type acc. to the ITD technology 2 3 4 Bending strength [N/mm2] - major axis 33 – 42 20 20 28 - minor axis 10 10 15 2 Modulus of elasticity [N/mm ] 3500 3500 4800 - major axis 3950 - 4620 1400 1400 1900 - minor axis Internal bond [N/mm2] 1.09 – 1.54 0.32 0.32 0.45 Internal bond after cyclical tests (option 1) 0.72 – 1.19 0.15 0.17 Tensile strength after boiling test (option 2) 0.12 – 0.26 0.13 0.15 [N/mm2] Swell in thickness, 24 h 5.1 – 6.0 20 15 12 Swell in thickness after cyclical tests 5.6 – 8.5 (option 1) [%] Density [ kg/m3] 660 - 710 491 492 Catalogue of technologies developed by Polish Research Institutes MECHANICS, BUILDING AND OPERATION OF MACHINES , PRODUCTION ENGINEERING 493 INSTITUTE FOR SUSTAINABLE TECHNOLOGIES – NATIONAL RESEARCH INSTITUTE (Instytut Technologii Eksploatacji) Organisation Contact Data 6/10 K. Pułaskiego st., 26 – 600 Radom, Poland phone: +48 48 364-42-41 fax: + 48 48 364-47-60 e-mail: [email protected] http://www.itee.radom.pl/lang/index.php The Institute for Sustainable Technologies – National Research Institute (ITeE–PIB) in Radom is a public R&D organisation that conducts basic and applied research and implementation tasks in the area of advanced technologies, particularly in the domain of machines structure and maintenance, materials engineering, environmental protection, systems engineering, research methodology, and the theory and practice of knowledge transformation and technology transfer. SCIENTIFIC AND INFRASTRUCTURE BASE: The Institute was established in 1986. In 2004 the Institute obtained the status of the National Research Institute. The 90s of the XX century saw tremendous infrastructural growth for the Institute. These were the years when Institute’s prominent research laboratories and scientific departments were built. Further expansion of the Institute’s laboratory infrastructure continues and currently a new complex of the Environmental Technologies Laboratories is being built. Along the expansion of Institute’s infrast ructure, the investment is also in the development of modern apparatus and analytical equipment, thanks to which the Institute has reached the level of research laboratories equal to leading EU Member States. The modernity of the research and laboratory infrastructure and high qualifications of the personnel have been officially recognised and certified by, inter alia, the Polish Centre for Accreditation, the Polish Ministry of Economy, or the German TUV NORD Group. The Institute has a great experience in the realisation of strategically important R&D programmes in the domain of innovativeness and advanced product and process technologies. The Institute has also realised numerous grant projects (ca. 120) and targeted projects (ca. 110) that finished with successful and effective implementation of their results. The Institute has also been appointed to realise and coordinate programmes and projects commissioned by the governmental and administrative bodies. Among them, the most prestigious and prominent was the “Development of Innovative Systems of Manufacturing and Maintenance 2004–2008” Multi-Year Programme jointly realised by the Institute and ca. 100 leading national research centres, enterprises and institutions from the business sector. 494 At the beginning of 2011, the “Advanced Industrial and Ecological Technologies for the Sustainable Development of Poland” technological foresight project coordinated by the Institute was completed. Among currently undertaken programmes, one of key importance is the “Innovat ive Systems of Technical Support for Sustainable Development of Economy” Strategic Programme realised within the Innovative Economy Operational Programme. Profile and scientific and research directions The scope of activity of the Institute is mainly concentrated on the structure and maintenance of machines, materials engineering and manufacturing technologies particularly concerning: modelling of knowledge transformation and technology transfer mechanisms and structures, methodology of empirical research and determination of development directions of innovative mechanisms and structures; systems engineering, tribology, surface engineering, operating fluids, diagnostics, mechatronics, bio-mechatronics, metrology, information technologies and life long learning; innovativeness of products and manufacturing and maintenance processes, in particular, optimisation methods, control systems for technical objects, computer systems for the support of technological and decision processes, methods and devices for materials and technical systems testing, surface technologies, operating fluids technologies and composite materials technologies; systems for the rationalisation of materials and energy resources usage in manufacturing and maintenance processes including, technologies for materials utilisation, recycling and reusable energy resources; organisational and technical systems to counteract and fight technical threats, dangers and disasters; environmental protection focused particularly on monitoring systems and technologies for the reduction of ecological contamination resulting from the widespread application of technical devices; standardisation and normalisation activity in the area of products, processes and technical safety; methods and systems for the support of quality systems in manufacturing and maintenance processes; continuing vocational education systems; improvement of R&D methods. The originality of the Institute’s approach to conduct scientific and R&D activity lies in the interdisciplinarity of both the scientific and technical aspects, which results in the multiplicative application of the developed solutions. In September 2010 the Institute was awarded the highest category in Polish scientific institutions classification, which together with already acquired reputation decided on 495 prestigious and strategically important scientific, R&D and investment programmes being granted to the Institute. Surface Engineering Department The scope of work at the Surface Engineering Department is concentrated on the realisation of research and application tasks in the field of surface engineering, in particular, processes of increasing the durability of tools and machine parts by means of PVD methods in particular. The results of scientific activities undertaken include advanced technologies of surface treatment enabling the modification of the surface layer of the material in order to give it desirable functional and operational properties. Activities conducted in this particular domain include a wide scope of undertakings of technological nature as: the design of new material solutions for coatings and layers, particularly hybrid layers, compound coatings (composite, multi-component and multi-layer) and layers with a nanometric structure; the development of advanced technologies of creating coatings and layers with a functional character by means of contemporary methods of thermo-chemical treatment and methods of surface treatment; the analysis of processes of manufacturing coating materials with plasma fraction, including in particular ion nitriding processes, magnetron sputtering, arc evaporation and EB PVD evaporation; the material research of thin films and coatings concentrated mainly on their mechanical and anti-wear properties; the development of technologies of removing PVD layers from the surface of tools, machine parts and structural elements; the design and construction of plasma sources, control systems, additional accessories and technological devices for the realisation of surface treatment processes, including hybrid treatment processes. Contact Person Data Head of Department: Prof. Jerzy Smolik e-mail: [email protected] Tribology Department The R&D activity of the Tribology Department comprises the problems of friction, wear and the lubricating of the components of machines, with particular attention paid to research methods and test devices. The main directions of research conducted at the department concentrate on: – the scientific investigation of friction and wear processes in macro-, micro- and nanoscale; – the development of methods facilitating tribological properties of machine elements; – the development of systems for the assessment of tribological properties of structural materials and lubricating substances; – the development of tribotesters and laboratory equipment for tribological investigations. 496 The department consists of Tribological Testing Laboratory and Laboratories of Scanning Microscopy and Metrology that have been accredited by the Polish Centre for Accreditation (PCA). The department cooperates with numerous national and international universities and research institutes, inter alia: technical universities in Cracow, Lodz, Rzeszow, Radom, Wroclaw and Poznan, Lodz University, the University of Warmia and Mazury, the University of Monterrey in Mexico, the Institute of Superhard Materials in Kiev, the Federal Institute for Materials Research and Testing (BAM Institute) in Berlin and Tribological Centre in Neustadt, Austria. The research and test apparatus designed at the department and manufactured at the Institute have been introduced at many national technical universities, research institutes and industrial R&D laboratories. Moreover, department’s original solutions are also exported to such countries as China, Israel, Mexico, Germany, USA, Hungary, Vietnam, Russia, South Korea, Croatia and Czech Republic. Contact Person Data Head of Department: Dr Witold Piekoszewski e-mail: [email protected] Control Systems Department The Control Systems Department conducts research activity directed mainly at the design and production of: – microprocessor systems, including hard real time systems; – specialised electronic devices in the field of control systems, plasma sources supply systems and other power electonic systems meant for plasma-vacuum devices such as, high power radio frequency generators and high power pulse generators; – control systems for technological processes, plasma-vacuum processes in particular; – control systems for research and test devices. The department is equipped with – tools for programming engineering and microprocessor techniques, i.e. DSP signal processors and FPGA systems; – surface-mount laboratory; – devices for high-power measurements; – software for the identification, modelling and simulation of control systems; – SCADA and HMI tools; – laboratory for testing devices to be CE certified. Contact Person Data Head of Department: Dr Andrzej Majcher e-mail: [email protected] Information Technologies Department The work of the Information Technologies Department focuses particularly on R&D tasks in the field of applied computer science, automation and test apparatus. The scope of activity 497 includes the integration of network and mobile information technologies with PLC control systems and measurement systems of varied structure. Moreover, the department deals with analytical issues, system engineering, knowledge engineering as well as mathematical and heuristic modelling. Undertakings executed by the department include: – local and internet data- and knowledge bases; – portals, vortals and internet platforms using latest information technologies available; – unique test and research apparatus, particularly climatic, environmental and volatile substances emission test chambers; – innovative systems for the control of technological processes, – computer systems for the monitoring and diagnosis of the condition of technical objects and technological processes; – original algorithmic models designed by means of numerical and Artificial Intelligence methods, computer simulations and knowledge engineering. The department applies various programming languages, (i.e. C, C++, C#, Delphi, Lisp, Java,Visual Basic), script languages (inter alia: PHP and JavaScript), structural languages and declarative languages. To create databases, Oracle, MySql, Postgress, FireBird, Access, DBASE, PARADOX standards are used, whereas scientific and engineering calculations, computer simulations, optimisation and prognosis are assisted by Matlab and Simulink Programme. The algorithms for advanced control systems and original test and research apparatus are designed with the use of LabView, VHDL and specialised software. Contact Person Data Head of Department: Dr Jerzy Dobrodziej e-mail: [email protected] 498 Mechatronics Department The multidisciplinary scientific-research activity of the Mechatronics Department comprises both conceptual studies and practical applications of advanced solutions in the field of mechatronic technologies used in the systems for the support of manufacturing and maintenance processes, research and test apparatus, and medical equipment. The department’s main research directions are as follows: – advanced methods and systems of multiparameter quality control in the industry by means of opto-mechatronic methods; – hybrid monitoring systems of technological processes with the use of optical inspection and thermo vision; – test and measurement apparatus satisfying the needs of both the R&D sector and the industry; – mechatronic systems for rehabilitation. The Mechatronics Laboratory undergoes constant development and is equipped with advanced test stands, high quality apparatus and devices necessary for the realisation of research projects. Contact Person Data Head of Department: Dr Tomasz Giesko e-mail: [email protected] 499 Environmental Technologies Department The main direction of the scientific and R&D activity of the Environmental Technologies Department is to develop and improve innovative industrial technologies enabling both the reduction of material and power consumption in manufacturing processes and the management of waste that would minimise the possibly environmentally harmful aspects of its disposal. The scope of activity of the department is particularly oriented towards systems for the reduction of a negative impact of manufacturing and maintenance processes on the environment, technologies of waste management and processing by means of biotechnological and membrane processes, production and application of ecological energy carriers, polymer composites-based machine regeneration, application of operational and maintenance materials waste as substitute fuels. Additionally, the department specialises in the development of ecological operating fluids and plastic greases on the basis of biodegradable raw materials from reusable sources, and the research on the course and the effects of corrosive processes causing serious damage to components of high power devices. The R&D undertakings executed by the department include laboratory analysis by means of specialist analytical apparatus for spectral and chromatographic tests and physico-chemical properties of operating fluids. Moreover, numerous novel solutions in the field of specialised technical devices making manufacturing and maintenance processes more environmentally friendly are developed at the department. The innovative devices developed allow the reduction of the amount of waste created by means of the recycling of operating fluids, including processing fluids, machine, compressor and hydraulic oils and antifreezes. The department cooperates with many national scientific and R&D centres such as Technical Universities in Warsaw and Cracow, University in Lodz, University of Warmia and Mazury, “Blachownia” Institue of Heavy Organic Synthesis and the Oil and Gas Institute. Moreover, the department closely cooperates with machine, transport and power industries. The results of this cooperation include numerous scientific papers, patents and industrial applications. Contact Person Data Head of Department: Dr Jarosław Molenda e-mail: [email protected] 500 Innovation Strategies Department The Innovation Strategies Department conducts scientific and development research in the field of technology transfer, innovativeness and entrepreneurial development, foresight projects and innovative systems management. The main areas of activity of the department include: systems for innovation – mechanisms and structures of knowledge transformation and technology transfer; trends in the area of knowledge transformation and advanced technology transfer; foresight projects realised at national, regional, sectoral and corporate levels and international and transnational programmes for the support of innovation implementation; evaluation of strategic research programmes, effectiveness of scientific, R&D and implementation research realisation; research results commercialisation procedures. The department coordinated undertakings executed within “Poland 2020” National Foresight Programme, particularly within “Sustainable Development of Poland” research panel. Additionally, the department was responsible for the execution of the sectoral foresight project “Advanced Industrial and Ecological Technologies for the Sustainable Development of Poland” realised within the Innovative Economy Operational Programme. The realisation of the project allowed for the generation of future research directions in the area of technical support for sustainable development, which formed the substantial basis for the “Innovative Systems of Technical Support for Sustainable Development of Economy” Strategic Programme realised and co-financed within European structural funds in the framework of national Innovative Economy Operational Programme. The department currently participates in the realisation of various research projects including “Design of Evaluation Model for the Eco-effectiveness of Technologies for Sustainable Development” Project and research tasks in one of the thematic groups of the Strategic Programme – “Systems of knowledge transformation, advanced technologies transfer and commercialisation of innovative solutions for the sustainable economy.” Contact Person Data Head of Department: Dr Beata Poteralska e-mail: [email protected] 501 Systems Research Department The main area of the activity of the Systems Engineering Department comprises the modelling of maintenance systems and processes and technical objects. The department also conducts research intended for the development of methods supporting the experimental research of the Institute in the domain of experiments planning and the analysis of their results from the point of view of the design of models describing the properties of objects tested. Tasks executed by the department encompass the following thematic areas: methodological support of experimental research; modelling of processes, particularly in the area of technical objects maintenance; modelling of computer systems supporting decision processes; developing procedures for the assessment of projects innovativeness; model research concerning the economic assessment of enterprises operation; - analysis of the effectiveness of economic undertakings; analysis of the condition and development tendencies of industry innovativeness. Contact Person Data Head of Department: Dr Magdalena Trzos e-mail: [email protected] Textile Technologies Department The Textile Technologies Department in Lodz realises R&D tasks in the domain of innovative manufacturing technologies including: – fibre extraction from plants; – consolidation of unconventional textile and fibrous products; – new fibrous composite products for agricultural technology, ecohydrology and construction industry; – diagnosis and assessment of textile goods manufacturing; – design and development of novel specialist test and measurement apparatus complying with European standards; – development of model test stands, experimental installations and prototypes in the field of textile technologies; – recycling of textiles. All the undertakings are of a transdisciplinary character and are based on a close cooperation with scientific centres in the Lodz region. Cooperation with the industry has led to the development of complete technological lines for manufacturing. Contact Person Data Head of Department: Prof. Marek Wiśniewski e-mail: [email protected] 502 Vocational Education Research Department The Vocational Education Research Department performs scientific-research, and project and implementation activity in the field of work pedagogy aimed particularly at the vocational training of advanced technologies specialists of all levels (higher, secondary and vocational). The scope of the activity of the Department includes: development of research methods of work pedagogy; comparative research of European vocational education systems and the implementation of EU tools supporting formal and non-formal education; development of methods of structuring, implementing and evaluating modular curricula; development of scientific and research networks and the accreditation of institutions and programmes realised within the Polish Network for Modular Education. The Department also identifies new problematic areas within work pedagogy concerning the implementation of European and Polish frameworks of qualifications. Research tasks currently coordinated by the Department include, inter alia, the “Innovative programmes and technologies of continuing education for the support of knowledge transformation and advanced technologies transfer” realised with the “Innovative Systems of Technical Support for Sustainable Development of Economy” Strategic Programme; and such international scientific projects as Leonardo da Vinci or GRUNDTVIG. Contact Person Data Head of Department: Dr Krzysztof Symela e-mail: [email protected] 503 Continuing Education Departament The scientific and research activity of the Continuing Education Department is particularly concentrated on issues connected with continuing vocational education including the following: research on the theoretical and methodological basis for the creation of a multilevel vocational education system; development of contemporary technologies for vocational training; analysis of global trends in vocational and continuing education; development of computer systems for the support of learning processes; e-learing and visualisation; development of national and international networks of innovation and cooperation between educational institutions, adult education associations and enterprises. The Department is in the possession of a modern Innovation Laboratory (i-Lab) – the centre of teachers, students and coaches competences development. The Department is engaged in the realisation of numerous national and international programmes and projects treating of the problems of vocational education and lifelong learning (i.e. EQUAL – WWW Entrepreneurship – the Internet as a Means for Higher Competitiveness – for which, in 2010, the Department won the DIE EUROPA Award, Vocational Support for People with Difficulties with Employment Access, Lifelong Learning Programme – “Wirtschaftsnahe Lernstrategien fur LLL in der Region (WiSaR)). Contact Person Data Head of Department: Dr Dorota Koprowska e-mail: [email protected] 504 INSTITUTE OF MINING TECHNOLOGY (Instytut Techniki Górniczej) Organisation Contact Data 37 Pszczyńska st., 44 – 101 Gliwice, Poland phone: +48 32 237 41 00 fax: + 48 32 23 74 518 e-mail: [email protected] http://komag.eu/en/ KOMAG Institute of Mining Technology realizes scientific, research and technical projects oriented onto a mechanization of mineral winning and processing systems in the mining industry. This research work refers to mechanization of cutting, loading and transportation of the-run-of-mine as well as to dewatering and ventilation of mines and processing of minerals, with special attention paid to the problems of environmental protection, work safety and ergonomics. KOMAG offer includes: technical documentation of mining machines and equipment, scientific and technical consultancy, testing of mining machines and equipment, training of machinery operators, modelling of complex anthropotechnical systems, ergonomic analyses, identification of health and safety hazards, reconstruction of accidents, computer simulation of machinery assembly jobs, projects concerning environmental protection and environmental management issues, environmental measurements of imissions and emissions, noise and mechanical vibrations, dust control systems and equipment. 505 KOMAG has the following authorizations: accreditation of certifying body issued by the Polish Centre for Accreditation – No. AC 023, status of notified body No. 1456 as regards 2006/42/EC “Machinery”, 2006/95/EC “Low Voltage”, 94/9/EC ATEX and 2009/48/EC “Toy” Directives, authorization for conducting tests and performing assessments of products resulting from the Decree of the Ministers’ Council from 30th April 2004, concerning an approval of products for use in mining plants. It is important to mention that KOMAG has the accredited Laboratory for Tests, equipped with the state-of-the-art rigs, enabling, among others, to test the strength and an operation of powered roof supports on the incline as well as to check a joint operation of three powered roof support units. The tests are realized against the orders of domestic and foreign producers of powered roof supports as well as of end-users of the equipment. Inviting you to a collaboration with KOMAG, we would like to assure you that an implementation of innovative technical and technological solutions, developed at our Institute, will contribute to an increase of your market. STATE-OF-THE-ART, INNOVATIVE SOLUTIONS FOR THE MINING INDUSTRY KOMAG Institute of Mining Technology, established in 1950, is a Polish state-owned research institute, subordinated to and supervised by the Ministry of Economy, employing 236 scientific research and technical specialists, offering new, competitive, technical and technological solutions in the domain of mechanical systems and environmental engineering. KOMAG plays an important role both in international as well as local developments. It is one of the national leaders in the domain of technical progress as regards research, designing and testing of mining machinery and equipment. The results of these multidisciplinary activities are used by machinery producers, selling their products to domestic and international markets. The technical solutions, offered by KOMAG, are known all over the world. They enable to implement advanced mechanical systems, meeting the requirements of increased operational safety, ergonomics and environmental protection. The mechanical systems, designed and tested at KOMAG, operate in NIS (Russia, Ukraine, Belarus, Kazakhstan) as well as in several other countries such as Spain, Argentina, Brazil, India, the USA, Australia and China. KOMAG has outstanding research and development achievements in mining mechanization systems. Its unique feature is a possibility of realizing a full research and development cycle, starting from the design and research through the development stages, including testing, to the industrial implementation. A realization of advanced research projects on the world level is possible due to the specialistic test rigs of unique character, equipped with the state-of-the-art instrumentation. Cooperation with the leading research institutes and laboratories all over the world guarantees an implementation of the state-of-the-art technical and scientific solutions. 506 A high level of development, research and design projects, confirmed by the certificates of the Polish Centre for Testing and Certification as well as the Polish Accreditation Centre is guaranteed by the Quality Management System according to the PN-EN ISO 9001 and the system of tests according to the PN-EN ISO/IEC 17025:2005 Standard. KOMAG is a European Notified Body, having an identification number 1456, in the scope of the 2006/42/EC Machinery Directive, 94/9/EC ATEX Directive, 2006/95/EC LVD Directive as well as 2009/48/EC ‘Toy” Directive. KOMAG is recognized by the European Commission as the Centre of Excellence in the domain of advanced mechanical systems on the European level. The objective is to increase a competitiveness of Polish technical solutions in the European market and to integrate the Polish Sector of Science and Technology with the European Research Area in the domain of designing, testing and manufacturing of machines. Broad, international relations and an interdisciplinary collaboration with foreign scientific and research institutes, technical universities, companies and enterprises, activities aiming at an integration with the European Research Area, extending traditional forms and scopes of collaboration, a generation of new products, in particular within the scope of the priority fields of activity, indicated by the European Union in the Framework Programmes and also a participation in international organizations, collaborative networks and technology platforms are the measures of the KOMAG’s successes. Some activities, oriented onto expanding traditional scopes and forms of collaboration and a development of new research programmes, are undertaken on a large scale. In particular, it concerns such subjects as: health, energy, mechatronics, new materials and technologies as well as ecology. A collaboration within the Research Fund for Coal and Steel develops in an effective way. KOMAG takes an active part in these activities, participating in the actions co-ordinated by the EURACOAL – European Association for Coal and Lignite. Direct contacts and partner collaborative links, shaped over the years, bring concrete effects in a form of contracts and trade agreements, concerning licenses and know-how as well as of different research and technical services, rendered for foreign partners. They constitute an important part of the international activity of the KOMAG Institute, which developed several projects of this type, among others, for Belarus, China, Great Britain, India, Kazakhstan, Russia, Spain, Ukraine and the USA. For foreign partners KOMAG offers mechanization systems for underground mining operations, coal preparation and environmental protection, including: Technical designs of mining machines as well as of preparation plant machinery and equipment. Conformity and expertise assessments, technical opinions. Technical and economic analyses as well as a selection of mining machines and equipment for mechanized longwall systems. Laboratory and in-situ tests as well as assessments and certification of machines and equipment. Implementation of machines and equipment in mines. 507 Training of colliery personnel, in particular machinery operators. Projects oriented onto investigating the relationships: man-machine-environment. Studies, research and tests in the domain of environmental protection and occupational safety. KOMAG’s activities in the domain of mining mechanization, minerals preparation and ecological systems The scope of mechanization systems developed by KOMAG comprises among others the following machines and equipment: longwall shearers, armoured face conveyors and beam stage loaders, belt conveyors, powered roof supports, drilling rigs, drilling jumbos, roadheaders, side-discharge loaders, locomotives and monorails as well as hoisting machines. It should be emphasized that KOMAG is authorized by the Chairman of the State Mining Authority to be an expert on mining plant activities, to elaborate and issue opinions within the scope of hoisting machines. The activities in the domain of preparation systems concern the hard coal mining industry and the mining industry of minerals. KOMAG’s offer comprises processes of beneficiation, classification, crushing, transport and also auxiliary activities. Some examples of realized projects are as follows: An elaboration of multi-branch projects of installations for a preparation and processing of hard coal. Designing of machines and equipment, such as jigs, classifiers, screens etc. Designing of installations for waste management and its preparation for secondary materials. Laboratory, technological and industrial tests. Apart from a development of the state-of-the-art mechanization systems and technologies, KOMAG elaborates the most advanced technological solutions to reduce the negative impact of industry on the environment and human health. The scope of activities within the ecological systems is as follows: Design and engineering projects concerning dust control installations for the mining industry, a modernization of operating waste water treatment plants, saline water monitoring systems, noise protection installations. Identification and assessment of air pollution and noise levels from technological processes and industrial plants. Elaboration of programmes for a revitalization of post-industrial areas. Testing of dust control systems and equipment. Presenting our offer as well as research and technical expertise, we would like to invite you to cooperate with us, guaranteeing a high level of our projects and services. 