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RANDCASTLE EXTRUSION SYSTEMS, INC. SFEM BATCH MIXERS: Peer Reviewed Technical Papers: “FACILE TPO DISPERSION USING EXTENSIONAL MIXING,” presented by Dow Chemical’s Stéphane Costeux at Antec 2011 concluded: Simply put? 1. “…the Randcastle SFEM batch mixer indicate that its dispersive capabilities are superior to the Mixing Bowl, while reducing the amount of material and time per blend. 2. It is confirmed that the SFEM’s primary deformation mode is elongational, which also contributes to limiting shear heating effects. 3. The same SFEM elements can be added to a single screw extruder, which achieve even better performance, which is encouraging from a scale-up standpoint. 4. This technology is suitable for single-screw extrusion of TPOs and other immiscible blends. “A NOVEL MICRO-BATCH MIXER THAT SCALES TO A SINGLE SCREW COMPOUNDER,” written with Rutgers University’s Jennifer Lynch and Tom Nosker Simply put? for Antec 2008, the paper concludes: The micro-batch mixer is shown to produce similar mixedness as the SSE for a variety of materials systems because of its similar geometry to the SSE compounder with SFEM elements. The mixing times are fairly short and comparable to extrusion residence times. This micro-batch mixer adds a powerful tool for the polymer researcher because only small quantities of material are necessary, and these experiments successfully scale-up to large-scale extrusion processing equipment. The micro-batch mixer is a vital, simple piece of equipment that provides results quickly and conveniently. RANDCASTLE EXTRUSION SYSTEMS, INC. SFEM BATCH MIXERS: Elongational batch mixers from 1 to 200cc capacity: Dispersity 10 times better than “mixing bowls.” Mixtures (below left) in one third the time of “mixing bowls.” Compounding equal to a twin screw extruder. Scales to our single screw mixers (same geometry). Conveniently extrudes your material into a strand: No need to scrape melted material from hot rotors. Continuous: 20PS/80HDPE Globules Quick strand cooling eliminate degradation. Domains: 0.2 to 2 Micron Randcastle No need to grind scrapings for later processing. Randcastle SFEM Batch SFEM Screw Find details in peer reviewed technical papers. Stéphane Costeux , Dow Chemical Mark Barger, Dow Chemical, et al FACILE TPO DISPERSION USING EXTENSIONAL MIXING Antec 2011 (left) Keith Luker, Randcastle Jennifer Lynch, Rutgers University Tom Nosker, Rutgers University A NOVEL MICRO-BATCH MIXER THAT SCALES TO A SINGLE SCREW EXTRUDER Antec 2008 (right) (A) (B) (A) (B) (C) (D) (C) (D) Co-Continuous: 30PS/70HDPE (E) (F) (E) (F) (G) (H) (G) (H) RANDCASTLE EXTRUSION SYSTEMS, INC. MODEL NUMBER BARREL ID INCH ROTOR L/D ~INPUT CC ~EXTRUDED OUTPUT SFEM-BM-2500-4 2.5 4 200 100 SFEM-BM-2500-2 2.5 2 100 50 SFEM-BM-2500-1 2.5 1 50 25 SFEM-BM-2000-4 2.0 4 100 50 SFEM-BM-2000-2 2.0 2 50 25 SFEM-BM-2000-1 2.0 1 25 12 SFEM-BM-1000-4 1.0 4 10 5 SFEM-BM-1000-2 1.0 2 5 2.5 SFEM-BM-1000-1 1.0 1 2.5 1.25 SFEM-BM-0750-4 0.75 4 5 2.5 SFEM-BM-0750-2 0.75 2 2.5 1.25 SFEM-BM-0750-1 0.75 1 1.25 0.6 close up extrusion Study May Boost Prospects For Single-Screw ‘Elongator’ Has the heated debate over whether a single screw can possibly provide elongational mixing akin to a twin screw now been settled? Dow Chemical Co., Midland, Mich., weighed in at last year’s SPE ANTEC (May 1-5 in Boston) with a paper discussing results of experiments it conducted on a novel elongational mixing device developed by Randcastle Extrusion Systems, Cedar Grove, N.J. The paper, delivered by Dow researcher Stephane Costeux, discussed the results of mixing tests using Randcastle’s SFEM series batch mixers versus a batch-mixing bowl, both running TPO blends of 70% polypropylene and 30% ethylene copolymers. The batch mixer had the same basic geometry as Randcastle’s SFEM patented elongational mixer for single screws, introduced in 2008. Dow’s testing confirmed that where typical batch mixers are shear-dominant, the Randcastle mixer has “stronger extensional flow” to achieve better TPO dispersion. The Dow study also used a Randcastle single-screw extruder with similar mixing geometry to determine that the “SFEM’s primary deformation mode is elongational (as opposed to shear-dominated),” and added that “a single-screw extruder equipped with SFEM mixing elements achieved even finer dispersion, usually achievable only with twinscrew extruders.” Keith Luker, president of Randcastle (randcastle.com), has been touting the elongational mixing capabilities of his device since he first developed it. The response, by and large, has been skeptical, as twin-screw extruders are generally considered the gold standard where mixing is concerned. “Elongation is a stretching force; its opposite is compression,” explains Luker. “Compression pushes material together, as in the compression section of a screw. If you take a cylinder and push on it from all sides nothing will happen. Take the same volume of a cylinder and stretch it out into a film, and you get an exponential increase in surface area. That quantifies the mixing improvement. The key is the pulling surface that stretches material from the inlet channel—just as nip rolls pull.” (See illustration of how it works.) The Dow paper also addressed the matter of scale-up: “The most important attribute of mixing equipment used to make such small-scale blends is that it achieves a degree of mixing or morphology that is consistent with that obtained with large-scale compounding equipment. If the geometry of the batch mixer is How the Elongational Mixer Works 1 ing Pull ing Pull r to Vec Sur A cylindrical concentration of unmixed material (purple) enters the first channel pushed along by pressure flow by upstream flights. It is immediately grabbed by the moving pulling surface-just as pull rolls would grab your finger. s face Pressure flow pushes the material along the inlet while pulling surface and drag flow begin to convert the cylinder into a film. 2 3 The concentration nears total conversion to film. The actual film is much longer than depicted because the drag velocity is much higher than that inlet channel velocity. very different from the mixing-element geometry of the largescale process (often involving a single-screw extruder), translation of laboratory formulation results to commercial scale becomes extremely challenging.” But Luker notes that the batch and screw SFEM mixers have essentially the same geometry. “You expect the same geometry to scale up,” states Luker. “You do not expect mixing-bowl geometry to scale up to because it does not resemble a single screw.” Luker notes that a previous paper delivered at ANTEC 2008 by Drs. Jennifer Lynch and Tom Nosker of the Dept. of Ceramic and Materials Engineering, Rutgers University, New Bruswick, N.J. confirmed the scale-up from batch mixer to extruder screw. Commercial applications of Luker’s SFEM elongational mixer to date include mixing of 35% calcium carbonate in a directextrusion application; mixing immiscible materials for pipe; mixing large mica flakes for pearlescent compounds; and blending high- and low-viscosity polymers. Luker says it takes only two mixing sections in a 24:1 LD screw to get about 125 times better mixing, or three mixers in a 32:1 LD to give you about 1000 times better mixing, than with a standard single screw. By James J. Callari, Editorial Director Plastics Technology january 2012 11