Sample Preparation Product Range ::: Clear Solutions in Sample Preparation
Transcription
Sample Preparation Product Range ::: Clear Solutions in Sample Preparation
Sample Preparation Product Range ::: Clear Solutions in Sample Preparation Multiwave PRO Master of Sample Preparation Methods 4The Multiwave PRO microwave reaction system delivers the sample preparation solutions you need to obtain excellent trace analysis results, even with complicated, demanding samples. 4Multiwave PRO masters high temperatures and provides comprehensive reaction control features. 4Its wide range of accessories allows digestion, leaching, oxygen combustion, solvent extraction, drying, evaporation, and UV digestion with one single system. Features 41500 Watt microwave power, unpulsed controllable 4Decomposition of up to 64 samples simultaneously 4Integrated high-performance cooling system 4Certified safety system 4Simultaneous measurement of pressure and temperature 4Infrared temperature measurement of all vessels 4Comprehensive application library HPA–S Unrivaled Performance The High Pressure Asher HPA–S is the reference instrument for wet chemical pressure decomposition. The instrument is TÜV certified and can prepare even the most difficult samples for reliable AAS, ICP-AES, ICP-MS and voltammetric analysis. The HPA-S enables the maximum decomposition parameters and the largest sample weight in hermetically sealed reaction vessels made of quartz glass or glassy carbon. Uniform heating and exact temperature control guarantee the highest level of reproducibility. Features Decomposition pressure up to 130 bar Decomposition temperature up to 320 °C Unlimited decomposition times Reaction vessels VolumeMaterial 15 ml Quartz 50 ml Quartz 90 ml Quartz 20 ml Glassy carbon Number 14 or 21 7 5 6 Multiwave PRO Abundantly Clear Highest sample throughput Digestion rotors with up to 64 vessels eliminate the bottleneck in sample preparation while being fast and easy to operate without compromising safety. Simple operation and a comprehensive library of applications make the Multiwave PRO a powerful tool for sample preparation. Integrated cooling The reaction vessels can be operated at maximum operating pressure and maximum temperature simultaneously. The integrated vessel cooling prevents overheating and ensures a higher sample throughput due to short cooling times. Vessels MG5 MF50 Liner material Glass (PTFE seal) PFA or PTFE-TFM MF100 PTFE-TFM Pressure jacket n/a PEEK PEEK Vessel volume 5 mL 50 mL 100 mL Operation parameters 200 °C @ 20 bar (290 psi) 200 °C @ 20 bar (290 psi) 200 °C @ Max. design pressure 33 bar (479 psi) 60 bar (870 psi) 115 bar (16 Max. design temperature 310 °C 260 °C (PFA), 310 °C (TFM) 310 °C HF resistant No Yes Yes Typical applications Biological material Water, effluents, sewage sludge, plant ma sediment, US-EPA procedures, biological Highest decomposition quality Operating pressures and temperatures up to 80 bar and 300 °C result in matrix-free solutions without contamination or loss of analytes, even for samples which are difficult to decompose or react violently. Everything under control Information about reaction parameters is delivered by installationfree pressure and temperature sensors from a reference vessel. Continuous pressure monitoring of all eight sample vessels allows for safe and precise reaction control, even with critical samples. An external IR sensor monitors the temperature of all reaction vessels at the base of each vessel. HF100 XF100 XQ80 PTFE-TFM PTFE-TFM n/a Ceramic Ceramic Quartz 100 mL 100 mL 80 mL 20 bar (290 psi) 240 °C @ 40 bar (580 psi) 260 °C @ 60 bar (870 psi) 300 °C @ 80 bar (1160 psi) 670 psi) 115 bar (1670 psi) 140 bar (2000 psi) 140 bar (2000 psi) 310 °C 310 °C 310 °C Yes Yes No Food samples, contaminated soil, metals, alloys, geological material, glass, quartz Mixed waste, semiconductors, ceramics, ores, ashes, slag, refractories Fatty foodstuffs, plastics, fibers, oil, fat, coal, pharmaceuticals, chemicals M aterial, soil, material Multiwave PRO Special Applications Microwave-assisted extraction Extraction above the solvent's boiling point for unmatched speed and safety. Oxygen combustion Microwave-induced combustion is a unique option for analysis of halogenes or metals in combustible samples. UV digestion Microwave-powered UV lamps completely destroy organic matter in liquid samples with little reagent and low analytical blanks. Hydrolysis Protein hydrolysis can be performed from milligram to gram scale in less than one hour, even under inert gas atmosphere. Evaporation Acids or silicates are removed under clean room conditions without changing the reaction vessel. Drying Samples are dried prior to digestion quickly and without bad smells. Multiwave ECO Routine Digestions - Simple and Quick Multiwave ECO is a quick and convenient microwave digestion system equipped with the lightweight Rotor 16HVT50. This rotor has a superior design for controlled release of overpressure. Multiwave ECO simplifies your routine handling of environmental, food and many other samples. The low investment and operating costs of Multiwave ECO and low costs for consumables make it a good investment. Benefits 4ECO heating concept - A smart microwave heating concept that does more with less 4ECO cooling concept - The fastest cooling of all laboratory microwaves 4Simplicity - Simplified handling of rotor and vessels 42 turns to tightness - Simple 3-part vessel concept 4Pressure-activated venting - Reliable, temperatureindependent system which handles pressure when the heat is on - high temperatures and high sample weights 4Rotor 1DRY as an option to dry samples before digestion 4Rotor 16HVT50 for large sample weights up to 2 g organic samples; Rotor 64MG5 for micro samples Photos: Croce & Wir Anton Paar® GmbH Anton-Paar-Str. 20 A-8054 Graz Austria - Europe Tel: +43 (0)316 257-0 Fax: +43 (0)316 257-257 E-mail: [email protected] Web: www.anton-paar.com Instruments for: Density & concentration measurement Rheometry & viscometry Sample Preparation Microwave synthesis Colloid science X-ray structure analysis Refractometry Polarimetry Petroleum testing High-precision temperature measurement Subject to change without notice 01/13 XCAIP013EN-E