DDPS Product Profile QVF Dual Stage Distillation System.indd

PRODUCT PROFILE
QVF DUAL STAGE
DISTILLATION SYSTEM
Overview
This purpose designed, electrically heated, QVF PILOT PLANT DUAL STAGE DISTILLATION SYSTEM by De Dietrich Process Systems
permits selective stripping and rectification of aqueous aromatic solutions. A LabVIEW interface allows flexible in control and
data logging of feed rates, reflux rates, feed points, operating pressure and other process parameters. The system was designed
using GMP guidelines where practical. To assure untainted product quality, all materials were selected to prevent trace contamination. Borosilicate glass was used for major components to provide maximum process visibility.
Specifications
System Design Pressure:
System Design Temperature:
Feed/Distillate Ratio:
Electric Power Requirement:
Mobile Glass Feed Vessel Volume:
Mobile Glass Receivers:
Stage 1 Bottoms
Stage 2 Bottoms
Stage 2 Distillate
Control System using LabVIEW:
Instrumentation readouts:
Controls:
-1 / 0.6 barg
-20°C to 150°C
10:1 per stage, 100:1 overall
60 Amps, 3 phase, 230 VAC
50 L
50L
10L
0.5L
Flow rates, temperature, pressure, level
Valves, vacuum pump, feed rates, reflux rates, level, and heating
Scope of Supply
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2 x QVF borosilicate glass, packed columns, one DN150 (6” diameter) and one DN80 (3” diameter). Multiple temperature probes spaced along the column length.
Stainless steel structured column packing, designed for maximum theoretical plates per meter. Packed height of
960mm per column.
Control system with PC based interface.
3 x Mobile QVF Cylindrical Glass Vessels with bottom drain valve and quick disconnect fittings for vacuum and liquid
lines. Used for feed stock and bottoms product.
Final Distillate Receiver, borosilicate glass, 0.5L, with screwed connection for easy removal.
3 x electric emersion heaters for Stage 1 feed preheat, Stage 1 Reboiler, and Stage 2 Reboiler.
5 x metering pumps.
1 x dedicated lab vacuum pump with solvent trap.
5 x QVF Water Cooled, Coil Condensers, borosilicate glass.
All required instrumentation, solenoid valves, and wiring.
Schedule 40 tubular galvanized steel support structure.
Complete engineering design package including:
- P&ID
- General Arrangement Drawings and Parts List
- Documentation and Owner’s Manual
E012
11/2011
PRODUCT PROFILE
QVF DUAL STAGE
DISTILLATION SYSTEM
Flow Transmitters
Pump VFDs
4
Two Distillation
Columns
1
2
5
Horizontal
Reboilers
3
6
QVF Glass
Coil Condensers
Dedicated Vacuum
Pump with Solvent Trap
7
LabVIEW Control System
De
Dietrich Process Systems, Inc.
De Dietrich Process Systems GmbH
244
Sheffield Street 36
Hattenbergstraße
Mountainside, NJ 07092
D-55122 Mainz
P 908.317.2585
www.ddpsinc.com
[email protected]
Tel.: +49
(0) 61 31/97 04-0
F 908.889.4960
[email protected]
www.qvf.com
Fax: +49 (0) 61 31/97 04-500
Copyright © De Dietrich Process Systems, Inc. All rights reserved. The information contained in this brochure is believed to be reliable general guidelines for consideration of the products and services described herein. The information is general in nature
and should not be considered applicable to any specific process or application. De Dietich Process Systems, Inc. expressly disclaims any warranty, expressed or implied of fitness for any specific purpose in connection with the information contained herein.