508 THE INSTITUTE OF ADVANCED MANUFACTURING TECHNOLOGY (Instytut Zaawansowanych Technologii Wytwarzania) Organisation Contact Data 37 A Wrocławska st., 30 – 011 Cracow, Poland phone: +48 12 63 17 100 fax: + 48 12 63 39 490 e-mail: [email protected] http://www.ios.krakow.pl/ The Institute of Advanced Manufacturing Technology – IZTW (previously The Institute of Metal Cutting – IOS), established in Kraków in 1949, is a research centre specialized in problems of manufacturing and machining techniques. Institute focuses on research and development in the area of manufacturing of highly processed industrial products and transfer of advanced technologies, products and knowledge to industry in the fields of metal cutting, abrasive machining, unconventional methods of machining, materials engineering, technical metrology, assembly technology and automation of manufacturing processes, packaging processes of liquid and solid substances. The Institute is a body authorized by Polish government and EU notified body (no. 1455) with regard to four directives: the Machinery Directive, LVD, EMC, and Noise Emissions Directive. The Institute is concerned with the development and commercialization of knowledge. The activity of IZTW is oriented to economic development, which may be proved by implementation of unique innovative solutions providing significant economic benefits to businesses. Thanks to this, the Institute has proof supporting its competences, high level of works and its ability to cooperate with industrial entities. IZTW carries research works oriented at implementation of innovative solutions with regard to the following areas: development of machining and abrasive machining processes, tools, tooling, specialpurpose machine tools and tool operation systems; engineering of tool materials and coatings resistant to wear and tear; nanomaterials and functional gradient materials used in special-purpose cutting tools and elements of machines and equipment; development of electro-erosion machining and electrochemical machining processes as well as erosion and hybrid machine tools; erosion and hybrid micro-machining methods; technical metrology, in particular involving geometric parameters of surface; methods of measurement used for micro- and nanotechnologies; development of specialized software to support machining, abrasive and erosion machining operations, including metrology software; 509 development of testing methods for machine tools, tools, tooling and working fluids, in particular with regard to their application, safety and environmental protection; security of manufacturing systems; technologies supporting health and environment protection, including waste recycling and disposal technologies; methods and systems of quality assurance for manufacturing systems; management of technologies and manufacturing systems; monitoring of technology development, technology foresight; transformation of knowledge, and transfer of knowledge and technology. Main fields of possible cooperation within the R&D activities of Institute are as follows: • machining and abrasive machining, tools, instrumentation, special machining centres, e.g.: designing special cutting tools with soldered and glued blades, special tools and instrumentation for CNC machine tools; - technology of abrasive diamond tools and tools made of cubic boron nitride (cBN); surfacing processes with the use of burnishing; • engineering of cutting materials and wear resistant coatings, including: ceramic cutting materials for machining plates; technologies for the manufacture of composites (sinters) made of polycrystalline diamond (PCD) and cubic boron nitride (PcBN); wear resistant tool coating technology with the use of PVD method • non-standard methods of machine parts generation, including: electrodischarge machining (EDM), electrochemical machining (ECM), abrasive water jet machining (AWJM), hybrid machining methods using EDM, ECM, USM (ultrasonic machining), abrasive and laser machining • technical metrology concerning particularly geometric quantities, including: coordinate measuring methods, machines and special measuring stands, including scanning techniques; methods and devices for measuring and analysis of surface topography, including 3D analysis; • special software, including: systems for CNC machining centres and erosion machine tools; software for coordinate measuring machines, as well as shape measuring instruments and profilometers; • products testing methods, mainly in the field of utilitarian features, usage safety and threats to humans and natural environment, concerning especially: machine tools and technological devices; cutting tools and instrumentation; machining liquid (cooling-lubricating liquid), dielectrics and electrolytes. 510 Catalogue of technologies developed by Polish Research Institutes MEDICAL SCIENCE 511 INSTITUTE OF PHYSIOLOGY AND PATHOLOGY OF HEARING (Instytut Fizjologoii i Patologii Słuchu) Organisation Contact Data Organisation Contact Data 17, Mokra st, Kajetany, 05 - 830 Nadarzyn, Poland phone: +48 22 356 03 66 fax: + 48 22 356 03 67 e-mail: [email protected] http://whc.ifps.org.pl/en/ 1, Zgrupowania AK Kampinos st, 01 - 943 Warsaw, Poland phone: +48 22 311 81 02 fax: + 48 22 311 81 18 e-mail: [email protected] http://whc.ifps.org.pl/en/ World Hearing Center of the Institute of Physiology and Pathology of Hearing Kajetany World Hearing Center (WHC) is a unit of the Institute of Physiology and Pathology of Hearing which provides a complex care for people with congenital and acquired hearing, voice, speech and balance disorders. This is a unique and the first on the international scale unit of such type. Its establishment is significant for all patients with hearing, voice and speech problems, as well as for the development of science and new methods of diagnostics and treatment of sensory impairments. The WHC is of a great importance for the integration of the scientific society around interdisciplinary issues which significantly influence the development of modern information society founded on requiring of knowledge and interpersonal communication. It is a modern hospital offering medical services at the highest world level, equipped with the unique medical instrumentation with vast technical support. It is a perfectly prepared Education Center for extensive research and educational activities. Education Center includes the only in Poland 2 multimedia studios of telemedicine, 7 conference rooms for 800 people, spacious exhibition area. The particular attention should be given to the Clinical Anatomy Laboratory – an integral part of the Education Center – with modern equipment for surgical trainings performed on anatomical specimens and computer simulators. 40 people can be trained there at the same time. It is the biggest laboratory of such profile in the world. The establishment of the WHC enabled to create and equip modern units: Implants and Auditory Perception Department, Epidemiology and Screening Department, Experimental Audiology Department, Genetics Department, Scientific Analysis Department, Balance Disorders Department, Bioimaging Research Center. 512 The WHC has 6 operating rooms equipped with state-of-the-art medical and multimedia equipment. Up to 50 operations per day is currently performed in the center. The number o hearing improving surgeries, as well as the number of long-lasting, complicated interdisciplinary procedures from the area of oral and maxillofacial surgery, reconstructive surgery and otoneurosurgery is still increasing. In a newly opened part of the Center there is 91 beds. The WHC is equipped with integrated system for audio and video recording. All telemedical connections used in everyday medical/clinical practice, such as telerehabilitation, telefitting, teleconsultations, are registered in a central data base. All surgical procedures can be registered and archived in a central surgical register. The whole video network works in Full HD resolution that ensures the picture of high definition and quality. The system allows to transmit live surgeries to any room in the Center. This creates outstanding educational possibilities, trainees can watch transmission on computer and projection screens. Thanks to this state-ofthe-art videoconference system we have a capability to connect with centers all over the world and realize live transmissions from operating and conference rooms. 513 EXCHANGE OF KNOWLEDGE: „WINDOW APPROACH WORKSHOP” -2 DAY COURSE Contemporary development of audiology and otosurgery enables us to bring effective help for almost every patient with hearing disorders and hearing loss. The examples of most fantastic solution for many people with hearing loss, giving them opportunity to get back to the world of sound are hearing implants. Meetings called Window Approach Workshops (WAW), held since 2006 at the Institute of Physiology and Pathology of Hearing, are devoted to technological developments and their practical applications. The workshop is devoted to the topic of partial deafness treatment and includes lectures, live surgeries and temporal bone training. The team of Prof. Skarzynski presents original surgical methods of cochlear implantation in cases of partial deafness and middle ear implantation in cases of mixed hearing loss applying round window approach (prof. Skarzynski’s technique). Participants of the meetings observe surgical transmissions of the operations conducted in the real time. Live operations are presented to the audience. For the operations various electrodes Flex, M, by Medel, SRA by Cochlear and standard electrode by Advanced Bionics are used. Middle ear implantations are performed with Vibrat SoundBridge by Med-El. Each of the operations is preceded by case presentation. Introductory presentation and supplementing lectures on cochlear implant fitting, speech therapy and technical solutions for rehabilitation are provided by Prof. Skarzynski and members od the Institute’s team. The most important part of the Workshop is the hands on training on the human specimens. The training part is held in the specially organized Education Center. WAW are organized in collaboration with the Institute of Sensory Organs and companies involved in elaboration of the cochlear implants – Cochlear, Med-El, Advanced Bionics companies. The workshop covers the topics interesting for: - the otosurgeons, biomedical engineers, rehabilitation specialists Workshop includes: - live transmissions of surgeries lectures temporal bone guided training (cochlear implantation in total and partial deafness, middle ear implants Contact Person Data [email protected] 514 INTERNATIONAL COURSE OF ENDOSCOPICE SINUSES – 2 DAYS International Course of Endoscopic Sinus Surgery has been organized by the Institute of Physiology and Pathology of Hearing since 2008. The course is meant for the rhinologist surgeons interested in FESS operations. The topics of the course cover a anatomy and radiology and a variety of techniques such as surgical approaches to maxillary, frontal, ethmoid and sphenoid sinuses; complications, postoperative complications, orbital decompression, new possibilities in endoscopic sinus surgery, endoscopic maxillary antrostomy, anterior and posterior ethmoidectomy, sphenoidotomy, endoscopic DCR, endoscopic sphenopalatine artery ligation (ESPAL), endoscopic modified Lothrop procedure, bath plug” technique” for CSF leak repair, lateral canthotomy and cantholysisendoscopic septoplasty and powered inferior turbinoplasty, maxillary sinus prephination, endoscopic approach to pituitary and clivus, endoscopic approach to the anterior cranial fossa. The formula of the meeting creates the opportunity to learn more about the theoretical aspects of paranasal sinus disorders, medical treatment and indications for surgery, and to individually conduct all procedures on fresh frozen head specimens. Moreover, there is an opportunity to share with others your own experience in the field of endoscopic sinus surgery. We encourage physicians who took part in the previous editions of the endoscopic sinus surgery course to come and share information about how the knowledge acquired at the course helped them in their everyday practice. The workshop covers the topics interesting for: - rhinosurgeons, -rhinologists, Workshop includes: - live transmissions of surgeries from the operating theatre lectures training on head specimens under the supervision of internationally renowned FESS surgeons/ image guided surgery Contact Person Data [email protected] 515 LISTENING IS „I CAN” - INTERNATIONAL SCIENTIFIC-TRAINING WORKSHOP FOR SPEECH THERAPISTS – 2 DAYS Listening is “I can” is conference series dedicated to the participants of the therapeutical process: patents, children, therapists, tutors, teachers, carers and grandparents. This workshop is devoted to dissemination of knowledge on rehabilitation of deaf and hard of hearing children who are candidates for cochlear implantation or are already implanted with the cochlear implant system. Basic rules of the presented rehabilitation methods: - Fastest possible diagnosis of the hearing impairment, - Providing the child with the best available device, - Immediate commencement of the therapy with the leading role of the parents, prepared and supported by the authorized specialists. The workshop covers the topics interesting for: - -speech therapists, educators, rehabilitation specialists, psychologists, parents and carers of the deaf and hard of hearing children Contact Person Data [email protected] 516 PRODUCTS: SYSTEM OF INTEGRATED COMMUNICATION OPERATIONS „SZOK”® Responding to social needs in terms of early detection of congenital and acquired defects and prophylaxis, the Institute of Physiology and Pathology of Hearing has built, in the years 20092011, a unique on a global scale System of Integrated Communication Operations “SZOK” ®. “SZOK”® integrates Institute’s information systems and introduces new possibilities, thanks to launching of the original software that enables novel ways of planning, implementing and managing large projects such as screening on a scale of the whole population of children in a given age-group. It enables implementing such projects on a countrywide or European scale. Innovativeness of the project lies in utilizing the remote system supporting patients’ diagnostics and allowing transferring the results of examinations to the health services sector. Integration of the patient’s data in the System’s Platform results in faster patient service leading to shortened waiting times for visits in the Institute and other specialist units. It may act as a comprehensive medical patient database. This system may also be successfully used in other health care providers and in different areas of medicine. It is a unique telemedical and e-Health solution. Innovative approach in screening programs performed by the Institute is based on mobile screening device – the Sense Examination Platform – allowing to conduct screening examinations outside medical units, e.g. in school, and to send the results to “SZOK”® automatically via the internet. Thanks to the diagnostic support tools the results coming though the “SZOK”® system are analyzed and evaluated by specialists quickly and efficiently. The open standard of transmission of the results of audiological screening results developed and implemented in “SZOK”® system enables acquiring results of tests performed by other institutions and collecting them in one place. Test results after evaluation are accumulated in the Base of Knowledge – a unit of “SZOK”® collecting data in the data warehouse and supporting advanced reporting capabilities thanks to the Business Intelligence class system. This solution collects , in form accessible for analysis, data from screening programs, from the Institute of Physiology and Pathology of Hearing medical data system, and from other sources, enabling epidemiological analyses. This program sets a novel direction in organizing screening programs. The Sense Examination Platform is a part of this system, it is a modern screening tool enabling early detection of hearing, vision and speech disorders. 517 NETWORK OF TELEAUDIOLOGY (proposal of cooperation within the network) Treatment of hearing impairments nowadays makes use of the numerous state-of-the-art technologies, such as hearing aids and various auditory implants, allowing hard-of-hearing and deaf people functioning in the word of sounds and communicating with others. These modern treatment methods usually entail complicated set-up, regulation and adjustment procedures requiring frequent consultations with an experienced specialist with access to dedicated equipment, usually available in specialist centers and hospitals. The treatment results are to a high degree dependent on the good organization of the medical care and rehabilitation. Patients’ visits in the specialist center often entail long trips from their domicile; they invest their time, sometimes take a full-day leave from work, and cover the cost of travel, which for many families may be a problem. Additionally, patients, particularly children and persons with collateral mental disorders, after the long travel are tired, irritated and unwilling to cooperate with the specialist. To remedy these problems and improve the quality of patient care, the Institute of Physiology and Pathology of Hearing (IFPS) developed and implemented into the clinical practice the National Network of Teleaudiology, a specialized network allowing the use of the internet and modern IT tools to provide medical care, rehabilitation and technical support for patients visiting a subsidiary or one of the affiliated policlinics of the Institute. The National Network of Teleaudiology was established in 2009. The system utilizes the newest software and videoconferencing equipment, as well as highly specialized procedures of pre and postoperative care over patients with hearing disorders. It enables the cooperation of medical doctors, clinical engineers, physicians, speech therapists and psychologists from all over the country to provide the best possible care to the patient. The National Network of Teleaudiology consists of: 19 cooperating centers in Poland, 1 center abroad (in Odessa, Ukraine), the network center in the World Hearing Center, over 40 highly trained support specialists. With the use of the National Network of Teleaudiology it is possible to assure the high level patient care in several areas, including: - Telediagnostics Medical teleconsultations Telefitting Telerehabilitation. Development of the National Network of Teleaudiology has been supported by the grant from the Norwegian Financial Mechanism “Programme for Development of National Network of Hearing Telerehabilitation”. 518 INSTITUTE OF RHEUMATOLOGY (Instytut Reumatologii im. prof. dr hab. med. Eleonory Reicher) Organisation Contact Data 1 Spartańska st., 02-637 Warsaw , Poland phone: +48 22 844 42 41 till 49 phone / fax: + 48 22 844-95-22 http://www.instytutreumatologii.pl/ Institute of Rheumatology is the leading institution in the fight against rheumatic diseases in Poland. It combines the latest scientific achievements with the diagnosis, treatment and rehabilitation. The idea of creating the Institute of Rheumatology in Poland dates back to 1930. At that time "The first convention regarding rheumatism diagnosis and treatment” took place in Inowrocław. The following conclusion was included in the resolutions passed at the convention: "the convention considers it is necessary to create an institute to test and treat skeletal disorders." However, this resolution was accomplished as late as after World War 2. The Institute offers highly specialized comprehensive hospital and outpatient treatment of adults and children with rheumatic diseases. In line with its mandate Institute of Rheumatology from the beginning deals with the research on rheumatic diseases. The results of clinical research and studies in basic fields help to explain the aetiopathogenesis of rheumatic diseases, to improve and widen diagnostic methods, to prepare and evaluate new methods of pharmacotherapy, surgical treatment and rehabilitation. The Institute conducts epidemiological studies the results of which are used in the treatment and prophylaxis of individual and social consequences of rheumatic diseases. As part of health promotion the Institute supports selfhelp support groups, publishes patient education materials, edits the journal "Złoty Środek", and cooperates closely with the media. Within 58 years the employees of the Institute of Rheumatology have published more than 4100 scientific articles, have been authors of 30 manuals in the field of rheumatology. The results of scientific research are presented at all important conventions and symposia in Poland and worldwide. The Institute of Rheumatology regularly cooperates with and conducts joint research with leading scientific and clinical centres worldwide. For the whole time of its existence the Institute has been involved in publishing activities, at first it published non-periodical publications, and since 1963 together with the Polish Society of Rheumatology it has been publishing a bimonthly (previously it was a quarterly) called "Reumatologia", and since 2000 a quarterly called "Central European Journal of Immunology.” 519 Since 1955 the Institute employees have been honoured with many prestigious awards and distinctions for their scientific achievements, and many of them are honoured members of Polish and foreign medical societies. Since its beginning the Institute has been training rheumatologists. In addition, the Institute organises training sessions for ward managers of other specialities, including general practitioners, nurses, rehabilitation therapists and students at the Warsaw Medical University in Warsaw - also for students studying in English. 520 INSTITUTE OF RURAL HEALTH (Instytut Medycyny Wsi im. Witolda Chodźki) Organisation Contact Data Contact Person Data 2, Jaczewskiego st., 20 – 090 Lublin, Poland Director of the Institute: Andrzej Wojtyła, MD, PhD phone: +48 81 71 84 410 fax: + 48 81 74 78 646 Deputy Director for Science: Prof. Jerzy Zagórski, MD, PhD e-mail: [email protected] http://www.imw.lublin.pl/index.php/instituteof-rural-health The Institute of Rural Health (IMW) was founded in 1951 by a group of physicians and researchers assembled around Prof. Witold Chodźko. It is a research and healthcare institution subordinate to the Ministry of Health, acting on behalf of the widely understood protection of health of the rural population and improvement of sanitary-hygienic standards in the rural environment. Main directions of the IMW activity: Scientific studies, research-development activities and projects for implementation; Diagnostic, treatment, rehabilitation and decision-making activities; Training courses, mainly for primary health care physicians; Editorial activity. The Institute of Rural Health employs over 250 staff, including specialists in various areas: physicians, veterinary doctors, biologists, toxicologists, chemists, physicists, psychologists, sociologists and computer scientists. Scope of research problems covered by the Institute: Evaluation of the state of health of the rural population; Evaluation of the environmental habitation and work in rural areas; Shaping health care in rural areas. 521 The scientific studies are performed based on research departments and independent scientific laboratories which specialize in the following areas: Classification and characteristics of biological hazards in all occupations, with particular consideration of agriculture, the food industry, forestry and timber industries; Etiopathogenesis and diagnostics of occupational diseases induced by aerogenic organic dust, with particular consideration of microbial agents present in dust; Complex (microbiological) studies of water from the municipal water supply and household systems, as well as water from wells. Studies of biological contaminants, wastewater, sewage sludge, organic and mineralorganic fertilizers, and issuing opinions concerning the effect of the above-mentioned fertilizers on human health; Seroepidemiologic studies of selected occupational zoonoses (brucellosis, haemorrhagic fever with renal syndrome – HFRS, Q fever, erysipeloid, echinococcosis), and Environmentally conditioned native parasitoses (echinococcosis, geohelmintoses), as well as imported zoonoses (malaria, etc.). Epidemiology, etiopathogenesis and diagnostics of zoonoses from the aspect of occupational exposure and risk for the rural population, with particular consideration of tick-transmitted diseases; diseases caused by parasitic protozoa, diagnosed with the use of serologic methods, modern molecular biology techniques, and parasitological methods. Health risk resulting from the contamination of the rural environment with pesticides and of the habitation environment with biocidal substances (field-laboratory activities); studies of the toxic effect of drugs; studies of the biological activity of substances of natural and synthetic origin; studies of animal-to-human transmission of biocidal substances. Ergonomic evaluation of work conditions on private farms, recognition and evaluation of exposure to hazardous physical factors among private farmers (exposure to noise, infrasound, mechanical vibration, agricultural dust, asbestos, unfavourable microclimate, hearing loss among farmers, physical load among farmers, pain complaints on the part of the musculoskeletal system. State of health of the rural population, including disabled rural inhabitants, and life situation of rural children; psycho-social risk for health and life among private farmers; health promotion – health promoting behaviours and promotion of work safety in agriculture. Detection of environmental health risk and analysis of the effect of selected xenobionts on genetic material with the use of molecular biology methods. Scientific studies in the area of the evaluation of the character of interactions between drugs, with the consideration of interactions taking place on the pharmacodynamic and pharmacokinetic levels. 522 Evaluation of anti-convulsant activity of substances of natural origin and those chemically synthetized, and their effect on the protective activity of anti-epileptic drugs; searching for anti-epileptic substances with strong potential of anti-epileptic activity. Evaluation of neurotoxic activity of pesticides in studies in vitro. Chemoprevention of cancer – investigation of new substances and preparations as potential dietary supplements, evaluation of anti-cancer activity of synthetic substances and substances of natural origin with the use of in vitro methods (human and animal cell cultures) and in vivo; studies of molecular mechanisms of the activity of a substance within a cell; studies of neuroprotective activity of substances, as well as investigating the biological activity of nano-structures. Monitoring of health problems of the rural population associated with exposure to hazardous factors in agriculture, evaluation of health behaviours and attitudes. Carrying out promotional and educational actions. Implementation of the latest achievements of the molecular sciences to solve clinical problems associated with disorders in the pathogenesis of which there occurs a fibroproliferative element, with particular consideration of lung diseases. Analysis of the quality of services provided by primary health care physicians; organization of training courses for Primary Health Care physicians. Carrying out studies, monitoring and analyses of differences occurring in health, especially in order to level-out differences between urban and rural inhabitants. Population studies of health behaviours of the Polish population. Health Care Services: Health care services are provided based on the Clinical Hospital with its Wards, Specialist Outpatient Department for Rural Occupational Diseases, within which function 26 specialist consultation rooms, a Rehabilitation Centre, Laboratory for Functional Examinations Research, Laboratory of Endoscopy, and Department of Radiology. Clinical Hospital The primary task of the Clinical Hospital are: diagnostics, treatment and rehabilitation making decisions and expertise on occupational disease claims decision-making for courts and the Regional Centre of Occupational Medicine; specialist training courses scientific research activity Clinic for Internal and Occupational Diseases and Toxicology Hospitalization of patients with cardiovascular disorders, respiratory diseases (including farmer’s lung), gastrointestinal system diseases, metabolic diseases, and endocrine disorders. 523 Department of Rehabilitation specializes in the rehabilitation of back pain syndrome, discopathy, degenerative joint disease, shoulder, elbow and wrist pain syndrome, nerve root syndrome, and motor system function disorders in post-injury conditions. Diabetology Ward is the only ward in the Lublin Region providing highly specialist treatment for all types of diabetes, including: treatment of diabetes and its complications, pre-pregnancy diabetes with the use of insulin pumps, juvenile diabetes, diabetic foot syndrome, metabolic disorders and obesity. Within the structure of the Clinical Hospital there also function: Department of Imaging Diagnostics specialized in mammographic examinations; Department of Clinical Endoscopy performing mainly gastroscopy and colonoscopy, Department of Functional Tests carrying out examinations of the respiratory and cardiovascular systems, and diagnostics and treatment of nocturnal dyspnea. 524 Specialist Outpatient Department The Outpatient Department provides treatment, diagnostics, consultations, medical opinions and didactics, mainly on behalf of the rural population. Within its structure, apart from consultation rooms, there are specialist laboratories: Densitometric Laboratory, Electroencephalographic Laboratory (EEG) Echocardiographic Laboratory (ECG) and Treatment Room, where fine needle aspiration biopsy is performed (BAC), and specimens taken for histopathologic tests. Rehabilitation Centre The Centre provides rehabilitation services for patients from the Rehabilitation Ward of the Institute’s Clinical Hospital, patients reporting to the Outpatient Department for Rehabilitation, and referred from other health care facilities. Services are provided for patients with disorders concerning the central and peripheral nervous system, those who have undergone injuries, fractures, patients with disorders concerning the motor organs, systemic diseases, and amputated extremities. The Rehabilitation Centre offers the following procedures: physical therapy hydrotherapy kinezitherapy therapeutic massage Educational Activity: The Department for Post-Graduate Education and Regional Centre for the Education of Family Physicians. The Institute also provides apprenticeships for physicians for specialization degree in the area of family medicine and internal diseases. In addition, the Institute is authorized to carry out training courses for physicians: to obtain qualifications for performing medical examinations of candidates for driving licenses, and is the appeal institution for decisions made in this respect by the authorized physician at the Regional Centre of Occupational Medicine, to obtain qualifications for performing medical examinations and issuing medical decisions for people who apply for a license to possess a firearm, and is the appeal institution for decisions made by authorized physicians. Editorial Activity: The Institute’s editorial activity covers the publication of periodicals and books. A high international position has been obtained by the scientific journal edited and published semiannually since 1994 - Annals of Agricultural and Environmental Medicine (AAEM – www.aaem.pl), which since 2000 has been indexed and abstracted in the CURRENT CONTENTS database and indexed by the Institute for Scientific Information (ISI) in Philadelphia. Since 2007, the Institute has been publishing the multidisciplinary periodical Journal of PreClinical and Clinical Research (JPCCR – www.jpccr.eu), aimed at promoting international cooperation in these disciplines.The thematic scope of the journal concerns especially such scientific disciplines as: human and animal physiology, clinical pharmacology, oncology, 525 molecular cell biology, toxicology, biotechnology and biophysics. Making the journal available on-line in English, and the creation of the international editorial committee, is aimed at expanding the scope of international exchange and scientific presentation from a wide scope of aspects combinding primary research with their applications in medicine and biology. The Journal of Pre-Clinical and Clinical Research is published on-line in a continuous way – the articles are printed twice a year The third journal published in by the Institute is the quarterly Medycyna Ogólna (General Medicine), addressed mainly to medical staff, a wide circle of hygienists and organizers of health care. Reports are also published concerning the environment of life and work, as well as psychosocial problems. From 2012, the quarterly will expand its contents by the addition of general health problems, adopting the name Medycyna Ogólna i Nauki o Zdrowiu – www.monz.pl (General Medicine and Health Science). In addition, since 1994, an editorial series has been published, Monographs of the Institute, within which more than 50 books have been published to-date. 526 INSTITUTE OF SENSORY ORGANS (Instytut Narządów Zmysłów) Organisation Contact Data JHS Editorial Office 1, Mokra st, Kajetany, 05 - 830 Nadarzyn, Poland phone: +48 22 887 86 12 fax: + 48 22 887 60 21 e-mail: [email protected] http://www.inz.waw.pl/en 1, Mokra st, Kajetany, 05 - 830 Nadarzyn, Poland phone: +48 22 3560389 fax: +48 22 3560367 e-mail: [email protected] Institute of Sensory Organs was established in 2008 with the main aim of designing, conducting and implementing the research and scientific works in the scope of prophylaxis, diagnosis, treatment and rehabilitation related to sense organ diseases. The first accomplished project consisted in development, testing and implementation of the Senses Organs Examination Platform software designed to conduct screening trials of hearing, sight and speech in children, youth and persons with particular education needs. Another task realized by the ISO is conducting trainings and workshops. To fulfill that aim, the ISO cooperates with the best domestic and international specialists and scientific research units. It cooperates with the Institute of Physiology and Pathology of Hearing and companies such as Med-El, Cochlear and Advanced Bionics. ISO organizes training workshops related to the modern otosurgery - „Window Approach Workshop”. It co-organizes International Course of Endoscopic Sinus Surgery. In order to offer an international forum for professionals and doctors from the whole world, thanks to which there will be possible an exchange of information, publications of achievements, researches and works, the Institute of Sensory Organs has started publication of medical journal “Journal of Hearing Science”. It is dedicated to current peer-reviewed scientific research in all areas of Otolaryngology, Audiology, Phoniatrics, and Rhinology. It also assists hearing practitioners by providing important knowledge helpful to patients with hearing, voice, speech, and balance disorders. JHS has a distinguished International Advisory Board and an impressive Editorial Board. Their high academic standing ensures that the journal produces multidisciplinary papers of the highest quality. The broad international membership promotes fair and thorough assessment. Journal is published both in paper and electronic form. Due to the Polish Presidency in European Union the Institute of Sensory Organs decided to establish international cooperation with foreign centers in order to exchange the knowledge and scientific experience and start new activities. International agreements of cooperation were signed between the “Institute of Sensory Organs” and “National Medical Center of Ministry of Health of Tajikistan Republic” (Dushanbe, Tajikistan), “Tashkent Medical Academy” (Tashkent, Uzbekistan), „Association of Polish origin doctors in Volyn” (Luck, Ukraine), „National Center of Motherhood and Childhood Protection” (Bishkek, Kirgizstan). 527 PRODUCTS: SENSE EXAMINATION PLATFORM SENSE EXAMINATION PLATFORM – device for hearing, vision and speech screening. The platform makes it possible to perform both the screening tests and storage the test results automatically in the central database as well as to analyze them comprehensively. The stored results feature a unique identifier, therefore the complete protection of personal data of the tested people is provided according to the operative legal regulations and recommendations of the Chief Inspector of Personal Data Protection (GIODO). This solution guarantees that the epidemiological analysis can be performed in the areas where any devices cooperating with Sense Examination Platform are used. The platform is based on the advanced, central computer system and netbooks provided with the audiometric earphones and the button of a tested person. The computers communicate with the central database by Internet. The device makes it possible to perform the following tests: audiometric test - "Audiogram 2009", hearing screening test - "I can hear 2009", speech screening test - "I can speak 2009", vision screening test - "I can see 2009", audiological questionnaire - "Questionnaire", DDT test, GDT test. Thanks to the applied on-line solutions, it is possible to provide every user of the platform with the statistics and to send them directly information about recommendations for persons whose test results are incorrect. The device is equipped with the automatic software update engine. All procedures related to checking of the software version and any update are performed automatically without any operation of a user. The device was presented at various fairs, exhibitions and conferences, where received multiple awards, medals and recognitions: Gold medal for the Senses Examination Platform, International Fair of Innovation, Scientific Research and New Technologies „MEDINNOVA 2011”, Casablanca, 2011; Award of the Minister of Science and Higher Education, Warsaw 2011; Gold medal for the Senses Examination Platform, International Inventions Fair in Seoul, Seoul 2010; Special award of Taiwan, International Inventions Fair in Seoul, Seoul 2010; Gold medal for the Home Rehabilitation Clinic, International Inventions Fair in Seoul, Seoul 2010; Special prize for the Home Rehabilitation Clinic, International Inventions Fair in Seoul, Seoul 2010; Gold medal, 62nd iENA Nuremberg International Trade Show – “Ideas-Inventions-New Products”, Nuremberg 2010 and numerous others. 528 EXCHANGE OF KNOWLEDGE: WINDOW APPRACH WORKSHOP – 2 DAYS The workshop is organized by the Institute since 2009. The “Window Approach Workshop” meetings are organized with the aim of exchanging knowledge and information on new surgery methods and application of the state-of-the-art technical solutions – hearing implants – between surgeons and experts dealing with the hearing disorders from Europe and all over the world. During the workshop, original methods for implanting cochlear implants in the case of persons with partial deafness and implants of middle ear in the case of mixed hearing impairments using surgery access through the round window, developed by the Institute, are presented. Participants of the meeting learn surgery techniques presented during surgeries which are transmitted to the conference hall. Participants can comment and ask questions to the surgeon at the moment of operation. The WAW workshop is supplemented by a practical training carried out at the specially organized Laboratory. WAW are organized in collaboration with the Institute of Physiology and Pathology of Hearing and companies involved in elaboration of the cochlear implants – Cochlear, Med-El, Advanced Bionics companies. The workshop covers the topics interesting for: - the otosurgeons, - -biomedical engineers, - -rehabilitation specialists Workshop includes: - live transmissions of surgeries, - lectures, - temporal bone guided training (cochlear implantation in total and partial deafness, middle ear implants) 529 INTERNATIONAL COURSE OF ENDOSCOPICE SINUSES – 2 DAYS International Course of Endoscopic Sinus Surgery has been organized since 2008. The course is organized in collaboration with the Institute of Physiology and Pathology of Hearing, Warsaw, Poland. The course is meant for the rhinologists who whould like to extend their knowledge and rhinologist surgeons interested in FESS operations. The topics of the course cover a anatomy and radiology and a variety of techniques such as surgical approaches to maxillary, frontal, ethmoid and sphenoid sinuses; complications, postoperative complications, orbital decompression, new possibilities in endoscopic sinus surgery, endoscopic maxillary antrostomy, anterior and posterior ethmoidectomy, sphenoidotomy, endoscopic DCR, endoscopic sphenopalatine artery ligation (ESPAL), endoscopic modified Lothrop procedure, bath plug” technique” for CSF leak repair, lateral canthotomy and cantholysis endoscopic septoplasty and powered inferior turbinoplasty, maxillary sinus prephination, endoscopic approach to pituitary and clivus, endoscopic approach to the anterior cranial fossa. The formula of the meeting creates the opportunity to learn more about the theoretical aspects of paranasal sinus disorders, medical treatment and indications for surgery, and to individually conduct all procedures on fresh frozen head specimens. Moreover, there is an opportunity to share with others your own experience in the field of endoscopic sinus surgery. We encourage physicians who took part in the previous editions of the endoscopic sinus surgery course to come and share information about how the knowledge acquired at the course helped them in their everyday practice. The workshop covers the topics interesting for: - rhinosurgeons, -rhinologists, Workshop includes: - live transmissions of surgeries from the operating theatre lectures training on head specimens under the supervision of internationally renowned FESS surgeons/ image guided surgery 530 JOURNAL OF HEARING SCIENCE – PEER REVIEWED JOURNAL represents a new publication by International Scientific Literature, Inc., USA. The journal is dedicated to current peer-reviewed scientific research in all areas of Otolaryngology, Audiology, Phoniatrics, and Rhinology including, but not limited to: Anatomy, Audiology, Biomedical Engineering, Bronchoesophagology, Communicative disorders, Epidemiology, Facial plastic and reconstructive surgery, Genetics, Head and neck surgery, Maxillofacial surgery, Oncology, Otolaryngology, Phoniatrics ,Physiology, Psychoacoustics, Radiographic imaging, Rehabilitation, Rhinology, Speech and hearing defects. Our primary mission is to offer an international forum for professional information exchange. Also, we would like to assist hearing practitioners by providing important knowledge helpful to patients with hearing, voice, speech, and balance disorders. The journal is an open access type of publication which allows all readers around the world free access to articles. Moreover, we declare no publication fees or page charges. Given these attractive features, we ask that you consider Journal of Hearing Science for your next paper. We sincerely invite you to submit your manuscript to JHS. JHS has a distinguished International Advisory Board and an impressive Editorial Board. Their high academic standing ensures that the journal produces multidisciplinary papers of the highest quality. The broad international membership promotes fair and thorough assessment. For more information about the Journal and manuscript submission please visit our website at http://www.journalofhearingscience.com 531 MARIA SKŁODOWSKA-CURIE MEMORIAL CANCER CENTER AND INSTITUTE OF ONCOLOGY (MSCMCCIO) (Centrum Onkologii-Instytut im. Marii Skłodowskiej-Curie) Organisation Contact Data 5, WK Roentgena st., 02-781 Warsaw , Poland phone: +48 22 644-02-00 fax: + 48 22 644-02-08 http://www.coi.waw.pl MSCMCCIO is the leading Polish comprehensive cancer center, as well as the primary government research institution devoted solely to oncology. Founded in 1932, currently it is divided into 9 specialized clinical departments responsible for the diagnostics and therapy of different tumor types and other departments devoted to therapy, epidemiology, prevention, pathology, imaging and basic research in the cancer biology. The clinical building houses 745 hospital beds; there is also a separate research building with laboratories and educational facilities. The size of the institution can be represented by a quota of numbers – in 2009 the inpatient clinics treated 28000 patients; another 26000 patients were treated in the One-Day Chemotherapy Section, and as many as 340 000 outpatient visits were recorded. MSCMCCIO is located in the southern suburbs of Warsaw, 5 km from the Warsaw airport and is easily accessible by public transport. The key points for future collaborations with other institutions are: Collected clinical records of nearly 500 000 patients for retrospective studies, including histopathological material. One of the unique possibilities is access to data of rare types of tumors with long-term follow-up. Prospective biobanking of tissues for translational studies, including tumor tissue and serum samples. Highly experienced medical staff involved in multimodal patient treatment in specified types of cancer. The quality of international cooperation is confirmed by the fact that MSCMCCIO belongs to Network of Core Institution of European Organisation for Research and Treatment of Cancer. Experienced team of researchers actively involved in high-throughput genomic technologies, cooperating in national and international scientific grants as well as EU projects. Administrative infrastructure for academia-initiated and sponsored clinical trials. Organization of molecular diagnostic units and oncological genetic counseling Development of new diagnostic tools used in molecular diagnostics of cancer MSCMCCIO would like to cooperation with the units interested in basic science as well as in translational research in the area of molecular basis of cancer. We are particularly interested in role proteins responsible for tissue specific expression of the genes. We 532 are also interested in the creation of tests which permit to divide patients in the same pathological diagnosis onto a groups in which they can get the maximal clinical benefit from particular treatment.. Basic science in the oncology Research in the Institute is also focused on issues of early detection of cancer cells in body fluids and secretions and possibility of usage of the miRNA as a marker of particular type of cancer 533 NATIONAL INSTITUTE OF TUBERCULOSIS AND LUNG DISEASES (Instytut Gruźlicy i Chorób Płuc) Organisation Contact Data Contact Person Data 26, Płocka st, 01-138, Warsaw, Poland Prof. Joanna Chorostowska-Wynimko MD PhD DSc, Scientific Director phone: +48 22 43 12 428, + 48 22 43 12 213 fax: +48 22 43 12 452 e-mail: [email protected] http://www.igichp.edu.pl/ phone: +48 22 43 12 386 fax: +48 22 43 12 358 e-mail: [email protected] National Tuberculosis and Lungs Diseases Research Institute in Warsaw is a leading Polish and East-European Research Centre in the field of tuberculosis, lung malignancies, pulmonary interstitial diseases, pulmonary vasculitis, chronic obstructive pulmonary disease (COPD) and many others. It represents a long-term experience in the research and implementation of practical measures in the domain of lung diseases. Its key medical and scientific position in Poland resulted in numerous publications in leading international medical journals as well as involvement in various national and international expert groups. The Institute is also the major teaching institution for respiratory professionals in Poland. It has regularly participated in several EU scientific programs and networks. 534 Ongoing research projects of the Institute are aimed at following topic: 1. Optimization of diagnostics and treatment of tuberculosis in Poland. 2. Epidemiology of tuberculosis in Poland. 3. Pathogenesis, diagnosis and treatment of respiratory system. 4. Optimization of diagnosis and treatment of respiratory tract infections. 5. Pathogenesis, diagnosis and treatment of respiratory insufficiency. 6. Evaluation of sleep breathing problems on cardiovascular. 7. Improved recognition of interstitial lung diseases. 8. Venous thromboembolism and pulmonary hypertension. 9. Optimization of diagnosis and treatment in diseases of trachea and proximal bronchi. 10. Optimization of diagnosis and treatment of bronchial asthma. 11. Improving methods of diagnosis and treatment of chronic respiratory diseases and method of rehabilitation. 12. Chronic Obstructive Pulmonary Disease. (COPD) Example of research projects performed by the Institute within international cooperation: European Reference Laboratory Network for Tuberculosis (ERLN-TB) – To strengthen TB Diagnosis, Drug Susceptibility Testing and International Coordination. PAN – European Network for the Study and Clinical Management of Drug Resistant Tuberculosis. (7PR- HEALTH –TB PAN-NET). Markers for emphysema versus airway disease in COPD (7PR- HEALTH-EVA) Indicators for Monitoring COPD and Asthma in the EU (IMCA II) COST – European Cooperation in Science and Technology - Obstructive Sleep Apnea Chronic Obstructive Pulmonary Disease Exacerbations 535 Geriatric Study in Europe on Health Effects of Air Quality in Nursing Homes. Transcontinental COPD Genetic Study (TCGS). Establishment of the Alpha-1-antitripson (A1AT) Deficiency Screening Program and A1AT deficiency register in Poland. Introducing Standards of the Best Medical Practice for the Patients with Inherited Alpha-1 Antitripsin Deficiency in Central Eastern Europe. 536 Institute also organizes national postgraduate courses in the field of: tuberculosis; pneumonology; endoscopy; lung cancer; COPD and cor pulmonale; pulmonary embolism; thoracic surgery; radiology; respiratory pathophysiology; microbiology and immunology. Annually it is number of 30 courses lasting 3 - 30 days and involving above 1000 participant/year. Institute can also offer individual trainings in diagnostic techniques: radiological molecular immunodiagnostics bronchoscope Moreover Institute edits and publishes following journals: 1. Acta Pneumologica Allergologica Pediatrica. 2.Pneumonologia i Alergologia Polska (since 1909!) (Polish Pneumonology and Alergology) Of those, Pneumonologia i Alergologia Polska is official journal of Polish Respiratory Society and the leading Polish journal in the field of pneumonology, indexed in MEDLINE and other bibliographic data-bases. Out of 80 research staff of the Institute 20 serve as editorial board members of national and international journals. 537 POLISH MOTHER'S MEMORIAL HOSPITAL - RESEARCH INSTITUTE (Instytut Centrum Zdrowia Matki Polki) Organisation Contact Data 281/289, Rzgowska st., 93 – 339 Łódź , Poland phone: +48 42 271 12 66 ; +48 42 271 16 76 fax: +48 42 646 66 53 e-mail: [email protected] http://www.iczmp.edu.pl/index_en.htm Clinical activity Polish Mother's Memorial Hospital- Research Institute, in Łódź (Lodz) is one of the largest highly specialized medical complexes in Poland. The Hospital is composed of two major units: Gynaecological/ Obstetric and Paediatric and is a leading medical institute of perinatology, gynaecology, obstetrics and paediatrics. Owing to its multi-profile character the Hospital provides comprehensive management of risk pregnancy complicated by maternal diabetes, hypertension, epilepsy, heart diseases or infections, as well as of cases characterized by the most difficult gynaecological pathology. The entire spectrum of specialties in the care of woman (mother) and child till the age of 18, the state-of-the-art level of medical diagnostics, the annual number of hospital admissions over 40 thousand, the annual number of out-patient admissions about 100 thousands are only a few characteristics of this huge medical post. The Institute collaborates with the Ministry of Science and Higher Education as well as Ministry of Health and participates in numerous national research programmes, of which those towards `Improvement of Perinatal Care` and `Prophylaxis & Early Detection of Uterine Cervix Cancer` seem most spectacular. The Gynaecology / Obstetrics part includes 16 clinical and diagnostic departments and offers about 500 beds including 110 for newborns. Modern diagnostic laboratories meeting international standards of quality, are fully supplied with the most sophisticated and up-to-date equipment. The Departments include: Perinatology & Gynaecology; Maternal-Fetal Medicine & Gynaecology; Endocrinology & Metabolic Diseases; Operative and Endoscopic Gynaecology; Obstetrics & Gynaecology; Gynaecology; Oncological Surgery and Breast Diseases; Gynaecology, Procreation & Fetus Therapy; Neonatology; Operative Gynaecology; Diagnosis 538 and Prophylaxis of Congenital Malformations; Genetics; Clinical Pathomorphology; Centre of Medical Laboratory Diagnostics; ICU. The Department of Diagnosis and Prophylaxis of Congenital Malformations carries out sonographic examinations of the fetus as well as echocardiography using colour doppler. Fetal imaging is also performed by means of MRI in the Department of Diagnostic Imaging. Specialists from the Gynaecology, Procreation & Fetus Therapy apply successfully intrauterine therapy in the fetus which was a completely unique achievement in Poland. Delivery Rooms are prepared to admit every obstetric and fetal pathology due to prematurity or intrauterine growth retardation. The Hospital promotes the idea of family delivery and rooming-in system. Department of Endocrinology covers the whole spectrum of hormone pathology in children, adolescents and in adult patients. The breast diseases are diagnosed comprehensively by team of radiologists, pathologists and oncologists and treated in the Department of Oncological Surgery and Breast Diseases. The Paediatric part houses 16 clinical and diagnostic departments, the total number of beds reaches 430 the profile of activity includes: general paediatrics, diseases of infants and neonates including congenital malformations, gastroenterology, allergology, cardiology, cardiac-surgery, neurology, neurosurgery, paediatric and neonatal surgery, orthopaedics, anaesthesiology, rehabilitation, ENT diseases, ophthalmology. Most cardiac-surgery operations are corrections of congenital heart anomalies in newborns and infants. Diagnostic Imaging uses high technology scanners: 3TMR and 256 slices CT. Modern administrative management system, competent information systems, collaboration with medical centres in Poland and abroad via the Internet, satellite or radio links result in the best quality of the services provided. 539 Scientific activity Polish Mother’s Memorial Hospital (PMMH), Research Institute was established in September 1997. As grade III referential centre, the Institute is a country leading medical post with research and service activities covering perinatology, gynaecology, obstetrics and paediatrics. Highly qualified medical staff, sophisticated equipment and effective organizational structures form solid fundamentals for excellent diagnosis and comprehensive treatment. The Institute houses 32 clinical departments and multi-profile diagnostic departments. Research policy is supervised by 32 professors of medicine and 30 associate professors. The Research Council acts as an advisory body which coordinates statutory actions of the Institute and is authorized to confer doctor and associate professor degrees in medicine. Priority scientific tasks carried out at the Institute concern: Studies on pathogenesis of disturbances in pregnancy complicated by EPH -gestosis, epilepsy, diabetes, intrauterine infections or heart diseases. Studies on the mechanisms of infertility. Applying new methods in the treatment of infertility. Assessment of diagnostic and therapeutic methods. Studies on pathogenesis and therapy of diseases of the perimenopausal period. Diagnosis, monitoring and therapy of congenital malformations of the central nervous system (CNS), circulatory system, respiratory system, alimentary tract, musculoskeletal system and other anomalies in the fetus, newborn and child. Diagnosis and treatment of newborns with low and very low body mass, macrosomy, infections, congenital malformations and other diseases. Diagnosis and treatment of the sense organ diseases in children. Diagnosis and treatment of diseases of alimentary system in children. Diagnosis and treatment of maternal and infantile infection. Autoimmune processes in the pathogenesis of disturbances in pregnancy, female diseases and diseases of the childhood. Assessment of clinical significance of monitored therapy. Diagnostics and therapy of neoplasms, particularly those of the female reproductory organ, the breast and endocrine glands, using molecular biology methods with constant clinical and morphological supervision. PMMH-RI offers advanced postgraduate courses in most of mentioned above medical specialties. It could be organized according to previously made individual arrangements. 540 THE CARDINAL STEFAN WYSZYŃSKI INSTITUTE OF CARDIOLOGY (Instytut Kardiologii) Organisation Contact Data 42, Alpejska st., 04 – 628 Warsaw, Poland phone: +48 22 343 44 50 fax: +48 22 343 45 00 e-mail: [email protected] http://www.iczmp.edu.pl/index_en.htm The Institute of Cardiology is the main Polish clinical center of cardiology and cardiosurgery with the highest reference score. It plays an important role in postgraduate training and education in cardiology. As a dynamically developing academic and research center and the country pioneer in introducing and propagating new methods of cardiac diagnosis and treatment, we would like to enable you to receive training, mainly in the field of CT imaging cardiology (Cardiac Magnetic Resonance and Multislice Computer Tomography), interventional cardiac treatment and cardiosurgical interventions. The clinical activity in the Institute focuses on interventional treatment of acute coronary syndromes, diagnosis and treatment of coronary artery disease and cardiac insufficiency as well as acquired and congenital heart defects. The clinical activity also includes diagnosing and treating arterial hypertension and arrhythmia. The procedures performed at the Institute include cardiosurgery and heart transplantation as well as imaging diagnostics. All main innovative interventional methods of non-surgical cardiac therapy now used in Poland have been introduced by the Institute of Cardiology specialists. Morover, Institute actively participates in congresses and workshops organized by Chinese and Hindi cardiologists. One of the best examples for that is that since 2006 the Director of the Institute, Professor Witold Rużyłło, has been inviting for “China Interventional Therapeutics” Congress organized by Chinese Medical Association. During this year’s Congress, which took part on 15th-18th March 2012, Professor Rużyłło was chairing the session and presented the latest Institute’s achievements in the fields of valvular heart disase. This is to mention, that Congress, which is one of the largest and most significant scientific and training events on interventional cardiology in Asian-Pacific Region, gathered over 5.000 experts from all around the world. Our Institute is also involved in cooperation with research institutions from India majoring in interventional cardiology. Thanks to many conferences either in India and Poland, we carry on 541 our cooperation. In October, 2010 Professor Adam Witkowski, the Head of Department of Cardiology and Interventional Angiology, was invited by Cardiovascular Society of India for PCR Conference held in Mumbai as a chairperson. In September 2011 Professor Witkowski also took part in the conference “Trend Asia Pacific 2011”, that took place in Hong Kong, where he presented Institute’s clinical experiences in interventional, transluminal / interventional treatment of resistant hypertension using the method of renal denervation. In February 2012 Professor Adam Witkowski took part in the National Course on Percutaneous Cardio-Vascular Interventions in New Delhi. It is essential to mention that the forthcoming April’s Course on Cardiovascular Interventions in Warsaw will be a great opportunity to discuss further scientific and development cooperation. As far as postgraduate training is concerned, we can offer you the following courses: 1) “Meet the experts” Advanced Course on Interventional Cardiology – 2 days What is the value of participating? As an Interventional Cardiology (IC), you will get access to the latest updates in the field of IC and to topics related to your professional development. You will be part of a diverse mix of independent experts and participants. In addition, you will be able to exchange and interact in group of experts and other course participants which facilitates a high level of open discussions and sharing of best practices. This program includes such imporatant topics such as: IVUS, FFR and OCT - Acute Coronary Syndrome Multivessel Coronary Artery Disease Left Main Valve therapy PFO/ASD/PDA closure Carotid stenting Pharnacology Course Description This course covers the main topics of IC and includes expert presentations, case-review sessions. The program features a highly interactive format. Target Audience The “MEET THE EXPERTS” programme has been developed specifically for IC Fellows in their mid and/or final years of training. 542 2) “Meet the experts” Echocardiography – its role in modern diagnosis and management – 3 days What is the value of participating? The course will give you a comprehensive and contemporary view on ultrasonic imaging of the heart. It will focus on general as well as detailed considerations in a field of coronary artery disease, valvular and congenital heart disease. Among presentations on selected issues, there will be an opportunity for open discussions and sharing opinion with experts. The specific section on interesting cases will provide you with more practical approach to data acquisition and its interpretation. Target Audience The “MEET THE EXPERTS” programme has been developed for cardiologists in their preliminary and mid years of training as well as to sonographers wishing to enrich their knowledge and experience. Topics: - Coronary Artery Disease - Valvular Heart Disease - Congenital Heart Disease 3) “Meet the experts” Advanced Course on ECG – 2 days What is the purpose of the course? The purpose of the course is the improvement in electrocardiography. The course is dedicated to doctors that are familiar with basic electrocardiology. This program includes such imporatant topics such as - ECG in diagnosis of genetic diseases ECG in patients with pacemakers Holter ECG Basic electrophysiology Course Description The course consists of lectures and interactive seminaries (using voting system) 543 4) “Meet the experts” Cardiovascular Imaging – Echocardiography, MRI, CT – 1 day What is the purpose of the course? The course is dedicated to doctors specializing in cardiology in their early and mid years of training. This program includes such imporatant topics such as - Multislice CT in the noninvasive diagnosis of coronary artery disease Magnetic resonance of the heart Usefulness of the available noninvasive methods in the assessment of function/perfusion/viability of the cardiac muscle Course Description The course covers the main topics of cardiovascular imaging and includes case presentations. 544 Catalogue of technologies developed by Polish Research Institutes MINING, TECHNICAL GEOLOGY, GEODESY, POWER ENGINEERING AND TRANSPORT 545 AUTOMOTIVE INDUSTRY INSTITUTE (Przemysłowy Instytut Motoryzacji) Organisation Contact Data Contact Person Data 55, Jagiellońska st, 03 – 301 Warsaw, Poland Paweł Goller phone: +48 22 7777 015 fax: + 48 22 7777 020 e – mail: [email protected] phone: +48 22 22 7777 051 e – mail: [email protected] http://en.pimot.org.pl/ Automotive Industry Institute (PIMOT) is a research and development unit under the Ministry of Economy. PIMOT was established in 1972 as a central unit to provide research and scientific support for the Polish automotive industry. At present, PIMOT is an A category research institute where scientific research and development works are carried out in the field of automotive engineering, vehicle development, road safety improvement, alternative vehicle powering methods, as well as fuels, biofuels, and renewable energy sources. These works are aimed at innovations but they are also deeply rooted in economic realities of Poland and they are consistent with the objectives and priorities of the EU Strategy 2020. The PIMOT mission is to provide Polish entrepreneurs (chiefly of the transport, fuels, and renewable energy sources sectors) with strong scientific and research support in the processes of product development and introduction of the products into world markets. PIMOT offers substantive technical support to the state administration bodies that pursue strategic objectives related to transport safety, environmental protection, and energy security of the country. From the outset of the introduction of a uniform system of type-approval and certification of vehicles and vehicle parts in Poland (the beginning of 1980s), the Automotive Industry Institute has been playing a key role in it as an element of the worldwide UN ECE type-approval system; since 2004, the Institute has also been playing such a role in the EU type-approval system. PIMOT has been authorised by the Minister appropriate for transport issues and by international organisations to carry out tests for conformity with over 40 UN ECE Regulations and a similar number of EU Directives. A characteristic feature of the tests carried out is their high quality confirmed by numerous ISO certificates and accreditation of the test procedures by the Polish Centre for Accreditation. 546 The Institute’s research potential is based on 15 unique in Poland, specialistic, accredited and continuously modernised testing laboratories. PIMOT staff members are authors of numerous scientific publications, patents, utility models, as well as papers and pronouncements presented during various seminars and conferences. The works carried out at PIMOT are oriented at direct practical applications. 547 PIMOT’s research and development activities are concentration on the following Laboratories and Departments: - Vehicle Safety Laboratory, Simulation Tests Laboratory, Braking Systems Laboratory, Vehicle Tests Laboratory, Electronics and Acoustics Laboratory, Environmental Protection and Natural Energy Use Department: Vehicle Engine and Chassis Section, Material Testing Section, Solar Collectors Laboratory, Fuels, Biofuels, and Lubricants Department, Oil Products and Biofuels Laboratory, Renewable Energy Resources Department. 548 CENTRAL MINING (Główny Instytut Górnictwa) Organisation Contact Data 1, Plac Gwarków st., 40 - 166 Katowice, Poland phone: +48 32 258 16 31 till 39 fax: + 48 32 259 65 33 e-mail: [email protected] http://www.gig.eu/eng The Główny Instytut Górnictwa (Central Mining Institute) is an unique institute among Polish scientific and development units. This results first of all from the scope of research and engineering problems solved by the Institute, possession of entire academic authorisations in two branches: mining and engineering geology as well as environmental engineering and protection. These authorisations and the realised research activities are based on experienced staff comprising: 14 professors, 14 doctors of science and 90 doctors, supported by engineering and technical personnel, as well as modern apparatus, laboratory and testing base of the highest world standard. This allows entirely to solve practically all problems of the extractive industry as well as ecological and social problems of industrial regions. The Główny Instytut Górnictwa (Central Mining Institute) as the first scientific unit in Poland has implemented the Integrated Management System. In 2004 the Institute gained authorisations to perform the certification process of products for the European mark “CE”, becoming the Notified Body No. 1453 within the range of the directives: 94/9/EC (ATEX), 98/37/EC (machinery), 93/15/EC (explosives for civil uses). The mission of the Główny Instytut Górnictwa (Central Mining Institute) is the creation of modern, energy-saving and clean technologies, technical solutions and undertakings serving the formation of favourable relations: man – industry – environment. The research works conducted at the Institute are characterised by a high degree of innovation and commercialisation, what causes that more than 70% of the Institute’s financial resources constitute market incomes. One of the strategic objectives of GIG is to gain the rank of an European research institute in the field of geoengineering, joining research specialities serving the solution of problems connected with phenomena and processes occurring underground, on the surface and in the direct surroundings. Such a wide development strategy and possibilities of activity are possible only due to the involved staff of excellent workers, responsible for the lots of the Institute and open towards new challenges. 549 The Główny Instytut Górnictwa (Central Mining Institute) was founded in April 1945 as a research unit of the scientific base of the Polish extractive industry of mineral raw materials. A part of the Institute became the established in 1925 Experimental Mine “Barbara” in Mikołów. The activity of the Institute concerned always the most essential problems of occupational safety, mining technologies and techniques as well as environmental protection against the effects of industrial activity, especially related to mining. The results of scientific and research works created the basis of modern and safe Polish Mining Industry, and many of them found application in the world mining. Currently GIG is: The world leader in the field of occupational safety in mining with the unique testing base of the Experimental Mine „Barbara”. An Institute that undertakes the most important research challenges, such as: development of clean coal technologies, geological CO2 storage, hydrogen generation using coal, economic use of methane and mine waters, modern sustainable development technologies with reference to mining areas Basic areas of the Institute’s activity: Mining and geoengineering Sustainable energy systems Environmental engineering and sustainable human resources management Sustainable waste economy management Occupational safety in the industry Materials engineering Social and economic studies Certification, conformity assessment, management systems We realise a number of international projects in the framework of: Framework Programmes of the European Union. Research Fund for Coal and Steel. European and Polish technological platforms. Centres of advanced technologies.. EU structural funds. The scientific workers of the Institute participate in the activities of European and international research consortia, realising works among other things in the Fifth, Sixth and Seventh Framework Programme of the EU, in the framework of the Research Fund for Coal and Steel and in projects financed or co-financed from European Union funds. These are among other ones such projects as: Biosynergy – realised by 17 institutes including GIG, concerning the use of biomass as raw material in the process of synthesis of substances and chemical reagents (fuels, solvents, synthesis gas) and in energy production (electric energy, associated energy production) 550 through the application of innovative, integrated and using the synergy effects biorefinery concepts. Monsupport – realised by 5 foreign partners and GIG, concerning the development and optimisation of effective systems for gate road support monitoring in conditions of rock stress. The results of the project should improve the competing position of European coal through the reduction of costs on account of support optimisation and will contribute to the improvement of safety. Mintos – realised by 7 institutions, including 3 foreign ones, concerning the development of an internet platform enabling the cooperation of designers and specialists with respect to occupational safety, health protection and ergonomics in all mining circles of European countries in order to promote improved and unified methods of design of transport systems and training standards. Prosafecoal – in the realisation of which participate 7 foreign institutions, concerning the increase in productivity and safety in European hard coal mines through the use of advanced techniques and design tools enabling better roof control in the zone of the longwall-road crossing. Flominet – in the realisation of which participate 4 foreign institutions, concerning the steering of underground mine flooding with regard to the regional network of mining connections. Efonet – in the realisation of which take part 13 foreign institutions and GIG, concerning the review of foresights and European strategies in the field of power engineering. Furthermore, the Institute is the co-founder of the Integrated Scientific-Technological Institute and Centre of Advanced Technologies. . The Główny Instytut Górnictwa (Central Mining Institute) realises the cooperation with foreign research and development units through bilateral contacts (working meetings, commissions, bodies) with such countries as:: Russia – where an agreement on bilateral cooperation with the A.A. Skochinsky Institute was signed recently with respect to industrial preventions and industrial explosion control, China – cooperation in the field of mining safety, seismological observations, Austria – common solving of problems connected with the labour market, Ukraine – cooperation in the field of safety, certification; moreover, cooperation with Ukrainian Universities relating to the same problems was conducted, Czech Republic – solving of problems regarding mining aerology, exploitation and mining supports, Slovakia –cooperation with respect to geothermal installations. Moreover, the Główny Instytut Górnictwa (Central Mining Institute) was and is still the place of meetings of many foreign partners. During the last 5 years GIG was visited by delegations from such countries as Ukraine, China, Mexico, United States of America, Morocco, France, Spain, Australia, Austria, Belgium, Portugal, Germany, Czech 551 Republic, Slovakia, Slovenia and the World Bank. In the course of common discussions topics were touched regarding bilateral cooperation in the field of mining, environmental engineering, occupational safety in the industry and training. The Główny Instytut Górnictwa (Central Mining Institute) possesses the implemented Integrated Management System (quality, industrial safety, environment). The Institute is the winner of many competitions as well as national and international exhibitions. 1) Development of a new method of measurement of lining geometry parameters of the shaft and its equipment Description of technology: The device enables accurate determination of the absolute optical perpendicular for the execution of measurements together with continuous stability control of this perpendicular The detection system enables precise measurement of the position of the shaft guide towards the laser spot and recording of measuring data in the digital recorder. A measuring system was created, which during the continuous run of the mine cage automatically conducts multi-point measurements in relation to the laser perpendicular. The laboratory tests and initial operational attempts have pointed out that the control system of laser transmitter stability in connection with the system of automatic determination of the laser spot centre enables entire realisation of shaft geometry tests. Simultaneously preparatory operations were eliminated connected with lowering and control of mechanical perpendiculars; to two persons was reduced the number of persons conducting the tests, essentially the time of measurements was shortened. The most modern solutions in the field of applied optoelectronics enabled: improvement of the collimation of the laser beam and its stability,, a new method of detection of its position in the space (among other things limitation of the effect of water molecules and air turbulence), obtaining of higher than required measurement accuracies. The developed system came into being during the realisation of the targeted project, and the test results and worked out sub-assemblies can be applied also in surface geodesy. 552 Awards: Gold Medal of the World Fair of Inventiveness, Scientific Research and New Technologies BRUSSELS INNOVA 2008 for the laser control system of geometry parameters of the shaft structure and shaft equipment. Diploma of the Minister of Science and Higher Education for GIG, granted for the project entitled “Laser control system of geometry parameters of the shaft structure and shaft equipment”. Gold Medal with Distinction of the International Warsaw Innovation Exhibition IWIS 2010 granted by the Competition Jury for the “Laser measuring system of geometry parameters of shaft lining and its equipment”. 553 2) Development and preparation for production of a new penetrometer for tests of rock strength parameters for the needs of mining, IRB Spółka z o.o. Description of technology: The borehole penetrometer of Pen206 type is a measuring instrument serving the determination of rock strength parameters in “in situ” conditions for the selection of support for roads and longwall workings of hard coal mines and other needs connected with mining operations. The set of the borehole parameter is composed of: -head, -manual high-pressure pump, -rods for head displacement in the borehole, -T-pipe for the connection of the pump with the high-pressure hose and pressure sensor, -conductors of the electric measuring system, -element for connection of conductors of the electric measuring system, -recording-steering control desk, -application software for the computer of PC class serving for: configuration of measurement sessions, reading in of measurement data from the control desk to the computer, generation of reports . General Advantages of the device: Automatic identification of the moment of rock crushing, Possibility of adaptation to current conditions of the environment (configurationrelated criteria), Easy recording of measuring results in the internal memory of the control desk, Computer aid of handling of measuring data and generation of reports, Classification of the device on account of the explosion hazard: Group I, Category M2, Ex „ial”, Internal memory of the control desk: 56 measuring sessions (56 holes), Own accumulator supply: 3.6 V, Working time with entirely loaded accumulator: min. 10 hours. Tightness class: head IP54 (control desk and element IP65). Awards: Bronze Medal for the borehole penetrometer of Pen206 type at the World Fair of Inventiveness, Scientific Research and New Technologies BRUSSELS INNOVA (BRUSSELS EUREKA). Congratulation letter of the Minister of Science and Higher Education for the solution entitled: “Borehole penetrometer of Pen206 type ”. 554 3) Portable optoelectronic (IR) methane concentration meter Description of technology: The invention came into being in the framework of the research project No. 6ZR82006C/06737. The result is the portable, intrinsically safe, optoelectronic methanometer of new generation, which fulfils all requirements imposed with respect to mining measuring instruments. The methane concentration measurement is the result of the absorption difference of monochromatic, infra-red laser radiation for two different wave lengths in the used band of methane absorption spectrum. High measurement accuracy, resistance to interferences relating to other gases and water vapour, digital measurement, recording, visualisation, alarm signalisation and data transmission were gained. The functions of recording of the time and location of the measurement through the introduction of the radio identification system RFID of the measurement site (mine district, working) were applied. The constructional solution was adapted to the safety requirements through the conformity with the Directive 94/9/EC. The device possesses the certification of EC type testing: KDB 09ATEX025 and OBAC 08 ATEX 158X – conformity with standards: PN-EN 50303:2004, PN-EN 60079-0:2006, PN-EN 6007911:2007, PN-EN 61779-1:2004, PN-EN 61779-2:2004, PN-EN 61779-3:2004 Awards: Gold Medal for the portable optoelectronic (IR) methane concentration meter at the World Fair of Inventiveness, Scientific Research and New Technologies BRUSSELS INNOVA (BRUSSELS EUREKA). Diploma and statuette of the Minister of Science and Higher Education for the solution entitled “Portable optoelectronic (IR) methane concentration meter”. 555 4) AMAX-GSI – Seismometric apparatus for monitoring of vibrations originating from mining tremors Description of technology: The apparatus AMAX-GSI is a multi-channel digital seismometric apparatus for recording of the velocity and acceleration of vibrations on the surface. The built-in in the apparatus software for the interpretation of seismograms is recorded in the Windows environment and enables convenient and quick graphical service as well as data analysis and assessment of the influence of tremors on building objects on the basis of the GSI scale (new mining scale worked out for tremors from the area of the Legnica-Głogów Copper Region and Upper Silesian Coal Basin) and on the basis of the MSK-64, SWD and DIN-4150 scales (scales for the analysis of tremors, firing using explosives charges and industrial vibrations). The apparatus AMAX-GSI can work independently in the terrain or cooperate from a distance with the office (modem or radio data transmission from the terrain). The apparatus possesses a 16-bit AC converter card, which ensures high dynamics and in consequence causes that vibrations even from the strongest mining tremors are not steered . The frequency of sampling of recorded phenomena is set up optionally by the user. The system can be easily installed in different places, in conformity with the needs and development of local seismicity. The interpretation software enables independent analysis of tremors by the user. The AMAX- GSI apparatus operates on the principle of watch and recording of all phenomena after exceeding the set up by the user vibration threshold. In the memory can be recorded many thousands of seismic phenomena, what enables continuous monitoring of the seismic risk through several months, even without interference of the service. The apparatus can be also used for the continuous measurement without the option of automatic release (e.g. in the case of vibrations from the street traffic, pile-drivers, vibrohammers etc.). The basic objective of use of the AMAX-GSI apparatus is the aid for local societies, working places etc. for the monitoring of potentially harmful vibrations originating from machines, firing using explosives or conducted mining activity. Due to this can be assessed the possible influence of these vibrations on the damages of tested objects, mainly habitable and industrial buildings. This allows to estimate in a measurable (financial) manner the value of incurred losses. 556 Awards: - - - - European Medal granted through the Business Centre Club and Office of the European Integration Committee for „Amax-GSI and Amax-99 Seismometric Apparatus for the monitoring of vibrations originating from mining tremors and industrial vibrations” Silver Medal of the 104th International Inventiveness Salon „Concours Lépine” for the multi-channel digital seismometric apparatus for recording of velocity and accelerations of vibrations on the terrain surface AMAX-99. Diploma of the Minister of Science and Higher Education for the “Multi-channel digital seismometric apparatus for recording of velocity and accelerations of vibrations on the terrain surface AMAX-99”. Distinction, jointly with the Coal Company JSC, in the competition Mining Success of the Year 2009 for the elaboration and implementation of the solution “Principles of use of the mining scale of vibration intensity GSI-GZWKW for the assessment of effects of influence of tremors induced by hard coal deposit exploitation in mines”. 557 5) Mining laser of EW-3 type Description of technology: The mining laser of EW-3 type is used in mines threatened by the occurrence of methane with the hazard degree C ( methane concentration up to 2%), according to the certificate No. OBAC 07/ATEX 175X. In the laser two types of laser heads are used: laser diode 635 nm (red ), power output < 1 mW, TEM00, laser on steady body Nd:YAG (second harmonic), 532 nm (green), power output < 1 mW TEM00. The type of the applied laser depends on the customer. Both lasers belong to laser devices of class A, i. e. they do not require the use of additional protections for the eyes. The laser head and low-voltage feeder are placed in a flame-proof cylindrical casing connected with the base for precise adjustment of the beam towards the required direction. It is intended for the determination of the direction of: road workings, all types of longwall front, for the placing of long devices and mining installations, such as conveyors, railway tracks, pipelines etc. Technical parameters: Length of radiation wave: 532 or 635 nm. Range ( according to the degree of atmospheric pollutions): min.150 - 500 m. Power output from the system: max. 1.0 mW. Diameter of laser beam at the distance of 150 m amounts to 15 mm. Range of rotation of the laser set around the vertical axis 360o Range of precise rotation around the vertical axis:: min. 5o Range of inclination of the laser set + 35o Supply voltage from the network (input voltage of the low-voltage feeder): 42 V, 60 Hz; 127 V, 60 Hz; or 230 V, 60 Hz. Mass: - laser with lifting sling: 4.5 kg - low-voltage feeder: 10.5 kg Dimensions: - laser 60 x 300 mm - low-voltage feeder: 250 x 200 x 100 mm Awards: - Gold Medal with Distinction of the Warsaw Innovation Exhibition IWIS 2010 granted by the Competition Jury for the “Mining laser of EW-3 type". 558 6) UV radiometer with a laser range-finder for the control of radiation emissions at workplaces Description of technology: The developed by the Główny Instytut Górnictwa (Central Mining Institute) UV radiometer with a laser range-finder allows the measurement of total UV radiation intensity at workplaces, especially impulses of such radiation of short duration that accompany welding operations for mandrels (welding-on of standardized metal pins with different sizes), finding application for instance in the automotive industry. The measuring set consists of a head for UV radiation detection equipped with a laser optical range-finder for the accurate measurement of the distance of the head from the point of radiation emissions and recorder. For radiation recording is used the detector UV-2500 on the GaN basis, with diameter of active surface 0.5 mm, not requiring any filter that does not react on visible light, with sharp cut-off of the visible spectrum part. The almost flat spectral characteristics in the area from 200 to 365 nm makes the radiometer especially useful for the determination of the total UV intensity in control processes of potential sources of such radiation and allows to embrace in one measurement the total intensity of ultraviolet C (Uv-C, with wave lengths below 280 nm), ultraviolet B (UV-B, 280-315 nm) and the majority of the ultraviolet A band (UV-A, 315-380 nm). The system of the preliminary amplifier of the detector is equipped with three measuring ranges x1, x10 and x100. The obtained data are processed in a laptop by means of software ensuring the integration of recorded impulses of short duration with step 1 ms and assessment of the total exposure dose on the UV radiation at the workplace when knowing the number of repeatable operations per man-shift. The existing measuring instruments allow to sum energy in long-lasting (many-second) impulses accompanying the conventional welding operations. The radiometer developed at GIG allows the determination of the total energy of short UV impulses (1-250 ms), occurring many times at workplaces and recurring in long time intervals. 559 Awards: - - - - - Gold Medal at the International Fair of Inventiveness, Scientific Research and New Technologies „Brussels Eureka 2006” for the UV radiometer with a laser range-finder for the control of radiation emissions at workplaces. Cup of the Minister of Internal Affairs and Administration of Vallonia for the UV radiometer with a laser range-finder for the control of radiation emissions at workplaces. Diploma of the Minister of Science and Higher Education for the “UV radiometer with a laser range-finder for the control of radiation emissions at workplaces”. Gold Medal at the International Invention Exhibition IWIS 2007 of the Association of Polish Inventors and Rationalisers for the “ UV radiometer with a laser range-finder for the control of radiation emissions at workplaces”. Nomination of the World Cup of Computer Implemented Inventions, International Federation of Inventors’ Associations (IFIA) for the „ UV radiometer with a laser rangefinder for the control of radiation emissions at workplaces”. GOLD MEDAL at the International Exhibition of Inventors in SuZhou in 2008 for the UV radiometer according to the invention No. P.386271 entitled ”Radiometer for remote measurement of intensity and dose of ultraviolet radiation and/or visible and infrared radiation at workplaces ”. 560 7) Method of system of noise monitoring in the external environment Description of technology: The system for noise monitoring is intended for execution of long-lasting acoustic measurements in an extensive terrain for the assessment of noise propagation in the external environment and connected with it hazards. It is composed of a set of autonomous measuring instruments, equipped with a digital memory. They ensure the measurement and recording of samples of sound level values simultaneously in many measuring points located in an extensive terrain, what considerably increases the effectiveness and reliability of gained acoustic data in undertakings connected with the preparation of acoustic maps of large areas. The supervising team, by means of a portable computer, takes the readings of recorded results. The results collected in the data base enable the analysis of observations in individual measuring points and, at the stage of numerical modelling, the determination of the spatial noise level distribution within the tested area. The acoustic maps constitute a tool supporting the processes of decision taking with respect to methods and means of noise reduction in threatened areas. The law „Law of Environmental Protection” from the year 2001 with later amendments and the connected with this area of problems directive of the European Union No. 202/49/EC oblige to work out acoustic maps, first of all for cities with more than 250,000 of inhabitants and in the further sequence for cities with more than 100,000 of inhabitants. Awards: - - - Gold Medal at the International Fair of Inventiveness, Scientific Research and New Technologies „Brussels Eureka 2007” for the „Method and system for noise monitoring in the external environment. European Medal granted by the European Economic-Social Committee, Office of the European Integration Committee and Business Centre Club for the „Method and system for noise monitoring in the external environment” . -Diploma of the Minister of Science and Higher Education for the „Method and system for noise monitoring in the external environment”. 561 INSTITUTE OF GEODESY AND CARTOGRAPHY (IGIK) (Instytut Geodezji i Kartografii IGiK) Organisation Contact Data 27, Modzelewskiego st., 02 – 679 Warsaw, Poland phone: +48 22 3291-900 fax: + 48 22 3291- 950 e-mail: [email protected] http://www.igik.edu.pl/index.php/en The Institute of Geodesy and Cartography has been established over 65 years ago as a research governmental institute, carrying out scientific investigation in geodesy, photogrammetry, remote sensing, cartography and geoinformation. It employs over 80 researchers and supporting staff. The Institute of Geodesy and Cartography has extensive experience in conducting research of environment with the use of satellite technologies. Our specialists are involved in a number of projects in this field, including projects at the international level. The Institute of Geodesy and Cartography is engaged in developing the Polish space technology sector. It plays an active role in GMES programme (Global Monitoring for Environment and Security), joint initiative of European Commission (EC) and European Space Agency (ESA), which is aimed at building up a European capacity for Global Monitoring of Environment and Security. One of the GMES project, in which IGiK plays an active role is GEOLAND. The Remote Sensing Department of the Institute is one of the partners of an international consortium formed to develop and demonstrate a range of reliable, affordable and cost efficient European geoinformation services, supporting the implementation of European directives at the national level. IGiK provides services for monitoring earth surface, land use, monitoring of crops and crisis management. 562 The Institute has developed and offers the technology in the following areas: Preparation cereals yield prognosis based on vegetation indices derived from NOAA/AVHRR; TERRA/MODIS and SPOT VEGETATION satellites. Assessment of biomass using the synergy of optical data and microwave data provided by satellites. Determination of the possibilities of energetic plants' cultivation in different regions. Detailed spectral analysis at different spectral bands registered by satellites on various time intervals in combination with terrain characteristics enables to determine areas useful for energetic plants' cultivation, considering their water demands. Assessment of soil moisture using radar data and optical data under crops and various vegetation. Monitoring and finding the ecosystems changes due to natural and anthropogenic issues. The developed method includes changes in evapotranspiration, soil moisture and land use. Assessment of Carbon Balance for different ecosystems and monitoring the changes using spatial distribution of biomass and soil moisture elaborated on the basis of satellite data. Mapping land use and its changes using high resolution satellite data. Assessment of the risks of forest fire with the use of remote sensing data. Estimating the threat, location of fire outbreak, burned area mapping, analysis of fire intensity and burn severity as well as assessment of post-fire vegetation recovery. Monitoring of fire events is performed with the use of various remotely sensed data captured in thermal, optical, infrared and microwave spectrums. Usage of satellite remote sensing methods for mapping flood extent. In GIS the extend of the water, due to flood has to be overlaid on land use maps to find out the flooded areas. Determining the areas where the soil moisture was high and caused the destruction of the crop using the optical and microwave data provided by satellites. 563 INSTITUTE OF INNOVATIVE TECHNOLOGIES (Instytut Technik Innowacyjnych) Organisation Contact Data 31, Leopolda st., 40 – 189 Katowice, Poland phone: +48 32 2007-700 fax: + 48 32 2007-701 (till 704), e-mail: [email protected] http://emag.pl/index.php?l=ang The Institute of Innovative Technologies EMAG is an R&D organization involved in the development and deployment of state-of-the-art devices, systems and technologies in particular for the mining industry. We carry out a number of scientific-, R&D- and construction projects as well as provide expertise in the range of electrical engineering, automation, telecommunications, information technology, sustainable consumption of fuels and energy, and environmental protection. This potential is complemented by the services provided by the Testing and Certification Centre with the PCA-accredited Electromagnetic Compatibility Laboratory, short-series production of apparatus and devices, specialized research, maintenance services, training, our own science- and technology-oriented periodical, and monographs. The Institute of Innovative Technologies EMAG is a leader in many sectors of the market, such as safety systems, natural hazards monitoring, apparatus, systems for automation and measurement of coal quality parameters. Below one can find short descriptions of our most popular products. 564 GEOPHISICAL SYSTEMS 1) ARAMIS M/E VISUALIZATION AND PROCESSING OF DATA ON SEISMIC EVENTS IN HARD COAL MINES The system is used to locate rock bursts in a mine, determine the energy of bursts and assess rock burst hazards. Depending on the extent of the mine, the system is based on seismometers or optionally on low frequency geophones. The system uses intrinsically safe data transmission, centrally supplied from the surface, which enables to transmit 1-, 2- or 3-axial velocity movements (X, Y, Z). The sampling of signals is performed by means of 24-bit Sigma Delta converters, providing high dynamics of conversion and recording. Number of measuring channels: 16 Registered frequency band: 0 – 150 Hz (from the input of the transmitter – without a seismometer), Sensors: SPI 70 seismometers (optionally low frequency geophones), Record and processing dynamics: 100 dB (optionally 120 dB), Underground transmission stations supply: intrinsically safe, central from the surface, Intrinsically safe transmission range: 10 km, Admission quality: ExiaI. 2) ARES-5/E ASSESSMENT OF ROCK-BURST HAZARDS IN THE LONGWALL AREAS OF MINES The function of the system is converting the velocity of mechanical vibrations of rock-mass into electrical signals by means of SP-5.28/E geophones which are fastened on anchors situated in the walls of top and bottom roads. Then the signals are sent to the surface, to the surface mining geophysics station, where they are digitally processed and computer-interpreted.The system can be used in the areas with methane explosion hazards. Number of measuring channels: 8 (maximum 64 with 8 surface stations). Mode of transmission: natural, current. Sensor type: SP-5.28/E. Processing dynamics of the signal: 54 dB. Casing protection degree of the underground part of the system: IP 54. 3) ARP 2000 P/E COMPLEX ASSESSMENT OF THE IMPACT OF ROCK BURSTS ON THE SURFACE The system is used for recording and analyzing low frequency vibrations of ground and buildings in the areas with rock-burst hazards. The modular structure of the system enables to apply distributed measuring networks. Wireless data transmission is carried out by a GSM network. Sensor type: Bruel & Kjaer piezoelectric accelerometers, Number of recorded vibration components: 3 Transmission of signals from the sensor to the local measuring concentrator: digital 565 Maximum distance between the sensors and the concentrator: 1 km Number of concentrators in the area: unlimited Maximum number of three-component sensors co-operating with the local concentrator: 4 Time synchronization: satellite GPS clock Data recording and processing dynamics: 90 dB Registered frequency band: (0.5 ÷100) Hz Maximum measuring range: (1000÷3000) mm/s2 Transmission type: wireless Transmission mode: data transmission in the GSM system Transmission speed: 9600 bauds There are different versions of the system available, depending on the area of application: ARP 2000 P – to be used in difficult environmental conditions, e.g. with extreme temperature changes from – 20°C to + 40°C, high air humidity and high dustiness; ARP 2000 H – to monitor accelerated vibrations of the shaft of a flotation-tailings tank caused by rock bursts; ARP 2000 SZ to record accelerated vibrations of the shaft lining. 4) PASAT M ASSESSMENT OF ROCK-BURST HAZARDS IN MINES. The apparatus enables seismic signals measurement, transmission of digital converted data and their further processing for: assessing strata stresses and their changes in space and time, determining geologic heterogeneity near the working front, identifying places for proper probes fixing in geophysical prospecting, identifying soil properties for constructional works, logging other data from intrinsically safe probes different than geophones. PASAT can be used with the following measurement methods: borehole survey in mining excavations, excavation tomography, borehole tomography, seismic probing, seismic carrotage. 566 PASAT is an intrinsically safe apparatus, group I, category M1. It is dustproof according to IP 54. Explosion-proof structure ia. Casing protection degree for SG3 probes, MPT, MWP, MWP-WF and PDA module: IP54 Intrinsic safety quality: I M1 Ex ia I. Number of registered channels: 2-48 (2 channels in one MPT module). Frequency band: Hz 4,5-10000 Maximum working time with loaded batteries: about 2 h (for MPT, MWP), about 4 h (for PDA). Input/output interface for PDA: Bluetooth. Power supply for MPT and MWP modules: IRIS-BATT/U 4 intrinsically safe battery 4.8V 1650 mAh. Data transmission bus: fibre optics CAN bus. Data interface: Bluetooth (own format, optionally SEG-1, SEG-2 or others). 567 INDUSTRIAL AUTOMATION 1) MAKS DBC WIRELESS CONTROL OF NEW GENERATION MINING MACHINES WITH REMOTE MONITORING OF THE MACHINE OPERATIONS AND VOICED COMMUNICATION BETWEEN OPERATORS The system is composed of mutually connected and co-operating electric-electronic subassemblies which make use of the CAN system bus, RS-485 interface and Bluetooth. The system is used in cutter loaders with electric or hydraulic drive advance. The system allows radio control of the machine operations along with on-line diagnostics and monitoring of its work. It is possible to set working parameters by means of radio operator controllers equipped with LCD monitors. The structure of particular subassemblies is universal. It is possible to use the system or its subassemblies in other solutions for the control of machines and devices, including those working on the surface. High computing power of the system allows to apply data processing algorithms for the purposes of control and diagnostics with high numerical complexity. Due to the application of new technologies and complex approach to the issues of control and monitoring, the MAKSDBC system is a significant step in the range of developing maintenance-free control systems for mining machines and longwall systems. The use of the system allows to lower the production costs of casings for the electric apparatus of machines, reduce downtime (enhanced diagnostic and servicing functions), improve the safety of operating the machine, improve working conditions for the personnel operating the machine. Power supply 5 V DC Communication Bluetooth standard Version intrinsically safe Place of installation inside the machine (apparatus box, chamber of the intrinsically safe casing, fire-proof chamber) Casing protection degree min. IP 54 The system is in compliance with the following directives of the EU: 94/9/WE ATEX, 2004/108/WE EMC and 2006/WE LVD. 568 2) MOPS MONITORING OF THE ROOF PRESSURE IN ROOF SUPPORT The MoPs system has been designed to monitor the roof pressure in the selected roof supporting devices of the powered roof support. The system monitors the current values and changes in the pressure of the medium used in the roof supporting devices. The measurement data are displayed on the POp-1 Operator Panel and archived in the PIMP-1 portable memory module or sent to the surface in real time. The system makes it possible to monitor the situations when boundary values of pressure increase in roof supporting devices are exceeded. It also enables to monitor the time in which the working load of the powered roof support is achieved in the successive work cycles. The system has been developed to work in the underground workings of mines, in nonmethane and methane fields, in the areas with the “a”, “b” or “c” explosion hazards degree, in compliance with the characteristics of the ExibI anti-explosion protection. Maximum number of sensors (at the total length of system bus cables up to 400m): 32 Maximum total length of system bus cables (distance between the last sensor and the Operator Panel): 600 m Maximum working pressure in roof supporting devices: 100 MPa Anti-explosion structure (POp-1): Ex ib I Devices group and category (POp-1): I M2 Anti-explosion structure (PAC-1): Ex ia I Devices group and category (PAC-1): I M1 569 GAS MONITORING AND TELECOMMUNICATIONS 1) SMP-NT/A MONITORING SAFETY AND PRODUCTION PARAMETERS IN MINES WITH METHANE AND COAL-DUST EXPLOSION HAZARDS The SMP-NT/A system is a state-of-the-art complex solution to monitoring safety and production parameters in mines with methane and coal-dust explosion hazards. The system enables to monitor on-line the parameters of mine environment, particularly: physical parameters, chemical composition of air, as well as the condition and working parameters of ventilation equipment, machines and process-line equipment. The system enables early detection and signalling of natural hazards, particularly methane- and fire hazards, along with other hazards related to production processes. Underground devices of the system execute the algorithms of bi-stable control of underground machines and devices, including immediate automatic power supply switch-off in the case of explosion hazards or high-energy rock bursts. Thanks to the integration with alarm and communications systems of the mine, such as STAR and SAT, the system enables automatic transmission of voiced alarm and evacuation messages which inform the personnel about the existing danger and about the evacuation ways. The modular structure of SMP-NT/A, both in the underground and surface IT part, makes it possible to configure and extend the system according to the size of the mine and the functions required. The structure of system devices and functions are in compliance with the ATEX directive and with mining regulations. The SMP-NT/A system can be applied in other industries – in all places where it is necessary to have a reliable and intrinsically safe system of control and monitoring devices. modem-based and disturbance-resistant communication with underground devices, advanced autodiagnostics, high reliability (redundancy mechanisms applied), user-friendly visualization of data collected from monitoring and measurement devices, making complex reports and lists, access to information stored in the data base and making them available to other higher-level systems, control of monitoring and measurement devices, possibility to adept the system configuration to the user’s needs 570 2) UTS -2 TRANSMISSION OF BI-STABLE AND ANALOGUE SLOWLY VARYING SIGNALS AND CONTROL The UTS-2 system has been designed to collect data about the condition of analogue and bistable underground sensors which monitor slowly varying processes. The data collected by the system are transferred to a visualization system located in the control and supervision room. The system enables to control actuators operating in the underground of the mine from the surface, from the control and supervision room. Additionally, the system allows: to detect the state of any type of sensors with insulated-contact inputs to provide remote power supply to and detect the state of a CP-10 bi-stable sensor or any type of sensor with a transistor output to provide remote power supply to any type of bi-stable sensor if its power demand does not exceed the voltage of 6V and current of 500uA galvanic separation between the sensors connected to the station and between the sensors and the transmission line of UTS-2 to connect another UTS-2 station of any type to the output to detect damages in the station connected to the output of the transmission line or to the transmission line itself when the damage is related to wrong power consumption from the station output to cut off the transmission line from the system after a defect has been detected and then connect it back to the system after the defect is removed to detect the state of any type of sensors with 0.4V-2V voltage outputs to provide power supply to different types of analogue sensors, to detect and locate defects such as: damage of the cable connecting the sensor with the underground station of UTS-2 or the cable connecting particular underground stations with one another and with the surface station. System capacity: 768 bi-stable sensors and actuators, or 128 analogue sensors and 256 bistable sensors and actuators (one analogue sensor replaces four bi-stable sensors). The device can work in difficult conditions in the underground of mines; temperature range: from -20°C to +40°C. 571 3) SD-2000 SUPERVISION OVER THE OPERATIONS OF THE MINE SD-2000 is a control and supervision system for a mine, based on advanced collection of digital and analogue data with a view to provide efficient management, warning, documentation, and analysis of production processes and to monitor the safety conditions in mines. The system provides the following basic functions: visualization and monitoring of technological processes with the use of the mine maps, natural hazards monitoring, alarming about critical states, alarming about hazards, registration of process variables, visualization of the working conditions and hazards, against the background of the mine map, on monitors and other displays, reports on: events in a mine statistical information and balance sheets data in the form of lists, tables and diagrams, data archiving. Charactetistics of the system: very high efficiency of data processing – record of the sensor indication, its analysis (whether the indication shows an alarm state) and archiving take 1-3 ms. quick access to data both from the current week or from last year. possibility to archive the data and make back-ups on all types of media with the possibility of data recovery and transfer to other computer, e.g. for analysis outside the mine. scalability, i.e. changing the computer on which the MS SQL server is installed into a faster one, or changing the processer – both make the system operations faster. possibility to implement a mirror server. The data from the main server get to the mirror server in about 2-4 seconds and are accessible to other users of the mine network. the SD-2000 system comprises the level of sensors, transducers and actuators, transmission system, supervision and monitoring level, and selected elements of information transfer to the management of the mine. 572 MEASUREMENT OF THE COAL QUALITY PARAMETERS 1) RODOS ON-LINE MEASUREMENT OF THE ASH CONTENT AND MASS OF HARD COAL, BROWN COAL, LIGNITES, AND WASTE PRODUCTS . The RODOS ash meter is a state-of-the-art., fully secure device for quality- and quantity monitoring of hard coal, brown coal, lignites, and waste products transported on conveyor belts. The measurement of ash content is based on natural gamma radiation of the tested material, while the measurement of mass is made with the use of belt-way scales. The RODOS meter is composed of the following elements: mechanical part of the ash meter with a measuring head, fixed on the belt conveyor, electronic block based on the system microcontroller, belt-way scales, computer with software for visualization and collecting of measuring data, displays The RODOS meter has the following advantages: wide measurement area – highly representative results, accuracy comparable with the accuracy of isotope ash meters, moisture and chemical composition of coal do not affect the accuracy of ash content measurement, grain size of coal 0-200/300 mm, can be used in control systems can be fixed on any type of belt (e.g. reinforced belts), modular, latest-generation electronics, co-operation with belt-way scales, advanced and professional software. RODOS has been admitted to work in the underground of mines – EC-type examination certificate KDB 06ATEX 119. The surface version of the RODOS ash meter can be extra equipped with an absorption moisture meter to form a non-isotope system for on-line monitoring of coal quality – RODOS W. 573 2) WALKER FAST, FULLY AUTOMATED MEASUREMENT OF ASH CONTENT IN COAL The Walker portable ash meter has been designed to quickly assess the quality of raw coal, coal preparation products, screened coal products, coal blends, unknown coal, or coal delivered to preparation plants and power plants. The measurements are very precise. Small size and weight of Walker, its measuring precision, reliability, along with easy calibration and operation make it an indispensable device to be used in all places where it is necessary to make fast measurements of ash content in coal: at storage yards, in tanks and on coal transporting vehicles (wagons, trucks). The device has an option which enables to calculate the calorific value based on correlations between the value of the measured ash content and the set value of moisture content. Walker does not have artificial sources of ionizing radiation. It co-operates with a computer enabling, among others, to make data bases and reports. Measuring method: measurement of natural gamma radiation of coal Power supply: 12 V/1.8 Ah battery; time of continuous operations depends on ambient temperature; min. 50 hours of continuous operation at ~20°C Working temperature: from - 10°C to 50°C The number of calibration curves in the microprocessor memory: 16 different calibration curves that can be entered by the user Duration of measurement: 5 – 999 s Readout of ash content A, %: instant Possibility to select language options on a display unit Measurement accuracy: mean measuring error ~ 1 % of ash content, depending on the type of coal Weight: about 7 kg Length: 900 mm 574 3) GAMMA NATURA METHOD AND DEVICE FOR MEASURING BASIC QUALITY PARAMETERS OF SOLID FUELS Gamma Natura is a unique device, the first solution of its kind in the world. It is a laboratory analyzer without isotope which enables fast measurements of ash content, moisture content and calorific value in small coal samples (0-20 mm) without the necessity to prepare the sample for measurement. The device can replace the isotope analyzers that have been used so far. It can be used without any limitations, both in coal processing plants and in quality control laboratories of mines, power plants or heat generating plants. It does not require admission from the National Atomic Energy Agency in Warsaw. The measuring method of basic quality parameters is based on simultaneous measurements of the intensity of natural gamma radiation of a solid fuel sample and the attenuation of microwave radiation after it goes through the sample, as well as the weight of the sample. Then the ash and moisture content, calorific value and other parameters are calculated according to experimentally determined formulas. The device employs an invention patent on the measuring method and the applied technological solution. The patent has been submitted to the Polish Patent Office by the team carrying out the Project No P-384059. Gamma Natura has been designed mainly for the mining and power engineering industries. It enables the users to offer quick services to coal buyers. Thanks to the use of the device, coal can be sold in accordance with its real quality. Additionally, the quality of the delivered coal can be assessed along with the quality of coal preparation products. The devices makes it possible to avoid financial losses that may be incurred when coal is sold at a price lower than its value, or when the seller has to pay forfeits for selling coal in the class that is lowered than the declared one. In the case of power plants and heat generating plants, the device enables to determine the parameters of a boiler before the coal delivered by a mine is burned or to find that the parameters of the supplied coal are not in accordance with the declared ones. Measuring range: 5÷100 % of ash content, 0÷50 % of moisture content Measuring duration: about 5 min. Measuring error: for the ash content in coal σ=0,5÷1,5 % (depending on the type of coal) for the moisture content in coal σ=0,2÷1 % Visualization of measuring results: embedded LCD touch screen Applied functions: archiving measuring results, making reports on conducted measurements. Size: 1100×800×400 mm 575 MOTOR TRANSPORT INSTITUTE (Instytut Transportu Samochodowego) Organisation Contact Data 80, Jagiellońska st., 03 – 301 Warsaw, Poland phone: +48 22 811 32 31 fax: + 48 22 811 09 06 e-mail: [email protected] http://www.its.waw.pl/start,2.html Motor Transport Institute (MTI – ITS in Polish) in its Centre for Materials Testing and Mechatronics (CBM) - performs the scientific - research and expert opinions and assessments on: investigation of material mechanical properties and their’s structures with respect on a safe use in major branches of industry i.e: automotive, power plant, aircraft and military; car fluids testing (especially: antifreeze, brake, windscreen and washer); friction test and developing of new technologies for effective recycling of vehicles withdrawn from service; technical consulting and expert activities. The Centre possess the status of the Accredited Research Laboratory of Polish Centre for Accreditation - Certificate No. AB 089. CBM consists of five laboratories: Strength of Materials, Structural Research, Physicochemical Testing, Mechatronics and Recycling. 576 Laboratory of Strength of Materials Research areas/activities: development of applied and elaboration of new measurement techniques for determination of stress/strain state components, elaboration of experimental procedure for investigation of mechanical properties of typical and modern engineering materials (steel, alloy, composite and others) having isotropic and anisotropic properties, behaviour and mechanical properties of materials under one-axial and complex (static or low and high fatigue) loading at within range of temperature from -160°C to 1200°C and corrosion environmental using standard and miniaturized specimens depending on test type i.e: flat, full, thin-walled tubular specimens, variations of material impact energy versus time at low and high temperature, analysis of crack propagation and critical value of stress intensity factor (K IC) using a compact tension mini-specimen (CTM), creep test of material with respect on applying in power plant industry at temperature up to 1000°C, expert activities to identify failure causes of elements used in many branches of industry. Laboratory of Structural Research Research areas/activities investigations of vehicle parts and subassemblies (made from traditional and modern materials, i.e.: metal matrix composites, gasars, syntactic foams, nanomaterials) focused on a vehicle safety exploitation and their reliability, development of new materials and technology in application for many industry areas in these in production of vehicle parts and subassemblies; R&D works connected with the qualitative and quantitative assessment of the effects of recycling processes of vehicles have been out of exploitation, recovery of raw materials and utilization; standardization activities, elaboration of ISO standards in cooperation with the Polish Standard Committee in the Commission no 123 to matters of metal research, to formulate opinions concerning the international standards, expert activity concerning the diagnostics of the damage/failure causes of semi finished products/ready products existing in various technical solutions; statutory research, and research realized in the frame of domestic and international projects focused on engineering materials obtained by means of traditional and innovative technologies. 577 Physicochemical Testing Laboratory Research areas/activities: testing of automotive service liquids, especially: brake fluids, antifreezes for the engines' cooling systems as well as windscreen washer fluids and to examine cleaning materials (for the purpose of their certification amongst the others); establishing metal content in the used up service fluids using atomic absorption spectroscopy; development of new and improvement of the existing recipes of engine coolants, cooling system de-scaling fluids, windscreen demisters and similar automotive products; corrosion resistance of materials, including the development of electrochemical characteristics, based on the method of accelerated; studies of energy conversion processes and the origin of the waste vegetable oil into liquid fuels (BtL and WtL processes); thermochemical studies determining the change in weight of different materials (e.g. biomass, metals, composites), depending on temperature and thus allow including to determine the kinetics of the processes of oxidation / reduction, analysis of phase transformations, study the thermal stability; developing of technologies of recycling service liquids to save natural environment; normative activities- participation in Technical Committee No. 222 for Polish Committee for Standardization. Mechatronics Laboratory Research areas/activities: new solutions of powertrains and power sources of hybrid electric vehicles; developing of new materials and solutions for vehicle lighting; developing of new measurement methods and testing stands for structural, mechanical and tribological tests; analysis of application nanomaterials and intelligent materials in transport; researching and developing of new mechatronic solutions, especially in transport area. 578 Division of Recycling Research areas/activities: opinion making, creating data bases for the legal regulations, scientific publications and information about the institutions dealing with an environmental protection and recycling; developing research methods and criteria for evaluating assemblies, parts and materials obtained as a result of dismantling devices and cars, testing components and materials retrieved in the recycling process; initiating and taking part in the research and implementation programs linked with the environmental protection, ecology and recycling; giving opinions on the standardization documents both domestic and foreign. The above activity of MTI is well supplemented by the wide range of vehicle and component type approval testing which covers the following: EU and National whole vehicle type approval tests (all vehicle category); environment tests (local emission, CO2 emission, noise, climatisation etc.); dynamics of vehicles (Vmax , manouvering) ; all aspects of lighting ; general safety (visibility, motocycle safety, etc.) ; There are next specific certificates of Polish Centre for Accreditation for the activity and EU/ UN notifications based on this certificates and made by 2 type approval authorities – Poland (E20) and Latvia (E 32). The precise scope can be found on the EU/ UN ECE website). EU : http://ec.europa.eu/enterprise/sectors/automotive/approval-authorities-technical services/index_en.htm UN ECE - http://www.unece.org/trans/main/wp29/wp29wgs/wp29gen/wp29fdocstts.html MTI has long tradition in performing TA tests (since 1984) and due this and modern equipment offers highest quality of testing. 579 OIL AND GAS INSTITUTE (Insytut Nafty i Gazu) Organisation Contact Data 25 A Lubicz st., 31 – 503 Cracow, Poland phone (secretary): +48 12 421-06-86 phone (exchange): + 48 12 421-00-33 fax: + 48 12 430-38-85 e – mail: [email protected] http://www.inig.pl/ The Oil and Gas Institute (INiG) is a research and development unit, subordinated to the Polish Ministry of Economy, working for the benefit of petroleum and natural gas industries. The register of documentation developed in the Institute makes a long and diverse list, which includes expert opinions, monographs on solutions of design and technology problems, significant comprehensive works which contributed to discovering new deposits of petroleum and natural gas, manufacturing and using tools allowing their exploitation and implementation of technologies necessary for cleaning, transport, processing and use. The directions of the substantive activity of the Institute have become a significant part of the domestic and European policy of the sustainable development of power industry: - evaluation of prospecting forecasts of oil and natural gas with methods of geology, geophysics, geochemistry and microbiology, - exploration and exploitation of deposits of hydro-carbons, - storage, transport, distribution and use of the natural gas, crude oil and petroleum products, - petroleum processing, - improving and monitoring of the petroleum products quality, - using the renewable sources of energy, - environmental protection in the oil and gas industry. Good, constantly supplemented research infrastructure: modern apparatuses, including the unique analysers, equipment allowing to conduct laboratory and field tests, the rich collection of a library, and buildings and technological halls, permits the Institute to create the interesting and diverse offer of scientific, research and development, and service works for the industry, including small and medium enterprises, as well as for the involvement in research projects, carried out by scientific consortiums. The Institute has implemented a Management System fulfilling the requirements of the ISO 9001:2008 standard. The System’s compliance was confirmed by Bureau Veritas Certification 580 and it covers research, experimentation, implementation and services in the fields of oil and gas mining, gas engineering, crude oil processing, production technology, the distribution and utilization of petroleum and derived products, environmental protection, specialized training services, the experimental and small-scale production of petroleum products, the issuing of technical and standardization approvals, and the certification of products. Oil and Gas Institute is a laureate of competitions: Cheetahs of Business, Gazelle, National Leaders of Innovation and Development, Teraz Polska and the Polish Top 50 Intellectual Capital. The action in the field of Corporate Social Responsibility has been twice awarded the Polish edition of the Great Place to Work - Best Place to Work. Oil and Gas Institute in 2011 was nominated for the European Business Awards 2010. In 2009 – 2010 the Institute was awarded over 100 medals its presentations at international exhibitions of innovations, inventions and solutions. The 34 gold, 27 silver 30 bronze medals, along with 9 distinctions and special awards were won by the Institute’s inventions presented at exhibitions in, inter alia, Brussels, Nuremberg, Moscow, Budapest, Geneva, Seoul, Kuala Lumpur, Sevastopol, Zagreb, Bucharest and Warsaw. For its remarkable activity in promoting inventions abroad, The Institute was twice awarded diplomas by the Ministry of Science and Higher Education. The INiG offer The INiG offer covers specialist works in distribution and usage of oil and petroleum products, crude oil processing, developing and quality testing of petroleum products: fuels, lube oils, paraffins, bitumes; developing of performance additives for crude oil, gas and fuels; geophysics, geology, well drilling, development and exploitation of oil and natural gas deposits, production, processing, purification, storage, transmission and distribution of gas fuels, control and automation of technological processes, use and construction of gas devices, assessment of gas fuel quality, environment protection facilities. Experience and regularly upgraded qualifications of the staff, as well as modern, accredited INiG laboratories with remarkable equipment, guarantee high quality tests and services and allow to deal with diverse specialist tasks. Division of Prospecting of Hydrocarbon Deposits Evaluation of the prospecting possibilities in the particular regions of the country Evaluation of the geological, exploitable and industrial resources of crude oil and natural gas Marking the physical and reservoir parameters and properties of composite liquids Using the means and methods of microbiology in drilling, exploiting the hydrocarbon deposits and the underground gas repositories. Division of Hydrocarbon Production Engineering (INiG Department in Krosno) Technology of drilling holes Technology of drilling liquids and procedures of cementing the drill holes The development and exploitation of crude oil and natural gas deposits Designing the procedures of stimulating the output of hydrocarbons Simulating the deposit procedures and underground gas repositories Technology of reconstructing boreholes. 581 Division of Petroleum Processing The analyses and technological evaluation of crude oils Laboratory simulations of processing crude oils (crude oil distillation, selective rafination, dewaxing oil fractions, dearomatization of crude fractions Researching the catalysts used in refining processes Developing the technology of producing liquid fuels, solid hydrocarbons, asphalts, plastic greases, grease oils, other crude oil products Synthesis and evaluation of the activity of the supplements to crude products Devising and modifying the analytic methods Quality control of the crude products Engine and exploitation tests of the fuels and grease oils Environmental protection and the safety of utilizing the crude products. Division of Gas Engineering The evaluation of materials from plastics used in gas industry Technical evaluation of the gas fittings of the measurement instruments Studying the changes of the metrology features of the gas-meters Quality and technical evaluation of the installations burning the hydrocarbon fuels New technologies of utilizing gas Problems of environmental protection in the gas and oil industry Renewable energy. 582 Major projects which have been implemented with the participation of the Institute. 1) Method for regeneration of used oils The present invention refers to a catalytic hydrogenation processing method for the regeneration of used petroleum oils to produce clear, free from coagulants base oil of full value providing a raw material for manufacturing of high quality lubricating oils.The innovation in this project is the combination of a new catalytic system and modification of parameters of used oil hydrofining process. A new catalytic system and the suitably selected parameters (temperature, pressure, velocity, the raw material volume) allow of a mixture of used oils to be recycled into high quality base oils, as an alternative to products of direct crude oil processing. The product of the modified regeneration process with a new catalytic system shows very good properties and is free from coagulants which permit its full use in substitution of base oils from direct crude oil processing. The presented catalytic hydrogenation processing method for the regeneration of used petroleum oils is the most efficient method for utilization of these wastes. The regenerated base oils provide both reduction in production capacity of new base oils from crude oil and limitation of the other more harmful to the environment methods eg. burning.The developed technology was implemented into the industrial scale production in RN Jedlicze SA in June 2008. The result of the implementation is the production and sale of the new generation base oils to leading producers of lubricating oils on domestic and foreign markets. The final products meet the requirements of the group I+ of base oils, and the industrial consumers confirm their quality by using them to manufacture of high quality lubricating oils.The invention was implemented into the industrial scale production in RN Jedlicze SA. The regeneration of used oils based on the presented invention is in progress from the middle of 2008. 2) Ecological Light Heating Oil The subject of invention is ecological light heating oil based on conventional petroleum fractions with low sulphur content and/or ester derivatives of fatty acids which the use provides for reduction the emission of toxic exhaust gas components and improvement of fuel combustion process. The improvement in the ecological and performance properties of the light heating oil according to the invention was ensured by the use of especially tailored additive package including detergent active substance which ensures injector nozzle cleanliness, an additive improving diesel fuel ignition, reducing the emission of toxic exhaust components and improving combustion process, lubricity additive modifying friction behaviour in fuel pump elements, corrosion inhibitor protecting metallic parts of fuel system (tanks, pipes. pump) against corrosion, demulsifier, and others. Each additive included in the package composition is playing important role in light heating oil exploitation. The invention was implemented into the industrial scale production in PKN Orlen SA. The production of the heating oil based on the presented invention lasts from 2004. 583 3) Biodegradable grease for rail traction The subject of the invention is biodegradable lubricating grease for use in control devices for rail vehicles operated in public transport. The grease is characterized by its increased antiwear properties which help minimize mechanical wear on the device elements and good rheological properties in low temperatures which permit the grease operation during full season, especially in winter conditions. .The grease good performance was ensured by properly selected components: base oils composition comprising ester oil of the natural origin and synthetic ester oil and the effective additive package with physical and chemical mechanism of action.The additional advantage of the lubricating grease according to the invention besides its good performance properties is the high degree of biological degradation of the preparation in soil and ground-water The lubricating grease according to the invented technology of the patent application No P 371.309 is manufactured in the Department of Experimental Production and Sales of Petroleum Chemicals of the Institute of Oil and Gas in Krakow and used in control devices for rail vehicles operated in Krakow urban agglomeration. 4) Purification of soil contaminated with petroleum pollutants with an in-situ method An in-situ method purification of soil, strongly contaminated with petroleum hydrocarbons, comprises of a stage introduction of the process, which enables gradual decrease in pollutants content. The process consists of the following stages: initial terrain reclamation by removal of petroleum substances from deeper layers with the use of a drainage-outflow system; basic bioremediation stimulated by bioaeration (oxygen providing by soil aeration); modification of soil reaction by lime (pH=7.5) and biogenic substances dosage as a mineral fertilizer (C:N:P=100:10:1) in order to cause activation of autochthonous microflora; bioaugmentation by inoculation with biopreparations (density 1*109 jtk/cm3) prepared on the basis of isolated, selected and multiplied non-pathogenic indigenous microorganisms.The purification process is monitored with the use of chromatographic, physico-chemical, microbiological and toxicological analyses.Purification of soil contaminated with petroleum pollutants with an insitu method has been applied in 11 areas chosen in an oil plant situated in south-east Poland. During the period of 3 years, the decrease in pollutants amount has been observed to a standard level of soil and ground quality. The purified terrains have been accepted as forest areas. 584 5) Manufacturing process for TDAE rubber plasticizer Treated Distillate Aromatic Extract (TDAE) plastificator is a petroleum product used as a softening agent in the India rubber curing process and as a component of rubber mixtures, and its contents in rubber products can reach up to 40 %(m/m). The TDAE plastificator is manufactured in accordance to the technology developed by INiG and Lotos S.A Group and it conforms to the requirements specified by the 2005/69/WE Directive. It can be used for manufacturing car tyres within the EU territory since 1 January 2010, replacing the hitherto used, carcinogenic, highly aromatic DAE plastificators. It is a pro-ecological product, as it is characterised by <3%(m/m) concentration of the DMSO extract and a limited contents of polycyclic aromatic hydrocarbons (WWA). In accordance to the presented invention, the TDAE plastificator manufacturing technology allows to launch an ecological product, ensuring that the high level of rubber product quality is upheld. This solution matches the strategy of limiting the negative influence of technological and industrial activities on the natural environment and of implementing the sustained development at a local, national and global scale. Application of the pro-ecological TDAE plastificator for the tyre manufacturing process shall positively influence the general health of the population by reducing the level of harmful, toxic, carcinogenic agents; thus the level of harmful pollutants generated by vehicle traffic, affecting the natural environment, will be lowered. The product was included in the LOTOS OIL S.A. trade offer under the name of Quantilus T50. It passed the application analyses and was allowed for use in the process of curing synthetic rubber and for manufacturing vehicle tyres. 6) High thermal stability detergent – dispersant additive package for diesel fuels The present invention relates to a high thermal stability detergent-dispersant additive package for diesel fuels designed particularly for Diesel engines with direct injection equipped in “common rail” fuel injection systems. The manufactures of Diesel engines strive from many years to improve their efficiency to optimal utilization of diesel fuels combustion and meet the stringent emission standards Euro 5 and Euro 6. At present all the new vehicles with Diesel engines are equipped in high-pressure direct injection “common rail” fuel injection systems (CRS). In specific working conditions of these engines fuel undergoes thermal degradation, and fuel deposit precursors under influence of temperature and pressure are subjected to thermalpressure flocculation giving adhesive deposits which accumulate on the surface of highpressure, multi-hole injectors hindering proper fuel atomization. Coke deposits accumulating in the multi-hole injector ducts decrease flow of fuel metered to the combustion chamber, which decreases the engine power output and its torque.The main purpose of the invention is to get a detergent-dispersant additive package preventing deposit adhesion on the multi-hole injector nozzles, compatible with other additives, which not only allow for keeping the injector cleanliness, but also protects against corrosion and wearing of fuel pump elements and the other parts of the fuel system. 585 7) Paraffin inhibitor for crude oil The subject of the invention is the paraffin inhibitor for crude oil, used as an additive to crude oil in the process of its exploitation, transportation and storage. Invented paraffin inhibitor prevents settlement of paraffin on machinery working in wellbores, surface of transmission pipelines and reservoirs. Exceptional activity of the inhibitor results in great lowering of crude oil viscosity which facilitates its free flow. Invented paraffin inhibitor is a clear, homogenous liquid in a wide range of temperatures from –30°C to + 55°C. Inhibitor is dosed continually to machinery working in wellbores and transmission pipelines in the amount of 200 – 750 ppm (by weight). Invented inhibitor is a mixture of ionic or non-ionic dispersants, polymeric crystallization modifier and specially selected organic solvents. It was found that the use of innovative non-ionic surfactants with ionic dispersants and copolymer, resulted in unexpectedly high effect of prevention against paraffin deposition from crude oil. Applied surfactants caused significant reductions in viscosity, pour point and cloud point of crude oil. Simultaneously, used surfactants protect wellbores and pipelines in oil wells from corrosion. Additional advantage of invented paraffin inhibitor is high (above 80%) degree of biodegradation of used alkoxylated surfactants. The way of preparation and using paraffin inhibitor is an object of notification in Polish Patent Office. 8) Diesel fuel for vehicles equipped with particulate filter systems The invention relates to diesel fuel for vehicles equipped with particulate filter systems with improved ecological and performance characteristics, which allow for limitation of the emissions of pollutants harmful to the environment, especially particles and nanoparticles with mutagenic effects, and therefore specifically designed for use in urban agglomerations, ecological protection zones and industrial objects such as mines with monitored harmful exhaust emissions, black smoke and particulate matter emissions. The particulate emissions from compression ignition engines are especially hazardous. Therefore it was necessary to introduce stringent regulations limiting particulate matter exhaust emissions. Euro 5 Regulation which came into force in 2008 distinguished nanoparticles and imposed on them severe limitations On account of this it is anticipated the use of Diesel Particulate Filters (DPF), Selective Catalytic Reduction (SCR), Lean NOx Traps (LNT) and Diesel Oxidation Catalysts (DOC). The diesel oil according to the invention comprise selected petroleum fractions and/or vegetable and/or animal derived components and also a multifunctional additive package containing FBC (Fuel Born Catalyst) precursors, which provides for entire continuous elimination of solid carbon particles in DFP. The diesel fuel according to the invention was implemented in municipal public transport buses equipped with Euro 3 engines. The application of the invention enabled to fulfil the Euro 5 requirements for the exhaust emission. 586 9) Drilling fluid Drilling fluid is a multicomponent colloidal dispersion system having definite physical-chemical properties, the basic function of which is to lift cuttings out of the wellbore and to maintain wellbore walls stability during drilling. The s u b j e c t of the invention is a potassium silicatebased drilling fluid for drilling through shale strata ranked to the brittle rocks which at the presence of water undergoes structural damage in the form of fissures and microfissures, and for rocks with increased content of silt minerals. The technical and functional value of the solution according to the invention is improved inhibition of drilled argillaceous rocks while simultaneously keeping proper rheological and structural parameters, filtration, and pH of the drilling fluid during the wellbore drilling. 10) Method for decreasing the content of hydrogen sulfide in drilling fluids Method related to the degree of microbial purity of base water, wherein a hydrogen sulfide neutralizer is introduced into the circulating drilling fluid in amount corresponding to the concentration of 0,05 to 0,2 % v/v. Then, depending on hydrogen sulfide concentration or/and the number of sulphur bacteria in the drilling fluid, another dose of H2S neutralizer is added in amount corresponding to the concentration of 0,01 to 0,02 % v/v accordingly to a drilling fluid volume. The H2S neutralizer is selected from the group consisting of triazine derivative and/or amine compounds. The invention is aimed at prevention of excessive emission of toxic biogenic hydrogen sulfide during drilling work, limiting harmfulness of drilling muds and wastes for the natural environment. 11) Combustion modifier, particularly for heating oil The subject of the invention is combustion modifier, particularly to heating oil, comprising substances catalyzing combustion process, which decreases toxic substances emissions. Changes of heating oil quality are forced by regulations and directives for environmental protection by controlling emissions of harmful substances into the atmosphere. The most important in the program CAFE (Clean Air for Europe) – is management of particulate matter emissions which are 10 microns and 2,5 microns in diameter and generate the most significant threat to human health. Very fine particles can reach the deepest regions of the lungs, causing serious pulmonary and cardiovascular diseases. Both emissions of harmful substances into the atmosphere and watt-hour efficiency of oil-fired boilers depend on the fuel quality and employed additives, particularly combustion process modifiers. The combustion modifier, according to the invention comprising substances catalyzing combustion, particularly for heating oil, is characterized by its content of catalyst of combustion process of hydrocarbon fuels and biofuels, and additives: detergent, antiwear, friction modifier, corrosion inhibitor, demulsifier, antifoam agent, antioxidant, biocide, tracer, and hydrocarbon solvent.The use of modifier according to the invention provides for engine emissions reduction mainly particulate matter and carbon oxide 587 POLISH GEOLOGICAL INSTITUTE – NATIONAL RESEARCH INSTITUTE (Państwowy Instytut Geologiczny – państwowy Instytut badawczy) Organisation Contact Data Contact Person Data 4, Rakowiecka st, 00 – 975 Warsaw, Poland International Cooperation Division: prof. Marek Graniczny e – mail: [email protected] phone: +48 22 459 20 00 e – mail: [email protected] http://www.pgi.gov.pl/en.html Ilona Smietanska, M.Sc e – mail: [email protected] phone: +48 22 4592 523 or +48 224592 210 Panstwowy Instytut Geologiczny – Państwowy Instytut Badawczy (Polish Geological Institute) is the National Research Institute under supervision of the Ministry of the Environment of the Republic of Poland. PGI-NRI is the largest geological R&D unit in Poland,responsible for geological inventory, monitoring, knowledge and research. It is entrusted with tasks of the Polish Geological Survey and the Polish Hydrogeological Survey. The tasks are implemented by the staff of about 800 high-skilled employees (75% with university degrees). Among its priority programmes are: Energy Security, Geology for Land Use Planning and Development, Raw Materials Security and Supply, Geohazards, Geotechnologies, Marine Geology, Climate and Environment Change, Geoinformtion, Groundwaters, Geodiversity Conservation and Geotourism and International Cooperation. PGI-NRI acts as the national legal entity responsible for the domestic safety in supply of mineral and hydrocarbon resources (including shale gas and tight gas), groundwater management, providing geoscientific information vital for climate policy (i.e. the CCS technology) and keeping the state geological archives. PGI-NRI is responsible for groundwater monitoring as well as monitoring of natural hazards e.g. mass movements and landslides. It is the custodian of much of the country’s geoscientific information and is the largest Polish editor and publisher of geological maps compiled in digital standard. PGI-NRI maintains the information system on the domestic mineral and groundwater resources for their management and protection. PGI-NRI carries out research on protection of the Earth surface and natural resources including spatial information on the environment, geoenvironmental and geochemical cartography, waste management, land and water contamination assessment and remediation means, environmental sampling and laboratory tests, environmental protection and monitoring. PGI588 NRI cooperates with scientific-research centres, institutes, organisations, industry, public administration and geological surveys of 40 countries all over the world. PGI-NRI offers scientific research cooperation with East Asian countries in joint projects as well as scientific consultancy, experises, geological works and survey in the following areas: Comprehensive studies and research projects of geological structure including multidimensional geodata modelling and visualisation, cartograhic works, mapping of superficial formations, modelling, geodata processing and interpretation. Scientific consultancy in geology, geochemistry, geophysics and others fields through examining the Earth properties and the rock layers and structures in so far as they concern the localization of mineral deposits, underground waters, geohazards and geoenergy. Expertises on a wide array of geological, hydrogeological and environmental issues. Geological works in the range of prospecting and exploration of deposits of mineral resources and groundwaters. Areas of proposed cooperation: Geohazards survey Preventing natural disasters is one of the most important challenges the East Asian countries face. PGI-NRI offers cooperation and expertises in assessment of hazards related to geodynamic phenomena. PGI-NRI has a long-term experience and achievements in research of areas of risk of mass movement, land surface mobility and subsidence hazards including coastal erosion with the use advanced methods and techniques such as teledetection and geodetic techniques including Optical High Resolution Imagery (HRI), radar interferometry (PSInSAR), airborne and terrestial LIDAR (ALS- Airborne Laser Scanning and TLS - Terrestrial Laser Scanning). These methods are used for identification, inventory and monitoring of landslides and mass movements in order to improve traditional methods of mapping. The data provided by radar interferometry are especially valuable for identification and mitigation of natural catastrophes such as rapid land subsidence, floods and flash floodings and accelerated soil erosion. Since year 2006 PGI –NRI has been the leader of the a national project called Landslide Counteracting System (SOPO). Its aim is to create detailed map of landslides in Poland. Based on these maps local governments can plan where to locate infrastructure without exposing it to damage. The provided products mainly include results of analyses in the form of maps, databases, portals and information and map services built with the use of advanced hadware. Moreover PGI-NRI offers assistance in establishment of laboratories, insitutional strengthening and training in remote sensing techniques and creation of services for dissemination of information to the public. 589 Sustainable management of mineral resources PGI-NRI is also deeply interested in opening and cultivating cooperation in sustainable management of mineral resources. The appropriate use of domestic base of mineral raw material resources and safety of their supplies are recognized nowadays as the issue of utmost importance for national economies in Europe and other parts of the world, which is well reflected by treatment of several mineral raw materials as necessary or even of critical importance for further development of national economies and industry. PGI-NRI comes here with tradition and experience in effective prospecting, exploration and exploitation of mineral raw materials, going back for several centuries in area of Poland and well evidenced by discoveries of several major mineral deposits, especially in the 20 th century. It should be added that the key to these successes was always a capability to combine the tradition with the use of modern approach and methods in prospecting and exploration and cooperation and exchange of experience with foreign partners in the country and abroad. PGI-NRI is deeply interested in exchange of experience and scientific research cooperation with East Asian countries in joint projects as well as scientific consultancy, expertises, geological works and survey. This is especially the case of supporting central and local administration is establishing policy in sustainable management of mineral raw material resources, including : - exploration and assessment of the resources; - compilation of mineral raw material maps for protection of the resources for the next generations in land-use plans; - rational and sustainable use of currently exploited mineral resources, reduction of waste stream and proper use of accompanying mineral raw materials and the mining waste. Carbon Capture and Storage (CCS) PGI-NRI is also interested in cooperation and exchange of knowledge and expertise in the field of Carbon Capture and Storage (CCS), regarded as the most efficient way to reduce carbon dioxide emissions from the major point sources, especially power and chemical plants. Since the year 2008, PGI –NRI has been the leader of the a national programme called Assessments of Formations and Structures for Safe CO2 Storage and Programme of Monitoring. That well advanced programme made it possible to identify first sites for pilot locations of underground CO2 storage. Further works within the frame of that programme make the PGI-NRI team interested in cooperation and partnership in R&D, particularly with Japan, China, Taiwan, South Korea in the follow-up or related projects of Carbon Capture and Use (CCU), especially those aimed at: conversion of carbon dioxide into methane in anoxic and hot aquifers used as underground CO2 storage sites ; combining geothermy and CCS ; new techniques in the use of CO2 injections in enhanced oil and gas recovery ; the use of CO injections in enhancing extraction of coal-bed methane. 590 THE INSTITUTE OF AVIATION (Instytut Lotnictwa) Organisation Contact Data Contact Person Data 110/114, Krakowska st, 02 – 256 Warsaw, Poland phone: +48 22 846 00 11 fax: +48 22 846 44 32 http://ioa.edu.pl/ Deputy Director – Commercial: Marcin Gawroński M.Sc. Eng phone: (+48) 22 846 11 00 ext. 274 e-mail: [email protected] www.facebook.com/instituteofaviation http://www.youtube.com/ilottv The Institute of Aviation is the oldest research establishments in Europe, officially registered in 1926 although its roots go back to 1918. For eighty six years of its activity the scientists and engineers employed in the Institute of Aviation contributed remarkably to the development of the Polish economy and defense. Before the Second World War all the Polish aircraft were constructed or tested in the Institute of Aviation in Warsaw. In 2011 the Institute of Aviation was granted prolongation of its highest A category, conferred on research institutes. At present over 1500 engineers, scientists and researchers are employed by the Institute with nine hundred of them no more than 30 years old. Four new laboratories have been set up during the last 12 months, with one laboratory dealing with the pressure tests for equipment recovering crude oil and gas being second largest in the world. The main fields of the Institute's activity are the space technologies, aero and missile engines, materials technology, aerodynamics, composite technologies, design and test of aircraft constructions, near-field noise, and research in the field of recovery of crude oil and gas. The Institute of Aviation is a member of the domestic and international research organizations. As from 2005 the Institute has become a partner in an AERONET - Aviation Valley project. It is a group comprising of several well positioned research units. In April 2008 the Institute of Aviation has been admitted to the Association of the EREA Research Institutes whose aim is to consolidate, coordinate and undertake joint incentives. On June 7, 2010, an international organization International Forum for Aviation Research (IFAR) was called into being in Germany, in Luebbenau. The Institute of Aviation representing Poland, played an important role in its establishment, becoming one of its founders. The Institute of Aviation organizes international conferences, symposiums, and is a moderator in the global research incentives. The strategy of the Institute of Aviation is ‘To provide service in the international market research’. The world market means the highest competitiveness of the research services 591 offered leading to the development of new technologies. Polish membership in the EU opened enormous possibilities of cooperation in the field of applied research and development work. The Institute cooperates on a big scale with universities, research institutes, research centers and industrial labs in Europe, the United States, Asia, Australia and Africa. The Institute closely cooperates with the aviation industry world leaders such as: General Electric, Boeing, Airbus, Pratt&Whitney, Sikorsky, Rolls-Royce. In 2008 the Institute of Aviation started the national programme „The Age of Engineers”. It is a programme for promoting engineering professions and technical sciences. Programme is addressed to gymnasium and high school students. The Institute comprises of four research centers: The New Technologies Center, Materials and Structures Research Center, Net Institute and Engineering Design Center. 592 Materials testing laboratory METALLIC MATERIALS TESTS Static strength tests (tension, compression, bending) at temperatures from -70°C to 900°C in accordance with ASTM - E 8, E 21, E 328, E 9, E 209, C 293. Low- and high- cycle fatigue tests control strain and load at temperatures to 900°C in accordance with ASTM - E 466, E 606, together with research reports in accordance with E 468, E 739. Creep tests at temperatures up to 1100°C in accordance with ASTM E 139. COMPOSITE MATERIALS TESTS Tests of mechanical properties and temporary resistance to tension, compression, bending, shearing in temperatures from -70°C to 300°C in accordance with ASTM - D 3039, D 3410, D 3518, D 4255. Tests of temporary resistance stick joints composites with metals. Fatigue tests at temperatures from -70 up to 300°C in accordance with ASTM – D 3479. Conditioning of composite samples in conditions of controlled humidity or at temperatures in the range of up to 300°C. RESEARCH FACILITIES AND EQUIPMENT Test type Low Cycle Fatigue tests High Cycle Fatigue tests Static strength tests (tension, compression, bending) Creep tests Specimen and elements testing Specimen in accordance with ASTM and other standards (length up to 500 mm) Specimen in accordance with ASTM and other standards (length up to 100 mm) Specimens in accordance with ASTM and other standards (length up to 800 mm) Specimen in accordance with ASTM and other standards (length up to 150 mm) Load range Test temperature Research equipment Tension and up to 900°C compress load: up to 250 kN Frequency: up to 5 Hz Tension and up to 900°C compress load: up to 250 kN Frequency: up to 60 Hz Tension and -70 up to 900°C compress load: up to 250 kN 27 test rigs (MTS, Instron ) Tension and up to 1100°C compress load: up to 50 kN 36 test rigs (Creeps) 593 27 test rigs (MTS, Instron) 14 test rigs (MTS, Instron) Structural testing laboratory STATIC AND FATIGUE TESTS - Full Scale and Component Static and Fatigue Tests according to individual orders (with design and manufacturing of Test Stand) – up to 24 load channels. Performed to collect experimental data of tested object behaviour (strain, displacement) under load. In case of fatigue testing – data to assess structure durability is provided. Functional tests of structures not loaded or under load, with load, displacement and strain measurements. Stiffness tests of mechanical structures. Static and fatigue tests of turboengine shafts or other axially symetric structures simultaneous (tension/torsion loads), also in elevated temperature. Laboratory can perform multichannel testing of large-size structures using fully computerized loading system. Tests can be performed in a complex way (with cooperation with other IoA divisions), it means with data analysis, design proposals increasing structure durability. In the area of strain gauging Laboratory can perform: preparation of strain gauge installation, measurement realization, data processing. Structures can be inspected during the test using NDT methods. DYNAMIC TESTS High-cycle resonance fatigue tests and of compressor blades and other elements. Frequency Check Tests. OTHER TESTS Burner Rig Thermal Barrier Coating Spallation Testing. High Temperature Oxidation Testing to materials and parts of aircraft engines. Test Stand "Windmill" Low-revolution wear testing of fan blades and discs. 594 Non – destructive testing laboratory Laboratory carry out non-destructive testing of structures and their components by the following methods: eddy current, penetrant, magnetic, ultrasound, visual X-ray. The laboratory performs testing of complete structures, their sub-assemblies and components as well as materials and semi-finished products. The laboratory is capable of detecting defects such as fatigue cracks, open cracks, corrosion cracks, blisters, inclusions, laps, cold shuts, leaks, welded joints defects etc. Tests can be conducted at different stages of production process: from input materials inspection to in-operation control to final control. We carry out in-service, field and lab tests. Temporary testing includes materials & structures diagnostics in compliance with the accepted standards or the client's special requirements. The laboratory is capable of performing non-standard non-destructive diagnostics. Our engineers are certified according to the EN 473 standard. Other services: Developing test programmes and conducting tests for the exploitation purposes – state diagnostics in the area of aeronautical and non-aeronautical applications Developing test programmes and conducting tests in the production process Developing test programmes and conducting research during elements and objects testing Upgrading existing research methods in accordance with relevant standards or client requirements Preparing manuals and technical documentation in the area of non-destructive research of materials and semi-finished products Developing programmes of training courses Organizing training courses Section of metallography We conduct tests in the range of: Hardness. Determining chemical composition by the EDS method (identifying materials, contaminants, estimating elements concentrations on the surface of the specimen). Microstructure analysis in an optical microscope. Surface analysis. 595 Fractography in a scanning electron microscope (crack location, checking material homogeneity). Roughness. Strength analysis team The team provides work which includes: Designing 3D test rigs for the purposes of Structural Testing Laboratory. Strength analysis of research stands with the use of Finite Element Method. Fatigue analysis of aircraft structures. Developing aircraft structures load spectra. Developing test programmes for static and tests or fatigue aircraft structures. Crack propagation analysis of metallic structures (2D & 3D) with Finite Element and Boundary Element Methods (ANSYS 10, FRANC2D, FRANC3D, AFGROW, NASGRO). Strength Analysis Team in collaboration with Structural Testing Laboratory offers complex research services from the test rig design and co-ordination of test rig manufacturing performed by proven subcontractors, to the final test report. Machining workshop Preparation of specimens for strength tests, on request and according to customers specification, and small fixtures, like gripping systems, used in high temperature tests, Production of small fixtures, like gripping systems, used in high temperature tests, Machining of very tough and hard alloys subjected to treatment used for aircraft engines production as Nickel alloys or Titanium alloys. 596 Aerodynamic department Wind Tunnel T3 (5 m) Capabilities: Wind tunnel testing of aircraft models to determine aerodynamic characteristics Aerodynamic load and pressure distribution measurements on aircraft element models (wings, propellers, horizontal and vertical tails, control surfaces, helicopter rotors, external stores etc.) Wind load measurements for buildings and their elements. Wind velocity and pressure distribution measurements in built-up areas. Flutter tests of aircraft models – investigation of flutter characteristics, vibration frequency, critical speed, vibration damping at subcritical speeds Store trajectory tests including forced deployment for external stores payload Flow visualization (tufts, smoke, fluorescent minitufts) Wind Tunnel T1 (1,5 m) Capabilities: weight and pressure distribution tests on models of airplanes, helicopters, automotive and railway vehicles and their elements Optimization of flap and slat position Hinge-moment optimization for ailerons and tail units Tufts and minitufts with UV-light flow visualizations Smoke flow visualization Tensometric balance force measurements Design of experiment (DoE) Low Turbulence Wind Tunnel TMT Capabilities: Laminar airfoils wind tunnel tests at turbulence level below 0.02% for velocities up to 40 m/s Calibration of wind measurement devices for meteorological purposes Smoke flow visualization 597 Trisonic Wind Tunnel N-3 Capabilities: Tunnel tests of aircraft models to determine aerodynamic characteristics and pressure distributions for the Mach number in the range from 0.1 – 2.3 Aerodynamic load measurements on airframe parts models (wings, horizontal and vertical tails, control surfaces, external pods and stores etc.) including the ability to individually measure load on each separate element Hinge-moment measurements for tail units Tests of airfoils including buffeting boundary determination at transonic velocities Visualization of flow using oil and Schlieren methods Tunnel tests of airfoils aerodynamic characteristics Aerodynamic design of aircraft, wings, airfoils high lift devices and high lift airframe configurations etc. Weight and pressure transducers calibration Unsteady pressure measurements using high precision vibration generator Computational Fluid Dynamic (CFD) and Flight Mechanics Group Analysis For computational analysis of flowfield, both commercial and in-house developed software is employed. In collaboration with other research facilities our group takes a part in developing the new software for academic purposes. Capabilities Simulation of flow around an aircraft and parts of airframe Simulation of flow around a helicopter and parts of airframe and interference with surrounding objects Unsteady flows in shape-shifting domain and around such geometries Fully three-dimensional simulation of flow around the main rotor of a helicopter (in forward flight and in hover) based on URANS (Unsteady Reynolds Averaged Navier Stokes) solution Fluid-structure interaction for modeling nonrigid blades of helicopter rotor including blade flapping Flow simulation in ducts (e.g. air intake ducts in aircraft engines) Spaceship flight simulation Flow issues related to non-aviation areas Flow in land and water based transport Flow in civil engineering (buildings, stadiums, bridges etc.) Simulation of air movement in urban areas; safety issues in high-altitude rescue actions Flow and load analysis for constructions subject to aerodynamic and hydrodynamic forces (e.g. strong gusts of wind) Flow in turbines, fans etc. Multiphase flows Supersonic and hypersonic flows including heat and radiation modeling Phase changing and chemical reactions simulation 598 Performance and stability analysis Landing Gear Department Strength analysis is performed using MSC NASTRAN/PATRAN and FEMAP/NASTRAN. We are capable of structure optimization with regard to strength, weight, and fatigue wear. Analyses performed include effects of contact, friction, geometric and material nonlinearity, thermal and dynamic analysis. Computational Simulation Methods for: load cases for landing gear components dynamic load conditions stability simulation with experimental validation “shimmy” phenomena behavior in extreme conditions computer simulation for aircraft touch-down dynamics for different landing gear concepts braking transients (dynamic, heat transfer, vibration). Analysis: Stiffness, strength, and flexibility evaluation of subassemblies and complete landing gears Optimization and integration of landing gear elements, braking systems, dampers, and control systems Evaluation of design process, conformance with quality standards, research methodologies Reliability and durability evaluation of landing gear elements using analytical and experimental methods Load analysis Tests – Laboratory The Landing Gear Lab is capable of performing complex tests in compliance with the FAR, EASA, MIL, and AP standards for helicopters and airplanes with the max. take-off mass of 20000 kg (44000 lb). Tests are made on complete assembly and specific elements with regard to power consumption, static, dynamic, and fatigue strength, dynamic and functional characteristics, and impact load resistance. Capabilities: static and quasistatic tests, dynamic tests, functional tests. Measuring and recording parameters: time, force, displacement and deformation, pressure, temperature, rotational speed, acceleration, voltage and current. Turbojet Engine Laboratory Capabilities: Dynamic stresses measurements of rotating engine parts (e.g. compressor and turbine blades) Turbine blades temperature measurements (in working engine) Analysis of engine vibrations Analysis of transient state rotating instability zones in turbine engine compressors Compressor stable operating window determination (in working engine) 599 Jet engines impact test stands (up to 180 m/s) Balancing rotating assemblies (engine and other) Discs and drums load capacity acceptability Rotor disc and drum low-cycle strength Piston Engine Laboratory Capabilities: Temperature measurements in the range from 0 – 200oC Temperature measurements in the range from 200 – 1000oC Rotational speed measurements Torque measurements Fuel consumption measurements Air and exhaust gas flows measurements Measurements and processing of high speed in-cylinder and injection system events Estimation of engine’s characteristics end emissions according to ECE Regulations R49 Estimation of speed-, full- and partial-load-, no-load and governor characteristic curves Research and technological development works in the domain of I.C. engines with power output 30 ÷ 400 kW including optimization of combustion process, intake and injection systems and turbocharging Acoustics Laboratory The Lab specializes in aircraft noise analysis in accordance with the FAR and ICAO regulations. The laboratory is also capable of conducting standard noise tests on industrial machinery. The Lab is equipped with the SVAN and Bruel&Kjaer instrumentation. Avionics& Systems Integration Department Capabilities: Computer aided design (2D & 3D design) Electronic, analog and digital system design, including microprocessor and microcontroller based systems Design of control systems for electro-mechanical objects Guidance, control, and navigation systems designed for unmanned vehicles Diagnostic and testing equipment design Modernization and modification of aircraft equipment and systems Integration of avionics systems Expertise & Experience The Department conducts tests of aircraft and systems equipment and issues statements of compliance with RTCA, ARINC, MIL, TSO, DO-160C standards and aircraft requirements. The Department has the potential for prototype manufacture and short-run production of precision measurement diagnostic & indicating systems. Our laboratories have been equipped with necessary test beds and measurement systems to carry out complex analysis of products. Environmental Lab Capabilities: 600 Strength and resistance to sinusoidal vibrations for objects of the mass up to 50 kg, within frequency range: 5 – 2000 Hz, and acceleration up to 200 m/s2 Strength and resistance to repeated mechanical shocks for objects of the mass up to 450 kg, acceleration up to 3200 m/s2 , frequency up to 3 Hz, and impulse duration range: 6 – 30 ms Resistance to high and low temperatures, max. size of tested objects: - 680 x 540 x 820 mm in the temperature range from 60oC -180oC - 1250 x 1900 x 2250 mm in the temperature range from -70oC to 130oC Resistance to cyclic temperature changes within the range from -60oC to +180oC for objects of the max. size: 680 x 540 x 600 mm Resistance to high level of humidity within the range from 10% to 98%. Maximum size of tested objects: 680 x 540 x 820 mm, maximum weight: 10 kg Resistance to low pressure (1 hPa), max. size of tested objects: 1250 x 1900 x 2250 mm Frost and moisture resistance for objects of maximal dimensions: 680 x 540 x 820 mm. Resistance to linear accelerations for objects of the mass up to 10 kg and dimensions up to 300 x 300 x 300 mm. Space Technologies Group The Space Technologies Group focuses on developing space technologies such as: new rocket/space propulsion systems, green fuels, rocket structures and rocket trajectories analysis (including ballistic rockets). Other Capabilities: propellant injection analysis propellant combustion analysis cooling systems analysis: radiative, regenerative, transpiration, ablation pressure and turbopump power systems analysis engine performance analysis on ground and in vacuum Aircraft Design Team Design Capabilities: Composite structures: Glass & carbon composite aircraft structures Technological equipment: Composite structures molds, Varied assembly devices. FEM Analysis: Static analysis Vibrations Nonlinear analysis (material and geometrical nonlinearity) Thermo-mechanical analysis Adaptronic Department Areas of Research: -Adaptive control systems (adaptive impact energy absorbers). -Micro ElectroMechanical Systems (MEMS). -Biomedical engineering (computer aided head surgery). -Structural Health Monitoring (SHM). 601 Flutter Flight Tests General Information During the development of a new aircraft, a new version of an already existing aircraft or, for military aircraft, various flight configurations with carryings (missiles, external tanks, etc.), flutter flight tests are performed to explore flight domain. Thus, flight tests are needed; the objective is to determine the structural dynamic and aeroelastic state of the aircraft and to monitor any signs of approach or appearance of flutter in its flight domain. During flight tests, all the modes in a certain frequency band are monitored; their evolution as a function of the airspeed Vc. It proceeds by selecting a steady flight configuration (constant Ma, non turbulent atmosphere), applying excitation (white noise, sine or impact) using control surfaces or specific surfaces (ailerons, pallets), data given by the accelerometers instrumented on the structure are transmitted to the ground to be treated (modal analysis) and, after each acquisition, the aircraft changes its flight configuration. Method Output Only (OO) method, i.e. the excitation is not controlled. Outputs in Real Time (displayed in cabin) One global result for all the measurements: vibration damping and shape of the most dangerous mode. Completely automatic identification of modes frequencies and damping ratios. Period of the update of the identified modes: 1- second. Modes frequency range: 0.5 – 60 Hz. Configuration To carry out flight tests, the aircraft is equipped with accelerometers and an in-board recorder (up to 24 channels). Measurements are made under stationary atmospheric conditions and stabilized flight level (constant altitude and airspeed). There is the possibility for using telemetry to reduce time of the tests. Results During flight tests, various signals are recorded then recovered on workstations to be processed in differed time. Our software allows us: to visualize parameters as a function of time, to compute modal parameters using various methods, to analyze parameters measured during the test and to visualize mode shapes. 602 Catalogue of technologies developed by Polish Research NON-CLINICAL RESEARCH UNITS 603 INSTITUTE OF BIOTECHNOLOGY AND ANTIBIOTICS (Instytut Biotechnologii i Antybiotyków) Organisation Contact Data 5 Starościńska st., 02 – 516 Warsaw, Poland phone: +48 22 37 86 333 fax. +48 22 37 86 334 e – mail: [email protected] http://www.iba.waw.pl/en/index.html The Institute of Biotechnology and Antibiotics (IBA) is a leading scientific institution in Poland and recognized in the world which commercializes its own scientific and developmental achievements in the field of pharmaceutical and medical biotechnology, mainly by implementation of biopharmaceutical technologies. IBA is a research institute transformed in 1992 from Research and Development Biotechnology Center that continuous activity of the previous Institute of Antibiotics. The IBA operates in the health service and pharmaceutical sector. It employs over 150 people, including over 30 scientists. The IBA’s mission is to: create new and useful knowledge in the field of modern pharmaceutical biotechnology and the development and implementation technologies of pharmaceuticals and other biologically active substances. build up and elevate the image and position of the IBA within the scientific communities and in the pharmaceutical sector disseminate the quality assurance policy for IBA operations. The mission is carried out through: scientific works and research implementation of developed technologies through into production production based on in-house technology services contracted by external institutions. 604 The Institute contributes to the achievements of Polish science in the following two fields: pharmaceutical biotechnology: genetic engineering of new gene expression systems, genome diagnostics, monoclonal antibodies and the production of highly purified biologically active compounds and protein structures (e.g. recombined human insulin, growth hormone, interferon) chemistry of therapeutic compounds, including research and production methods for ß-lactam, aminoglycosides, macrolide and anthracycline antibiotics. IBA cooperates with a number of domestic and foreign scientific establishments and other companies in the pharmaceutical and medical industries. Major developments and implementations: IBA is an author of 43 implementations of its own pharmaceuticals and therapeutic substances. Technologies developed in the Institute were implemented in the then major pharmaceutical plants such as “Polfa" Pharmaceutical Plant in Tarchomin, “Polfa” Pharmaceutical Plant in Kraków (Krakowskie Zakłady Farmaceutyczne Polfa) and “Polfa” Pharmaceutical Plant in Pabianice (Pabianickie Zakłady Farmaceutyczne Polfa), and after 1990 in BIOTON S.A. Key developments: The 60s. Streptomycin, tetracycline, erythromycin and neomycin, semi-synthetic erythromycin derivatives such as erythromycin propionate lauryl sulphate and erythromycin stearate, ampicillin, nafcillin, carbenicillin, vibramycin, rondomycin; semi-synthetic beta-lactam antibiotics, penicillins and cephalosporins and tetracycline derivatives were investigated; technology to obtain polyfungin (an original antifungal antibiotic) was developed and implemented through into production based on an inhouse grown and patented strain; a technology for the synthetic antigen (trade name Testarpen) for penicillin allergy identification was developed. The 70s. More innovative antibiotics such as lincomycin, oxytetracycline, polymyxin and its derivative colistin, bacitracine were investigated; technology for obtaining a new erythromycin derivative (cyclic erythromycin carbonate) was developed and introduced in treatment under the trade name of Davercin (an original Polish drug). The 80s. New generation cephalosporins in mass (ceftriaxon, cefamandol, cefuroxime) and aminoglycoside antibiotics such as amikacin for injections and as eye drops implemented under the trade name of Biodacyna; new technology for obtaining Ldopa, Gyno-Trosyd, restrictive enzymes, monoclonal antibodies; semi-synthetic penicillin were introduced through into production in the “Polfa” Tarchomin Plant under the trade name of “Pipril”; antineoplastic anthracycline antibiotics began to be investigated. The 90s. 2nd and 3rd generation cephalosporins were developed and implemented through into production. These included ceftriaxon (Biotrakson), cefotaxim (Biotaksym), cefuroxime (Biofuroksym), ceftazidime (Biotum) and cefoperazone (Cefobid) and oral forms (tablets and syrup) of cefuroxime axetil (Bioracef); moreover clarithromycin, clindamycin and linkomycin manufacturing technology was developed; anthracycline antibiotic preparations were developed such as doxorubicin (Biorubina) and epirubicin (Bioepicyna) and a technology for obtaining daunomycin; antilaeukemic preparation under the name of Biodribin (cladribine) was implemented through into production. 605 2000-2005. A many-year team effort to develop the technology for obtaining recombined human insulin was successfully completed. In December 2000, a biosynthetic human insulin preparation solution, isophane biosynthetic human insulin preparation and their mixtures (a total of 17 pharmaceutical forms) were registered and implemented through into production in BIOTON under the name of Gensulin. The following preparations were developed and implemented through in BIOTON as eye drops: betaxolol (Betabion), diclofenac (Diclobion), potassium and sodium iodides (Vidibion), tropicamide (Tropicabion) and tetryzoline hydrochloride (Zalbion). The Institute currently operates within the following distinct areas of expertise that do however partly overlap: Science and Research. These operations are aimed at identifying application purposes, new methodologies, new applications, new fields of research, development, and implementation as well as selection of new research and development projects. Initially, projects predominantly related to the development of generic drugs (cephalosporins) in respect of their chemical technology, and then to biotechnological generic medicines (human insulin analogues, human growth hormone, interferons). Currently, IBA runs research on innovative biotechnology drugs and biosimilar products. Analytical, chemical and pharmaceutical testing, and testing in the area of biotechnology. As a result of these operations, the laboratory has became a leading establishment operating in line with GLP, GMP and ISO standards. The laboratory holds a number of certificates (Statement of GLP Compliance, GMP Certificate, ISO 9001:2008 Certificate) and provides analytical services in respect of trials and tests of medicinal substances and products, and their bioavailability and bioequivalence. Production of medicinal products. The Institute has created three major antineoplastic drugs: Biorubina® (doxorubicin) - An anthracycline antibiotic used in the treatment of solid tumours: breast carcinoma, pulmonary carcinoma, urinary bladder carcinoma, thyroid carcinoma, ovarian carcinoma, sarcomas and haematological and lymphatic malignancies. Bioepicyna® (epirubicin) - An anthracycline antibiotic used in the treatment of a number of malignancies (inter alia breast carcinoma, ovarian carcinoma, pulmonary carcinoma and soft tissue sarcomas) primarily as a component of multidrug chemotherapy. Biodribin® (cladribine) - A deoxyadenosine nucleoside derivative used in hairy cell leukaemia, chronic lymphocytic leukaemia and malignant non-Hodgkin’s lymphomas. Support Activities (scientific and patent medical information). All operations to assist in the creation of research programs, development of production, organization of nonclinical and clinical trials. 606 Competitive Advantage. The Institute holds a competitive advantage that is extra specialist experience in the process of commercialization of research results that leads to implementation of newly developed technologies and the launch of new medicinal products into production. This is mainly practical knowledge of drug registration requirements for the European Union countries and the conditions that affect interest of potential producers. To this end, the Institute: determines the research areas for a future therapy and those with high development potential, determines research areas with high application potential and economic profitability, and those which are not patent protected, acknowledges the rationale of patent-protection with the view of commercialization in the global market, at least in the European and the US markets, carries out research and development based on a recognized and certified quality system (GMP, GLP, GCP, ISO), carries out research, development and implementation projects in the technical conditions compliant with those required from drug candidates and potential drugs, records results for research, development and implementation projects in compliance with requirements that are set by relevant biotechnological drug regulation authorities (biosimilar or innovative drug procedures), manufactures medicinal substances at each stage of their production in compliance with legal regulations and GMP. The following assisting divisions operate within the Institute: Bioengineering Department Chemical Analysis Department Chemical Departments Scientific and Medical Information Department 607 Bioengineering Department The major objective of the Bioengineering Department is to produce recombinant proteins for therapeutic and scientific applications. For this purpose bacteria strains where synthesis of third-party protein takes place are constructed, isolated, purified and identified. Most of the statutory works and grants are subordinated to this purpose, and the results of these works are the grounds for cooperation in targeted projects that lead to bioactive compounds being obtained by genetic engineering methods in an industrial scale. Another group of activities is the assessment of the purity of industrially-produced recombinant protein by specific genetic engineering, immunologic and enzymologic techniques. Routine assays of protein and DNA remnants in pharmaceutical preparations are also carried out. As implied by the type of examination and the equipment needed for this, the Bioengineering Department is divided into: immunology, tissue culture, genetic engineering, microbiological, protein purification and analysis, bacterial genetics, mass spectrometry and biochemical laboratories, where the following operations are performed: Preparation of the antibodies for analytical purposes (control of the immunization efficacy in the process of obtaining polyclonal sera, purification of the polyclonal and monoclonal antibodies by affinity chromatography method, marking of antibodies). Development of ELISA tests for evaluating the purity of recombinant pharmaceuticals (marking the level of protein contaminants in E. coli host strain (ECP), marking the remnants of enzymatic preparations used in the process) and other proteins. Determination of the level of recombinant protein expression in the transgenic material by immunological techniques. Evaluation of the immunogenicity of recombinant antigens by parenteral immunization. Development of determination methods for biological activity of protein drugs in cultured cells. Production of relevant monoclonal antibodies necessary for analyses. Undertaking attempts to obtain stable expressions of the selected proteins in cultured cells. Isolation of plasmid and chromosomal DNA. Construction of E. coli production strains producing proteins and peptides that are useful in biotechnology, medicine and science. Development of new expression vectors based on plasmids isolated from natural environments (isolation, sequencing, analysis of properties). Evaluation of the replication biology of cryptic plasmids. Searching for the specific proteases that are useful in, for example, production of medication (e.g. obtaining production strains of E. coli synthesizing deubiquitinating protease that is an analogue of the yeast protease UBP1). DNA sequencing. Development of methods for culturing bacteria strains in laboratory scale fermenters. Laboratory scale development, of a method for the isolation and purification of proteins and peptides produced by production strains, and with consideration to the conditions necessary for transfer to industrial scale using various chromatographic techniques: under low, medium and high pressure conditions (FPLC and HPLC) at room temperature or +4OC. 608 Maintenance of the vitality of the IBA microorganism collection (over 800 strains, including 145 under reference IAW in the Catalogue of the Polish Collection of Microorganisms since 1990, membership in ECCO since 1995, membership in WFCC since 1996). Preparation of strains for sale and exchange within ECCO and WFCC, sharing the strains with other scientific and research establishments. Preparation and maintenance of the Master Cell Bank (MCB) and Research Cell Bank (RCB). Genetic modification within the vector leading to optimization of the expression level of produced protein, as well as improvement of the production strain stability. Molecular analysis of antigen suitability for construction of new generation vaccines (subunit vaccines) and the development of new carriers to deliver vaccine antigens through mucous membranes. Quantitative assay of plasmid and bacterial DNA contaminants in biosimilar pharmaceuticals by quantitative PCR method. Evaluation of proteins and peptides in respect of: distribution, identification, quantitative and sequence analysis, modification evaluation. Genetic identification of bacteria by MicroSeq system from Life Technologies, which may be used to evaluate the microbiological purity of pharmaceutics, cosmetics and food, etc. Continued control of the microbiological purity of the work space is possible. Determination of the mass profile of LC/MS/MS +HPLC peptide map. Determination of the mass profile of MALDI TOF/TOF peptide map. Evaluation of average and/or monoisotopic MALDI TOF/TOF molecular weight. Evaluation of average and/or monoisotopic MALDI TOF/TOF molecular mass + ZipTip C4 / ZipTipC18 purification. 2D - PF2D protein mapping, no fractioning 2D - PF2D protein mapping, no fractionation (+ digestion). All the facilities used by the Bioengineering Department are furnished with top quality appliances that are required for molecular biology research and examinations. All devices and equipment comply with GLP requirements and GMO handling standards. Bioengineering Department achievements: Constructed and patented E. coli production strains for therapeutic human proteins – human growth hormone, alfa 2a, alfa 2b, gamma, beta 1a and 13 interferon, short and prolonged action insulin analogue. Constructed in-house prokaryotic expression systems, to include a vector, proteolytic enzyme and culturing method in fermenters without an antibiotic. Constructed in-house vaccine antigens of human and animal viruses. Developed in-house analytical methods for marking contaminants in pharmaceutical preparations produced in bacteria or eukaryotic cultures in accordance with the requirements of the European Medicines Agency. Scientific research in the area of basic research concerning replication of new wild plasmids. 609 Chemical Analysis Department Research Research and studies are directly related to both, the subject areas and tasks executed by the Institute of Biotechnology and Antibiotics and by third-party companies, which run scientific and implementation projects within the scope of drug development, namely: develop, implement and validate research methods for chemical and biotechnological substances as well as pharmaceutical formulations and medicinal products; carry out research and studies in respect of the analytical control of technological processes, including the critical points, contamination profiles and process validation; design and carry out analytical studies of proteins at various stages of manufacturing of active substances and medicinal products of protein-origin, namely peptide mapping, proteolysis product analysis, development of new methods and analytical procedures for identification and quantitative assays. Services Services are provided in the field of chemical analyses and analytical research and studies. They include: analysis of medicinal products, active substances and chemical raw materials according to the normative documentation provided by a customer, suitable pharmacopoeias or in-house methods; validation of analytical methods; testing pharmaceutical availability of drugs; testing bioavailability, bioequivalence and pharmacokinetics of drugs and their metabolites; trials in respect of monitoring a therapy with immunosuppressant drugs; testing the stability of active substances and medicinal products; comprehensive analytical services for research projects related to the development of new drugs: development of research and trial methods, validation of analytical methods and manufacturing process, drafting of specifications, etc. To assure a high standard of services the Chemical Analysis Department operates three quality systems: ISO 9001:2008 in respect of “Chemical analyses and analytical studies” – certificate no. 110381-2012-AQ-POL-RvA issued by Det Norske Veritas; Good Laboratory Practice for bioanalytical and pharmacokinetic studies – certificate nr 4/2012/DPL; Good Manufacturing Practice – certificate GMP no. GIF-IW-N-4022/8/11. The Department holds a Medicinal Product Manufacturing License no. GIF-IW-N4001/245/10. 610 Chemical Laboratories Processes developed at Modified Antibiotics Department 1 The technology for manufacturing a number of antibiotics and semi-finished products for antibiotics at laboratory and semi-technical scale were developed at Modified Antibiotics Department 1. Specification of devices, process design and drug form were also developed. Most of the processes are patent-protected. 1. 2. 3. 4. 5. 6. 7. 8. 9. Antibiotics α-aminobenzyl penicillin (ampicillin) as a free acid and sodium salt α –carboxybenzyl penicillin (carbenicillin) as a free acid and sodium salt Piperacillin as a monohydrate and sodium salt Cephuroxim – 2nd generation cephalosporin, Cephoperazon – 3rd generation cephalosporin Cephuroxitin – 2nd generation cephalosporin Cefetamet and cefetamet pivoxil – 3rd generation cephalosporin Aztreonam as a free acid and sodium salt – monobactam Sulbactam – β-lactamase inhibitor commingled with ampicillin N,N-(1’,6’- hexamethyleneformamidine)-penicillin acid inhydrated and anhydrous form, as 1-acetoxyethyl ester and pivaloyloxymethyl ester chydrochloride – amidinopenicillin 1. 2. 3. 4. 5. 6. 7. 8. Semi-finished products for antibiotics D(-) - α-aminophenylacetic acid D(-)-4-phenyloxazolidinedion-2,5 α-carboxybenzoic acid 1-chlorocarbonyl-2,3-dioxo-4-ethylopiperazine Pivaloilooxymethyl chloride 1-acetyloxyethyl bromide Z-2-metoxyimino-2-(2-fluoro)-acetic acid chloride N-phenylacetyl-O-mesyl-L-threonine amide 1. 2. 3. 4. 5. 6. 7. Other therapeutic compounds PPL (penicilloyl-poly-L-lysine) antigen for penicillin allergy detection Sildenafil Human growth hormone Cardioxane (dexrazoxane) – cardioprotective drug Betabion (eye drops) Zalbion (eye drops) Viscobion (eye drops) 611 New anthracycline antibiotic derivatives Anthracycline antibiotics are the most commonly used biosynthetically manufactured cytostatics with high antineoplastic activity. Drug resistance has been a more common and is a very alarming issue recently. It was observed in many patients who undergo long-lasting therapy. A new chemically modified anthracycline antibiotic derivatives have been synthesized and tested at the Institute. These derivatives have demonstrated high cytostatic activity that is higher or similar to that of the parent antibiotics. Moreover, the majority of them are significantly less toxic and less cardiotoxic as compared to their respective equivalents and most importantly they have the unique property of overcoming drug resistance. Based on the outcomes of the research carried out to date, pre-clinical trials are planned to be held at the Institute of Biotechnology and Antibiotics to enable the selected compound to be recommended for clinical trials in order to register a new drug. In addition to antineoplastic activity, these derivatives are highly active against hepatitis C (HCV), demonstrating higher activity than any drugs used to date. 612 Modified Antibiotics Department 2 + Macrocyclic Antibiotics Department 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. Developed and implemented processes Testapren (penicilloyl-poly-L-lysine, a synthetic antigen for penicillin allergy detection) Testapren (penicilloyl-poly-L-lysine, a synthetic antigen for penicillin allergy detection) – pharmaceutical preparation Nafcillin (semi-synthetic penicillin) Ryfamycin SV sodium salt (semi-synthetic rifamycin SV) Lincomycin Clindamycin (semi-synthetic lincomycin derivative) 7-aminocephalosporanic acid Cefamandol (semi-synthetic 2nd generation cephalosporin) Ceftriaxon (semi-synthetic 3rd generation cephalosporin) Cefotaxim (semi-synthetic 3rd generation cephalosporin) Erythromycin A cyclic 11,12-carbonate (semi-synthetic erythromycin derivative) Amikacin (semi-synthetic lincomycin kanamycin) Amikacin (semi-synthetic lincomycin kanamycin) – three pharmaceutical preparations Sildenafil Insulin – 17 pharmaceutical preparations Diclobion – pharmaceutical preparation Vidibion – pharmaceutical preparation 1. 2. 3. 4. 5. 8. 9. Developed processes Ceftadizime (semi-synthetic 3rd generation cephalosporin) Cefpodoxime (semi-synthetic 3rd generation cephalosporin) Rifabutin (semi-synthetic rifamycin S derivative) TAEM (synthetic semi-finished product for ceftadizime) Cyclosporine Interferon alfa-2a – pharmaceutical preparation Interferon alfa-2a – pharmaceutical preparation 1. 2. 613 Scientific and Medical Information Department The Scientific and Medical Information Department operates in the following fields of expertise: Development of scientific and medical information based on professional literature and available databases of current research, development, and prospective plans of the Institute. Evaluation of selected medical preparations from the pharmacological, clinical and safety of use view point and from the view point of their current and future therapeutic significance, in particular evaluation of drugs of various therapeutic application obtained through genetic engineering. Patent research, and assurance of protection of intellectual and industrial property. Designing, organizing and development (in respect of pharmacokinetics, statistics) of the bioequivalence tests for various medicinal substances. Studies of pharmacokinetics and pharmacodynamics of medicinal substances, including drugs. Regular review of Polish and European pharmaceutical laws in respect of pre-clinical and clinical trials for medicinal products. Designing, arranging for and monitoring of pre-clinical trials at all stages of biotechnological product development. A wide range of pre-clinical trials have been carried out under project no. POIG.01.01.0200-007/08-00. The purpose of these trials has been to bring about the first in man trial, and subsequently the commercialization of innovative biosimilar medicinal products containing human insulin analogue. The team plans, arranges for and supervises progress of the following works: Pharmacological studies in vitro Testing binding with insulin and IGF-1 receptors (affinity, dissociation level) on cell lines, assessment of autophosphorylation and phosphorylation of receptor signal elements, confirmation of biological activity and metabolic effects of the tested substance. Testing glucose uptake. Testing stimulation of cellular proliferation in tissue cultures by evaluating mitogenic effect of the tested substance. Pharmacological studies in vivo Testing on healthy animals (rats, dogs, monkeys) with artificially induced diabetes with and without glucose loading. Pharmacologic testing in respect of safety. Pharmacokinetic studies in vivo Testing on rodents with the use of a marker to evaluate distribution of the substance into tissues, organs and metabolism. Pharmacokinetics after single iv and sc dose administered to one specie (rat). 614 In-house research to compare pharmacokinetic properties of insulin analogues with a different primary structure. Studies to evaluate pharmacokinetic profile Evaluation of ADME (absorption, distribution, metabolism, elimination) process in various mammal species. Toxicity studies Evaluation of adverse effects on various animal species after administration of multiple doses of the tested compounds by various way of administration. Evaluation of toxicity after single administration Extended toxicity testing Chronic toxicity testing with carcinogenicity effect assessment Local tolerance testing During the research and studies we cooperate with top class establishments in Poland and throughout the world who have experience, equipment and relevant quality certificates, including GLP. 615 This page is left intentionally blank 616 Catalogue of technologies developed by Polish Research Institutes PHYSICS AND ASTRONOMY 617 INSTITUTE OF PLASMA PHYSICS AND LASER MICROFUSION, EURATOM – ASSOCIATION (Instytut Fizyki Plazmy i Laserowej Mikrosyntezy) Organisation Contact Data 23 Hery st., 01 – 497 Warsaw, Poland phone: +48 22 638 14 60 fax. +48 22 666 83 72 e – mail: [email protected] http://www.ifpilm.pl/ifpilm.pl/en/ The Institute of Plasma Physics and Laser Microfusion (IPPLM) was founded on the 1st January of 1976. Since June, 2001 it has carried its activities under the authority of the Ministry of Economy of the Republic of Poland while the research program has been under surveillance and co-financing of the Ministry of Science and Higher Education. The research carried out at the IPPLM includes studies of plasma physics and applications as well as scientific and technological efforts to investigate thermonuclear fusion, to provide a safe energy source for the future. The IPPLM is an institution which is authorized by the Ministry of Science and Higher Education to coordinate the research on magnetic confinement fusion (MCF) in Poland under EURATOM Community nuclear fusion program on the basis of the Contract of EURATOM-IPPLM Association signed with EURATOM Community (represented by the European Commission). These works concern plasma physics and technology for MCF toroidal thermonuclear devices (tokamaks and stellarators). Studies of laser fusion (an important method of development of inertial fusion energy - IFE) and laser plasma are carried out as a part of the European HiPER project, projects supported by LASERLAB-Europe Consortium and by EURATOM Community within IFE keep-in-touch activity to a limited extent. The Institute employs about 80 persons including 6 professors and 20 doctors. The structure of the IPPLM includes two research divisions: Division of Laser-Produced Plasma (DLPP), and Division of Plasma in Magnetic Field (DPMF). The DPMF of IPPLM includes the International Centre for Dense Magnetised Plasmas established in agreement with UNESCO. This laboratory is dedicated to science, education and technology transfer. Most of the IPPLM’s activity is carried out within broad international cooperation, mainly supported by European projects. 618 The scope of activity of the IPPLM includes: • study of physical processes in and technology of tokamaks and stellarators • theoretical analysis and numerical simulations of magnetically confinement plasmas in tokamaks and stellarators • study of plasma-wall interaction technologies with application of laser methods and visible spectrometry • development and application of diagnostics of X-rays, VUV and visible radiation as well as neutrons emitted from plasmas in tokamaks and stellarator W-7X • studies and applications of dense magnetized plasmas generated in Plasma Focus device PF 1000 as an intense pulsed source of X-rays and neutrons • optimization of Hall plasma thrusters • study of laser-produced plasma physics and technological applications • study of processes related to inertial confinement fusion (laser fusion) • study of laser-matter interaction physics at ultrahigh laser beam intensities • study of hydrodynamic processes accompanying the laser-matter interactions • development and applications of advanced diagnostics for laser-produced plasmas (ion and X-ray diagnostics, interferometry). The Institute offers its expertise and know-how in above mentioned research areas, development of measuring methods and technologies. We are interested in developing scientific and R/D cooperation and executing common research projects in these areas. In IPPLM there were elaborated and implemented into research practice and technology, among others: • technology of small Plasma Focus devices as a pulsed sources of X-ray radiation and neutrons • various ion and neutron diagnostics for hot and dense plasmas (laser-produced plasmas, plasmas generated in Z-pinch and Plasma Focus discharges) • multi-frame laser interferometry for measuring of pulse plasma dynamics • laser-induced material technology (including a removal of surface layers, ion implantation for modification of semiconductor materials) • advanced Hall thrusters for space technology • visible (including Laser-Induced Breakdown Spectrometry – LIBS), VUV and X-ray spectroscopy (including gas electron multiplier detectors (GEM), pulse height analysis (PHA) and multi-foil spectroscopy (MFS) systems. Most of above mentioned methods, equipment and diagnostic systems can be easily adapted for non- plasma applications. The IPPLM’s offer includes: research projects, technology projects concerning devices, measuring equipment, cooperation and consultancy regarding those projects, support in delivery of equipment as well as personnel training. 619 NATIONAL CENTRE FOR NUCLEAR RESEARCH (Narodowe Centrum Badań Jądrowych) Organisation Contact Data 7 Andrzeja Sołtana st., 05 – 400 Otwock, Poland phone: +48 22 71 80 001 fax. +48 22 77 93 481 e – mail: [email protected] http://www.ncbj.gov.pl/en Radioisotope Centre POLATOM carries out research programs related to the application of radioactive preparations and radiolabelled compounds in various fields in medicine, research and industry. Main areas of research activity of Radioisotope Centre POLATOM present multidisciplinary character and combine chemistry and physics of radionuclides, radiochemistry, analytical chemistry, metrology of ionizing radiation, biology, pharmacy and nuclear medicine. The main research and development domains are: Investigation of novel biomolecules as carrier for radionuclides and preliminary assessment of their diagnostic and/or therapeutic utility Development of technologies for production of high specific activity radionuclides in nuclear reactors and accelerators, using highly enriched target materials and modern separation techniques Development of methods for radioactivity measurement and assessment of radionuclidic purity (determination of , β, and impurities) Chemical and pharmaceutical development and biological activity assessment using in vitro and in vivo methods of new radiopharmaceuticals for clinical application. Based on the research programs POLATOM offers technologies for manufacturing of radiochemicals and sealed radiation sources for various application, radiopharmaceuticals and related services. POLATOM offers also neutron irradiation services in the Maria Research Reactor. Among various services related to the radiation protection POLATOM offers design and manufacturing of biological shielding against , β and radiation and shielding for specialized devices for the pharmaceutical and nuclear industry. 620 Laboratory of Radioactivity Standards in the Radioisotope Centre POLATOM in Otwock, Poland, is the only laboratory in Poland performing radioactivity measurements of α-, β- and emitters by absolute methods and performing calibration of standard solutions and radioactive sources. President of the Central Office of Measures in Poland (GUM) in 1999 established and with Decision No. 1/2004 of 21 April 2004 confirmed the establishment of the National Standard of Radionuclides Activity in Poland. The standard is stored and used in the Laboratory of Radioactivity Standards. It consists of triple-to-double coincidence ratio (TDCR) system, 4π(LS)- coincidence/anticoincidence system and X- coincidence system. These are unique measuring systems of the highest metrological quality in Poland, which are used for the absolute methods of radioactivity measurements. LRS transmit the unit of radioactivity to users of radioactive sources, providing them with standard solutions and sources, and performing the calibration of dose calibrators. LRS also participates in international key comparisons of radioactivity measurements, enabling the linking to the global system of national standards. These comparisons are organized by the International Bureau of Weights and Measures BIPM and the European Association of National Metrology Institutes EURAMET. The laboratory also participates in comparisons within the framework of the International Reference System SIR. Other systems available at LRS, such as liquid scintillation counter TriCarb 2910 TR, liquid scintillation counter Wallac 1411, set of four scintillation counters with NaI(Tl) detectors, set of three 4π ionization chambers, dose calibrator Capintec CRC-15β and three spectrometric systems with HPGe detectors can be used for determination of radionuclides radioactivity as secondary systems related to the National Standard in an unbroken chain of comparisons. LRS is also equipped in 2π and 4π gas proportional counters adequate to determining particle flux leaving the area of the source and the dose rate meter MAD 2000 for assessment of absorbed dose. Laboratory of Radioactivity Standards offers activity standards in the form of solutions and solid sources: Solutions of individual radionuclides Mixed solutions – intended to serve as calibration solutions for systems used to measure aqueous samples of low activity Point sources of individual radionuclides – photon spectrometers Point sources from a mixture of various radionuclides Check sources – intended for the control of dose calibrators used in nuclear medicine departments Volume sources from a mixture of various radionuclides – intended for the calibration of systems used to measure environmental samples 621 The LRS has implemented and maintained quality management system compliant with the international standard ISO / IEC 17025:2005. As a calibration laboratory it is accredited by Polish Centre for Accreditation, a signatory to EA MLA and ILAC MRA that include recognition of calibration certificates. Laboratory of Radioactivity Standards as accredited calibration laboratory (accreditation no. AP 120) offers following services: Calibration of dose calibrators with ionization chambers Calibration of radioactive solutions with primary and secondary methods Calibration of radioactive point sources of -emitters Calibration of radioactive control sources for use with dose calibrators Calibration of radioactive area sources Outside accreditation scope LRS offers following services: Calibration of radioactive multigamma solutions and sources Analysis of radionuclidic composition and determination of radionuclides activity in different materials Dose rate measurements for ophthalmic applicators Contact Person Data Laboratory Manager: Tomasz Dziel phone: + 48 22 718 0718 fax: + 48 22 718 0350 e-mail: [email protected] 622 Department of Nuclear Equipment HITEC NCBJ Organisation Contact Data 7 Andrzeja Sołtana st., 05 – 400 Otwock, Poland phone: +48 22 718 05 00 fax. +48 22 718 05 01 e – mail: [email protected] http://www.hitecpoland.eu/hitec.php?strona=onas&lang=en HITEC is a manufacturing department of the Polish state owned research and development laboratory: National Centre for Nuclear Research (in Polish – Narodowe Centrum Badan Jadrowych). The Centre, being one of the largest scientific institutes in Poland, carries out pure and applied research on subatomic physics, i.e. the elementary particle and nuclear physics, reactor physics, hot plasma physics, material engineering and related fields. The Centre is localized in Otwock, the satellite city of the country capital, Warsaw. The 44 ha campus houses numerous research facilities, most notably the research nuclear reactor MARIA. The reactor is used not only for scientific purposes but in equal manner for production of radiopharmaceuticals. The Centre employs over 1000 employees, among whom almost 200 are professors or Ph.D. degree holders. HITEC (also known under its Polish name Zaklad Aparatury Jadrowej) benefits out of the research capabilities and experience of the parent Centre and puts scientific ideas for practical use. HITEC specializes in the applications of accelerator technologies in medicine and industrial radiography. For over 40 years the company has been designing, manufacturing and marketing a range of medical and industrial electron accelerators along with complementary equipment and software. HITEC is headquartered in Otwock, at the main campus of National Centre for Nuclear Research. Over 90 employees of HITEC collaborates closely with the research part of the Centre on improving current products and developing the new ones. 623 HITEC line of medical accelerators consists of three devices intended for carrying out cancer radiotherapy: Coline 10 - medical accelerator provides photon and electron beams irradiation with energy from 6 up to 10 MeV. In addition to solid therapeutic parameters, Coline 10 distinguishes itself with a minimal footprint which allows for its installation in the environment frequently not available for other manufacturers. Coline 6 – is a state of the art medical accelerator with 6 MeV photon beam, fully capable of delivering modern treatment techniques, IMRT and IGRT. For that purpose, Coline 6 can be equipped with a custom Multileaf Collimator and an Electronic Portal Imaging Device. Coline 4 - medical accelerator provides 4 MeV photon beam. Coline 4 has been designed as an inexpensive replacement for cobalt units. The International Atomic Energy Agency advocates gradual decommissioning of cobalt units for therapeutic and safety reasons. Coline 4, having the same small footprint as Coline 10, allows its users to benefit from all the advantages of the accelerator technique while keeping the costs under control. 624 The other HITEC products intended for use in the area of medicine are the following: Simax - radiotherapy simulator used in the preparation for the actual irradiation. Accurate treatment simulation is vital for the success of radiotherapy and Simax is equipped with all the elements that allow it. Polkam 16 - treatment table, designed for precise patient positioning during the irradiation process or simulations. Polkam 16 is also manufactured in a Mould Room version, specialized for the patient preparation for radiotherapy. Polkam TBI – a unique treatment table solution designed for patient positioning and fixation during total body irradiation in preparation for a bone marrow transplantation. HITEC industrial products are centered around two linear accelerator models designed for non-destructive examination using radiographic method: Lillyput 3 - linear accelerator provides 7 and 9 MeV photon beams. Lillyput 3 is offered in both stationary and mobile configuration. Lillyput 4S – linear accelerator provides 4 and 2 MeV photon beams. Extremely compact design and excellent beam parameters make it an ideal entry-level radiographic linac. Both models of HITEC industrial accelerators can be supplemented by additional accessories: imaging devices and manipulators. HITEC also designs and manufactures custom-built linear accelerators. For both medical and radiographic application, HITEC manufactures X-Ray shielding doors – manufactured according to the highest standards for protection against ionization radiation of energy up to 25 MeV. HITEC manufactures various components or instruments for scientific applications in the area of accelerator physics, either electron or proton, for leading European high energy physics laboratories. HITEC manufacturing process has been ISO 9001 certified. All HITEC products carry the CE mark. 625 626 Catalogue of technologies developed by Polish Research Institutes SAFETY AND OTHER GENERAL TECHNICAL ASPECTS 627 AIR FORCE INSTITUTE OF TECHNOLOGY (Instytut Techniczny Wojsk Lotniczych) Organisation Contact Data Contact Person Data 6, Księcia Bolesława st, 01 – 494 Warsaw, Poland Documentation Office: phone.: +48 22 685 11 69 fax: +48 22 836 44 71; +48 22 685 10 28 phone/ fax: +48 22 685 10 13 Director Genera Ryszard Szczepanik, PhD D.Sc. Eng. phone.: +48 22 685 10 09 e – mail: [email protected] Scientific & Research Director: Andrzej Żyluk, PhD D.Sc. Eng. phone.: +48 22 685 10 19 Logistics Director: Mirosław Kowalski, PhD Eng. phone.:+48 22 685 11 04 Department for Business Development: phone.: (+48 22) 685 10 60 e-mail: [email protected] Department for Research Planning & Co-ordination: phone.:(+48 22) 685 10 72; (+48 22) 685 11 50 e-mail:planowanie@itwl http://www.itwl.pl/en/index.php 628 The Air Force Institute of Technology (AFIT) is a scientific and research organization established in 1953. It is supervised by the Polish MOD. Its mission is scientific support and research into problems of operating the military products of aeronautical engineering. The Institute's development strategy intends to increase research potential through participation in international projects conducted within the programs of the European Union, as well as the European Defence Agency as well as offset programs. AFIT holds NATO NCAGE code 0481H. In addition, it has the state concession number B404/2003, granted by the Ministry of the Interior and Administration for economic activities in the manufacture and trading of weapons, munitions, and other military and police-intended products and technologies. Its quality-management system is consistent with both the NATO AQAP and national one PN-EN standardization documents, and its research laboratories have certificates of accreditation from the Polish centre for accreditation. It also has an internal control system. The Institute provides aeronautical engineering research and development and services in the following fields: Ground and flight tests Air armament Simulation and modelling Reliability and safety Reconnaissance and command-and-control systems Avionics Diagnostics of aeronautical engineering, and airfield and road infrastructure Fuel and utility-fluid testing List and short description of offered products and services Ground and in-flight tests Aircraft weapon systems Aircraft simulation, training and modeling Aircraft safety and reliability testing Unmanned aerial vehicles (UAVs) Aircraft surveillance systems Avionics systems Aeronautical and airfield systems diagnostics Aircraft fuel and utility fluid testing 629 Ground and flight tests AFIT provides a wide variety of complex ground and in-flight tests, including aircraft and helicopters certificate tests. It also tests pilot's individual equipment, airborne high-altitude and rescue systems, airborne and ground systems to transmit or display flight parameters, and it designes and develops of flight-test dedicated measuring and recording systems. It also provides certification tests of aeronautical products introduced into service with the Polish Air Force, including air armament, as well as simulation tests based on models of aircraft flight dynamics. AFIT additionally develops and tests aerial rocket targets used for air defence forces training. Aircraft weapon systems AFIT can upgrade weapon systems for aircraft, as well as develop new designs of air weapons and aerial targets (bombs, airborne rocket launchers and bomb fuses), and new ground-based and flying testing systems for air forces. It also tests air weapons after warranty periods guaranteed by deliverers/OEMs to extend service-life, upgrades the on-board attack avionics systems for aircraft and helicopters. Aircraft simulation, training and modeling The aircraft simulation and modeling capabilities of AFIT include formulation of mathematical models of aircraft-flight dynamics and air weapons, performance of radar stations and missileguiding stations, certification tests of aircraft-flight simulators, and development of multimedia training systems (e-learning). It also provides training systems and flight simulators for flight control officers, interception navigators, pilots, and air-traffic controllers. Aircraft safetyand reliability testing AFIT emphasis on reliability and safety means It provides air-accident investigation development, computer-aided systems to assist aircrafts' operational-phase management, and testing of materials used in aeronautical structural components. It also supplies systems to record parameters of aero-engine performance, non-destructive testing of structures engineering objects, service-life tests of structural components, and flight-data decoding systems. 630 In addition, it examines operational damage and failures to aeronautical structures, and can help extend aircraft service-life and the time necessary between overhauls. Unmanned aerial vehicles (UAVs) AFIT provides new UAVs and applications, UAV software, air-reconnaissance-delivered imagery analysis and distribution systems, and UAV operator training. Aircraft surveillance systems AFIT supplies stationary and mobile terrain aircraft surveillance systems and systems to protect widespread areas (e.g. airbases and harbors). Avionic systems Avionics system ground and airborne equipment Integration of avionics systems into aircraft and helicopters Development of operational-phase assisting diagnostic instruments and systems Integration and maintenance of LINK, GPS and CSAR systems Integrated self – 7 protection systems Aeronautical and airfield systems diagnostics AFIT can conduct aircraft engine certification tests, and geological and engineering surveys of soils. It also develops diagnostic software, designs diagnostic stations to test components of aeronautical structures and predicts the service lives of aeronautical structure materials. Aircraft fuel and utility fluid testing AFIT supplies quality assessment of engine fuels, lubricating oils, lubricating greases, preservatives, engine coolants, break fluids, industrial (processing) fluids, bio-fuels and biocomponents for fuels and oils. It also develops technologies for operating fluids of synthetics, mineral and bio-components. 631 Laboratories There are 9 research laboratories at the Air Force Institute of Technology, which are awarded Certificates of Accreditation by the Polish Centre for Accreditation: Fuel and Lubricants Mechanical and Climatic Hazards Pressure Measuring Health Monitoring of Fluid-Flow Machines Working Liquids Materials Strength Testing Material Research on Aircraft Structures Unit for Product Certification LINK-16 System Integration Others However, we are not confined in our work to commercial activity only. We are deeply engaged in activities – under statutory obligations - intended to provide support to scientific research. The periodical "Prace Naukowe ITWL" ("The Proceedings of ITWL"), the "Journal of KONBiN" (i.e. of International Conference on Safety and Reliability), AKLOT - the quarterly to popularize new scientific ideas, the editorial series under a common title "The Problems of Studying, Testing and Operating Aeronautical Systems" are published at the Institute. We also organize / co-organize international conferences and seminars. The Institute is the only military R&D centre authorized to confer the "Doctor of Science" degree in the field of „machine building and operation”. 632 AFIT Divisions: Division for Air Armament The aim of the Division for Air Armament is development and upgrading of air armament. Essential research and design lines: Reliability and safety tests by means of analyzing reliability of airborne armament and correctness of air weapons performance; Examination of systems of operating the weapons; Investigating into feasibility of prolonging service lives of air weapons after the warranty periods guaranteed by manufactures/suppliers have expired; New design air weapons; Upgrading the aircraft and helicopters' on-board equipment by means of applying new, technologically advanced solutions to attack avionics; Development of new systems of the engineered means to provide the air force units with ground-based and flying training; Evolving new methods of field and flight tests of air weapons on the grounds of research work in the following lines: dynamics of objects, ballistics, effectiveness of combat applications, pyrotechnics, opto-electronics, and navigation. Contact Person Data Head of Division: Wiesław BULER PhD Eng. phone: + 48 22 685 11 14 e-mail: [email protected] 633 C4ISR Systems Integration Division Research Institute for Integration of Command, Control, Communications, Computer, Intelligence, Surveillance and Reconnaissance (C4ISR). Main research fields covered by this newly established division: Integration and Maintenance of LINK System; Integration and Maintenance of GPS & CSAR System; Integration of Self-defence systems. This division includes 3 additional Labs: Integration and Maintenance of LINK 16 System; Integration and Maintenance of GPS & CSAR System; Integration of Self-defence systems. LINK 16 System Integration Laboratory Main research fields covered by this section: LINK 16 system integration with ground elements of C4ISR system (backbone network designing; installation and configuration of multi-interface systems); LINK 16 system integration with airborne systems (ground stations and aircrafts; Design and implementation of LINK 16 network for mission and training purposes and further distribution; Monitoring and in-depth analyses of LINK 16 for development purposes; Dynamic management of LINK 16 network; Analyses of LINK 16 and other Integration Systems; LINK 16 system components testing; LINK 16/WAN Multi-system interfaces testing; Building LINK 16 multi-interface translators & LINK 16 data presentation apps; Data flow analyses, researches and optimization in multilink environments based on LINK 16 system; LINK 16 best-practices development and further in-depth analyses; Development and researches of proprietary LINK 16 based apps; Development of Network Centric Warfare solutions. 634 GPS & CSAR System Integration Laboratory Main research fields covered by so-called technical component of the GPS Main Military Point of Contact are: Military Receiver Servicing (based on agreements with vendors); Setting up Military Receivers on the ground stations and aircrafts (integration with airborne systems); Periodic checks of Civilian and Military Receivers; Working out new exploitation techniques of Military and Civilian Receivers; Developing, researching, and analysing of new version of apps based on the following systems: GPS, GLONASS, Galileo and QZSS; Development and analysis of Management & Assignment System of Beacon Identification Codes; Development in fields of operation & coordination of Civilian & Military Rescue Systems; COSPAS-SARSAT Beacons programming; CSAR, COSPAS-SARSAT beacons analyses; Beacons integration with airborne systems; Integration of Search Systems with airborne systems; Beacon servicing. Integrated Self-Defence Laboratory: Main research fields covered by this section: Detection, observation and tracking Systems working in bandwidth from 3e-4 to 4e-7 m; Analysis and development of new techniques and tests of already operated/unimplemented systems of active/passive aircraft protection system; Analysis and development of new techniques and algorithms to fighting against different weapons system; Optimization of passive self-defence systems. Contact Person Data Head of Division: Jarosław Sulkowski PhD Eng. phone: + 48 22 685 19 47 phone/fax: +48 22 685 19 48 e-mail: [email protected] 635 Division for Airfield Systems The aim of the division is building, maintenance and diagnosing of airfield pavements. Essential research and design lines: new engineering processes of repairs and maintenance of artificial airfield pavements; adaptation of military airfields to the needs of NATO; new engineering processes of rebuilding airfield pavements after wartime ("W") destruction; pavement constructions for operational airfields used by fighters and transport aircraft; physical and mechanical testing of airfield/road pavements intended materials; highways as used in air force missions; airfield-pavement diagnosing system; development of new methods of airfield/road pavements testing; investigation into effects of modern aeronautical systems upon airfield pavements; consultations and engineering supervision in the course of repairs and maintenancededicated testing work; professional advice, expert opinions. Contact Person Data Head of Division: Adam Poświata PhD Eng phone: + 48 22 685 10 24 phone/fax: +48 22 836 45 43 e-mail: [email protected] 636 Division for Reliability and Safety of Aeronautical Systems The main tasks of the Division for Reliability and Safety of Aeronautical Systems are studies under the methods of operating the military engineering for aviation, like: Computer-aided systems to assist aircraft's operational-phase management; Testing of materials (metals and alloys, rubber goods, polymers, adhesive-bonded joints) used in aeronautical structural components; Non-destructive testing of structures of engineered objects; Extension of aircraft service life and time between overhauls; Service-life tests of structural components; Examination of the operation-effected damages/failures to aeronautical structures; Development of theory of maintenance, safety and reliability of aircraft. The Division also has got the Laboratory for Materials Strength Testing and the Nondestructive Testing Laboratory. Laboratory of Non Destructive Testing The Laboratory's scope of activity includes the following: We develop procedures, test instructions, control technologies; We have competence certificates in NDT level II and III issued by BINDT, DGZfP and UDT-CERT; We make technology and maintenance tests; Possibility to control technical condition of different structural components; Possibility of providing maintenance supervision. Used testing methods: magnetic particle, eddy current, ultrasound, penetrant, shearography, acoustic, visual, d-sight. 637 Testing methods: Magnetic particle inspection For detecting surface & subsurface defects, in materials with good magnetic characteristics. Low-cost method, legible defectograms, quickly obtained test results, possible tests without taking off the tested surface’s paint coat and other non-magnetic layers. Tests of elements of the airframe and the engine of different aircraft types: turbine shaft, compressor blades of an engine, clamping joints of a wing, clamping frames of an engine on an airframe. After the tests – necessity of removing residual magnetism in magnetically hard materials. Eddy current inspection For detecting surface and under-surface defects. The method used for electrically conductive materials. Manual and automated tests (using the P-C interface); C-scan visualization mode; Data backup option; Data backup option; Data backup option; Using Faraday effect phenomenon for data visualization. Ultrasound inspection Using phenomena accompanying during generation and propagation of mechanic vibrations in tested elements. Possibility of detecting defects: under-surface, surface and inside-material. Testing hard to reach and unseen surfaces: manual and automated testing (using the P-C interface); A – scan, B – scan, C – scan visualization modes; data backup possibility; possibility of four-channel inspection; measurement techniques: pulse-echo, through-transmission; using hybrid technique ET and UT for testing riveted joints; using Phased Array type transducers and possibility of visualization „Dynamic B-scan”. Penetrant inspection capillarity phenomenon is used; for detecting surface defects of materials of any type; high sensitivity of tests; visible any intelligible defectograms; any shapes and sizes of the elements tested; low inspection costs. Applications: flame tubes, compressor and turbine blades of any type of engines; aircraft skin, riveted joints, clamping joints. It detects changes in structure of material after heat treatment, size of the zones affected by corrosion etc. 638 Shearography inspection Applications: testing composites and bonded elements, as well as honeycomb structures; detecting low-energy impact defects in honeycomb elements; data backup possibility; water inclusions detection; data analysis based on the P-C interface; using thermic and vacuum loads. Acoustic inspection: mia, pitch-catch, resonance Applications: composite, bonded and multilayer materials; elements with honeycomb; testing helicopter rotor blades; manual and automated testing (using the P-C interface); C-scan visualization mode; data backup possibility; detecting disbonds, delaminations. Visual inspection Inspection and assessment of the element’s surface condition: discontinuity detection; changes of color (corrosion); spalling; defects. Inspection of hard to reach elements: pipes containers; Fast verification, detecting damages in the early stage of development. D-SIGHT inspection Applications: Detecting, hidden corrosion in joint structures; Detecting low-energy impact damages in honeycomb structures; Data backup possibility; Data analysis based on the P-C interface. Contact Person Data Head of Division: Lt Col Andrzej Leski PhD Eng. phone: + 48 22 685 10 31, +48 22 836 45 62 phone/fax: +48 22 685 11 05 639 e-mail: [email protected] Division for it Support of Logistics The mission of the Division for IT Support of Logistics is support of military and civilian technics with IT tools. Its vision is establish modern, strong and effective team to compete in the IT market. Main tasks: Development, implementation and sustainment of IT systems for technics (esp. Areonauatical systems): Fleet management, Aircraft Configuration Management, Operational Phase Management, Planning Management, Supply Management, Inventory Management, Human Resources Management, Operation Risk Management, Life Cycle Management; Collecting, processing and delivering data to users; Conducting analytical works in the field of: CAMO / PART M, IT Safety (Crypto), NATO standards compatibility, Optimisation of processes in Logistics, Operation Risk Assessment, Flight Safety Assessment, Reliability, Maintainability and Availability Assessment, Spare Parts Forecasts, Reliability, Maintainability and Availability Prediction, Reliability Centered Maintenance, Life Cycle Management; Supporting IT activities in ITWL (incl. CAD/CAM) Computer Aided Measurement and Control System. 640 Portfolio (the products): SIWESF-16 – System for IT Support of F-16 A/C (implementation phase 2010-2011); SAMANTA – system to analyze and evaluate the operational phase of military A/C = Polish Armed Forces A/C Quantity & Quality Central Data Bank; TURAWA – IT system to analyze and assess flight safety of military aircraft (implementation phase 2010-2011); Multinational Mi-17 Airworthiness and Safety Database (MMASD). Contact Person Data Head of Division: Lt Col Ryszard Kaleta PhD Eng. phone: + 48 22 685 10 76 e-mail: [email protected] 641 Division for Aero Engines The primary tasks of the Division for Aero-engines are: diagnostics of aeronautical systems through developing new research methods; monitoring and diagnostics of aero-engines of all types, including: • Conducting the certification tests of power units implemented to military aviation; • Technical diagnostics of power units; • Development of new methods of diagnosing aero-engines; • Systems to analyze the phase-mapping effected displays; • The microwave probe to measure and monitor turbine blades' vibration spectrum; • Implementation of diagnostic systems; • Engine life extension; • Analyses of wear products in working liquids; • Tests of expert opinions resulting from analyses of events occurring in the course of operating aero-engines. Aero-Engines Division is one of the main divisions in the structure of Air Force Institute of Technology (AFIT). It consists of three laboratories: Diagnostic Laboratory, Laboratory for Diagnosing Tribological Systems and Laboratory for Health Monitoring of Fluid-Flow Machines. The last two are certified by Polish Centre for Testing and Accreditation. Diagnostic Laboratory is dealing with problems of engines diagnostics, using engine parameters analysis, vibrations analysis and method of gas turbines blades vibrations measuring. To measure various parameters they use not only commercially available sensors and additional equipment, but also develop his own. For example inductive sensor designed for method of gas turbines blades vibrations measuring, passed the tests in temperatures up to 1100K. As mentioned, in this laboratory is used equipment of well known manufacturers, like: Endevco, Brüel & Kjær, National Instruments. The engineers from this laboratory are experts in programming with Delphi, LabView modeling in MATLAB and Simulink and designing in CAD/CAM/CAE (AutoCad, Autodesk Inventor and Comsol MultiPhysics). Laboratory for Diagnosing Tribological Systems uses research methods in determining particles in oil and physical and chemical properties of oil as a carrier of information about the technical condition of diagnosed object. Laboratory uses research/testing methods such as: optical emission spectrometry to directly determine concentrations of 19 elements (wear metals, contaminants, additives) in lubricating oil; purity of working liquids – direct determination of the grade of purity of hydraulic and lubricating oils; 642 ferrography – visual analysis of wear products; finding rates that feature the wear-andtear of aero-engine bearing systems; X-ray fluorescence (XRF) to determine concentrations of selected elements in lubricating oil; viscosity - one of an oil’s most important physical properties which has a direct link with the condition of the diagnosed system. Laboratory for Health Monitoring of Fluid-Flow Machines involved in aircraft engine diagnostics using non-destructive methods (NDT). Main research method used in the laboratory is visual, utilizing the latest endoscopic equipment from renowned international companies such as GE, OLYMPUS. The laboratory is also working on developing new, nondestructive methods of diagnosing the state of the engines. Are also conducted research into the causes of damage and accident. Contact Person Data Head of Division: Jarosław Spychała PhD Eng. phone: + 48 22 685 10 34 e-mail: [email protected] 643 Division for Aeroplanes and Helicopters The aim of the Division is operation/maintenance-dedicated ground and flight tests of aircraft and aeronautical systems. Essential lines of research: Flight tests of aircraft; Ground tests of aircraft airframes: structures and systems thereof; Tests of AFIT-designed constructions; Special tests (incl. those ordered by the Air Accident Investigation Board) and simulation-based ones; Development of training and simulation systems; Development of flight-data recording systems; Engineering support of operational/maintenance practice; Certification (state) tests of aeronautical systems introduced into service with military aviation; Complex flight tests of aircraft; Design and development of measuring/recording systems for ground and flight tests; Testing/monitoring of aircraft power plants' health/maintenance status to increase reliability of operated fleet; Assessment of aircraft behavior under extreme flight conditions to determine preventive-treatment and emergency-applicable procedures; Design, development and testing of systems intended to give training in fighting aerial targets; UAVs used to fill this role included; Development and testing of unmanned air-surveillance systems; Simulation-based testing work with AFIT's own models of aircraft flight dynamics employed (ones generated using parameters recorded in the course of flight tests); Airborne inputs-processing systems; Airborne and ground-based systems to transmit/display flight parameters; Expert examination of airframe systems and operation-dedicated media. Environmental and mechanical tests of assemblies/subassemblies of military aeronautical systems, conducted in the accredited Laboratory for Mechanical & Climatic Hazards. Contact Person Data Head of Division: Mirosław Nowakowski PhD Eng. phone: + 48 22 685 10 36 phone./fax: +48 22 836 46 03, +48 22 685 10 68 e-mail: [email protected] 644 Division for Avionicx The major task of the Division for Avionics is searching for solutions to problems of avionics for aeroplanes and helicopters. Essential lines of research: Design and integration of airborne avionics systems; Upgrading and supplementing military aircraft with avionics; Reliability and effectiveness of using avionics to perform air missions; Development of methodologies of testing work; tests of airborne avionics; Investigations into causes of incorrect performance of systems, development of preventive-treatment procedures; Investigations into capabilities of extending operation lives of systems' components after the manufacture-warranted service lives thereof have expired; Tests and development of aircrew-dedicated survival equipment; Pressure equipment calibration. The Division for Avionics has got the accredited Laboratory for Pressure Measuring. Laboratory for Pressure Measuring has been accredited by the Polish Centre of Accreditationin the area of calibration of pressure measuring devices. Besides, it has been granted the certificate in the field of pressure gauge testing, pressure measurement in closed containers and leaktightness testing. The Laboratory operates in accordance with the internal quality management system consistent with both the NATO AQAP 2210 standardization document and the ISO 9001 standard. The Laboratory has been accredited in the field of calibration of the following types of pressure gauges: indicating pressure gauges with elastic measuring elements, load-piston manometers, aneroid, electronic read-out pressure gauges, pressure converter, boost gauge. The Laboratory carries out calibration of: monitoring systems & measuring devices used for checking on-board pilotage and navigational systems; altimeters, speedometers, machmeters and variometers. Contact Person Data Head of Division: Lt Col Sławomir MICHALAK PhD Eng. phone/fax: 48 22 685 10 43, +48 22 685 12 07 e-mail: [email protected] 645 Division for Air Training and Command and Control Systems The tasks of the Division are studies and implementation work related with development and improvement of: air & air defence command and control systems; simulation-based training systems to satisfy needs of air-defencededicated virtual battlefield; interactive training systems. Essential research and design lines: identification and verification of mathematical models of virtual-battlefield-inherent objects; development of methods and systems to integrate simulators with objects of a real air defence system; development of hardware/software structures for real-time systems; development of simulation-based systems to design and test newly-made military hardware; certification tests of aircraft-flight simulators; development of research methodologies and investigation into training and combat systems of the C2I level. Contact Person Data Head of Division: Lt Col Przemysław Mądrzycki PhD Eng. phone: +48 22 685 10 51 e-mail: [email protected] 646 Division for Fuels and Lubricants Fuels and Lubricants Division area of interest: research and development (R&D) projects covering: fuels (marine, ground and aeronautics equipment), biofuels and biocomponents (fuels, lubricants and greases application), application of alternative fuels in transport and other energy areas, process of fuel combustion, tribology, lubricants, engine lubricanting oils, transmission fluids, hydraulic oils etc.), other petroleum products (icl. cooling fluids, braking systems fluids, special liquids for industry etc.); design activity in the area of construction and research work in the field of equipment and POL infrastructure (mobile laboratories, mobile devices); testing of working liquids (new and used) in a certified laboratory; monitoring of fuels and working liquids quality; preparing standardisation documents, standardisation of petroleum products and testing methods; fuels and working liquids monitoring systems; preparing new technologies for production of synthetic, mineral and bio-based pr